CN108568138A - A kind of device and its extracting method extracting tanshinone compound from Radix Salviae Miltiorrhizae - Google Patents
A kind of device and its extracting method extracting tanshinone compound from Radix Salviae Miltiorrhizae Download PDFInfo
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- CN108568138A CN108568138A CN201810742779.2A CN201810742779A CN108568138A CN 108568138 A CN108568138 A CN 108568138A CN 201810742779 A CN201810742779 A CN 201810742779A CN 108568138 A CN108568138 A CN 108568138A
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- Prior art keywords
- extractor
- fixedly connected
- babinet
- temperature
- cooling piece
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- AIGAZQPHXLWMOJ-UHFFFAOYSA-N tanshinone IIA Natural products C1=CC2=C(C)C=CC=C2C(C(=O)C2=O)=C1C1=C2C(C)=CO1 AIGAZQPHXLWMOJ-UHFFFAOYSA-N 0.000 title claims abstract description 49
- 229930183118 Tanshinone Natural products 0.000 title claims abstract description 40
- -1 tanshinone compound Chemical class 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 15
- 238000001816 cooling Methods 0.000 claims abstract description 41
- 238000000605 extraction Methods 0.000 claims abstract description 23
- 238000005192 partition Methods 0.000 claims abstract description 16
- 239000000284 extract Substances 0.000 claims abstract description 11
- 239000002828 fuel tank Substances 0.000 claims description 17
- 238000001514 detection method Methods 0.000 claims description 13
- 239000002904 solvent Substances 0.000 claims description 9
- 241001072909 Salvia Species 0.000 claims description 5
- 235000017276 Salvia Nutrition 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 4
- 239000004480 active ingredient Substances 0.000 claims description 3
- 238000005057 refrigeration Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 238000010521 absorption reaction Methods 0.000 claims 1
- 235000013399 edible fruits Nutrition 0.000 claims 1
- 239000008188 pellet Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 description 7
- GVKKJJOMQCNPGB-UHFFFAOYSA-N Cryptotanshinone Natural products O=C1C(=O)C2=C3CCCC(C)(C)C3=CC=C2C2=C1C(C)CO2 GVKKJJOMQCNPGB-UHFFFAOYSA-N 0.000 description 3
- GVKKJJOMQCNPGB-JTQLQIEISA-N Cryptotanshinone Chemical compound O=C1C(=O)C2=C3CCCC(C)(C)C3=CC=C2C2=C1[C@@H](C)CO2 GVKKJJOMQCNPGB-JTQLQIEISA-N 0.000 description 3
- XDUXBBDRILEIEZ-LJQANCHMSA-N (6s)-6-(hydroxymethyl)-1,6-dimethyl-8,9-dihydro-7h-naphtho[1,2-g][1]benzofuran-10,11-dione Chemical compound O=C1C(=O)C2=C3CCC[C@](C)(CO)C3=CC=C2C2=C1C(C)=CO2 XDUXBBDRILEIEZ-LJQANCHMSA-N 0.000 description 2
- HYXITZLLTYIPOF-UHFFFAOYSA-N Tanshinone II Natural products O=C1C(=O)C2=C3CCCC(C)(C)C3=CC=C2C2=C1C(C)=CO2 HYXITZLLTYIPOF-UHFFFAOYSA-N 0.000 description 2
- XDUXBBDRILEIEZ-UHFFFAOYSA-N Tanshinone IIB Natural products O=C1C(=O)C2=C3CCCC(C)(CO)C3=CC=C2C2=C1C(C)=CO2 XDUXBBDRILEIEZ-UHFFFAOYSA-N 0.000 description 2
- 230000003110 anti-inflammatory effect Effects 0.000 description 2
- 230000004087 circulation Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- YFDKIHAZVQFLRC-UHFFFAOYSA-N methuyl tanshinonate Chemical compound C1=2OC=C(C)C=2C(=O)C(=O)C2=C1C=CC1=C2CCCC1(C)C(=O)OC YFDKIHAZVQFLRC-UHFFFAOYSA-N 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- AZEZEAABTDXEHR-UHFFFAOYSA-M sodium;1,6,6-trimethyl-10,11-dioxo-8,9-dihydro-7h-naphtho[1,2-g][1]benzofuran-2-sulfonate Chemical compound [Na+].C12=CC=C(C(CCC3)(C)C)C3=C2C(=O)C(=O)C2=C1OC(S([O-])(=O)=O)=C2C AZEZEAABTDXEHR-UHFFFAOYSA-M 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000032258 transport Effects 0.000 description 2
- HARGZZNYNSYSGJ-UHFFFAOYSA-N 1,2 dihydrotanshinquinone Natural products C1=CC2=C(C)C=CC=C2C(C(=O)C2=O)=C1C1=C2C(C)CO1 HARGZZNYNSYSGJ-UHFFFAOYSA-N 0.000 description 1
- 206010002383 Angina Pectoris Diseases 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- HARGZZNYNSYSGJ-JTQLQIEISA-N Dihydrotanshinone I Chemical compound C1=CC2=C(C)C=CC=C2C(C(=O)C2=O)=C1C1=C2[C@@H](C)CO1 HARGZZNYNSYSGJ-JTQLQIEISA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 241000304195 Salvia miltiorrhiza Species 0.000 description 1
