CN109464980A - A kind of hydrolysis kettle of improved Medicine intermediate production - Google Patents
A kind of hydrolysis kettle of improved Medicine intermediate production Download PDFInfo
- Publication number
- CN109464980A CN109464980A CN201811588913.4A CN201811588913A CN109464980A CN 109464980 A CN109464980 A CN 109464980A CN 201811588913 A CN201811588913 A CN 201811588913A CN 109464980 A CN109464980 A CN 109464980A
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- rotary shaft
- hydrolysis kettle
- medicine intermediate
- intermediate production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000006460 hydrolysis reaction Methods 0.000 title claims abstract description 21
- 239000003814 drug Substances 0.000 title claims abstract description 13
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 229940079593 drugs Drugs 0.000 title claims abstract description 11
- 238000005273 aeration Methods 0.000 claims abstract description 10
- 239000007921 spray Substances 0.000 claims abstract description 6
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- 238000005260 corrosion Methods 0.000 claims description 5
- 230000000694 effects Effects 0.000 abstract description 4
- 230000001376 precipitating Effects 0.000 abstract description 2
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- 239000002994 raw material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 208000008425 Protein Deficiency Diseases 0.000 description 1
- 238000005039 chemical industry Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000003628 erosive Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
- B01J19/285—Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/56—Mixers with shaking, oscillating, or vibrating mechanisms having a vibrating receptacle provided with stirring elements, e.g. independent stirring elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/40—Mixers using gas or liquid agitation, e.g. with air supply tubes
- B01F33/402—Mixers using gas or liquid agitation, e.g. with air supply tubes comprising supplementary stirring elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/40—Mixers using gas or liquid agitation, e.g. with air supply tubes
- B01F33/407—Mixers using gas or liquid agitation, e.g. with air supply tubes by blowing gas on the material from above
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/40—Mixers using gas or liquid agitation, e.g. with air supply tubes
- B01F33/409—Parts, e.g. diffusion elements; Accessories
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
Abstract
The present invention relates to a kind of hydrolysis kettle more particularly to a kind of hydrolysis kettles of improved Medicine intermediate production.The technical solution adopted by the present invention is that: a kind of hydrolysis kettle of improved Medicine intermediate production, including autoclave body, feed inlet is equipped at the top of autoclave body, autoclave body bottom is equipped with discharge port, blender is equipped with inside autoclave body, blender includes rotary shaft, paddle is equidistantly equipped in rotary shaft, anti- precipitating brush is installed below the lowermost paddle, the bottom end of anti-precipitating brush is close to autoclave body bottom, autoclave body is arranged on the support column, support baseboard is provided between support column and autoclave body, elastic parts is equipped between autoclave body and support column, the lower end of support baseboard is provided with high frequency oscillator, the outer upper ends of autoclave body are connected with roots blower, roots blower lower part is connected with aerated conduit, aerated conduit is deep into the side inside autoclave body and is connected with aeration spray head.The invention has the advantages that structurally reasonable, mixing effect is good, is conducive to improve product quality.
Description
Technical field
The present invention relates to a kind of hydrolysis kettle more particularly to a kind of hydrolysis kettles of improved Medicine intermediate production.
Background technique
Hydrolysis kettle is the equipment that reaction is hydrolyzed, and is widely used in the industries such as chemical industry, medicine, and usual hydrolysis kettle carries out anti-
Seasonable use process once fills it up with raw material, and residue and product are once discharged after the reaction was completed.The hydrolysis kettle stirring effect used now
Rate is low, and mixing effect is bad, is unable to fully degraded organic matter, seriously affects product quality.In addition, existing hydrolysis kettle is also deposited
It is easy to be deposited on autoclave body bottom in reactant, the situation that can not be stirred to has seriously affected product quality.Therefore, it should mention
It solves the above problems for a kind of new technical solution.
Summary of the invention
The purpose of the present invention is: against the above deficiency, provide it is a kind of structurally reasonable, among the good Medicine of using effect
The hydrolysis kettle of body production.
