CN108607490A - A kind of graphite reaction kettle convenient for cleaning - Google Patents

A kind of graphite reaction kettle convenient for cleaning Download PDF

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Publication number
CN108607490A
CN108607490A CN201810507942.7A CN201810507942A CN108607490A CN 108607490 A CN108607490 A CN 108607490A CN 201810507942 A CN201810507942 A CN 201810507942A CN 108607490 A CN108607490 A CN 108607490A
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CN
China
Prior art keywords
reaction kettle
graphite
kettle ontology
upper cover
fixedly connected
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810507942.7A
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Chinese (zh)
Inventor
林前锋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hunan Guosheng Graphite Technology Co Ltd
Original Assignee
Hunan Guosheng Graphite Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hunan Guosheng Graphite Technology Co Ltd filed Critical Hunan Guosheng Graphite Technology Co Ltd
Priority to CN201810507942.7A priority Critical patent/CN108607490A/en
Publication of CN108607490A publication Critical patent/CN108607490A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/02Apparatus characterised by being constructed of material selected for its chemically-resistant properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00245Avoiding undesirable reactions or side-effects
    • B01J2219/00252Formation of deposits other than coke
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/02Apparatus characterised by their chemically-resistant properties
    • B01J2219/0204Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
    • B01J2219/0227Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of graphite

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

The present invention relates to reaction kettle fields,More particularly to a kind of graphite reaction kettle convenient for cleaning,Including reaction kettle ontology,Upper cover body and tube body,It is connected with upper cover body above reaction kettle ontology,And it is fixedly connected with tube body above upper cover body,Closely it is welded with stabilizer blade below reaction kettle ontology,And observation window is installed in front of reaction kettle ontology,It is fixedly connected with feed inlet above upper cover body and on the left of tube body,This kind is convenient for the graphite reaction kettle of cleaning,After motor Y250M2 4B35 types start operation,Shaft will be driven,And shaft is made to stretch upwards,After shaft stretches upwards,Sliding block can be made along vertical pivot upward sliding,After sliding block upward sliding,Agitating shaft also simultaneously upward sliding,And drive the stirring thing of top,The stirring thing of top is set to deposit downwards and be uniformly mixed with the stirring thing of bottom,This kind can effectively solve the problems, such as that stirring thing stirring is non-uniform convenient for the graphite reaction kettle of cleaning,Improve the practicability of reaction kettle.