- 235000011135 Salvia miltiorrhiza Nutrition 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 208000029078 coronary artery disease Diseases 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- KXNYCALHDXGJSF-UHFFFAOYSA-N dihydroisotanshinone I Natural products CC1=CC=CC2=C(C(C=3OCC(C=3C3=O)C)=O)C3=CC=C21 KXNYCALHDXGJSF-UHFFFAOYSA-N 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 239000002547 new drug Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000002137 ultrasound extraction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 230000029663 wound healing Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0207—Control systems
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0261—Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
- B01D11/0265—Applying ultrasound
Landscapes
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Automation & Control Theory (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention discloses a kind of from Radix Salviae Miltiorrhizae extracts the device and its extracting method of tanshinone compound, including bottom plate, it is fixedly connected with babinet at the top of the bottom plate, it is fixedly connected with partition board between the both sides of the cabinet wall, and extractor is fixedly connected at the top of partition board, the back side of the extractor is fixedly connected with heat conductive rod, it is fixedly connected with cooling piece between the both sides of the cabinet wall and positioned at the back side of extractor, and cooling piece is in contact close to the side of extractor with the one end of heat conductive rod far from extractor, the side of the cabinet wall and oil pump is fixedly connected with by link block positioned at the back side of cooling piece, it is related to tanshinone compound extractive technique field.Using the above structure with method, it can be achieved that the temperature in ultrasonic wave extraction tanshinone compound is strictly controlled, the accuracy of temperature is improved, has not only reduced the labor intensity of staff, but also good condition is created for subsequent extraction work.
Description
Technical field
The present invention relates to tanshinone compound technical fields, specially a kind of to extract tanshinone compound from Radix Salviae Miltiorrhizae
Device and its extracting method.
Background technology
Tanshinone is also known as total-tanshinone, is the fat-soluble phenanthrenequione chemical combination with bacteriostasis of middle extraction from salviamiltiorrhizabung
Object therefrom gets more than 10 tanshinone lists such as Tanshinone I, tanshinone IIA, tanshinone ⅡB, Cryptotanshinone and different Cryptotanshinone
Body, wherein Cryptotanshinone, dihydrotanshinone II, this 5 monomers of hydroxyl tanshinone, methyl tanshinonate and tanshinone ⅡB have anti-
Bacterium acts on, and still has anti-inflammatory and cooling effect, the sulfonated products sodium tanshinon Ⅱa silate of tanshinone IIA that can be dissolved in water, is tried through clinic
With treatment angina pectoris significant effect is proved, Small side effects, to treat the new drug of coronary heart disease, total-tanshinone has antibacterial, anti-inflammatory, promoting blood circulation
Many-sided effect such as stagnation resolvation and promotion wound healing, long-term use there are no apparent side effect.
It is important to note that tanshinone since tanshinone compound has a variety of medical values, when so being extracted in Radix Salviae Miltiorrhizae
The quality of compound, the method extracted at present have very much, and ultrasonic extraction is relatively common and practical extracting method,
In extraction process, need to carry out stringent control to temperature, by manually carrying out operation and control, not to temperature controlled accuracy
Height also brings many influences for subsequent extraction work.
