CN108584930A - A kind of production equipment of graphene - Google Patents

A kind of production equipment of graphene Download PDF

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Publication number
CN108584930A
CN108584930A CN201810715175.9A CN201810715175A CN108584930A CN 108584930 A CN108584930 A CN 108584930A CN 201810715175 A CN201810715175 A CN 201810715175A CN 108584930 A CN108584930 A CN 108584930A
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slot
wall
hole
side inner
reaction chamber
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CN201810715175.9A
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CN108584930B (en
Inventor
陈永贵
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Datong Xincheng New Material Co Ltd
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Datong Xincheng New Material Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/15Nano-sized carbon materials
    • C01B32/182Graphene
    • C01B32/184Preparation

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

The invention discloses a kind of production equipments of graphene, including reaction chamber, placing groove is offered on the both sides inner wall of the reaction chamber, the same placement ware is connected in two placing grooves, the bottom side for placing ware is installed with mounting blocks, the top side of the mounting blocks offers mounting groove, it is installed with motor on the bottom side inner wall of the mounting groove, placement ware top side vertical direction offers first through hole, shaft is rotatablely equipped in first through hole, and the both ends of shaft all extend to outside first through hole, the bottom end of the shaft is fixedly connected on the output shaft of motor, the top of shaft extends to outside first through hole and is fixedly connected with bull stick, feed inlet is offered on the top side inner wall of the reaction chamber.The configuration of the present invention is simple, can the more folding feed inlet of safe ready under the high temperature conditions, and graphite is evenly dispersed in and is placed on ware, facilitated people's operation, improve the uniformity of reaction, meet use demand.

