CN108609852A - A method of for identification LOGO on metallized ceramic pipe glaze - Google Patents
A method of for identification LOGO on metallized ceramic pipe glaze Download PDFInfo
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- CN108609852A CN108609852A CN201810396604.0A CN201810396604A CN108609852A CN 108609852 A CN108609852 A CN 108609852A CN 201810396604 A CN201810396604 A CN 201810396604A CN 108609852 A CN108609852 A CN 108609852A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
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Abstract
The invention discloses a kind of methods for identification LOGO on metallized ceramic pipe glaze, including steps are as follows：Colored glaze slip is prepared according to LOGO colors；Hollow processing is carried out by the pattern of LOGO same colors LOGO gear tools are made with aluminium sheet；Metallized ceramic pipe after nickel plating or print nickel is put into baking oven, is taken out after keeping the temperature 10 30 minutes at a temperature of 120 150 DEG C；Metallized ceramic is managed and protected with LOGO gear tools, is required according to the color of LOGO, colored glaze slip is added in glaze spraying pressurized tank and carries out glaze spraying；Then it is sprayed according to the colored glaze slip of LOGO color replacements and corresponding LOGO gear tools, until spraying complete LOGO；Metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800 950 DEG C, the identification LOGO on metallized ceramic pipe glaze is completed.This method can realize chromatography glaze spraying, disclosure satisfy that the requirement of multiple color composition LOGO, the nickel layer of ceramic pipe surface and LOGO can be made to be completed at the same time sintering in a process, identification pattern is clear, and color stability, glaze is smooth, and the class of product can be improved.
Description
Technical field
The present invention relates to a kind of production technology, more particularly to a kind of sides for identification LOGO on metallized ceramic pipe glaze
Method.
Background technology
Ceramics and metal sealing technology are widely used in manufacturing the vacuum electron devices such as electron tube, vacuum switch tube.In electricity
The quality of metallized ceramic tubes performance is very crucial for the quality of product in vacuum industry, therefore added value is higher, industry
Competition is very fierce.Leading enterprise deep accident and quality dispute caused by by counterfeit and shoddy goods in electrovacuum industry are stranded
It disturbs, constantly seeks the means and method of preventing fake products impact.
For this purpose, some high-end customers require to identify in metallized ceramic Guan Shangzuo LOGO.User's body can be allowed by mark
Confidence of the production company to product can be arrived, to allow client to remember company's main body and brand culture, quickly improves Products
Popularity, and the impact and dispute that can effectively avoid fake products from bringing.The country there is no the relevant technologies and product at present.
The country there is no the color glaze of the identification LOGO on metallized ceramic pipe glaze at present, and high-temperature glaze fusing point is higher cannot be very
Good Yangjing on glaze, low temperature color glaze contain lead, under reducing atmosphere glaze layer blackening can not develop the color.Unleaded color glaze thermally expands system
Number is big with 95 alumina ceramics and high-temperature glaze gap, and cooling procedure is easy to fall off or adhesion strength is low.
Invention content
Technical problem to be solved by the invention is to provide a kind of sides for identification LOGO on metallized ceramic pipe glaze
Method, this method can realize chromatography glaze spraying, disclosure satisfy that the requirement of multiple color composition LOGO, can make the nickel layer of ceramic pipe surface
It is completed at the same time sintering in a process with LOGO, simple for process, identification pattern is clear, and color stability, glaze is smooth, can be improved
The class of product simultaneously has antiforge function.
