CN108559610A - A kind of preparation method of cooling and the good cutting fluid of cleaning performance - Google Patents
A kind of preparation method of cooling and the good cutting fluid of cleaning performance Download PDFInfo
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- CN108559610A CN108559610A CN201810600461.0A CN201810600461A CN108559610A CN 108559610 A CN108559610 A CN 108559610A CN 201810600461 A CN201810600461 A CN 201810600461A CN 108559610 A CN108559610 A CN 108559610A
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
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- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
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- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/04—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions having a silicon-to-carbon bond, e.g. organo-silanes
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- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
Abstract
The invention discloses a kind of preparation methods of cooling and the good cutting fluid of cleaning performance, include the following steps:(1)The preparation of modification biological carbon dust,(2)Raw material weigh it is spare,(3)Raw material is mixed with.The present invention optimizes the preparation method for improving cutting fluid, processing step is simple, it is reasonable to arrange in pairs or groups, and is easy to replicate and produce in batches, and corresponding manufactured cutting fluid cooling velocity is fast, cleaning performance is good, significantly improve quality and the service life of workpiece and cutter, the great market competitiveness and application value.
Description
Technical field
The invention belongs to metal cutting process processing technology fields, and in particular to a kind of to cool down and the good cutting of cleaning performance
The preparation method of liquid.
Background technology
Metal cutting process is most common, most widely used one kind in intermetallic composite coating.With advances in technology, cutting essence
Degree is higher and higher with strength demand, and the requirement to cutting fluid is also higher and higher.Most of research all concentrates on improving its profit at present
In sliding and antirust, but metal will produce amount of heat during the cutting process, makes workpiece temperature is excessively high to easy to produce thermal deformation, influences
Workpiece Machining Accuracy, cutting element are shortened with life of product, and What is more, and the temperature of cutting region can be made excessively high, are led to smog, are risen
Phenomena such as fiery.During the cutting process can the cooling effect of cutting fluid be by cutting fluid and the cutter to generate heat by cutting, chip
Convection current and vaporization between workpiece are taken away cutting heat from cutter and workpiece, to be effectively reduced cutting temperature, subtract
The thermal deformation of few workpiece and cutter, keeps the hardness of cutter, improves machining accuracy and tool life.Meanwhile in cutting process
In will produce certain dirt, if the cleaning performance of cutting fluid is bad, cutting members must be cleaned again, because
And under the premise of not influencing cutting fluid performance, the cutting fluid that research and development rate of temperature fall is high and cleaning performance is good has
There is highly important realistic meaning.
Invention content
The purpose of the present invention is for existing problem, provide a kind of preparation of cooling and the good cutting fluid of cleaning performance
Method.
The present invention is achieved by the following technical solutions:
A kind of preparation method of cooling and the good cutting fluid of cleaning performance, includes the following steps:
(1)It is prepared by modification biological carbon dust:
A. after first removing the other branch last years of maize straw, then with clear water to maize straw flushing one time, last segment is spare;
B. will operation a treated that maize straw is put into vapor tight tank, the water that temperature is 105 ~ 107 DEG C is passed through into vapor tight tank
Steam, while the pressure in vapor tight tank is increased into 0.5 ~ 0.55MPa, after heat-insulation pressure keeping handles 8 ~ 10min, then quickly unload to room temperature
Normal pressure finally takes out maize straw spare;
C. will operation b treated that maize straw is put into reaction kettle, first to reaction kettle vacuumize process, 18 ~ 20min is backward
Injection solution A submerges maize straw in reaction kettle, and the pressure in reaction kettle is then increased to 0.7 ~ 0.75MPa, and pressurize processing 35 ~
Maize straw is taken out after 38min, then maize straw is put into calcining furnace, the temperature in heating holding calcining furnace is