Description

A kind of graphite reaction kettle convenient for cleaning
Technical field
The present invention relates to reaction kettle technical fields, and in particular to a kind of graphite reaction kettle convenient for cleaning.
Background technology
The broad understanding of reaction kettle has the container physically or chemically reacted, is matched with parameter by the structure design to container Set, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed, reaction kettle be widely used in oil, chemical industry, Rubber, pesticide, dyestuff, medicine, food, for completing the pressure of the technical process such as vulcanization, nitrification, hydrogenation, hydrocarbonylation, polymerization, condensation Force container, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.;Material generally has carbon manganese steel, stainless steel, zirconium, Ni-based(It breathes out Family name, Monel, inconel)Alloy and other composite materials.
But the existing graphite reaction kettle convenient for cleaning, since in stirring, the stirring thing of bottom can only be stirred, And the stirring thing of top is unable to get sufficient stirring, causes stirring thing stirring uneven, and after long-time reaction kettle, reaction Bottom portion can accumulate many dirts, long, the Er Qiehui that washed away the not only time to reactor bottom using solution or high pressure water Corrosion reacting kettle bottom, the effect is unsatisfactory.
Invention content
The purpose of the present invention is intended to solve due to that in stirring, can only be stirred the stirring thing of bottom, and top Stirring thing be unable to get sufficient stirring, cause stirring thing stirring uneven, and after long-time reaction kettle, reactor bottom Many dirts can be accumulated, it is long to be washed away the not only time to reactor bottom using solution or high pressure water, but also can corrode anti- Bottom portion is answered, the technical issues of the effect is unsatisfactory provides a kind of graphite reaction kettle convenient for cleaning.
To achieve the above object, the present invention provides following technical solutions:A kind of graphite reaction kettle convenient for cleaning, including Reaction kettle ontology, upper cover body and tube body, the reaction kettle ontology top are connected with upper cover body, and solid above the upper cover body Surely it is connected with tube body, stabilizer blade is closely welded with below the reaction kettle ontology, and observation is installed in front of the reaction kettle ontology Window is fixedly connected with feed inlet above the upper cover body and on the left of tube body, motor Y250M2- is equipped in the tube body 4B35 types, and be equipped with below the motor Y250M2-4B35 types and be fixedly connected with vertical pivot, it is fixedly connected in the reaction kettle ontology There is inner cavity, is equipped with shaft at left and right sides of the vertical pivot, and slidably connect sliding block on the vertical pivot, the vertical pivot rotated down connects It is connected to bolt, agitating shaft is closely welded at left and right sides of the sliding block, reaction kettle ontology bottom end card has outlet valve, described interior Intracavitary portion is equipped with disk, and is closely welded with nut above the disk, and the nut is connect with bolt thread, described Nut inner wall full-filling has one layer of graphite powder, and swipe is fixedly connected with below the disk.
The present invention is further arranged to:The sliding block is connect by shaft with motor Y250M2-4B35 types, and the sliding block It is slided along vertical pivot.
The present invention is further arranged to:Filled layer is filled in the gap that the inner cavity is connect with reaction kettle ontology, it is described Filled layer is formed by graphite-filled.
The present invention is further arranged to:The observation window includes frame and transparent glass, and the observation window and reaction kettle Ontology is fixedly connected.
The present invention is further arranged to:The bolt is internally provided with bull stick, and the bull stick passes through vertical pivot and motor Y250M2-4B35 types connect.
The present invention is further arranged to:The swipe is equipped at least 100, and the swipe is uniformly arranged under disk Side.
The present invention is further arranged to:The reaction kettle body bottom portion sets that there are one the chassis that are made by graphite, and The thickness on the chassis is 3cm.