Invention content
（One）The technical issues of solution
In view of the deficiencies of the prior art, the present invention provides a kind of from Radix Salviae Miltiorrhizae extracts the device of tanshinone compound, solves
When extracting tanshinone compound, temperature control it is inaccurate to influence compound quality the problem of.
（Two）Technical solution
In order to achieve the above object, the present invention is achieved by the following technical programs：One kind extracting tanshinone from Radix Salviae Miltiorrhizae
Close the device of object, including bottom plate is fixedly connected with babinet at the top of the bottom plate, fixed between the both sides of the cabinet wall to connect
It is connected to partition board, and is fixedly connected with extractor at the top of partition board, the back side of the extractor is fixedly connected with heat conductive rod, the case
Be fixedly connected with cooling piece between the both sides of internal wall and positioned at the back side of extractor, and cooling piece close to the side of extractor with
The one end of heat conductive rod far from extractor is in contact, the side of the cabinet wall and solid by link block positioned at the back side of cooling piece
Surely it is connected with oil pump, the oil outlet of the oil pump is communicated with flowline, the other side of the cabinet wall and positioned at cooling piece
The back side is fixedly connected with refrigerator, the other side of the cabinet wall and is fixedly connected with fuel tank positioned at the bottom of refrigerator, institute
It states the one end of flowline far from oil pump with the side of fuel tank to be connected, between the both sides of the cabinet wall and positioned at cooling piece
The back side is fixedly connected with heat conducting pipe, and the oil inlet of the oil pump is communicated with oil inlet pipe.
Preferably, the one end of the oil inlet pipe far from oil pump is connected with the side of heat conduction pipe surface, the bottom of the fuel tank
Portion is communicated with oil exit pipe, and the bottom end of the oil exit pipe is connected with the other side of heat conduction pipe surface.
Preferably, the top, bottom and both sides of the extractor offer mounting groove, and the inside of mounting groove is fixed and connected
It is connected to heater strip.
Preferably, the both sides at the extraction top tank structure back side have been fixedly connected with ultrasonic wave vibration plate, the cabinet wall back of the body
The side in face is fixedly connected with supersonic generator.
Preferably, the basal sliding of the cabinet wall is connected with sliding panel, and is fixedly connected with and connects at the top of sliding panel
Batch can, is communicated with feed pipe at the top of the extractor, and the top of the feed pipe is through babinet and extends to the top of babinet,
The bottom of the extractor is communicated with discharge nozzle, and the bottom end of the discharge nozzle runs through partition board and extends to the bottom of partition board, described
The inside of discharge nozzle is fixedly connected with solenoid valve.
Preferably, the other side at the cabinet wall back side is fixedly connected with rectangular box, and the inside of rectangular box is solid respectively
Surely it is connected with central processing unit and data comparing unit, the front of the babinet is hinged with chamber door, and chamber door surface by hinge
The side of bottom be fixedly connected with control switch, the front of the babinet and positioned at control switch bottom be fixedly connected with by
Key is fixedly connected with detection unit at the top of the extraction top tank structure.
Preferably, the output end of the central processing unit respectively with heater strip, cooling piece, supersonic generator, refrigerator,
Data comparing unit is connected with the input terminal of oil pump, the input terminal of the central processing unit respectively with control switch, power module,
Feedback module is connected with the output end of button, and the output end of the power module connects with the input terminal of detection unit and button respectively
Connect, and the output end of detection unit is connect with the input terminal of data comparing unit, the output end of the data comparing unit with it is anti-
The input terminal connection of module is presented, the data comparing unit includes the first data comparator and the second data comparator, the inspection
It includes the first temperature sensor and second temperature sensor, the output end and the first data of first temperature sensor to survey unit
The input terminal of comparator connects, and the output end of the second temperature sensor is connect with the input terminal of the second data comparator.