450 ~ 480 DEG C, maize straw is taken out after 1 ~ 1.2h of isothermal holding spare;The solution A by following parts by weight substance group
At:33 ~ 38 parts of butyl titanates, 2.5 ~ 3.5 parts of disodium ethylene diamine tetraacetates, 5 ~ 7 parts of cyclodextrin, 8 ~ 10 parts of silane coupling agents, 6
~ 8 parts of sodium pyrophosphates, 25 ~ 30 parts of ether, 780 ~ 800 parts of deionized waters;
D. will operation c treated that maize straw is immersed in solution B, it is 48 ~ 53 DEG C that heating, which keeps the temperature of solution B, is impregnated
Maize straw taking-up is put into ultraviolet irradiation instrument after 2 ~ 2.5h of processing, is taken out after 1 ~ 1.5h of radiation treatment spare;It is described
Solution B by following parts by weight material composition:5 ~ 7 parts of silver nitrates, 1 ~ 3 part of ammonium nitrate, 4 ~ 6 parts of sodium tetraborates, 90 ~ 100 parts
Deionized water;
E. will operation d treated that maize straw is put into pulverizer crosses 600 mesh after pulverization process to obtain modification biological carbon dust standby
With;
(2)Raw material weighs spare:
It is spare that following raw materials according is weighed by corresponding parts by weight:6 ~ 9 parts of polyethylene glycol, 10 ~ 15 portions of cottonseed oils, 15 ~ 20 portions of sunflower oils,
10 ~ 14 parts of dodecyl sodium sulfates, 2 ~ 4 parts of antifoaming agent, 20 ~ 25 parts of ethyl acetate, 10 ~ 14 parts of lauric monoglycerides, 3 ~ 6 parts
Kodalk, 8 ~ 11 parts of steps(1)Modification biological carbon dust obtained, 180 ~ 200 parts of deionized waters;
(3)Raw material is mixed with:
By step(2)All raw materials weighed are put into agitator tank jointly, then heating be kept stirring temperature in tank be 58 ~
63 DEG C, after high-speed stirred handles 40 ~ 45min, then 1 ~ 2h of ultrasonic homogenization.
Further, step(1)Quickly unloading to normal temperature and pressure described in operation b is in unloading vapor tight tank to normal in 35s
Normal temperature and pressure.
Further, step(1)It is silane coupling agent kh550, silane coupling agent to operate the silane coupling agent described in c
Any one in kh560, silane coupling agent kh570.
Further, step(1)Operate d described in radiation treatment when control ultraviolet irradiation instrument power be 1200 ~
1400W, the wavelength for controlling ultraviolet light are 300 ~ 350nm.
Further, step(2)Described in antifoaming agent be polyglycol ether.
Further, step(3)Described in high-speed stirred processing speed of agitator be 2000 ~ 2400 revs/min.
Further, step(3)Described in ultrasonic homogenization when ultrasonic wave frequency be 480 ~ 520kHz.
Present invention improves the preparation methods of cutting fluid, improve the use quality of cutting fluid well, ensure that cutting
Quality.First special a kind of modification biological carbon dust ingredient in its preparation process is made using substance based on maize straw,
The discarded harm burned to natural environment of maize straw is not only avoided, and the utilization rate and value of substance can be improved well,
In the preparation process of modification biological carbon dust, the explosion treatment that high temperature and pressure-quickly unloads warm release first has been carried out to maize straw,
Institutional framework inside loose maize straw well, expands fiber spacing, enhances its specific surface area and adsorption capacity,
It lays a good foundation for subsequent processing, the solution A then prepared with uniqueness carries out immersion modification, by butyl titanate, ring
The ingredients such as dextrin, silane coupling agent penetrate into maize straw, and wherein butyl titanate can be at follow-up 450 ~ 480 DEG C of calcining
Nano-titanium dioxide is formed when reason, while maize straw wood fibre is carbonized to form carbon fiber, nano-titanium dioxide is attached to
On carbon fiber surface, a kind of fiber tubular structure of complex cross-linked is generated, large specific surface area, adsorption capacity are strong, and stability is high,
Cyclodextrin and silane coupling agent ingredient can improve the surface property of biological carbon dust, promote its dispersing uniformity and to metal fragment
The adsorption capacity of particle, the solution B then prepared again with uniqueness carry out immersion modification, are then irradiated with ultraviolet light, in purple
Under the action of outside line irradiation reduction, the silver ion in solution B forms little particle metallic silver and is attached on three-dimensional carbon fiber pipe, a side
It can further promote the specific surface area and adsorption capacity of fibre pipe entirety in face, and on the other hand it is with good thermal conductivity, profit
In the quick conduction of cutting heat, the temperature of cutting is reduced.Coordinate being used in conjunction with for remaining ingredient, improves the effect of cutting.