Technical scheme is as follows：
A method of for identification LOGO on metallized ceramic pipe glaze, including steps are as follows：
1, colored glaze slip is prepared according to LOGO colors
1.1, it chooses following raw material according to weight percent and is mixed into colored glaze powder：The Unlead low-smelting point glass of 30-75%
Powder, the inorganic pigment of 10-40%, the silica flour of 5-15% or alumina powder, the clay of 1-5%, 4-10% wollastonites in powder, 1-
10% borax；The colored glaze powder of multiple color is obtained by selecting the inorganic pigment of different colours, to meet a variety of face of LOGO
Color demand；
1.2, the colored glaze powder for the multiple color being mixed into is separately added into the ball grinder of planetary ball mill, and liquid is added
Body alcohol forms glaze slip, and it is 4 to make solid-to-liquid ratio:1-1:1；Glaze slip particle is ground to 1-5 μm by planetary ball mill；
1.3, it is methocel solution that addition mass concentration, which is 1-5%, and addition is the 1-10% of glaze slip weight, then
The colored glaze slip of multiple color is made in ball milling 20-30 minutes；
2, hollow processing is carried out by the pattern of LOGO same colors with aluminium sheet, LOGO gear tools, the quantity of LOGO gear tools is made
It is suitable with the number of colors in LOGO；
3, the metallized ceramic pipe after nickel plating or print nickel is put into baking oven, 10-30 is kept the temperature at a temperature of 120-150 DEG C
It is taken out after minute；
4, metallized ceramic is managed and protected with LOGO gear tools, is required, is prepared by step 1 colored according to the color of LOGO
Glaze slip is added in glaze spraying pressurized tank, using forced carry out glaze spraying；Then according to the band color glaze of LOGO color replacement different colours
Slurry and corresponding LOGO gear tools are sprayed, until spraying complete LOGO；
5, the metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800-950 DEG C, completed
The identification LOGO on metallized ceramic pipe glaze.
As further preferred, the temperature of metallized ceramic pipe is 80-120 DEG C when glaze spraying in the step 4.
As further preferred, by planetary ball mill ball milling 20-60 minutes in the step 1.2, glaze slip particle is made to grind
It cuts to 1-5 μm.
The beneficial effects of the invention are as follows：
1, colored glaze slip prepared by the present invention uses lead-free glass powder with low melting point as major ingredient, can be in metallized ceramic
It is sintered simultaneously with nickel layer in the glaze layer double sintering process of pipe, reduces unnecessary process；Be added silica flour or alumina powder,
Wollastonite in powder and borax can adjust the physical properties such as glaze layer coefficient of thermal expansion, fusing point and surface tension, increase bottom glaze layer with
The adhesion strength of mark avoids LOGO marks from falling off；Clay and methylcellulose, which is added, can improve viscosity and the dispersion of glaze slip
Performance and glaze spraying operability；Using alcohol as solvent, make during glaze spraying can rapid curing it is qualitative, prevent glaze slip
Diffusion and other pollutions.
2, this method can realize chromatography glaze spraying, disclosure satisfy that the requirement of multiple color composition LOGO, can make ceramic pipe surface
Nickel layer and LOGO be completed at the same time sintering in a process, simple for process, identification pattern is clear, and color stability, glaze is smooth,
The electrically and mechanically performance of metallized ceramic pipe can be met the requirements after mark, still kept through 200 DEG C of thermal shocks, 10 marks
It is good.Due to blocking glaze spraying using LOGO gear tools, can solve metallized ceramic pipe curved surface be difficult to print, bat printing when identify it is excessive,
The yielding problem of pattern can spray upper LOGO patterns in entire glaze, can improve the class of product and have anti-fake work(
Energy.
Specific implementation mode
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is general
All other embodiment that logical technical staff is obtained without creative efforts, belongs to protection of the present invention
Range.Embodiment 1
A kind of method for identification LOGO on metallized ceramic pipe glaze of the present invention, including steps are as follows：
1, colored glaze slip is prepared according to LOGO colors
1.1, the colored glaze powder that following raw material is mixed into two kinds of colors is chosen：
A, lead-free glass powder with low melting point 30kg, cobalt system blue inorganic pigment 40kg, silica flour 10kg, clay 5kg, wollastonite
Powder 5kg, borax 10kg；
B, lead-free glass powder with low melting point 30kg, chromium system inorganic green pigment 40kg, silica flour 10kg, clay 5kg, wollastonite
Powder 5kg, borax 10kg；
The colored glaze powder of two kinds of colors is obtained by selecting the inorganic pigment of two kinds of different colours, to meet the two of LOGO
Kind color demand；
1.2, the colored glaze powder of be mixed into two kinds of colors is separately added into the ball grinder of planetary ball mill, and added respectively
Enter liquid alcohol and form glaze slip, it is 4 to make solid-to-liquid ratio:1；Start planetary ball mill, glaze slip particle is ground to by ball milling 20 minutes
1-5 μm；
1.3, it is methocel solution that addition mass concentration, which is 1%, and addition is the 1% of glaze slip weight, then ball milling
20 minutes, the colored glaze slip of two kinds of colors is made.
