CN108515596B - A kind of preparation method of insect prevention timber - Google Patents

A kind of preparation method of insect prevention timber Download PDF

Info

Publication number
CN108515596B
CN108515596B CN201810290262.4A CN201810290262A CN108515596B CN 108515596 B CN108515596 B CN 108515596B CN 201810290262 A CN201810290262 A CN 201810290262A CN 108515596 B CN108515596 B CN 108515596B
Authority
CN
China
Prior art keywords
timber
coagulation
treatment liquid
liquid
insect prevention
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201810290262.4A
Other languages
Chinese (zh)
Other versions
CN108515596A (en
Inventor
吕莉
施衍
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fujian Longxing Jiuyuan Technology Co.,Ltd.
Original Assignee
Wu Ping Longxing Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Wu Ping Longxing Technology Co Ltd filed Critical Wu Ping Longxing Technology Co Ltd
Priority to CN201810290262.4A priority Critical patent/CN108515596B/en
Publication of CN108515596A publication Critical patent/CN108515596A/en
Application granted granted Critical
Publication of CN108515596B publication Critical patent/CN108515596B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/025Controlling the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/16Inorganic impregnating agents
    • B27K3/20Compounds of alkali metals or ammonium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/34Organic impregnating agents
    • B27K3/50Mixtures of different organic impregnating agents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/001Heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/003Treating of wood not provided for in groups B27K1/00, B27K3/00 by using electromagnetic radiation or mechanical waves
    • B27K5/0035Electron beam-radiation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/02Staining or dyeing wood; Bleaching wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/04Combined bleaching or impregnating and drying of wood
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K2240/00Purpose of the treatment
    • B27K2240/20Removing fungi, molds or insects

Abstract

The invention belongs to timber fields, and in particular to a kind of preparation method of insect prevention timber.The present invention is during preparing insect prevention timber, by the way that timber is immersed in ammonium bicarbonate soln, infiltrate ammonium hydrogen carbonate adequately to wood internal, it is heated, ammonium hydrogen carbonate is decomposed during heating, then timber is handled using coagulation liquid, medical PVA is improved to the wellability of timber by fatty alcohol polyoxyethylene ether in coagulation liquid, wrap up polyvinyl alcohol more fully to wood internal, utilize the different rosemary glycoside of acetone solution in two stage treatment liquid, it is sufficiently diffused into wood internal, and wood internal absorbed portion acetone, pass through the processing of tertiary treatment, improve insect resistant effect, under the action of the catalysis of soda acid is adjusted, furfural is promoted to be reacted with acetone, protective layer is formed in wood surface, further increase the insect resistant effect of wooden, it is prepared by the present invention anti- Worm wood preservation from decay effect is good, and environmental pollution is small.

