CN108593516A - Fireflood experimental provision and its manufacturing method - Google Patents

Fireflood experimental provision and its manufacturing method Download PDF

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Publication number
CN108593516A
CN108593516A CN201810309443.7A CN201810309443A CN108593516A CN 108593516 A CN108593516 A CN 108593516A CN 201810309443 A CN201810309443 A CN 201810309443A CN 108593516 A CN108593516 A CN 108593516A
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Prior art keywords
trepanning
natural core
experimental provision
casting
fireflood
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CN108593516B (en
Inventor
李秋
蒋有伟
关文龙
唐君实
郑浩然
周久宁
王晓春
易雷浩
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China Petroleum and Natural Gas Co Ltd
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China Petroleum and Natural Gas Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/0806Details, e.g. sample holders, mounting samples for testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample

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  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Mold Materials And Core Materials (AREA)
  • Molds, Cores, And Manufacturing Methods Thereof (AREA)

Abstract

The invention discloses a kind of fireflood experimental provision and its manufacturing methods, are related to combustion in situ experimental study field, and the manufacturing method of the fireflood experimental provision includes the following steps:The mold to match is formulated according to the size shape of natural core;The natural core is placed in the mold, and makes that there is gap between the natural core and model;Molten metal liquid is poured into the gap of the mold so that the metal liquid wraps the natural core;The natural core and the metal body of casting are taken out after metal liquid cooling;The first trepanning and the second trepanning are drilled on the metal body of casting, first trepanning and second trepanning are connected with the natural core.The present invention can carry out fireflood experiment using natural core.