The invention also discloses a kind of from Radix Salviae Miltiorrhizae extracts the extracting method of tanshinone compound device, specifically include with
Lower step：
S1, first judgement need to input two temperature values in extractor, set a minimum value and maximum value, then pass through button
Minimum value and maximum value are separately input in the first data comparator and the second data comparator, as comparing data, first
Temperature sensor can be detected the temperature inside extractor, and the temperature value detected, which is then transmitted to the first data, compares
In device, the temperature value detected is compared with the minimum value of input in the first data comparator, the first data comparator
Numerical value is fed back into central processing unit through feedback module, if it is less than the minimum value of input, means that the temperature of extractor is too low,
Central processing unit can open heater strip simultaneously, and heater strip can heat up to extractor.
S2, second temperature sensor can be detected the temperature inside extractor, then pass the temperature value detected
It transports in the second data comparator, compares the maximum value of the temperature value detected and input in the second data comparator
Compared with numerical value is fed back to central processing unit by the second data comparator through feedback module, if it is greater than the maximum value of input, is meant that
Temperature in extractor is excessively high, while central processing unit opens control switch so that oil pump, cooling piece and refrigerator start work
Make, the heat generated inside extractor is transmitted to by heat conductive rod in cooling piece, and cooling piece can absorb heat, then pass through oil pump
Conduction oil after cooling in fuel tank is pumped by flowline and oil inlet pipe in heat conducting pipe, the heat on cooling piece is inhaled
It receives, then the conduction oil after absorbing heat is discharged into fuel tank by oil exit pipe and is cooled down again, circulation loop is consequently formed, with
On temperature control can keep certain temperature in ultrasonic wave extraction to tanshinone compound, and control certain
Within the scope of, subsequent extraction work can be conducive in this way.
S3, according to being controlled the temperature in extractor in S1 and S2 after, will by impregnate crushed after Salvia miltiorrhiza
Material is put by feed pipe in extractor, and solvent is added, and opens supersonic generator by central processing unit, ultrasonic wave occurs
Device drives the cavitation bubble collapse that ultrasonic wave vibration plate makes the red rooted salvia in extractor instantaneously generate in a solvent so that in tissue
Cell rupture so that the active ingredient in cell enters in solvent to the extraction conducive to tanshinone compound, finally extracts
Object is dropped by discharge nozzle in splice jug, and this completes entire work.
（Three）Advantageous effect
The present invention provides a kind of from Radix Salviae Miltiorrhizae extracts the device of tanshinone compound.Has following advantageous effect：
（1）, should from Radix Salviae Miltiorrhizae extract tanshinone compound device, heat conduction is fixedly connected with by the back side in extractor
Stick is fixedly connected with cooling piece between the both sides of cabinet wall and positioned at the back side of extractor, and cooling piece is close to extractor
Side be in contact with the one end of heat conductive rod far from extractor, pass through company in the side of cabinet wall and positioned at the back side of cooling piece
It connects block and is fixedly connected with oil pump, flowline is communicated in the oil outlet of oil pump, in the other side of cabinet wall and be located at cooling piece
The back side be fixedly connected with refrigerator, be fixedly connected with fuel tank in the other side of cabinet wall and positioned at the bottom of refrigerator,
The one end of flowline far from oil pump is connected with the side of fuel tank, the back side between the both sides of cabinet wall and positioned at cooling piece
It is fixedly connected with heat conducting pipe, is communicated with oil inlet pipe in the oil inlet of oil pump, then pass through oil exit pipe, mounting groove, heater strip, ultrasonic wave
Vibration plate, supersonic generator, central processing unit, data comparing unit, control switch, button, detection unit, power module and instead
Feedback module is equipped with, it can be achieved that the temperature in ultrasonic wave extraction tanshinone compound is strictly controlled, without people
Work is operated, and the accuracy of temperature is improved, and has not only reduced the labor intensity of staff, but also create for subsequent extraction work
Good condition is made.
（2）, should from Radix Salviae Miltiorrhizae extract tanshinone compound device, be connected with by the basal sliding in cabinet wall
Sliding panel, and splice jug is fixedly connected at the top of sliding panel, it can be achieved that carrying out unification to the tanshinone compound after extraction
Collection is handled, and is improved work efficiency, time saving and energy saving, is conveniently operated.