Description

A kind of production equipment of graphene
Technical field
The present invention relates to technical field of graphene more particularly to a kind of production equipments of graphene.
Background technology
In recent years, grapheme material is always the Disciplinary Frontiers of scientific and technical innovation.Because of its outstanding electric conductivity, the electricity of superelevation The advantages such as transport factor and specific surface area, high heat conduction, high light transmission, high fracture strength and good chemical stability, are known as 21 The magical material in century is extremely wide in the application prospect of numerous technical fields.Therefore, develop low cost, large area, scale It prepares and realizes that the structure of graphene becomes the main research of current researchers with the regulatable technology of performance Target.
The patent of Publication No. CN207404847U discloses a kind of graphene production equipment, including microwave cavity, microwave Transmitter, support plate, places ware, spring, feed hopper and finished product receiving flask at vibrating mass, by placing setting vibration below ware Block can ensure that graphite oxide particle can be laid in and place on ware, can be full and uniform receive microwave irradiation, oxidation Rate of reduction is speeded, that is, has been speeded the speed of production of graphene, reduced resource waste, but the reaction temperature of graphene production Very high, the feed hopper and sealing plug manual operation difficulty of the device are big, and graphite is difficult to be uniformly dispersed on placing ware, therefore The use demand of people cannot be met, there are rooms for improvement.
Invention content
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of production of the graphene proposed is set It is standby.
To achieve the goals above, present invention employs following technical solutions:
A kind of production equipment of graphene, including reaction chamber, offer placing groove on the both sides inner wall of the reaction chamber, two The same placement ware is connected in placing groove, the bottom side for placing ware is installed with mounting blocks, the mounting blocks Top side offers mounting groove, and motor, placement ware top side vertical direction are installed on the bottom side inner wall of the mounting groove First through hole is offered, shaft is rotatablely equipped in first through hole, and the both ends of shaft all extend to outside first through hole, described turn The bottom end of axis is fixedly connected on the output shaft of motor, and the top of shaft extends to outside first through hole and be fixedly connected with bull stick, Offer feed inlet on the top side inner wall of the reaction chamber, offer locating slot on the side inner wall of the feed inlet, it is described into Loose slot is offered on the side inner wall of the remotely located slot of material mouth, and movable plate, and movable plate are movably installed in the loose slot Side extend to outside loose slot, and be adapted with locating slot, the movable plate top side is installed with outside loose slot Pushing hands, and the top of pushing hands extends to outside reaction chamber, the movable plate top side offers the groove in loose slot, described recessed It is rotatablely equipped with kelly on the side inner wall of the remotely located slot of slot, card slot is offered on the top side inner wall of the loose slot, it is described The second through-hole is offered on the top side inner wall of card slot, inserted link is movably installed in second through-hole, and the both ends of inserted link are prolonged It extends to outside the second through-hole.
Preferably, multiple microwave emitters, multiple microwave emitters are installed on the surrounding inner wall of the reaction chamber It is located at and places ware surrounding.
Preferably, the side of the remotely located slot of the movable plate is fixedly connected with one end of the first spring, the first spring The other end is fixedly welded on the side inner wall of the remotely located slot of loose slot.
Preferably, rotation slot is offered on the side inner wall of the remotely located slot of the groove, one end of kelly passes through rotation Axis is rotatably installed in rotation slot, and the other end bottom side of kelly is fixedly connected with one end of second spring, second spring it is another End is fixedly welded on the bottom side inner wall of groove.
Preferably, the top of the inserted link extends to outside reaction chamber and is installed with button, and the bottom end of the inserted link is prolonged It extends in card slot, and is flexibly connected with kelly.
Preferably, the fixed block in the second through-hole is arranged on the inserted link, the both sides of fixed block are fixedly mounted There is sliding block, sliding slot is offered on the both sides inner wall of the second through-hole, sliding block is slidably connected with sliding slot, and fixed block bottom side is fixedly connected There are one end of third spring, the other end of third spring to be fixedly connected on the bottom side inner wall of sliding slot.
Compared with prior art, the beneficial effects of the invention are as follows:
In the present invention, made by the cooperation of placing groove, placement ware, mounting blocks, mounting groove, motor, shaft, first through hole, bull stick With realizing can be evenly dispersed in from the graphite that feed inlet is put on placement ware, make graphite heated more abundant, pass through charging Mouth, locating slot, loose slot, movable plate, the first spring, groove, kelly, card slot, pushing hands, button, second through-hole, inserted link are matched It closes, realizes the more convenient safe folding of feed inlet, the configuration of the present invention is simple can under the high temperature conditions, more safe ready Folding feed inlet, and by graphite be evenly dispersed in place ware on, facilitate people operation, improve the uniformity of reaction, Meet use demand.Microwave emitter model 2M261-M32.
Description of the drawings
Fig. 1 is a kind of structural schematic diagram of the production equipment of graphene proposed by the present invention;
Fig. 2 is a kind of structural schematic diagram of the production equipment part A of graphene proposed by the present invention;
Fig. 3 is a kind of structural schematic diagram of the parts production equipment A1 of graphene proposed by the present invention.