To achieve the above object, the technical solution adopted by the present invention is that:
A kind of hydrolysis kettle of improved Medicine intermediate production, including autoclave body, the autoclave body top are equipped with charging
Mouthful, autoclave body bottom is equipped with discharge port, is equipped with blender inside the autoclave body, and the blender includes rotary shaft, and the one of rotary shaft
The motor held and be arranged on autoclave body connects, and the other end of rotary shaft extend into autoclave body, equidistantly sets in the rotary shaft
There is paddle, anti-precipitating brush is installed, the bottom end of the anti-precipitating brush is close to the autoclave body bottom below the lowermost paddle
Portion, the autoclave body are arranged on the support column, support baseboard are provided between support column and autoclave body, in the autoclave body and support
Elastic parts is equipped between column, the lower end of the support baseboard is provided with high frequency oscillator, the outer upper ends connection of the autoclave body
There is roots blower, the roots blower lower part is connected with aerated conduit, and the aeration tube road is deep into the company of the side inside autoclave body
It is connected to aeration spray head.
Further technical solution is:
Described elastic parts one end is welded in the autoclave body, and the other end is welded on the support baseboard.
The surface that the inner wall surface of the autoclave body, the surface of rotary shaft, the surface of paddle, anti-precipitating are brushed is equipped with one layer
Corrosion-resistant coating.
The corrosion-resistant coating is polytetrafluorethylecoatings coatings.
Due to the application of above-mentioned technical proposal, the invention has the following advantages over the prior art:
1, hydrolysis kettle of the invention, it is structurally reasonable, provided with the aerated conduit being connected with roots blower, pass through aeration spray head
It injects air into reaction kettle, so that material dispersion is more evenly.
2, hydrolysis kettle of the invention is arranged dither in autoclave body bottom, autoclave body high frequency vibrating is driven in whipping process
It is dynamic, react the intracorporal raw material of kettle sufficiently.
3, anti-precipitating brush is arranged in autoclave body, ensure that the remnants of the smallest sediment of hydrolysis kettle for hydrolysis kettle of the invention
Amount, can be not only deposited on to avoid reactant autoclave body stirring less than the phenomenon that generation, decrease corruption of the reactant to autoclave body
Erosion.
Detailed description of the invention
Attached drawing 1 is schematic structural view of the invention.
In the figures above: 1, autoclave body, 2, feed inlet, 3, discharge port, 4, rotary shaft, 5, paddle, 6, anti-precipitating brush, 7, branch
Dagger, 8, support baseboard, 9, elastic parts, 10, aeration spray head, 11, high frequency oscillator, 12, roots blower, 13, aerated conduit,
14, motor.
Specific embodiment
The invention will be further described with reference to the accompanying drawings and embodiments:
Embodiment one:
As shown in Figure 1, as one embodiment of the invention, a kind of water of improved Medicine intermediate production
Kettle, including autoclave body 1 are solved, feed inlet 2 is equipped at the top of the autoclave body 1,1 bottom of autoclave body is equipped with discharge port 3, sets inside the autoclave body 1
There is blender, the blender includes rotary shaft 4, and one end of rotary shaft 4 is connect with the motor 14 being arranged on autoclave body 1, rotation
The other end of shaft 4 is extend into autoclave body 1, paddle 5 is equidistantly equipped in the rotary shaft 4, under the lowermost paddle 5
Side is equipped with anti-precipitating brush 6, and close to 1 bottom of autoclave body, the autoclave body 1 is arranged in the branch for the bottom end of the anti-precipitating brush 6
On dagger 7, it is provided with support baseboard 8 between support column 7 and autoclave body 1, elasticity is equipped between the autoclave body 1 and support baseboard 8
Component 9, the lower end of the support baseboard 8 are provided with high frequency oscillator 11, and the outer upper ends of the autoclave body 1 are connected with roots blower
12,12 lower part of roots blower is connected with aerated conduit 13, and the aeration tube road 13 is deep into the connection of the side inside autoclave body 1
There is aeration spray head 10.