The present invention is further arranged to:Include a stainless steel core and one inside the agitating shaft made of graphite Graphite pipe sleeve, and the graphite-pipe hard-pressed bale that is locked is rolled in stainless steel core surface.
It is an advantage of the invention that:Compared with prior art:
1. this kind will drive shaft, and make convenient for the graphite reaction kettle of cleaning after motor Y250M2-4B35 types start operation Shaft stretches upwards, after shaft stretches upwards, sliding block can be made along vertical pivot upward sliding, after sliding block upward sliding, stirring Axis also upward sliding simultaneously, and drive the stirring thing of top makes the stirring thing of top deposition and mixed with the stirring thing of bottom downwards It closes uniformly, this kind can effectively solve the problems, such as that stirring thing stirring is non-uniform convenient for the graphite reaction kettle of cleaning, improve reaction kettle Practicability.
2. then opening upper cover body, and nut is directed at bolt, disk is made to be fixed with bolt, since nut inner wall is smeared There is one layer of graphite powder, and graphite powder has lubricity and acid resistance, so even if bolt is placed in bolt in dirt for a long time It will not occur to generate corrosion phenomenon, in order to repeatedly install disk, then bolt starts motor Y250M2-4B35 types, works as motor After Y250M2-4B35 types start running, and vertical pivot is driven, vertical pivot will drive bull stick, and after bull stick starts rotation, disk is opened immediately Begin to rotate, under the rotation of disk, swipe will quickly scrub the dirt deposited inside reaction kettle, not only efficient, and will not Injury response kettle, can be rapidly and effectively clean by dirt removal, the service life of extended reaction kettle.
The invention will be further described with specific embodiment with reference to the accompanying drawings of the specification.
Description of the drawings
Fig. 1 is the overall structure diagram of the embodiment of the present invention.
Fig. 2 is the reaction kettle ontology partial structurtes floor map of the embodiment of the present invention.
Fig. 3 is the disk partial structural diagram of the embodiment of the present invention.
In attached drawing:1- reaction kettle ontologies;2- stabilizer blades;3- observation windows;4- upper cover bodies;5- feed inlets;6- tube bodies;The inner cavities 7-; 8- filled layers;9- vertical pivots;10- shafts;11- agitating shafts;12- outlet valves;13- sliding blocks;14- motor Y250M2-4B35 types;15- Disk;16- swipes;17- nuts;18- bolts.
Specific implementation mode
Referring to Fig. 1-3, a kind of graphite reaction kettle convenient for cleaning disclosed by the invention, including reaction kettle ontology 1, upper cover body 4 and tube body 6,1 top of the reaction kettle ontology is connected with upper cover body 4, and 4 top of the upper cover body is fixedly connected with tube body 6,1 lower section of the reaction kettle ontology is closely welded with stabilizer blade 2, and 1 front of the reaction kettle ontology is equipped with observation window 3, described It is fixedly connected with feed inlet 5 above upper cover body 4 and positioned at 6 left side of tube body, motor Y250M2-4B35 is installed in the tube body 6 Type 14, and 14 lower section of the motor Y250M2-4B35 types is equipped with and is fixedly connected with vertical pivot 9, it is fixed in the reaction kettle ontology 1 to connect It is connected to inner cavity 7,9 left and right sides of the vertical pivot is equipped with shaft 10, and sliding block 13 is slidably connected on the vertical pivot 9, the sliding block 13 are connect by shaft 10 with motor Y250M2-4B35 types 14, and the sliding block 13 is slided along vertical pivot 9, works as motor After Y250M2-4B35 types 14 start operation, shaft 10 will be driven, and keeps shaft 10 flexible upwards, after shaft 10 is flexible upwards, Sliding block 13 can be made along 9 upward sliding of vertical pivot, after 13 upward sliding of sliding block, the also upward sliding simultaneously of agitating shaft 11 and drives The stirring thing of top makes the stirring thing of top deposit downwards and be uniformly mixed with the stirring thing of bottom, this kind is convenient for the stone of cleaning Black reaction kettle can effectively solve the problems, such as that stirring thing stirring is