2, hollow processing is carried out by the pattern of LOGO same colors with aluminium sheet, LOGO gear tools, the quantity of LOGO gear tools is made
Suitable with the number of colors in LOGO, the present embodiment is by taking LOGO has two kinds of colors as an example.
3, the metallized ceramic pipe after nickel plating or print nickel is put into baking oven, is taken after keeping the temperature 30 minutes at a temperature of 120 DEG C
Go out.
4, metallized ceramic is managed and protected with LOGO gear tools, is required according to the color of LOGO, one kind prepared by step 1
The colored glaze slip of color is added in glaze spraying pressurized tank, using forced carry out glaze spraying；Then according to the other face of LOGO color replacements
The colored glaze slip of color and corresponding LOGO gear tools are sprayed, until spraying complete LOGO；Metallized ceramic pipe when glaze spraying
Temperature is 80-120 DEG C.
5, the metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800-950 DEG C, completed
The identification LOGO on metallized ceramic pipe glaze.
Embodiment 2
A kind of method for identification LOGO on metallized ceramic pipe glaze of the present invention, including steps are as follows：
1, colored glaze slip is prepared according to LOGO colors
1.1, the colored glaze powder that following raw material is mixed into two kinds of colors is chosen：
A, lead-free glass powder with low melting point 75kg, cobalt system blue inorganic pigment 10kg, silica flour 8kg, clay 1kg, wollastonite in powder
4kg, borax 2kg；
B, lead-free glass powder with low melting point 75kg, chromium system inorganic green pigment 10kg, silica flour 8kg, clay 1kg, wollastonite in powder
4kg, borax 2kg；
The colored glaze powder of two kinds of colors is obtained by selecting the inorganic pigment of two kinds of different colours, to meet the two of LOGO
Kind color demand；
1.2, the colored glaze powder of be mixed into two kinds of colors is separately added into the ball grinder of planetary ball mill, and added respectively
Enter liquid alcohol and form glaze slip, it is 2 to make solid-to-liquid ratio:1；Start planetary ball mill, glaze slip particle is ground to by ball milling 40 minutes
1-5 μm；
1.3, it is methocel solution that addition mass concentration, which is 3%, and addition is the 5% of glaze slip weight, then ball milling
25 minutes, the colored glaze slip of two kinds of colors is made.
2, hollow processing is carried out by the pattern of LOGO same colors with aluminium sheet, LOGO gear tools, the quantity of LOGO gear tools is made
Suitable with the number of colors in LOGO, the present embodiment is by taking LOGO has two kinds of colors as an example.
3, the metallized ceramic pipe after nickel plating or print nickel is put into baking oven, keeps the temperature at a temperature of 130 DEG C and takes after twenty minutes
Go out.
4, metallized ceramic is managed and protected with LOGO gear tools, is required according to the color of LOGO, one kind prepared by step 1
The colored glaze slip of color is added in glaze spraying pressurized tank, using forced carry out glaze spraying；Then according to the other face of LOGO color replacements
The colored glaze slip of color and corresponding LOGO gear tools are sprayed, until spraying complete LOGO；Metallized ceramic pipe when glaze spraying
Temperature is 80-120 DEG C.
5, the metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800-950 DEG C, completed
The identification LOGO on metallized ceramic pipe glaze.
Embodiment 3
A kind of method for identification LOGO on metallized ceramic pipe glaze of the present invention, including steps are as follows：
1, colored glaze slip is prepared according to LOGO colors
1.1, the colored glaze powder that following raw material is mixed into two kinds of colors is chosen：
A, lead-free glass powder with low melting point 50kg, cobalt system blue inorganic pigment 25kg, silica flour 15kg, clay 3kg, wollastonite
Powder 5kg, borax 1kg；
B, lead-free glass powder with low melting point 50kg, chromium system inorganic green pigment 25kg, silica flour 15kg, clay 3kg, wollastonite
Powder 5kg, borax 1kg；
The colored glaze powder of two kinds of colors is obtained by selecting the inorganic pigment of two kinds of different colours, to meet the two of LOGO
Kind color demand；
1.2, the colored glaze powder of be mixed into two kinds of colors is separately added into the ball grinder of planetary ball mill, and added respectively
Enter liquid alcohol and form glaze slip, it is 1 to make solid-to-liquid ratio:1；Start planetary ball mill, glaze slip particle is ground to by ball milling 60 minutes
1-5 μm；
1.3, it is methocel solution that addition mass concentration, which is 5%, and addition is the 10% of glaze slip weight, then ball
Mill 25 minutes, is respectively prepared the colored glaze slip of two kinds of colors.