Description

Fireflood experimental provision and its manufacturing method
Technical field
The present invention relates to combustion in situ experimental study field, more particularly to a kind of fireflood experimental provision and its manufacturing method.
Background technology
Currently, domestic explored heavy oil reserves up to 1,300,000,000 tons or so, account for about the 25%-30% of domestic total petroleum reserves. Because viscous crude has, density is big, viscosity is high, the characteristic of poor fluidity, and conventional waterflooding behavior method development effectiveness is poor, and fiery Drive technology has become one of the main method for improving thick oil recovery ratio.Fireflood technology is continuously injected into stratum by gas injection well Air simultaneously lights oil reservoir, realizes burning in layer, to which in-place oil to be pushed to a kind of oil production method of producing well from gas injection well.
One-dimensional combustion pipe tests the important parameters such as sedimentation of fuel amount during can measuring fireflood, is commented in fireflood studio One of important experimental method of valence.Current One-dimensional combustion pipe experiment generally uses sandpack column to carry out, i.e., fills out quartz sand In the pipe for entering steel, saturation crude oil is then passed to simulate reservoir condition.But sandpack column has certain disadvantages:1. Using quartz sand or bead as the framework material of model, surface is smooth, differs larger with true stratum interstitial space; It is micro- that 2. quartz sand and glass bead surface can not adhere to various metallic compounds developed in clay mineral and stratum etc., because And influence of the trace element to experimentation can not be simulated;3. sandpack column permeability is higher, low permeability reservoir, example can not be simulated As permeability is less than the reservoir of 1md.
Invention content
In order to overcome the drawbacks described above of the prior art, the technical problem to be solved is that provide one kind for the embodiment of the present invention Fireflood experimental provision and its manufacturing method can solve one of at least the above.
The specific technical solution of the embodiment of the present invention is:
A kind of manufacturing method of fireflood experimental provision, the manufacturing method of the fireflood experimental provision include the following steps:
The mold to match is formulated according to the size shape of natural core;
The natural core is placed in the mold, and makes that there is gap between the natural core and model;
Molten metal liquid is poured into the gap of the mold so that the metal liquid wraps the natural rock The heart;
The natural core and the metal body of casting are taken out after metal liquid cooling;
Be drilled with the first trepanning and the second trepanning on the metal body of casting, first trepanning and second trepanning with The natural core is connected.
In a preferred embodiment, the manufacturing method of the fireflood experimental provision is further comprising the steps of:
Multiple third trepannings are drilled on the metal body of casting, the third trepanning is located at first trepanning and described Between two trepannings, the third trepanning is connected with the natural core;
Multiple thermocouples are mounted respectively in the third trepanning.
In a preferred embodiment, the natural core is cylinder, and the inner cavity of the mold is cylinder, institute It states inner cavity and is more than the natural core.
In a preferred embodiment, the metal liquid includes at least following one:Iron, copper, aluminium, metal close Gold.
In a preferred embodiment, first trepanning and second trepanning are located at the phase of the metal body of casting To both ends.
In a preferred embodiment, the third trepanning is located on the side wall of the metal body of casting, linearly arranges Row, the third trepanning reach the center of the natural core.
In a preferred embodiment, the manufacturing method of the fireflood experimental provision is further comprising the steps of:
Thermal insulation material is wrapped up in the outside wall surface of the metal body of casting.
In a preferred embodiment, the natural core is the natural sandstone rock core drilled through in appearing in the wild.
A kind of fireflood experimental provision, the fireflood experimental provision include:
Natural core;The metal body of casting being wrapped in outside the natural core, be drilled on the metal body of casting the first trepanning, Second trepanning and multiple third trepannings, first trepanning and second trepanning are located at the opposite end of the metal body of casting, First trepanning and second trepanning are connected with the natural core, and the third trepanning is located at first trepanning Between second trepanning, the third trepanning reaches the center of the natural core;
Thermocouple in the third trepanning.
In a preferred embodiment, the natural core is cylinder, and first trepanning and described second is opened Hole is respectively communicated with the end face of the natural core, and the third trepanning is connected to the side wall of the natural core.
In a preferred embodiment, the fireflood experimental provision further includes:It is wrapped in the outer of the metal body of casting The thermal insulation material of wall surface.
In a preferred embodiment, the material of the metal body of casting includes at least following one:Iron, copper, aluminium, gold Belong to alloy.
In a preferred embodiment, internal thread, the third are all had in first trepanning and the second trepanning There is internal thread in trepanning.
Technical scheme of the present invention has following notable advantageous effect:
Fireflood experimental provision and its manufacturing method in the application can make using true rock core carry out fireflood experiment, Natural core can be given increasing sealing and shell that high pressure can be born by foundry engieering, it so not only can be with So that contacting close between the metal body of casting and natural core, the gas that when experiment is passed through natural core will not be along natural core side Wall surface alter into;Moreover, the metal body of casting is also possible that can use arbitrary high pressure, that is, the gas injected when testing in an experiment It can be arbitrary high pressure gas, metal casting body can bear the pressure.Carrying out fireflood experiment using true rock core can be with mould Influence of the trace element such as various metallic compounds developed in quasi- clay mineral and stratum to experimentation, effectively prevents existing Have in technology that quartz sand or bead are as framework material, since above-mentioned material surface is smooth, with true formation pore sky Between differ larger temperature, meet the natural core of requirement of experiment furthermore it is possible to need to choose according to experiment, for example, can make The natural core of selection reaches the requirement of low-permeability, so as to carry out the experiment of simulation low permeability reservoir.