The present invention has the following advantages compared with prior art:
The present invention optimizes the preparation method for improving cutting fluid, and processing step is simple, collocation is reasonable, is easy to replicate and batch is raw
Production, corresponding manufactured cutting fluid cooling velocity is fast, cleaning performance is good, hence it is evident that improves quality and the service life of workpiece and cutter, pole
Have the market competitiveness and application value.
Specific implementation mode
Embodiment 1
A kind of preparation method of cooling and the good cutting fluid of cleaning performance, includes the following steps:
(1)It is prepared by modification biological carbon dust:
A. after first removing the other branch last years of maize straw, then with clear water to maize straw flushing one time, last segment is spare;
B. will operation a treated that maize straw is put into vapor tight tank, the water that temperature is 105 DEG C is passed through into vapor tight tank and is steamed
Gas, while the pressure in vapor tight tank is increased into 0.5MPa, after heat-insulation pressure keeping handles 8min, then quickly unload to normal temperature and pressure, finally
Maize straw is taken out spare;
C. will operation b treated that maize straw is put into reaction kettle, first to reaction kettle vacuumize process, to anti-after 18min
Injection solution A submergence maize straw in kettle is answered, the pressure in reaction kettle is then increased into 0.7MPa, pressurize will after handling 35min
Maize straw takes out, and then maize straw is put into calcining furnace, and it is 450 DEG C that heating, which keeps the temperature in calcining furnace, heat preservation
Maize straw is taken out after processing 1h spare;The solution A by following parts by weight material composition:33 parts of butyl titanates,
2.5 parts of disodium ethylene diamine tetraacetates, 5 parts of cyclodextrin, 8 parts of silane coupling agents, 6 parts of sodium pyrophosphates, 25 parts of ether, 780 parts go from
Sub- water;
D. will operation c treated that maize straw is immersed in solution B, it is 48 DEG C that heating, which keeps the temperature of solution B, immersion treatment
Maize straw taking-up is put into ultraviolet irradiation instrument after 2h, is taken out after radiation treatment 1h spare;The solution B is by as follows
The material composition of parts by weight:5 parts of silver nitrates, 1 part of ammonium nitrate, 4 parts of sodium tetraborates, 90 parts of deionized waters;
E. will operation d treated that maize straw is put into pulverizer crosses 600 mesh after pulverization process to obtain modification biological carbon dust standby
With;
(2)Raw material weighs spare:
It is spare that following raw materials according is weighed by corresponding parts by weight:6 parts of polyethylene glycol, 10 portions of cottonseed oils, 15 portions of sunflower oils, 10 part 12
Sodium alkyl sulfonate, 2 parts of antifoaming agent, 20 parts of ethyl acetate, 10 parts of lauric monoglycerides, 3 parts of kodalks, 8 parts of steps(1)System
Modification biological carbon dust, 180 parts of deionized waters;
(3)Raw material is mixed with:
By step(2)All raw materials weighed are put into agitator tank jointly, and it is 58 that then heating, which is kept stirring the temperature in tank,
DEG C, after high-speed stirred handles 40min, then ultrasonic homogenization 1h.
Further, step(1)Quickly unloading to normal temperature and pressure described in operation b is in unloading vapor tight tank to normal in 35s
Normal temperature and pressure.
Further, step(1)It is silane coupling agent kh550 to operate the silane coupling agent described in c.
Further, step(1)The power of control ultraviolet irradiation instrument is 1200W when operating the radiation treatment described in d,
The wavelength for controlling ultraviolet light is 300 ~ 350nm.
Further, step(2)Described in antifoaming agent be polyglycol ether.
Further, step(3)Described in high-speed stirred processing speed of agitator be 2000 revs/min.
Further, step(3)Described in ultrasonic homogenization when ultrasonic wave frequency be 480kHz.
