CN107298993A - A kind of environment-friendlygasoline gasoline additive and preparation method thereof - Google Patents

A kind of environment-friendlygasoline gasoline additive and preparation method thereof Download PDF

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Publication number
CN107298993A
CN107298993A CN201710741652.4A CN201710741652A CN107298993A CN 107298993 A CN107298993 A CN 107298993A CN 201710741652 A CN201710741652 A CN 201710741652A CN 107298993 A CN107298993 A CN 107298993A
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parts
mixture
oil
preparation
environment
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黄海宁
唐宏泉
徐文兵
汪建军
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Cofco Biochemical Anhui Co Ltd
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Cofco Biochemical Anhui Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/143—Organic compounds mixtures of organic macromolecular compounds with organic non-macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/16—Hydrocarbons
    • C10L1/1625—Hydrocarbons macromolecular compounds
    • C10L1/1633—Hydrocarbons macromolecular compounds homo- or copolymers obtained by reactions only involving carbon-to carbon unsaturated bonds
    • C10L1/1641—Hydrocarbons macromolecular compounds homo- or copolymers obtained by reactions only involving carbon-to carbon unsaturated bonds from compounds containing aliphatic monomers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/1802—Organic compounds containing oxygen natural products, e.g. waxes, extracts, fatty oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
    • C10L1/1822—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms
    • C10L1/1824—Organic compounds containing oxygen containing hydroxy groups; Salts thereof hydroxy group directly attached to (cyclo)aliphatic carbon atoms mono-hydroxy
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/188—Carboxylic acids; metal salts thereof
    • C10L1/1881—Carboxylic acids; metal salts thereof carboxylic group attached to an aliphatic carbon atom
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/19—Esters ester radical containing compounds; ester ethers; carbonic acid esters
    • C10L1/191—Esters ester radical containing compounds; ester ethers; carbonic acid esters of di- or polyhydroxyalcohols
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/192—Macromolecular compounds
    • C10L1/198—Macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds homo- or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon to carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid
    • C10L1/1985—Macromolecular compounds obtained otherwise than by reactions involving only carbon-to-carbon unsaturated bonds homo- or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon to carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid polyethers, e.g. di- polygylcols and derivatives; ethers - esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2431—Organic compounds containing sulfur, selenium and/or tellurium sulfur bond to oxygen, e.g. sulfones, sulfoxides
    • C10L1/2437—Sulfonic acids; Derivatives thereof, e.g. sulfonamides, sulfosuccinic acid esters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2493—Organic compounds containing sulfur, selenium and/or tellurium compounds of uncertain formula; reactions of organic compounds (hydrocarbons, acids, esters) with sulfur or sulfur containing compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/28—Organic compounds containing silicon
    • C10L1/285—Organic compounds containing silicon macromolecular compounds

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Polyethers (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

The present invention relates to a kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is made up of following ratio by weight：8 15 parts of ethene, 36 parts of butadiene, 25 parts of TBHQ, 30 45 parts of poly- a alkene, 5 10 parts of silicone oil, 48 parts of polyoxyethylene polyoxypropylene polyethers, 26 parts of octadecanoid acid, 6 10 parts of oleic acid ethylene glycol junket, 59 parts of sulfuration cottonseed oil, 25 parts of sulfonate, 3 10 parts of AEO, 23 parts of Tea Polyphenols, 8 10 parts of ethanol.Material of the present invention is easy to get, and cost is low, environment-friendly and green, stability is strong, and oxidation resistance is good, and film is formed in metal surface, effective antirust, improves lubricity, and abrasion resistance index is high, frictional index is small, effectively lifts power, water oil good separating effect, it is quick to remove carbon deposit, oil circuit is cleaned, fuel oil is saved, increases the service life.