With reference to following description and accompanying drawings, only certain exemplary embodiments of this invention is disclosed in detail, specifies the original of the present invention Reason can be in a manner of adopted.It should be understood that embodiments of the present invention are not so limited in range.In appended power In the range of the spirit and terms that profit requires, embodiments of the present invention include many changes, modifications and are equal.For a kind of reality The feature that the mode of applying is described and/or shown can be made in a manner of same or similar in one or more other embodiments With, it is combined with the feature in other embodiment, or substitute the feature in other embodiment.
Description of the drawings
Attached drawing described here is only used for task of explanation, and is not intended to limit model disclosed by the invention in any way It encloses.In addition, the shape and proportional sizes etc. of each component in figure are only schematical, it is used to help the understanding of the present invention, and It is not the specific shape and proportional sizes for limiting each component of the present invention.Those skilled in the art under the teachings of the present invention, can Implement the present invention to select various possible shapes and proportional sizes as the case may be.
Fig. 1 is the step flow chart of the manufacturing method of fireflood experimental provision in the embodiment of the present invention;
Fig. 2 is the schematic diagram of natural core in the manufacturing method of fireflood experimental provision in the embodiment of the present invention;
Fig. 3 is that natural core is placed in the signal in mold in the manufacturing method of fireflood experimental provision in the embodiment of the present invention Figure;
Fig. 4 is the structural schematic diagram of fireflood experimental provision in the embodiment of the present invention.
The reference numeral of the figures above:
1, natural core;2, mold;3, the metal body of casting;31, the first trepanning;32, the second trepanning;33, third trepanning;4, hot Galvanic couple;5, thermal insulation material.
Specific implementation mode
With reference to the drawings and the description of the specific embodiments of the present invention, the details of the present invention can clearly be understood.But It is the specific implementation mode of invention described herein, is only used for explaining the purpose of the present invention, and cannot understands in any way At being limitation of the present invention.Under the teachings of the present invention, technical staff is contemplated that the arbitrary possible change based on the present invention Shape, these are regarded as belonging to the scope of the present invention.It should be noted that when element is referred to as " being set to " another yuan Part, it can be directly on another element or there may also be elements placed in the middle.When an element is considered as " connection " Another element, it can be directly to another element or may be simultaneously present centering elements.Term " installation ", " connected ", " connection " shall be understood in a broad sense, for example, it may be mechanical connection or electrical connection, can also be inside two elements Connection, can be directly connected, can also indirectly connected through an intermediary, for the ordinary skill in the art, The concrete meaning of above-mentioned term can be understood as the case may be.Term as used herein " vertical ", " horizontal ", "upper", "lower", "left", "right" and similar statement for illustrative purposes only, are not offered as being unique embodiment. Unless otherwise defined, all of technologies and scientific terms used here by the article and the those skilled in the art for belonging to the application Normally understood meaning is identical.The term used in the description of the present application is intended merely to describe specifically to implement herein The purpose of mode, it is not intended that in limitation the application.Term as used herein "and/or" includes one or more relevant institutes Any and all combinations of list of items.
In order to directly carry out fireflood experiment using natural core, a kind of fireflood experimental provision is proposed in this application Manufacturing method, Fig. 1 is the step flow chart of the manufacturing method of fireflood experimental provision in the embodiment of the present invention, such as Fig. 1, and fireflood is real The manufacturing method of experiment device may comprise steps of:
S101:The mold 2 to match is formulated according to the size shape of natural core 1.
In this step, natural core 1 is drilled through in first appearing in the wild.The natural core 1 can select natural sandstone rock The heart, natural sandstone rock core can be used for simulating low permeability reservoir, to measure sedimentation of fuel amount etc. during low permeability reservoir fireflood Important parameter.In the application any restriction is not done to the shape of natural core 1, preferably, Fig. 2 is in the embodiment of the present invention The schematic diagram of natural core 1 in the manufacturing method of fireflood experimental provision, as shown in Fig. 2, natural core 1 can be cylinder.Example Such as, the diameter of rock core can be 100mm, and length can be selected in 500mm between 1000mm, and certainly, the size of rock core can root Setting is required according to the experiment.The mold 2 to match is formulated according to the size shape of natural core 1, for example, when natural core 1 is in circle When cylindricality, the inner cavity of mold 2 can also be cylinder, and inner cavity is more than natural core 1, and the diameter of grinding tool inner cavity is more straight than rock core Big 20mm of diameter or so, length 20mm longer than rock core length or so, so that natural core can be placed into the inner cavity of mold 2 1。
S102:Natural core 1 is placed in mold 2, and makes that there is gap between natural core 1 and model.
In this step, natural core 1 is placed in mold 2, Fig. 3 is the manufacture of fireflood experimental provision in the embodiment of the present invention Natural core 1 is placed in the schematic diagram in mold 2 in method, as shown in figure 3, keeping rock core and 2 surrounding of mold contactless, makes day So there is between rock core 1 and model gap.As the diameter of grinding tool inner cavity 20mm bigger than core diameter or so, length is than rock core length When long 20mm or so, the gap substantially 10mm or so.
S103:Molten metal liquid is poured into the gap of mold 2 so that metal liquid wraps natural core 1.
In this step, molten metal liquid is poured into the gap of mold 2, metal liquid is made to wrap natural core 1, Ensure that there is metal liquid covering in each face of rock core.Metal liquid can select the higher metal of metal strength after solidification, example Such as, metal liquid includes at least following one:Iron, copper, aluminium, metal alloy etc..
S104:Natural core 1 and the metal body of casting 3 are taken out after metal liquid cooling.
In this step, after metal liquid cooling, metal liquid is frozen into the metal body of casting 3, then by natural core 1 and gold Belong to the body of casting 3 to take out from mold 2.
S105:The first trepanning 31 and the second trepanning 32 are drilled on the metal body of casting 3, the first trepanning 31 and the second trepanning 32 are It is connected with natural core 1.
In this step, Fig. 4 is the structural schematic diagram of fireflood experimental provision in the embodiment of the present invention, as shown in figure 4, in gold Belong to and is drilled with the first trepanning 31 and the second trepanning 32 on the body of casting 3.When natural core 1 is cylindrical, the first trepanning 31 and second is opened Hole 32 is located at the opposite end of the metal body of casting 3, and the first trepanning 31 and the second trepanning 32 are connected with natural core 1.First Internal thread can be opened up in trepanning 31 and the second trepanning 32, so conveniently adopting manifold with note is connected.