Embodiment 2
A kind of preparation method of cooling and the good cutting fluid of cleaning performance, includes the following steps:
(1)It is prepared by modification biological carbon dust:
A. after first removing the other branch last years of maize straw, then with clear water to maize straw flushing one time, last segment is spare;
B. will operation a treated that maize straw is put into vapor tight tank, the water that temperature is 106 DEG C is passed through into vapor tight tank and is steamed
Gas, while the pressure in vapor tight tank is increased into 0.53MPa, after heat-insulation pressure keeping handles 9min, then quickly unload to normal temperature and pressure, finally
Maize straw is taken out spare;
C. will operation b treated that maize straw is put into reaction kettle, first to reaction kettle vacuumize process, to anti-after 19min
Injection solution A submergence maize straw in kettle is answered, the pressure in reaction kettle is then increased into 0.73MPa, pressurize will after handling 37min
Maize straw takes out, and then maize straw is put into calcining furnace, and it is 460 DEG C that heating, which keeps the temperature in calcining furnace, heat preservation
Maize straw is taken out after processing 1.1h spare;The solution A by following parts by weight material composition:35 parts of four fourths of metatitanic acid
Ester, 3 parts of disodium ethylene diamine tetraacetates, 6 parts of cyclodextrin, 9 parts of silane coupling agents, 7 parts of sodium pyrophosphates, 28 parts of ether, 790 parts go from
Sub- water;
D. will operation c treated that maize straw is immersed in solution B, it is 50 DEG C that heating, which keeps the temperature of solution B, immersion treatment
Maize straw taking-up is put into ultraviolet irradiation instrument after 2.2h, is taken out after radiation treatment 1.3h spare;The solution B by
The material composition of following parts by weight:6 parts of silver nitrates, 2 parts of ammonium nitrate, 5 parts of sodium tetraborates, 95 parts of deionized waters;
E. will operation d treated that maize straw is put into pulverizer crosses 600 mesh after pulverization process to obtain modification biological carbon dust standby
With;
(2)Raw material weighs spare:
It is spare that following raw materials according is weighed by corresponding parts by weight:8 parts of polyethylene glycol, 13 portions of cottonseed oils, 18 portions of sunflower oils, 12 part 12
Sodium alkyl sulfonate, 3 parts of antifoaming agent, 23 parts of ethyl acetate, 12 parts of lauric monoglycerides, 5 parts of kodalks, 10 parts of steps(1)
Modification biological carbon dust obtained, 190 parts of deionized waters;
(3)Raw material is mixed with:
By step(2)All raw materials weighed are put into agitator tank jointly, and it is 60 that then heating, which is kept stirring the temperature in tank,
DEG C, after high-speed stirred handles 43min, then ultrasonic homogenization 1.5h.
Further, step(1)Quickly unloading to normal temperature and pressure described in operation b is in unloading vapor tight tank to normal in 35s
Normal temperature and pressure.
Further, step(1)It is silane coupling agent kh560 to operate the silane coupling agent described in c.
Further, step(1)The power of control ultraviolet irradiation instrument is 1300W when operating the radiation treatment described in d,
The wavelength for controlling ultraviolet light is 300 ~ 350nm.
Further, step(2)Described in antifoaming agent be polyglycol ether.
Further, step(3)Described in high-speed stirred processing speed of agitator be 2200 revs/min.
Further, step(3)Described in ultrasonic homogenization when ultrasonic wave frequency be 500kHz.
Embodiment 3
A kind of preparation method of cooling and the good cutting fluid of cleaning performance, includes the following steps:
(1)It is prepared by modification biological carbon dust:
A. after first removing the other branch last years of maize straw, then with clear water to maize straw flushing one time, last segment is spare;
B. will operation a treated that maize straw is put into vapor tight tank, the water that temperature is 107 DEG C is passed through into vapor tight tank and is steamed
Gas, while the pressure in vapor tight tank is increased into 0.55MPa, after heat-insulation pressure keeping handles 10min, then quickly unload to normal temperature and pressure, most
Maize straw is taken out afterwards spare;
C. will operation b treated that maize straw is put into reaction kettle, first to reaction kettle vacuumize process, to anti-after 20min