In figure:1 reaction chamber, 2 microwave emitters, 3 placing grooves, 4 place wares, 5 mounting blocks, 6 mounting grooves, 7 motors, 8 shafts, 9 first through hole, 10 bull sticks, 11 feed inlets, 12 locating slots, 13 loose slots, 14 movable plates, 15 first springs, 16 grooves, 17 cards Bar, 18 card slots, 19 pushing hands, 20 buttons, 21 second through-holes, 22 inserted links.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Referring to Fig.1-3, a kind of production equipment of graphene, including reaction chamber 1 open up on the both sides inner wall of reaction chamber 1 There is placing groove 3, the same placement ware 4 is connected in two placing grooves 3, the bottom side for placing ware 4 is installed with mounting blocks 5, the top side of mounting blocks 5 offers mounting groove 6, and motor 7 is installed on the bottom side inner wall of mounting groove 6, and it is perpendicular to place 4 top side of ware Histogram is rotatablely equipped with shaft 8, and the both ends of shaft 8 all extend to first and lead to first through hole 9 is offered in first through hole 9 Outside hole 9, the bottom end of shaft 8 is fixedly connected on the output shaft of motor 7, and the top of shaft 8 extends to outside first through hole 9 and fixes It is connected with bull stick 10, feed inlet 11 is offered on the top side inner wall of reaction chamber 1, positioning is offered on the side inner wall of feed inlet 11 Slot 12 offers loose slot 13 on the side inner wall of 11 remotely located slot 12 of feed inlet, activity is movably installed in loose slot 13 Plate 14, and the side of movable plate 14 extends to outside loose slot 13, and be adapted with locating slot 12,14 top side of movable plate is fixedly mounted There is the pushing hands 19 outside loose slot 13, and the top of pushing hands 19 extends to outside reaction chamber 1,14 top side of movable plate, which offers, to be located at Groove 16 in loose slot 13 is rotatablely equipped with kelly 17 on the side inner wall of 16 remotely located slot 12 of groove, loose slot 13 Card slot 18 is offered on the inner wall of top side, offers the second through-hole 21 on the top side inner wall of card slot 18, activity peace in the second through-hole 21 Both ends equipped with inserted link 22, and inserted link 22 all extend to outside the second through-hole 21, by placing groove 3, place ware 4, mounting blocks 5, peace Tankage 6, motor 7, shaft 8, first through hole 9, bull stick 10 are used cooperatively, and realize that the graphite put into from feed inlet 11 can be uniform Ground, which is dispersed in, to be placed on ware 4, makes graphite heated more abundant, by feed inlet 11, locating slot 12, loose slot 13, movable plate 14, First spring 15, groove 16, kelly 17, card slot 18, pushing hands 19, the cooperation of button 20, the second through-hole 21, inserted link 22, realize into The more convenient safe folding of material mouth 11, the configuration of the present invention is simple, can under the high temperature conditions, more the folding of safe ready into Material mouth, and graphite is evenly dispersed in and is placed on ware, people's operation is facilitated, improves the uniformity of reaction, meeting makes Use demand.
Multiple microwave emitters 2 are installed on the surrounding inner wall of reaction chamber 1, multiple microwave emitters 2 are located at 4 surrounding of ware is placed, the side of 14 remotely located slot 12 of movable plate is fixedly connected with one end of the first spring 15, the first spring 15 The other end is fixedly welded on the side inner wall of 13 remotely located slot 12 of loose slot, the side inner wall of 16 remotely located slot 12 of groove On offer rotation slot, one end of kelly 17 is rotatably installed in by rotation axis in rotation slot, and the other end bottom side of kelly 17 is solid Surely it is connected with one end of second spring, the other end of second spring is fixedly welded on the bottom side inner wall of groove 16, inserted link 22 Top extends to outside reaction chamber 1 and is installed with button 20, and the bottom end of inserted link 22 extends in card slot 18, and lives with kelly 17 It is dynamic to connect, it is arranged with the fixed block in the second through-hole 21 on inserted link 22, the both sides of fixed block are installed with sliding block, the Sliding slot is offered on the both sides inner wall of two through-holes 21, sliding block is slidably connected with sliding slot, and fixed block bottom side is fixedly connected with third The other end of one end of spring, third spring is fixedly connected on the bottom side inner wall of sliding slot, by placing groove 3, places ware 4, peace Dress block 5, mounting groove 6, motor 7, shaft 8, first through hole 9, bull stick 10 are used cooperatively, and realize the graphite put into from feed inlet 11 Can be evenly dispersed in and place on ware 4, make graphite heated more abundant, by feed inlet 11, locating slot 12, loose slot 13, Movable plate 14, the first spring 15, groove 16, kelly 17, card slot 18, pushing hands 19, button 20, second through-hole 21, inserted link 22 are matched It closes, realizes the more convenient safe folding of feed inlet 11, the configuration of the present invention is simple can under the high temperature conditions, more secure side Just folding feed inlet, and graphite is evenly dispersed in and is placed on ware, people's operation is facilitated, the uniform of reaction is improved Property, meet use demand.
Operation principle:Lower button 20 is pressed downwards, and the sliding in third through-hole 21 downwards of inserted link 22, inserted link 22 is driven to squeeze card Bar 17, second spring are compressed so that and kelly 17 is detached from card slot 18, under the elastic force effect of the first spring 15,14 quilt of movable plate Loose slot 13 is released, when movable plate 14 enters locating slot 12, feed inlet 11 is closed, release button 20, then button 20 is the The effect of three springs is lower to be resetted, and when needing opening feed inlet 11 to feed intake, is pulled pushing hands 19, is made pushing hands 19 to the side far from card slot 12 To movement, movable plate 14 is driven to be detached from locating slot 12, the first spring 15 is compressed, when kelly 17 enters card slot 18, kelly 17 It is snapped into card slot 18 under second spring effect, movable plate 14 is fixed, conveniently feeds intake, and graphite is fallen into after the input of feeding port 11 It places on ware 4, opens motor 7, bull stick 10 is slowly rotated in the case where the rotary action of shaft 8 drives so that graphite is on placing ware 4 It uniformly spreads out so that heated evenly more abundant.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto, Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.