S106:Multiple third trepannings 33 are drilled on the metal body of casting 3, third trepanning 33 is located at the first trepanning 31 and second and opens Between hole 32, third trepanning 33 is connected with natural core 1.
In this step, as shown in figure 4, being drilled with multiple third trepannings 33 on the metal body of casting 3.When natural core 1 is circle When cylindricality, third trepanning 33 between the first trepanning 31 and the second trepanning 32, meanwhile, third trepanning 33 is located at the metal body of casting 3 Side wall on, be arranged in a linear, third trepanning 33 reaches the center of natural core 1.Interior spiral shell can be opened up in third trepanning 33 Line so can be used for being connected with thermocouple 4.
S107:Multiple thermocouples 4 are mounted respectively in third trepanning 33.
In this step, as shown in figure 4, multiple thermocouples 4 are mounted respectively in third trepanning 33, the spiral shell of thermocouple 4 Line and the internal thread of third trepanning 33 are mutually twisted, and can so ensure the leakproofness of third trepanning 33 on the metal body of casting 3.Thermocouple 4 It is then inserted into the center of natural core 1, the temperature at the center for measuring natural core 1 in experiment.
S108:Thermal insulation material 5 is wrapped up in the outside wall surface of the metal body of casting 3.
In this step, as shown in figure 4, the outside wall surface in the metal body of casting 3 wraps up thermal insulation material 5, thermal insulation material 5 can select Asbestos are selected, thickness can be depending on specific heat insulation effect.
A kind of fireflood experimental provision is also proposed in this application, as shown in figure 4, the fireflood experimental provision may include: Natural core 1;The metal body of casting 3 being wrapped in outside natural core 1 is drilled with the first trepanning 31, the second trepanning 32 on the metal body of casting 3 With multiple third trepannings 33, the first trepanning 31 and the second trepanning 32 are located at the opposite end of the metal body of casting 3, the first trepanning 31 and Two trepannings 32 are connected with natural core 1, and third trepanning 33 is between the first trepanning 31 and the second trepanning 32, third trepanning 33 reach the center of natural core 1;Thermocouple 4 in third trepanning 33.In first trepanning 31 and the second trepanning 32 With internal thread, the first trepanning 31 and the second trepanning 32 are connected for adopting manifold with note, have internal thread in third trepanning 33, Be used to be connected with thermocouple 4 by the internal thread, at the same time it can also be ensured that on the metal body of casting 3 third trepanning 33 leakproofness.
Metal liquid can select the higher metal of metal strength after solidification, for example, the material of the metal body of casting 3 includes at least Following one:Iron, copper, aluminium, metal alloy.
In a preferred embodiment, natural core 1 can be cylinder, and the first trepanning 31 and the second trepanning 32 divide Not Lian Tong natural core 1 end face, third trepanning 33 be connected to natural core 1 side wall.For example, third trepanning 33 can be linear Arrangement, third trepanning 33 reaches the center of natural core 1, in this way, the temperature at 1 different location of natural core can be measured.
In a preferred embodiment, fireflood experimental provision further includes:It is wrapped in the guarantor of the outside wall surface of the metal body of casting 3 Adiabator 5, thermal insulation material 5 can select asbestos, thickness can be depending on specific heat insulation effect.Through the above way may be used To be kept the temperature to natural core 1 in fireflood experimentation, be conducive to the standard that 1 inside different location temperature of natural core measures True property.
Fireflood experimental provision and its manufacturing method in the application can make using true rock core carry out fireflood experiment, It can increase a shell seal and that high pressure can be born to natural core 1 by foundry engieering, so not only may be used So that contacting close between the metal body of casting 3 and natural core 1, the gas that when experiment is passed through natural core 1 will not be along natural 1 side wall surface of rock core alter into;Moreover, the metal body of casting 3 is noted it is also possible that can use in an experiment when arbitrary high pressure, i.e. experiment The gas entered can be arbitrary high pressure gas, and the metal body of casting 3 can bear the pressure.It is real that fireflood is carried out using true rock core Influence of the trace element such as various metallic compounds that can be simulated and be developed in clay mineral and stratum to experimentation is tested, effectively Quartz sand in the prior art or bead are avoided as framework material, since above-mentioned material surface is smooth, and truly Layer interstitial space differs larger temperature, furthermore it is possible to be needed to choose the natural core 1 for meeting requirement of experiment, example according to experiment Such as, the natural core 1 of selection can be made to reach the requirement of low-permeability, so as to carry out the experiment of simulation low permeability reservoir.
All articles and reference disclosed, including patent application and publication, for various purposes by quoting knot Together in this.The term " substantially by ... constitute " for describing combination should include identified element, ingredient, component or step and reality Other elements, ingredient, component or the step of the basic novel feature of the combination are not influenced in matter.Using term "comprising" or " comprising " describes the combination of element here, ingredient, component or step it is also contemplated that substantially by these elements, ingredient, component Or the embodiment that step is constituted.Here by using term " can with ", it is intended to illustrate that " can with " includes described any Attribute is all optional.Multiple element, ingredient, component or step can be carried by single integrated component, ingredient, component or step For.Alternatively, single integrated component, ingredient, component or step can be divided into multiple element, ingredient, component or the step of separation Suddenly.Open "a" or "an" for describing element, ingredient, component or step do not say in order to exclude other elements, at Point, component or step.
Each embodiment in this specification is described in a progressive manner, the highlights of each of the examples are with The difference of other embodiment, the same or similar parts between the embodiments can be referred to each other.Above-described embodiment is only Illustrate the technical concepts and features of the present invention, its object is to those skilled in the art can understand the contents of the present invention And implement according to this, it is not intended to limit the scope of the present invention.It is all according to equivalence changes made by spirit of the invention Or modification, it should be covered by the protection scope of the present invention.