Description

A kind of environment-friendlygasoline gasoline additive and preparation method thereof
Technical field
The present invention relates to additive agent field, and in particular to a kind of environment-friendlygasoline gasoline additive and preparation method thereof.
Background technology
With the requirement of social development, environmental protection turns into modern theme, and continuing to develop for automobile industry causes global change The hidden danger such as warm is, it is necessary to processing in time.There is labile element in fuel oil, oxidative dimerization is produced at high temperature, form carbon distribution Particulate, the clean kept type additive added in gasoline, from all quarter surrounds these carbon particulates, forms oil-soluble one by one Micella, using intermicellar electrostatic repulsion and steric hindrance, prevents them from assembling and becomes big, it is impossible to be deposited on metal surface, so that Improve fuel qualities.
The content of the invention
A kind of environment-friendlygasoline gasoline additive and preparation method thereof is provided the invention aims to overcome the shortcomings of the above.
Technical scheme includes：A kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is by weight Amount number is made up of following ratio：8-15 parts of ethene, 3-6 parts of butadiene, 2-5 parts of TBHQ, 30-45 parts of poly- a alkene, silicone oil 5- 10 parts, 4-8 parts of polyoxyethylene polyoxypropylene polyethers, 2-6 parts of octadecanoid acid, 6-10 parts of oleic acid ethylene glycol junket, sulfuration cottonseed oil 5-9 Part, 2-5 parts of sulfonate, 3-10 parts of AEO, 2-3 parts of Tea Polyphenols, 8-10 parts of ethanol.
Further improvement of the present invention is：Its preparation method is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 250-340 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.5-6.8 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 700-800r/min, 15- 20min obtains mixture C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 8000-9000HZ, and rotating speed is to take out supernatant liquor after 7000-8000r/min, filtering, obtains product.
Beneficial effects of the present invention：
Material of the present invention is easy to get, and cost is low, environment-friendly and green, and stability is strong, and oxidation resistance is good, and film is formed in metal surface, Effective antirust, improves lubricity, and abrasion resistance index is high, and frictional index is small, effectively lifts power, and water oil good separating effect is quick clear Except carbon deposit, oil circuit is cleaned, fuel oil is saved, increases the service life.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is made up of following ratio by weight：Ethene 10 parts, 5 parts of butadiene, 3 parts of TBHQ, 35 parts of poly- a alkene, 8 parts of silicone oil, 6 parts of polyoxyethylene polyoxypropylene polyethers, octadecanoid acid 4 Part, 8 parts of oleic acid ethylene glycol junket, 7 parts of sulfuration cottonseed oil, 3 parts of sulfonate, 5 parts of AEO, 2 parts of Tea Polyphenols, ethanol 9 parts.
Its preparation method is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 300 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.7 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 720r/min, and 18min must be mixed Compound C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 8200HZ, and rotating speed is to take out supernatant liquor after 7500r/min, filtering, obtains product.
Embodiment 2
A kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is made up of following ratio by weight：Ethene 15 parts, 4 parts of butadiene, 3 parts of TBHQ, 45 parts of poly- a alkene, 10 parts of silicone oil, 4 parts of polyoxyethylene polyoxypropylene polyethers, octadecanoid acid 2 parts, 6 parts of oleic acid ethylene glycol junket, 6 parts of sulfuration cottonseed oil, 3 parts of sulfonate, 3 parts of AEO, 3 parts of Tea Polyphenols, second 8 parts of alcohol.
Its preparation method is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 320 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.6 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 800r/min, 15-20min Obtain mixture C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 8400HZ, and rotating speed is to take out supernatant liquor after 7600r/min, filtering, obtains product.
Embodiment 3
A kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is made up of following ratio by weight：Ethene 13 parts, 3 parts of butadiene, 3 parts of TBHQ, 45 parts of poly- a alkene, 5 parts of silicone oil, 4 parts of polyoxyethylene polyoxypropylene polyethers, octadecanoid acid 3 Part, 7 parts of oleic acid ethylene glycol junket, 8 parts of sulfuration cottonseed oil, 3 parts of sulfonate, 5 parts of AEO, 3 parts of Tea Polyphenols, ethanol 8 parts.
Its preparation method is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 280 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.8 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 780r/min, 15-20min Obtain mixture C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 8200HZ, and rotating speed is to take out supernatant liquor after 8000r/min, filtering, obtains product.
Embodiment 4
A kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is made up of following ratio by weight：Ethene 8 parts, 3 parts of butadiene, 2 parts of TBHQ, 30 parts of poly- a alkene, 5 parts of silicone oil, 4 parts of polyoxyethylene polyoxypropylene polyethers, octadecanoid acid 2 Part, 6 parts of oleic acid ethylene glycol junket, 5 parts of sulfuration cottonseed oil, 2 parts of sulfonate, 3 parts of AEO, 2 parts of Tea Polyphenols, ethanol 8 parts.
Its preparation method is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 340 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.8 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 800r/min, and 20min is obtained Mixture C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 9000HZ, and rotating speed is to take out supernatant liquor after 8000r/min, filtering, obtains product.
Embodiment 5
A kind of environment-friendlygasoline gasoline additive and preparation method thereof, raw material constituent is made up of following ratio by weight：Ethene 10 parts, 5 parts of butadiene, 3 parts of TBHQ, 42 parts of poly- a alkene, 6 parts of silicone oil, 7 parts of polyoxyethylene polyoxypropylene polyethers, octadecanoid acid 3 Part, 8 parts of oleic acid ethylene glycol junket, 6 parts of sulfuration cottonseed oil, 4 parts of sulfonate, 5 parts of AEO, 3 parts of Tea Polyphenols, ethanol 10 parts.
Its preparation method is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 320 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.6 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 750r/min, and 18min must be mixed Compound C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 8000HZ, and rotating speed is to take out supernatant liquor after 7000r/min, filtering, obtains product.
In above example, embodiment 5 is most preferred embodiment, and more preferably, permeability is strong, and stability is good for lubricant effect；Step B In be slowly added in four times polyoxyethylene polyoxypropylene polyethers ensure emulsion resistance machine uniformity, improve antifoaming speed.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc. should be included in Within protection scope of the present invention.