2, hollow processing is carried out by the pattern of LOGO same colors with aluminium sheet, LOGO gear tools, the quantity of LOGO gear tools is made
Suitable with the number of colors in LOGO, the present embodiment is by taking LOGO has two kinds of colors as an example.
3, the metallized ceramic pipe after nickel plating or print nickel is put into baking oven, keeps the temperature at a temperature of 150 DEG C and takes after twenty minutes
Go out.
4, metallized ceramic is managed and protected with LOGO gear tools, is required according to the color of LOGO, one kind prepared by step 1
The colored glaze slip of color is added in glaze spraying pressurized tank, using forced carry out glaze spraying；Then according to the other face of LOGO color replacements
The colored glaze slip of color and corresponding LOGO gear tools are sprayed, until spraying complete LOGO；Metallized ceramic pipe when glaze spraying
Temperature is 80-120 DEG C.
5, the metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800-950 DEG C, completed
The identification LOGO on metallized ceramic pipe glaze.
Embodiment 4
A kind of method for identification LOGO on metallized ceramic pipe glaze of the present invention, including steps are as follows：
1, colored glaze slip is prepared according to LOGO colors
1.1, the colored glaze powder that following raw material is mixed into two kinds of colors is chosen：
A, lead-free glass powder with low melting point 50kg, cobalt system blue inorganic pigment 25kg, silica flour or alumina powder 5kg, clay
3kg, wollastonite in powder 10kg, borax 7kg；
B, lead-free glass powder with low melting point 50kg, chromium system inorganic green pigment 25kg, silica flour or alumina powder 5kg, clay
3kg, wollastonite in powder 10kg, borax 7kg；
The colored glaze powder of two kinds of colors is obtained by selecting the inorganic pigment of two kinds of different colours, to meet the two of LOGO
Kind color demand；
1.2, the colored glaze powder of be mixed into two kinds of colors is separately added into the ball grinder of planetary ball mill, and added respectively
Enter liquid alcohol and form glaze slip, it is 3 to make solid-to-liquid ratio:1；Start planetary ball mill, ball milling 20-60 minutes, until by glaze slip particle
It is ground to 1-5 μm；
1.3, it is methocel solution that addition mass concentration, which is 5%, and addition is the 8% of glaze slip weight, then ball milling
25 minutes, the colored glaze slip of two kinds of colors is respectively prepared.
2, hollow processing is carried out by the pattern of LOGO same colors with aluminium sheet, LOGO gear tools, the quantity of LOGO gear tools is made
Suitable with the number of colors in LOGO, the present embodiment is by taking LOGO has two kinds of colors as an example.
3, the metallized ceramic pipe after nickel plating or print nickel is put into baking oven, keeps the temperature at a temperature of 150 DEG C and takes after ten minutes
Go out.
4, metallized ceramic is managed and protected with LOGO gear tools, is required according to the color of LOGO, one kind prepared by step 1
The colored glaze slip of color is added in glaze spraying pressurized tank, using forced carry out glaze spraying；Then according to the other face of LOGO color replacements
The colored glaze slip of color and corresponding LOGO gear tools are sprayed, until spraying complete LOGO；Metallized ceramic pipe when glaze spraying
Temperature is 80-120 DEG C.
5, the metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800-950 DEG C, completed
The identification LOGO on metallized ceramic pipe glaze.
Although the embodiments of the present invention have been disclosed as above, but its institute not only in the description and the implementation
Row use, it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can hold
It changes places and realizes other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is simultaneously
It is not limited to specific details.