Claims (13)

1. a kind of manufacturing method of fireflood experimental provision, which is characterized in that the manufacturing method of the fireflood experimental provision include with Lower step:
The mold to match is formulated according to the size shape of natural core;
The natural core is placed in the mold, and makes that there is gap between the natural core and model;
Molten metal liquid is poured into the gap of the mold so that the metal liquid wraps the natural core;
The natural core and the metal body of casting are taken out after metal liquid cooling;
Be drilled with the first trepanning and the second trepanning on the metal body of casting, first trepanning and second trepanning with it is described Natural core is connected.
2. the manufacturing method of fireflood experimental provision according to claim 1, which is characterized in that the fireflood experimental provision Manufacturing method is further comprising the steps of:
Multiple third trepannings are drilled on the metal body of casting, the third trepanning is located at first trepanning and described second and opens Between hole, the third trepanning is connected with the natural core;
Multiple thermocouples are mounted respectively in the third trepanning.
3. the manufacturing method of fireflood experimental provision according to claim 1, which is characterized in that the natural core is in cylinder The inner cavity of shape, the mold is cylinder, and the inner cavity is more than the natural core.
4. the manufacturing method of fireflood experimental provision according to claim 1, which is characterized in that the metal liquid at least wraps Include following one:Iron, copper, aluminium, metal alloy.
5. the manufacturing method of fireflood experimental provision according to claim 1, which is characterized in that first trepanning and described Second trepanning is located at the opposite end of the metal body of casting.
6. the manufacturing method of fireflood experimental provision according to claim 2, which is characterized in that the third trepanning is located at institute It on the side wall for stating the metal body of casting, is arranged in a linear, the third trepanning reaches the center of the natural core.
7. the manufacturing method of fireflood experimental provision according to claim 1, which is characterized in that the fireflood experimental provision Manufacturing method is further comprising the steps of:
Thermal insulation material is wrapped up in the outside wall surface of the metal body of casting.
8. the manufacturing method of fireflood experimental provision according to claim 7, which is characterized in that the natural core is out of office The natural sandstone rock core drilled through in appearing outside.
9. a kind of fireflood experimental provision, which is characterized in that the fireflood experimental provision includes:
Natural core;The metal body of casting being wrapped in outside the natural core is drilled with the first trepanning, second on the metal body of casting Trepanning and multiple third trepannings, first trepanning and second trepanning are located at the opposite end of the metal body of casting, described First trepanning and second trepanning are connected with the natural core, and the third trepanning is located at first trepanning and institute Between stating the second trepanning, the third trepanning reaches the center of the natural core;
Thermocouple in the third trepanning.
10. fireflood experimental provision according to claim 9, which is characterized in that the natural core is cylinder, and described One trepanning and second trepanning are respectively communicated with the end face of the natural core, and the third trepanning is connected to the natural core Side wall.
11. fireflood experimental provision according to claim 9, which is characterized in that the fireflood experimental provision further includes:Package In the thermal insulation material of the outside wall surface of the metal body of casting.
12. fireflood experimental provision according to claim 9, which is characterized in that the material of the metal body of casting includes at least Following one:Iron, copper, aluminium, metal alloy.
13. fireflood experimental provision according to claim 9, which is characterized in that in first trepanning and the second trepanning With internal thread, there is internal thread in the third trepanning.
CN201810309443.7A 2018-04-09 2018-04-09 Fireflood experimental device and manufacturing method thereof Active CN108593516B (en)

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