Injection solution A submergence maize straw in kettle is answered, the pressure in reaction kettle is then increased into 0.75MPa, pressurize will after handling 38min
Maize straw takes out, and then maize straw is put into calcining furnace, and it is 480 DEG C that heating, which keeps the temperature in calcining furnace, heat preservation
Maize straw is taken out after processing 1.2h spare;The solution A by following parts by weight material composition:38 parts of four fourths of metatitanic acid
Ester, 3.5 parts of disodium ethylene diamine tetraacetates, 7 parts of cyclodextrin, 10 parts of silane coupling agents, 8 parts of sodium pyrophosphates, 30 parts of ether, 800 parts
Deionized water;
D. will operation c treated that maize straw is immersed in solution B, it is 53 DEG C that heating, which keeps the temperature of solution B, immersion treatment
Maize straw taking-up is put into ultraviolet irradiation instrument after 2.5h, is taken out after radiation treatment 1.5h spare;The solution B by
The material composition of following parts by weight:7 parts of silver nitrates, 3 parts of ammonium nitrate, 6 parts of sodium tetraborates, 100 parts of deionized waters;
E. will operation d treated that maize straw is put into pulverizer crosses 600 mesh after pulverization process to obtain modification biological carbon dust standby
With;
(2)Raw material weighs spare:
It is spare that following raw materials according is weighed by corresponding parts by weight:9 parts of polyethylene glycol, 15 portions of cottonseed oils, 20 portions of sunflower oils, 14 part 12
Sodium alkyl sulfonate, 4 parts of antifoaming agent, 25 parts of ethyl acetate, 14 parts of lauric monoglycerides, 6 parts of kodalks, 11 parts of steps(1)
Modification biological carbon dust obtained, 200 parts of deionized waters;
(3)Raw material is mixed with:
By step(2)All raw materials weighed are put into agitator tank jointly, and it is 63 that then heating, which is kept stirring the temperature in tank,
DEG C, after high-speed stirred handles 45min, then ultrasonic homogenization 2h.
Further, step(1)Quickly unloading to normal temperature and pressure described in operation b is in unloading vapor tight tank to normal in 35s
Normal temperature and pressure.
Further, step(1)It is silane coupling agent kh570 to operate the silane coupling agent described in c.
Further, step(1)The power of control ultraviolet irradiation instrument is 1400W when operating the radiation treatment described in d,
The wavelength for controlling ultraviolet light is 300 ~ 350nm.
Further, step(2)Described in antifoaming agent be polyglycol ether.
Further, step(3)Described in high-speed stirred processing speed of agitator be 2400 revs/min.
Further, step(3)Described in ultrasonic homogenization when ultrasonic wave frequency be 520kHz.
Comparative example 1
This comparative example 1 compared with Example 2, eliminates step(1)Solution A leaching in modification biological carbon dust preparation manipulation c
Bubble processing, method and step all same in addition to this.
Comparative example 2
This comparative example 2 compared with Example 2, eliminates step(1)Modification biological carbon dust preparation manipulation d processing, in addition to this
Method and step all same.
Comparative example 3
This comparative example 3 compared with Example 2, in step(2)Raw material weigh it is spare in, with etc. mass parts commercially available corn stalk
Stalk biology carbon dust step of replacing(1)Modification biological carbon dust ingredient obtained, method and step all same in addition to this.
Control group
The very high cutting fluid of certain existing commercially available sales volume.
In order to compare effect of the present invention, to above-described embodiment 2, comparative example 1, comparative example 2, comparative example 3
Corresponding cutting fluid obtained and the corresponding cutting fluid of control group are tested for the property, and specific correction data is as shown in table 1 below:
Table 1
Note:Cutting temperature described in upper table 1 is the temperature of the workpiece measured when cutting;Temperature is cutting after the cutting 5s
Apply the temperature of the workpiece measured after cutting fluid 5s;The cleaning rate is the cleaning removal rate to cutting clast.
Made from the method for the present invention it can be seen from upper table 1 cut liquid energy quickly heat is taken away, reduce workpiece and
The temperature of cutter, while cutting clast can be removed well, it ensure that cleanliness factor, the machining accuracy product of workpiece can be improved in turn
Matter, great application value and the market competitiveness.