non-uniform, improve the practicability of reaction kettle, and 9 lower section of the vertical pivot turns Dynamic to be connected with bolt 18, the bolt 18 is internally provided with bull stick, and the bull stick passes through vertical pivot 9 and motor Y250M2-4B35 types 14 connect, and then open upper cover body 4, and nut 17 is directed at bolt 18, so that disk 15 is fixed with bolt 18, due to nut 17 Inner wall is coated with one layer of graphite powder, and graphite powder has lubricity and acid resistance, so even if bolt 18 is placed in dirt for a long time In dirt, bolt 18 will not occur to generate corrosion phenomenon, in order to repeatedly install disk 15, then start motor Y250M2- 4B35 types 14 after motor Y250M2-4B35 types 14 start running, and drive vertical pivot 9, and vertical pivot 9 will drive bull stick, when bull stick is opened Begin after rotation, disk 15 immediately begins to rotate, and under the rotation of disk 15, swipe 16 will be scrubbed quickly and be deposited inside reaction kettle Dirt, it is not only efficient, and will not injury response kettle, can be rapidly and effectively clean by dirt removal, extended reaction The service life of kettle, 13 left and right sides of the sliding block are closely welded with agitating shaft 11, and 1 bottom end card of the reaction kettle ontology has discharging Valve 12, the inner cavity is equipped with disk 15, and 15 top of the disk is closely welded with nut 17, and the nut 17 It is threadedly coupled with bolt 18,17 inner wall full-filling of the nut has one layer of graphite powder, 15 lower section of the disk to be fixedly connected with swipe 16。
Preferably, being filled with filled layer 8, the filled layer in the gap that the inner cavity 7 is connect with reaction kettle ontology 1 8 are formed by graphite-filled, since the heat-resisting quantity and acid resistance of graphite are good, can extend 1 service life of reaction kettle ontology.
Preferably, the observation window 3 includes frame and transparent glass, and the observation window 3 and reaction kettle ontology 1 are solid Fixed connection can be convenient for experiment and discharge by observation window with the situation inside observing response kettle ontology 1.
Preferably, the swipe 16 is equipped at least 100, and the swipe 16 is uniformly arranged in 15 lower section of disk, After disk 15 starts rotation, swipe 16 will be close to the bottom of inner cavity 7, and scrubs the dirt that 7 bottom of inner cavity is deposited repeatedly.
Preferably, 1 bottom of reaction kettle ontology is set, there are one the chassis being made by graphite, and the chassis Thickness be 3cm,, can gradual corrosion reacting kettle after long-time due to being easy many solution residues of accumulation in reaction kettle ontology 1 The bottom of ontology 1, and 1 bottom of reaction kettle ontology is caused to crack, since the chassis is made by graphite, and the high temperature resistant of graphite Property and acid resistance it is good, so can prevent 1 bottom of reaction kettle ontology crack the problem of.
Preferably, including a stainless steel core and a graphite-pipe made of graphite inside the agitating shaft 11 Set, and the graphite-pipe hard-pressed bale that is locked is rolled in stainless steel core surface, since the graphite-pipe hard-pressed bale that is locked is rolled in the surface of stainless steel core, So working as 11 long-time of agitating shaft using rear surface corrosion, graphite pipe sleeve and stainless steel core need to only be taken out, and be mounted on newly In agitating shaft 11, you can complete to replace, while decreasing cost.
Above-described embodiment is served only for that invention is further explained to the specific descriptions of the present invention, should not be understood as Limiting the scope of the present invention, it is non-that the technician of this field according to the content of foregoing invention makes some to the present invention The modifications and adaptations of essence are each fallen within protection scope of the present invention.
The 1- reaction kettle ontologies used in the present invention;2- stabilizer blades;3- observation windows;4- upper cover bodies;5- feed inlets;6- tube bodies; The inner cavities 7-;8- filled layers;9- vertical pivots;10- shafts;11- agitating shafts;12- outlet valves;13- sliding blocks;14- motors Y250M2-4B35 Type;15- disks;16- swipes;17- nuts;18- bolts, can be as obtained by being bought market or individual is customized.