（3）, should from Radix Salviae Miltiorrhizae extract tanshinone compound device, by being communicated with discharging in the bottom of extractor
Pipe runs through partition board in the bottom end of discharge nozzle and extends to the bottom of partition board, solenoid valve is fixedly connected in the inside of discharge nozzle, can
Realization plays the tanshinone compound after extraction certain guiding role, brings many facilities to staff, adds
Fast extraction progress.
Description of the drawings
Fig. 1 is schematic structural view of the invention；
Fig. 2 is the sectional view of structure of the invention；
Fig. 3 is the vertical view of internal structure of the present invention；
Fig. 4 is the structural schematic diagram of heat conducting pipe of the present invention；
Fig. 5 is the structural principle block diagram of present system.
In figure：1 bottom plate, 2 babinets, 3 partition boards, 4 extractors, 5 heat conductive rods, 6 cooling pieces, 7 oil pumps, 8 flowlines, 9 refrigerators,
10 fuel tanks, 11 heat conducting pipes, 12 oil inlet pipes, 13 oil exit pipes, 14 mounting grooves, 15 heater strips, 16 ultrasonic wave vibration plates, 17 ultrasonic waves occur
Device, 18 sliding panels, 19 splice jugs, 20 feed pipes, 21 discharge nozzles, 22 solenoid valves, 23 rectangular boxes, 24 central processing units, 25 data
Comparing unit, 251 first data comparators, 252 second data comparators, 26 chamber doors, 27 control switches, 28 buttons, 29 detections
Unit, 291 first temperature sensors, 292 second temperature sensors, 30 power modules, 31 feedback modules.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
- 5 are please referred to Fig.1, the embodiment of the present invention provides a kind of technical solution：One kind extracting tanshinone chemical combination from Radix Salviae Miltiorrhizae
The top of the device of object, including bottom plate 1, bottom plate 1 is fixedly connected with babinet 2, be fixedly connected between the both sides of 2 inner wall of babinet every
Plate 3, and the top of partition board 3 is fixedly connected with extractor 4, the back side of extractor 4 is fixedly connected with heat conductive rod 5,2 inner wall of babinet
It is fixedly connected with cooling piece 6 between both sides and positioned at the back side of extractor 4, and cooling piece 6 is close to the side of extractor 4 and heat conduction
The one end of stick 5 far from extractor 4 is in contact, the side of 2 inner wall of babinet and positioned at cooling piece 6 the back side pass through link block fix connect
It is connected to oil pump 7, the oil outlet of oil pump 7 is communicated with flowline 8, the other side of 2 inner wall of babinet and is fixed positioned at the back side of cooling piece 6
It is connected with refrigerator 9, the other side of 2 inner wall of babinet and the bottom for being located at refrigerator 9 are fixedly connected with fuel tank 10, and flowline 8 is remote
One end from oil pump 7 is connected with the side of fuel tank 10, is fixed between the both sides of 2 inner wall of babinet and positioned at the back side of cooling piece 6
It is connected with heat conducting pipe 11, the oil inlet of oil pump 7 is communicated with oil inlet pipe 12.
In the present invention, the one end of oil inlet pipe 12 far from oil pump 7 is connected with the side on 12 surface of heat conducting pipe, the bottom of fuel tank 10
Portion is communicated with oil exit pipe 13, and the bottom end of oil exit pipe 13 is connected with the other side on 12 surface of heat conducting pipe.
In the present invention, top, bottom and the both sides of extractor 4 offer mounting groove 14, and the inside of mounting groove 14 is solid
Surely it is connected with heater strip 15.
In the present invention, the both sides at the 4 inner wall back side of extractor have been fixedly connected with ultrasonic wave vibration plate 16, the 2 inner wall back side of babinet
Side be fixedly connected with supersonic generator 17.