Claims (7)
1. a kind of preparation method of cooling and the good cutting fluid of cleaning performance, which is characterized in that include the following steps:
(1)It is prepared by modification biological carbon dust:
A. after first removing the other branch last years of maize straw, then with clear water to maize straw flushing one time, last segment is spare;
B. will operation a treated that maize straw is put into vapor tight tank, the water that temperature is 105 ~ 107 DEG C is passed through into vapor tight tank
Steam, while the pressure in vapor tight tank is increased into 0.5 ~ 0.55MPa, after heat-insulation pressure keeping handles 8 ~ 10min, then quickly unload to room temperature
Normal pressure finally takes out maize straw spare;
C. will operation b treated that maize straw is put into reaction kettle, first to reaction kettle vacuumize process, 18 ~ 20min is backward
Injection solution A submerges maize straw in reaction kettle, and the pressure in reaction kettle is then increased to 0.7 ~ 0.75MPa, and pressurize processing 35 ~
Maize straw is taken out after 38min, then maize straw is put into calcining furnace, the temperature in heating holding calcining furnace is
450 ~ 480 DEG C, maize straw is taken out after 1 ~ 1.2h of isothermal holding spare;The solution A by following parts by weight substance group
At:33 ~ 38 parts of butyl titanates, 2.5 ~ 3.5 parts of disodium ethylene diamine tetraacetates, 5 ~ 7 parts of cyclodextrin, 8 ~ 10 parts of silane coupling agents, 6
~ 8 parts of sodium pyrophosphates, 25 ~ 30 parts of ether, 780 ~ 800 parts of deionized waters;
D. will operation c treated that maize straw is immersed in solution B, it is 48 ~ 53 DEG C that heating, which keeps the temperature of solution B, is impregnated
Maize straw taking-up is put into ultraviolet irradiation instrument after 2 ~ 2.5h of processing, is taken out after 1 ~ 1.5h of radiation treatment spare;It is described
Solution B by following parts by weight material composition:5 ~ 7 parts of silver nitrates, 1 ~ 3 part of ammonium nitrate, 4 ~ 6 parts of sodium tetraborates, 90 ~ 100 parts
Deionized water;
E. will operation d treated that maize straw is put into pulverizer crosses 600 mesh after pulverization process to obtain modification biological carbon dust standby
With;
(2)Raw material weighs spare:
It is spare that following raw materials according is weighed by corresponding parts by weight:6 ~ 9 parts of polyethylene glycol, 10 ~ 15 portions of cottonseed oils, 15 ~ 20 portions of sunflower oils,
10 ~ 14 parts of dodecyl sodium sulfates, 2 ~ 4 parts of antifoaming agent, 20 ~ 25 parts of ethyl acetate, 10 ~ 14 parts of lauric monoglycerides, 3 ~ 6 parts
Kodalk, 8 ~ 11 parts of steps(1)Modification biological carbon dust obtained, 180 ~ 200 parts of deionized waters;
(3)Raw material is mixed with:
By step(2)All raw materials weighed are put into agitator tank jointly, then heating be kept stirring temperature in tank be 58 ~
63 DEG C, after high-speed stirred handles 40 ~ 45min, then 1 ~ 2h of ultrasonic homogenization.
2. the preparation method of a kind of cooling and the good cutting fluid of cleaning performance according to claim 1, which is characterized in that step
Suddenly(1)Quickly unloading to normal temperature and pressure described in operation b is in unloading vapor tight tank to normal temperature and pressure in 35s.
3. the preparation method of a kind of cooling and the good cutting fluid of cleaning performance according to claim 1, which is characterized in that step
Suddenly(1)It is silane coupling agent kh550, silane coupling agent kh560, silane coupling agent kh570 to operate the silane coupling agent described in c
In any one.
4. the preparation method of a kind of cooling and the good cutting fluid of cleaning performance according to claim 1, which is characterized in that step
Suddenly(1)The power of control ultraviolet irradiation instrument is 1200 ~ 1400W when operating the radiation treatment described in d, controls the wave of ultraviolet light
A length of 300 ~ 350nm.
5. the preparation method of a kind of cooling and the good cutting fluid of cleaning performance according to claim 1, which is characterized in that step
Suddenly(2)Described in antifoaming agent be polyglycol ether.
6. the preparation method of a kind of cooling and the good cutting fluid of cleaning performance according to claim 1, which is characterized in that step
Suddenly(3)Described in high-speed stirred processing speed of agitator be 2000 ~ 2400 revs/min.
7. the preparation method of a kind of cooling and the good cutting fluid of cleaning performance according to claim 1, which is characterized in that step
Suddenly(3)Described in ultrasonic homogenization when ultrasonic wave frequency be 480 ~ 520kHz.
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CN104437361A (en) * | 2014-10-24 | 2015-03-25 | 东华大学 | Method for preparing functional biological carbon by in-situ impregnation |
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