Claims (6)

1. a kind of production equipment of graphene, including reaction chamber(1), which is characterized in that the reaction chamber(1)Both sides inner wall on Offer placing groove(3), two placing grooves(3)Inside it is connected with the same placement ware(4), the placement ware(4)Bottom Side is installed with mounting blocks(5), the mounting blocks(5)Top side offer mounting groove(6), the mounting groove(6)Bottom side Motor is installed on inner wall(7), the placement ware(4)Top side vertical direction offers first through hole(9), first through hole (9)Inside it is rotatablely equipped with shaft(8), and shaft(8)Both ends all extend to first through hole(9)Outside, the shaft(8)Bottom end It is fixedly connected on motor(7)Output shaft on, shaft(8)Top extend to first through hole(9)Outside and it is fixedly connected with bull stick (10), the reaction chamber(1)Top side inner wall on offer feed inlet(11), the feed inlet(11)Side inner wall on open up There is locating slot(12), the feed inlet(11)Remotely located slot(12)Side inner wall on offer loose slot(13), the work Dynamic slot(13)Inside it is movably installed with movable plate(14), and movable plate(14)Side extend to loose slot(13)Outside, and with positioning Slot(12)It is adapted, the movable plate(14)Top side is installed with positioned at loose slot(13)Outer pushing hands(19), and pushing hands (19)Top extend to reaction chamber(1)Outside, the movable plate(14)Top side is offered positioned at loose slot(13)Interior groove (16), the groove(16)Remotely located slot(12)Side inner wall on be rotatablely equipped with kelly(17), the loose slot(13) Top side inner wall on offer card slot(18), the card slot(18)Top side inner wall on offer the second through-hole(21), described Two through-holes(21)Inside it is movably installed with inserted link(22), and inserted link(22)Both ends all extend to the second through-hole(21)Outside.
2. a kind of production equipment of graphene according to claim 1, which is characterized in that the reaction chamber(1)Surrounding Multiple microwave emitters are installed on inner wall(2), multiple microwave emitters(2)It is located at placement ware(4)Surrounding.
3. a kind of production equipment of graphene according to claim 1, which is characterized in that the movable plate(14)Far from fixed Position slot(12)Side be fixedly connected with the first spring(15)One end, the first spring(15)The other end be fixedly welded on activity Slot(13)Remotely located slot(12)Side inner wall on.
4. a kind of production equipment of graphene according to claim 1, which is characterized in that the groove(16)It is remotely located Slot(12)Side inner wall on offer rotation slot, kelly(17)One end be rotatably installed in rotation slot by rotation axis, block Bar(17)Other end bottom side be fixedly connected with one end of second spring, the other end of second spring is fixedly welded on groove(16) Bottom side inner wall on.
5. a kind of production equipment of graphene according to claim 1, which is characterized in that the inserted link(22)Top prolong Extend to reaction chamber(1)Outside and it is installed with button(20), the inserted link(22)Bottom end extend to card slot(18)It is interior, and with card Bar(17)Flexible connection.
6. a kind of production equipment of graphene according to claim 1, which is characterized in that the inserted link(22)On be arranged with Positioned at the second through-hole(21)The both sides of interior fixed block, fixed block are installed with sliding block, the second through-hole(21)Both sides in Sliding slot is offered on wall, sliding block is slidably connected with sliding slot, and fixed block bottom side is fixedly connected with one end of third spring, third bullet The other end of spring is fixedly connected on the bottom side inner wall of sliding slot.
CN201810715175.9A 2018-07-03 2018-07-03 Production facility of graphite alkene Active CN108584930B (en)

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Application Number Priority Date Filing Date Title
CN201810715175.9A CN108584930B (en) 2018-07-03 2018-07-03 Production facility of graphite alkene

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Application Number Priority Date Filing Date Title
CN201810715175.9A CN108584930B (en) 2018-07-03 2018-07-03 Production facility of graphite alkene

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CN108584930B CN108584930B (en) 2020-04-21

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111022594A (en) * 2019-12-01 2020-04-17 邳州高新区生物医药研究院有限公司 Medical treatment chemical waste gas high efficiency treatment equipment

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150050193A1 (en) * 2013-08-19 2015-02-19 Chang Gung University System for manufacturing graphene nanoribbon by continuous microwave
CN204999615U (en) * 2015-07-29 2016-01-27 中国科学院山西煤炭化学研究所 Quick expanded furnace of graphite alkene
CN206359250U (en) * 2016-12-26 2017-07-28 青岛迈可威微波创新科技有限公司 A kind of graphene preparation facilities
CN206705681U (en) * 2017-04-18 2017-12-05 青岛华高墨烯科技股份有限公司 A kind of continous way graphene microwave reduction stove
CN107539978A (en) * 2017-10-13 2018-01-05 南京旭羽睿材料科技有限公司 A kind of graphene production equipment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150050193A1 (en) * 2013-08-19 2015-02-19 Chang Gung University System for manufacturing graphene nanoribbon by continuous microwave
CN204999615U (en) * 2015-07-29 2016-01-27 中国科学院山西煤炭化学研究所 Quick expanded furnace of graphite alkene
CN206359250U (en) * 2016-12-26 2017-07-28 青岛迈可威微波创新科技有限公司 A kind of graphene preparation facilities
CN206705681U (en) * 2017-04-18 2017-12-05 青岛华高墨烯科技股份有限公司 A kind of continous way graphene microwave reduction stove
CN107539978A (en) * 2017-10-13 2018-01-05 南京旭羽睿材料科技有限公司 A kind of graphene production equipment

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111022594A (en) * 2019-12-01 2020-04-17 邳州高新区生物医药研究院有限公司 Medical treatment chemical waste gas high efficiency treatment equipment

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