In the present invention, the basal sliding of 2 inner wall of babinet is connected with sliding panel 18, and the top of sliding panel 18 is fixedly connected with
Being equipped with for splice jug 19, sliding panel 18 and splice jug 19 can be achieved to carry out unified receipts to the tanshinone compound after extraction
Collection processing, improves work efficiency, time saving and energy saving, is conveniently operated, the top of extractor 4 is communicated with feed pipe 20, feed pipe 20
Top through babinet 2 and extend to the top of babinet 2, the bottom of extractor 4 is communicated with discharge nozzle 21, the bottom end of discharge nozzle 21
Through partition board 3 and the bottom of partition board 3 is extended to, the inside of discharge nozzle 21 is fixedly connected with solenoid valve 22, discharge nozzle 21 and electromagnetism
Valve 22, which can be realized, plays the tanshinone compound after extraction certain guiding role, to staff bring it is many just
Profit accelerates extraction progress.
In the present invention, the other side at the 2 inner wall back side of babinet is fixedly connected with rectangular box 23, and the inside difference of rectangular box 23
It is fixedly connected with central processing unit 24 and data comparing unit 25, the front of the model ARM9 of central processing unit 24, babinet 2 are logical
It crosses hinge and is hinged with chamber door 26, and the side of 26 surface bottom portion of chamber door is fixedly connected with control switch 27, the front and position of babinet 2
It is fixedly connected with button 28 in the bottom of control switch 27, detection unit 29 is fixedly connected at the top of 4 inner wall of extractor.
In the present invention, the output end of central processing unit 24 respectively with heater strip 15, cooling piece 6, supersonic generator 17, system
Cooler 9, data comparing unit 25 are connected with the input terminal of oil pump 7, the input terminal of central processing unit 24 respectively with control switch 27,
Power module 30, feedback module 31 are connected with the output end of button 28, the output end of power module 30 respectively with detection unit 29
It is connected with the input terminal of button 28, and the output end of detection unit 29 is connect with the input terminal of data comparing unit 25, data ratio
Output end compared with unit 25 is connect with the input terminal of feedback module 31, and data comparing unit 25 includes the first data comparator 251
With the second data comparator 252, detection unit 29 includes the first temperature sensor 291 and second temperature sensor 292, the first temperature
The output end of degree sensor 291 is connect with the input terminal of the first data comparator 251, the output end of second temperature sensor 292
It is connect with the input terminal of the second data comparator 252.
The invention also discloses a kind of from Radix Salviae Miltiorrhizae extracts the extracting method of tanshinone compound device, specifically include with
Lower step：
S1, first judgement need to input two temperature values in extractor 4, a minimum value and maximum value are set, then by pressing
Minimum value and maximum value are separately input in the first data comparator 251 and the second data comparator 252 by key 28, as comparing
Data, the first temperature sensor 291 can be detected the temperature inside extractor 4, then transmit the temperature value detected
Into the first data comparator 251, the temperature value detected and the minimum value of input are carried out in the first data comparator 251
Compare, numerical value is fed back to central processing unit 24 by the first data comparator 251 through feedback module, if it is less than the minimum of input
Value, means that the temperature of extractor 4 is too low, while central processing unit 24 can open heater strip 15, and heater strip 15 can be to extraction
Tank 4 heats up；
S2, second temperature sensor 292 can be detected the temperature inside extractor 4, then pass the temperature value detected
Transport in the second data comparator 252, in the second data comparator 252 by the temperature value detected and the maximum value of input into
Row compares, and numerical value is fed back to central processing unit 24 by the second data comparator 252 through feedback module 31, most if it is greater than input
Big value, means that the temperature in extractor 4 is excessively high, while central processing unit 24 opens control switch 27 so that oil pump 7, refrigeration
Piece 6 and refrigerator 9 are started to work, and the heat that 4 inside of extractor generates is transmitted to by heat conductive rod 5 in cooling piece 6, cooling piece 6
Heat can be absorbed, then conduction oil after cooling in fuel tank 10 is pumped into and is led by flowline 8 and oil inlet pipe 12 by oil pump 7
The heat on cooling piece 6 is absorbed in heat pipe 11, then the conduction oil after absorbing heat is discharged by oil by oil exit pipe 13
It is cooled down again in case 10, circulation loop is consequently formed, the control of above temperature can carry tanshinone compound in ultrasonic wave
Certain temperature can be kept when taking, and is controlled within the scope of certain, can be conducive to subsequent extraction work in this way；
S3, according to being controlled the temperature in extractor 4 in S1 and S2 after, will by impregnate crushed after red rooted salvia lead to
It crosses feed pipe 20 to be put into extractor 4, adds solvent, supersonic generator 17, ultrasonic wave are opened by central processing unit 24
Generator 17 drives the cavitation bubble collapse that ultrasonic wave vibration plate 16 makes the red rooted salvia in extractor 4 instantaneously generate in a solvent, makes
Obtain the cell rupture in tissue so that the active ingredient in cell enters in solvent to carrying conducive to tanshinone compound
It takes, last extract is dropped by discharge nozzle 21 in splice jug 19, and this completes entire work.