Claims (5)

1. a kind of graphite reaction kettle convenient for cleaning, including reaction kettle ontology(1), upper cover body(4)And tube body(6), the reaction Kettle ontology(1)Top is connected with upper cover body(4), and the upper cover body(4)Top is fixedly connected with tube body(6), feature It is:The reaction kettle ontology(1)Lower section is closely welded with stabilizer blade(2), and the reaction kettle ontology(1)Front is equipped with observation Window(3), the upper cover body(4)Top and be located at tube body(6)Left side is fixedly connected with feed inlet(5), the tube body(6)Interior installation There are motor Y250M2-4B35 types(14), and the motor Y250M2-4B35 types(14)Lower section is equipped with and is fixedly connected with vertical pivot(9), The reaction kettle ontology(1)Inside it is fixedly connected with inner cavity(7), the vertical pivot(9)The left and right sides is equipped with shaft(10), and it is described perpendicular Axis(9)On slidably connect sliding block(13), the vertical pivot(9)Rotated down is connected with bolt(18), the sliding block(13)Left and right Both sides are closely welded with agitating shaft(11), the reaction kettle ontology(1)Bottom end card has outlet valve(12), the inner cavity installation There is disk(15), and the disk(15)Top is closely welded with nut(17), and the nut(17)With bolt(18)Spiral shell Line connects, the nut(17)Inner wall full-filling has one layer of graphite powder, the disk(15)Lower section is fixedly connected with swipe(16);Institute State inner cavity(7)With reaction kettle ontology(1)Filled layer is filled in the gap of connection(8), the filled layer(8)By graphite-filled At the swipe(16)Equipped at least 100, and the swipe(16)Uniformly it is arranged in disk(15)Under, the agitating shaft (11)Inside includes a stainless steel core and a graphite pipe sleeve made of graphite, and the graphite-pipe hard-pressed bale that is locked is rolled in Stainless steel core surface.
2. a kind of graphite reaction kettle convenient for cleaning according to claim 1, it is characterised in that:The sliding block(13)Pass through Shaft(10)With motor Y250M2-4B35 types(14)Connection, and the sliding block(13)Along vertical pivot(9)It is slided.
3. a kind of graphite reaction kettle convenient for cleaning according to claim 1, it is characterised in that:The observation window(3)Packet Include frame and transparent glass, and the observation window(3)With reaction kettle ontology(1)It is fixedly connected.
4. a kind of graphite reaction kettle convenient for cleaning according to claim 2, it is characterised in that:The bolt(18)It is internal Equipped with bull stick, and the bull stick passes through vertical pivot(9)With motor Y250M2-4B35 types(14)Connect.
5. a kind of graphite reaction kettle convenient for cleaning according to claim 1, it is characterised in that:The reaction kettle ontology (1)Bottom sets that there are one the chassis that are made by graphite, and the thickness on the chassis is 3cm.
CN201810507942.7A 2018-05-24 2018-05-24 A kind of graphite reaction kettle convenient for cleaning Pending CN108607490A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810507942.7A CN108607490A (en) 2018-05-24 2018-05-24 A kind of graphite reaction kettle convenient for cleaning

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810507942.7A CN108607490A (en) 2018-05-24 2018-05-24 A kind of graphite reaction kettle convenient for cleaning

Publications (1)

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CN108607490A true CN108607490A (en) 2018-10-02

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111518675A (en) * 2020-04-29 2020-08-11 中粮营养健康研究院有限公司 Agitating unit and lactic acid fermentation jar

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203944379U (en) * 2014-06-10 2014-11-19 赣县鑫亿化工有限公司 A kind of chemical reaction still
CN204093455U (en) * 2014-10-13 2015-01-14 曲阜市润海化工有限公司 Hydrogen peroxide bleaching stabilizer reactor
CN204503088U (en) * 2015-03-25 2015-07-29 洪泽时代生物科技有限公司 For the production of the reactor with cleaning device of inositol
CN105435728A (en) * 2015-12-25 2016-03-30 常州市金坛翰广科技有限公司 Reaction kettle with movable stirring structure
CN206415100U (en) * 2016-11-17 2017-08-18 骏能化工(龙南)有限公司 A kind of highly effective reaction kettle

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN203944379U (en) * 2014-06-10 2014-11-19 赣县鑫亿化工有限公司 A kind of chemical reaction still
CN204093455U (en) * 2014-10-13 2015-01-14 曲阜市润海化工有限公司 Hydrogen peroxide bleaching stabilizer reactor
CN204503088U (en) * 2015-03-25 2015-07-29 洪泽时代生物科技有限公司 For the production of the reactor with cleaning device of inositol
CN105435728A (en) * 2015-12-25 2016-03-30 常州市金坛翰广科技有限公司 Reaction kettle with movable stirring structure
CN206415100U (en) * 2016-11-17 2017-08-18 骏能化工(龙南)有限公司 A kind of highly effective reaction kettle

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111518675A (en) * 2020-04-29 2020-08-11 中粮营养健康研究院有限公司 Agitating unit and lactic acid fermentation jar

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Application publication date: 20181002