Claims (2)

1. a kind of environment-friendlygasoline gasoline additive and preparation method thereof, it is characterised in that：Raw material constituent is by weight by following Ratio is constituted：8-15 parts of ethene, 3-6 parts of butadiene, 2-5 parts of TBHQ, 30-45 parts of poly- a alkene, 5-10 parts of silicone oil, polyoxy second 4-8 parts of alkene polyoxypropylene polyether, 2-6 parts of octadecanoid acid, 6-10 parts of oleic acid ethylene glycol junket, 5-9 parts of sulfuration cottonseed oil, sulfonate 2- 5 parts, 3-10 parts of AEO, 2-3 parts of Tea Polyphenols, 8-10 parts of ethanol.
2. a kind of environment-friendlygasoline gasoline additive according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method It is as follows：
Under A, an atmospheric pressure, ethene, butadiene, poly- a alkene and silicone oil are subjected to mixing polycondensation, ethanol is catalyst, temperature 250-340 DEG C, obtain mixture A；
B, octadecanoid acid, AEO, sulfuration cottonseed oil and oleic acid ethylene glycol junket mixed, it is uniform after Polyoxyethylene polyoxypropylene polyethers is slowly added in four times, is 6.5-6.8 to PH, is obtained mixture B；
C, TBHQ and sulfonate mixed, add mixture A and stir, stir speed (S.S.) is 700-800r/min, 15- 20min obtains mixture C；
D, by mixture C addition mixture B be stirred, add Tea Polyphenols, input centrifuge in enter water-filling oil separation, centrifuge Frequency is 8000-9000HZ, and rotating speed is to take out supernatant liquor after 7000-8000r/min, filtering, obtains product.
CN201710741652.4A 2017-08-25 2017-08-25 A kind of environment-friendlygasoline gasoline additive and preparation method thereof Pending CN107298993A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108624367A (en) * 2018-05-24 2018-10-09 宁波蒙曼生物科技有限公司 A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive
CN108676590A (en) * 2018-05-24 2018-10-19 宁波蒙曼生物科技有限公司 A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive
CN108690667A (en) * 2018-05-24 2018-10-23 宁波蒙曼生物科技有限公司 A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive
CN108753379A (en) * 2018-05-24 2018-11-06 宁波蒙曼生物科技有限公司 A kind of Preparation equipment of environment-friendlygasoline gasoline additive and preparation method thereof and the additive

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Publication number Priority date Publication date Assignee Title
CN1357605A (en) * 2001-08-31 2002-07-10 石生玉 Additive for synthetic water-diesel oil fuel and its prepn and application
CN101082004A (en) * 2007-07-05 2007-12-05 中国农业科学院油料作物研究所 Biological diesel modifying agent and preparation method thereof
CN104694228A (en) * 2013-12-10 2015-06-10 张希顺 Efficient antifriction lubricating oil for automobile

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Application publication date: 20171027