It should be noted that herein, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also include other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (8)
1. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae, including bottom plate（1）, it is characterised in that：The bottom plate（1）
Top be fixedly connected with babinet（2）, the babinet（2）It is fixedly connected with partition board between the both sides of inner wall（3）, and partition board（3）
Top be fixedly connected with extractor（4）, the extractor（4）The back side be fixedly connected with heat conductive rod（5）, the babinet（2）
Between the both sides of inner wall and it is located at extractor（4）The back side be fixedly connected with cooling piece（6）, and cooling piece（6）Close to extractor
（4）Side and heat conductive rod（5）Far from extractor（4）One end be in contact, the babinet（2）The side of inner wall and positioned at refrigeration
Piece（6）The back side oil pump is fixedly connected with by link block（7）, the oil pump（7）Oil outlet be communicated with flowline（8）, institute
State babinet（2）The other side of inner wall and be located at cooling piece（6）The back side be fixedly connected with refrigerator（9）, the babinet（2）Inner wall
The other side and be located at refrigerator（9）Bottom be fixedly connected with fuel tank（10）, the flowline（8）Far from oil pump（7）One
End and fuel tank（10）Side be connected, the babinet（2）Between the both sides of inner wall and it is located at cooling piece（6）The back side fix connect
It is connected to heat conducting pipe（11）, the oil pump（7）Oil inlet be communicated with oil inlet pipe（12）.
2. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae according to claim 1, it is characterised in that：It is described
Oil inlet pipe（12）Far from oil pump（7）One end and heat conducting pipe（12）The side on surface is connected, the fuel tank（10）Bottom connect
It is connected with oil exit pipe（13）, the oil exit pipe（13）Bottom end and heat conducting pipe（12）The other side on surface is connected.
3. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae according to claim 1, it is characterised in that：It is described
Extractor（4）Top, bottom and both sides offer mounting groove（14）, and mounting groove（14）Inside be fixedly connected with heating
Silk（15）.
4. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae according to claim 1, it is characterised in that：It is described
Extractor（4）The both sides at the inner wall back side have been fixedly connected with ultrasonic wave vibration plate（16）, the babinet（2）The side at the inner wall back side is solid
Surely it is connected with supersonic generator（17）.
5. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae according to claim 1, it is characterised in that：It is described
Babinet（2）The basal sliding of inner wall is connected with sliding panel（18）, and sliding panel（18）Top be fixedly connected with splice jug（19）,
The extractor（4）Top be communicated with feed pipe（20）, the feed pipe（20）Top run through babinet（2）And extend to case
Body（2）Top, the extractor（4）Bottom be communicated with discharge nozzle（21）, the discharge nozzle（21）Bottom end run through partition board
（3）And extend to partition board（3）Bottom, the discharge nozzle（21）Inside be fixedly connected with solenoid valve（22）.
6. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae according to claim 1, it is characterised in that：It is described
Babinet（2）The other side at the inner wall back side is fixedly connected with rectangular box（23）, and rectangular box（23）Inside be fixedly connected with respectively
Central processing unit（24）With data comparing unit（25）, the babinet（2）Front chamber door is hinged with by hinge（26）, and case
Door（26）The side of surface bottom portion is fixedly connected with control switch（27）, the babinet（2）Front and positioned at control switch
（27）Bottom be fixedly connected with button（28）, the extractor（4）Detection unit is fixedly connected at the top of inner wall（29）.