Preferably, as second embodiment of the invention, the present embodiment is further limiting to embodiment one, described
9 one end of elastic parts is welded in the autoclave body 1, and the other end is welded on the support baseboard.
Preferably, as third embodiment of the invention, the present embodiment is the further improvement to embodiment two, described
The inner wall surface of autoclave body 1, the surface of rotary shaft 4, the surface of paddle 5, the anti-surface for precipitating brush 6 are equipped with one layer of anticorrosion
Layer.
Preferably, as the 4th embodiment of the invention, the present embodiment is further limiting to embodiment three, described
Corrosion-resistant coating is polytetrafluorethylecoatings coatings.
The above is a preferred embodiment of the present invention, it is noted that for those skilled in the art
For, without departing from the principles of the present invention, it can also make several improvements or replace, these are improved or replacement
It should be regarded as protection scope of the present invention.
Claims (4)
1. a kind of hydrolysis kettle of improved Medicine intermediate production, it is characterised in that: including autoclave body (1), the autoclave body
(1) top is equipped with feed inlet (2), and autoclave body (1) bottom is equipped with discharge port (3), and blender is equipped with inside the autoclave body (1), described
Blender includes rotary shaft (4), and one end of rotary shaft (4) is connect with the motor (14) being arranged on autoclave body (1), rotary shaft
(4) the other end is extend into autoclave body (1), is equidistantly equipped with paddle (5) on the rotary shaft (4), the lowermost paddle
(5) anti-precipitating brush (6) is installed, the bottom end of the anti-precipitating brush (6) is close to the autoclave body (1) bottom, the autoclave body below
(1) it is arranged on the support column (7), support baseboard (8) is provided between support column (7) and autoclave body (1), in the autoclave body
(1) elastic parts (9) are equipped between support baseboard (8), the lower end of the support baseboard (8) is provided with high frequency oscillator
(11), the outer upper ends of the autoclave body (1) are connected with roots blower (12), and roots blower (12) lower part is connected with aeration tube
Road (13), the aeration tube road (13) are deep into the internal side of autoclave body (1) and are connected with aeration spray head (10).
2. a kind of hydrolysis kettle of improved Medicine intermediate production according to claim 1, it is characterised in that: institute
It states elastic parts (9) one end to be welded in the autoclave body (1), the other end is welded on the support baseboard (8).
3. a kind of hydrolysis kettle of improved Medicine intermediate production according to claim 1, it is characterised in that: institute
The surface for stating the inner wall surface of autoclave body (1), the surface of rotary shaft (4) and paddle (5) is equipped with one layer of corrosion-resistant coating.
4. a kind of hydrolysis kettle of medicine intermediate production according to claim 3, it is characterised in that: the corrosion-resistant coating
For polytetrafluorethylecoatings coatings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811588913.4A CN109464980A (en) | 2018-12-24 | 2018-12-24 | A kind of hydrolysis kettle of improved Medicine intermediate production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811588913.4A CN109464980A (en) | 2018-12-24 | 2018-12-24 | A kind of hydrolysis kettle of improved Medicine intermediate production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109464980A true CN109464980A (en) | 2019-03-15 |
Family
ID=65677218
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811588913.4A Withdrawn CN109464980A (en) | 2018-12-24 | 2018-12-24 | A kind of hydrolysis kettle of improved Medicine intermediate production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109464980A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111672452A (en) * | 2020-06-25 | 2020-09-18 | 毛俭英 | Mix excellent portable reation kettle of effect |
| CN112246158A (en) * | 2020-09-30 | 2021-01-22 | 黄兴元 | Anti-solidification type magnetic stirring device for low-viscosity building coating |
-
2018
- 2018-12-24 CN CN201811588913.4A patent/CN109464980A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111672452A (en) * | 2020-06-25 | 2020-09-18 | 毛俭英 | Mix excellent portable reation kettle of effect |
| CN112246158A (en) * | 2020-09-30 | 2021-01-22 | 黄兴元 | Anti-solidification type magnetic stirring device for low-viscosity building coating |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190315 |
|
| WW01 | Invention patent application withdrawn after publication |