Claims (3)
1. a kind of method for identification LOGO on metallized ceramic pipe glaze, it is characterized in that comprising steps are as follows：
(1) colored glaze slip is prepared according to LOGO colors
1.1, it chooses following raw material according to weight percent and is mixed into colored glaze powder：The lead-free glass powder with low melting point of 30-75%,
The inorganic pigment of 10-40%, the silica flour of 5-15% or alumina powder, the clay of 1-5%, 4-10% wollastonites in powder, 1-10%
Borax；The colored glaze powder of multiple color is obtained by selecting the inorganic pigment of different colours, to meet the multiple color need of LOGO
It asks；
1.2, the colored glaze powder for the multiple color being mixed into is separately added into the ball grinder of planetary ball mill, and liquid alcohol is added
Glaze slip is formed, it is 4 to make solid-to-liquid ratio:1-1:1；Glaze slip particle is ground to 1-5 μm by planetary ball mill；
1.3, it is methocel solution that addition mass concentration, which is 1-5%, and addition is the 1-10% of glaze slip weight, then ball milling
20-30 minutes, the colored glaze slip of multiple color is made；
(2) carry out hollow processing by the pattern of LOGO same colors with aluminium sheet, be made LOGO gear tool, LOGO gear tool quantity with
Number of colors in LOGO is suitable；
(3) the metallized ceramic pipe after nickel plating or print nickel is put into baking oven, 10-30 minutes is kept the temperature at a temperature of 120-150 DEG C
After take out；
(4) metallized ceramic is managed and protected with LOGO gear tools, is required according to the color of LOGO, band color glaze prepared by step (1)
Slurry is added in glaze spraying pressurized tank, using forced carry out glaze spraying；Then according to the colored glaze slip of LOGO color replacement different colours
It is sprayed with corresponding LOGO gear tools, until spraying complete LOGO；
(5) the metallized ceramic pipe after glaze spraying is put into secondary hydrogen-burning stove, is sintered at 800-950 DEG C, completed in gold
Identification LOGO on categoryization ceramic tube glaze.
2. a kind of method for identification LOGO on metallized ceramic pipe glaze according to claim 1, it is characterized in that：It is described
The temperature of metallized ceramic pipe is 80-120 DEG C when glaze spraying in step (4).
3. a kind of method for identification LOGO on metallized ceramic pipe glaze according to claim 1, it is characterized in that：It is described
By planetary ball mill ball milling 20-60 minutes in step 1.2, glaze slip particle is made to be ground to 1-5 μm.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810396604.0A CN108609852A (en) | 2018-04-28 | 2018-04-28 | A method of for identification LOGO on metallized ceramic pipe glaze |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810396604.0A CN108609852A (en) | 2018-04-28 | 2018-04-28 | A method of for identification LOGO on metallized ceramic pipe glaze |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109626825A (en) * | 2019-01-17 | 2019-04-16 | 北京汉能光伏投资有限公司 | Inorganic glaze and preparation method thereof, colored glazed glass and preparation method thereof |
| CN112794735A (en) * | 2021-03-23 | 2021-05-14 | 季华实验室 | Preparation method of decorative wall brick and decorative wall brick |
| CN115957953A (en) * | 2022-12-30 | 2023-04-14 | 大亚车轮制造有限公司 | Lettering and color registering process for wheel |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103214269A (en) * | 2013-05-03 | 2013-07-24 | 景德镇神飞特种陶瓷有限公司 | Underglaze ceramic pigment paste and method for burning marks of electro-vacuum ceramic tube casing by using same |
-
2018
- 2018-04-28 CN CN201810396604.0A patent/CN108609852A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103214269A (en) * | 2013-05-03 | 2013-07-24 | 景德镇神飞特种陶瓷有限公司 | Underglaze ceramic pigment paste and method for burning marks of electro-vacuum ceramic tube casing by using same |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109626825A (en) * | 2019-01-17 | 2019-04-16 | 北京汉能光伏投资有限公司 | Inorganic glaze and preparation method thereof, colored glazed glass and preparation method thereof |
| CN112794735A (en) * | 2021-03-23 | 2021-05-14 | 季华实验室 | Preparation method of decorative wall brick and decorative wall brick |
| CN115957953A (en) * | 2022-12-30 | 2023-04-14 | 大亚车轮制造有限公司 | Lettering and color registering process for wheel |
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