7. a kind of device extracting tanshinone compound from Radix Salviae Miltiorrhizae according to claim 6, it is characterised in that：It is described
Central processing unit（24）Output end respectively with heater strip（15）, cooling piece（6）, supersonic generator（17）, refrigerator（9）、
Data comparing unit（25）And oil pump（7）Input terminal connection, the central processing unit（24）Input terminal opened respectively with control
It closes（27）, power module（30）, feedback module（31）And button（28）Output end connection, the power module（30）Output
End respectively with detection unit（29）And button（28）Input terminal connection, and detection unit（29）Output end and data it is more single
Member（25）Input terminal connection, the data comparing unit（25）Output end and feedback module（31）Input terminal connection, institute
State data comparing unit（25）Including the first data comparator（251）With the second data comparator（252）, the detection unit
（29）Including the first temperature sensor（291）And second temperature sensor（292）, first temperature sensor（291）It is defeated
Outlet and the first data comparator（251）Input terminal connection, the second temperature sensor（292）Output end and second number
According to comparator（252）Input terminal connection.
8. a kind of extracting method for extracting tanshinone compound device from Radix Salviae Miltiorrhizae, which is characterized in that specifically include following step
Suddenly：
S1, first judgement need to input extractor（4）Two interior temperature values set a minimum value and maximum value, then pass through
Button（28）Minimum value and maximum value are separately input to the first data comparator（251）With the second data comparator（252）In,
As comparing data, the first temperature sensor（291）It can be to extractor（4）Internal temperature is detected, and then will be detected
Temperature value be transmitted to the first data comparator（251）In, in the first data comparator（251）It is interior by the temperature value detected with
The minimum value of input is compared, the first data comparator（251）Numerical value is fed back into central processing unit through feedback module（24）,
If it is less than the minimum value of input, extractor is meant that（4）Temperature it is too low, while central processing unit（24）Heating can be opened
Silk（15）, heater strip（15）It can be to extractor（4）It heats up；
S2, second temperature sensor（292）It can be to extractor（4）Internal temperature is detected, the temperature that then will be detected
Value is transmitted to the second data comparator（252）In, in the second data comparator（252）It is interior by the temperature value detected with input
Maximum value is compared, the second data comparator（252）By numerical value through feedback module（31）Feed back to central processing unit（24）, such as
Fruit is more than the maximum value of input, means that extractor（4）Interior temperature is excessively high, while central processing unit（24）Open control switch
（27）So that oil pump（7）, cooling piece（6）And refrigerator（9）It starts to work, extractor（4）The heat that inside generates passes through heat conduction
Stick（5）It is transmitted to cooling piece（6）It is interior, cooling piece（6）Heat can be absorbed, then passes through oil pump（7）By fuel tank（10）After interior cooling
Conduction oil pass through flowline（8）And oil inlet pipe（12）It is pumped into heat conducting pipe（11）It is interior to cooling piece（6）On heat inhaled
It receives, then passes through oil exit pipe（13）Conduction oil after absorption heat is discharged into fuel tank（10）It is inside cooled down again, is consequently formed and follows
Loop back path, the control of above temperature can keep tanshinone compound in ultrasonic wave extraction certain temperature, and
Control can be conducive to subsequent extraction work in this way within the scope of certain；
S3, according in S1 and S2 to extractor（4）It, will be by impregnating the red rooted salvia after crushed after interior temperature is controlled
Pass through feed pipe（20）It is put into extractor（4）It is interior, solvent is added, central processing unit is passed through（24）Open supersonic generator
（17）, supersonic generator（17）Drive ultrasonic wave vibration plate（16）Make extractor（4）Interior red rooted salvia instantaneously produces in a solvent
Raw cavitation bubble collapse so that the cell rupture in tissue so that the active ingredient in cell enters in solvent to conducive to pellet
Join the extraction of ketone compounds, last extract passes through discharge nozzle（21）Drop into splice jug（19）Interior, this completes whole
A work.
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| CN201810742779.2A CN108568138A (en) | 2018-07-09 | 2018-07-09 | A kind of device and its extracting method extracting tanshinone compound from Radix Salviae Miltiorrhizae |
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| CN201810742779.2A CN108568138A (en) | 2018-07-09 | 2018-07-09 | A kind of device and its extracting method extracting tanshinone compound from Radix Salviae Miltiorrhizae |
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Application publication date: 20180925 |