Description

A kind of preparation method of insect prevention timber
Technical field
The invention belongs to timber fields, and in particular to a kind of preparation method of insect prevention timber.
Background technique
The high molecular material that timber is made of cellulose, hemicellulose and lignin, and there is beautiful texture, color day So, the advantages that texture is comfortable, plasticity is good, easy to process, thus by the ideal material as construction and decoration and Furniture manufacture.Its Interior is the natural place of pest oviposition and breeding containing nutriments and moisture such as soluble sugar point, starch, but timber is due to length Phase contacts with oxygen, light, moisture, is easy to be eaten by entomogenous fungi and lose, this will significantly limit the application effect and application field of timber.Cause This, timber before use, appropriate insect-proof agent is often selected to carry out protective treatment, will play the good foxiness, mould of delaying Change and other effects.However, most of traditional wood preservation from decay agent makes environment and the mankind containing harmful components such as heavy metal, formaldehyde With great potential hazard will be caused.
Currently, the method for wood preservation from decay processing mainly has infusion process, diffusion method, hot and cold bath method and fumigating system, wherein impregnating Method is most widely used, it, which refers to, is immersed directly in timber in insect prevention solvent, and insect-proof agent penetrates into wood internal.This method The advantages of be that timber integrally can rapidly absorb mould proof solvent, but subsequent also need to be dried and will lead to a part of medicament Loss, cause insect resistant effect poor, and pollute the environment.
Summary of the invention
The technical problems to be solved by the invention: being lost for medicament is easily led to during current wood preservation from decay, reduces anti- Worm effect, and the problem of pollute the environment, the present invention provides a kind of preparation methods of insect prevention timber.
In order to solve the above technical problems, the present invention is using technical solution as described below:
A kind of preparation method of insect prevention timber, this method comprises the following steps:
(1) it takes timber to be immersed in ammonium bicarbonate soln, and is stood at 20~25 DEG C, take out the timber after impregnating, put Enter dry at 60~65 DEG C timber after collection is dry, the timber after drying is put into coagulation liquid and is impregnated, carries out level-one Handle 1~3h;
(2) after coagulation, timber is taken out, and natural drying obtains coagulation timber, and coagulation timber is complete For complete immersion in two stage treatment liquid, the pH value for adjusting two stage treatment liquid is 8.5~9.0, and oscillation second level is carried out at 70~75 DEG C Handle 1~2h;
(3) timber is taken out after vibrating two stage treatment, then be fully immersed in tertiary treatment liquid, adjust the pH for the treatment of fluid Value 4.5~5.0 is warming up to 80~90 DEG C, 1~2h of isothermal holding, Geniposide is being added, additional amount is timber in tertiary treatment liquid The 0.2~0.4% of quality is warming up to 100~105 DEG C, keeps the temperature 2~4h of tertiary treatment;
(4) it after keeping the temperature tertiary treatment, is cooled to room temperature, timber is taken out, be placed under ultraviolet lamp and be irradiated 30~50min, then natural drying can obtain insect prevention timber.
In the step (1) coagulation liquid be formulated as by medical PVA, water and fatty alcohol polyoxyethylene ether by Mass ratio 3:8~9:0.6 is heated at 95~98 DEG C, collects heating mixture, and heating mixture is stored in 96 DEG C In to get coagulation liquid.
Two stage treatment liquid is formulated as mixing different rosemary glycoside, acetone 1:3 in mass ratio in the step (2) It closes to get two stage treatment liquid.
Tertiary treatment liquid is formulated as furfural, 2 hydroxy ethylamine and water 2~4:0.3 in mass ratio in the step (3) ~0.5:9 is uniformly mixed to get tertiary treatment liquid.
The present invention is compared with other methods, and advantageous effects are:
The present invention, first by the way that timber to be immersed in ammonium bicarbonate soln, makes carbon during preparing insect prevention timber Sour hydrogen ammonium is adequately infiltrated to wood internal, then is heated, and ammonium hydrogen carbonate is decomposed during heating, is expanded in timber The gap in portion increases subsequent raw material to the wetting property of timber, while what is generated can carry out sterilization and micro- to wood internal The effect for measuring bleaching, is then handled timber using coagulation liquid, passes through fatty alcohol polyoxy second in coagulation liquid Alkene ether improves medical PVA to the wellability of timber, while the processing of early period also improves leaching of the polyvinyl alcohol to timber Profit, wraps up polyvinyl alcohol more fully to wood internal, then contact of the timber with air recycles second level It is sufficiently diffused to wood internal, and wood internal absorbed portion acetone by the different rosemary glycoside of acetone solution in treatment fluid, The insect resistant effect of timber is improved, then by the processing of tertiary treatment, one side furfural is infiltrated to wood internal, with therein third Ketone is contacted, while carrying 2 hydroxy ethylamine entrance, improves insect resistant effect, the effect on the other hand adjusted in the catalysis of soda acid Under, promote furfural react forming furfural acetone resin with acetone, forms protective layer, and the Geniposide pair being added in wood surface Wood internal is crosslinked, and further increases the insect resistant effect of wooden, insect prevention wood preservation from decay effect prepared by the present invention is good, to ring Border pollution is small.
Specific embodiment
Coagulation liquid is formulated as medical PVA, water and fatty alcohol polyoxyethylene ether 3:8~9 in mass ratio: 0.6,40min is heated at 95~98 DEG C, collects heating mixture, and heating mixture is stored in 96 DEG C to get one Grade treatment fluid.
Two stage treatment liquid is formulated as different rosemary glycoside, acetone 1:3 being in mass ratio stirred mixing to get second level Treatment fluid.
Tertiary treatment liquid is formulated as mixing furfural, 2 hydroxy ethylamine and water 2~4:0.3 in mass ratio~0.5:9 equal It is even to get tertiary treatment liquid.
A kind of preparation method of insect prevention timber, this method comprises the following steps:
(1) it takes timber to be immersed in ammonium bicarbonate soln, and stands 70min at 20~25 DEG C, take out the wood after impregnating Material is put at 60~65 DEG C dry 2h, and the timber after drying is put into coagulation liquid and impregnates by the timber after collecting drying, Carry out 1~3h of coagulation;
(2) after coagulation, timber is taken out, and natural drying 1~2 day, coagulation timber is obtained, by coagulation Timber is fully immersed in two stage treatment liquid, and the pH value for adjusting two stage treatment liquid is 8.5~9.0, is shaken at 70~75 DEG C Swing 1~2h of two stage treatment;
(3) timber is taken out after vibrating two stage treatment, then be fully immersed in tertiary treatment liquid, adjust the pH for the treatment of fluid Value 4.5~5.0 is warming up to 80~90 DEG C, 1~2h of isothermal holding, Geniposide is being added, additional amount is timber in tertiary treatment liquid The 0.2~0.4% of quality is warming up to 100~105 DEG C, keeps the temperature 2~4h of tertiary treatment;
(4) it after keeping the temperature tertiary treatment, is cooled to room temperature, timber is taken out, be placed under ultraviolet lamp and be irradiated 30~50min, then natural drying 2 days, insect prevention timber can be obtained.
Embodiment 1
Coagulation liquid is formulated as medical PVA, water and fatty alcohol polyoxyethylene ether 3:9:0.6 in mass ratio, 40min is heated at 98 DEG C, collects heating mixture, and heating mixture is stored in 96 DEG C to get coagulation liquid.
Two stage treatment liquid is formulated as different rosemary glycoside, acetone 1:3 being in mass ratio stirred mixing to get second level Treatment fluid.
Tertiary treatment liquid is formulated as furfural, 2 hydroxy ethylamine and water 4:0.5:9 being in mass ratio uniformly mixed to get three Grade treatment fluid.
A kind of preparation method of insect prevention timber, this method comprises the following steps:
(1) it takes timber to be immersed in ammonium bicarbonate soln, and stands 70min at 25 DEG C, take out the timber after impregnating, put Enter dry 2h at 65 DEG C, the timber after drying is put into coagulation liquid and impregnates, carries out at level-one by the timber after collecting drying Manage 1~3h;
(2) after coagulation, timber is taken out, and natural drying 2 days, obtains coagulation timber, by coagulation wood Material is fully immersed in two stage treatment liquid, and the pH value for adjusting two stage treatment liquid is 9.0, and oscillation two stage treatment is carried out at 75 DEG C 2h;
(3) timber is taken out after vibrating two stage treatment, then be fully immersed in tertiary treatment liquid, adjust the pH for the treatment of fluid Value 5.0 is warming up to 90 DEG C, isothermal holding 2h, and Geniposide is being added, and additional amount is 0.4% of lumber quality in tertiary treatment liquid, 105 DEG C are warming up to, tertiary treatment 4h is kept the temperature;
(4) it after keeping the temperature tertiary treatment, is cooled to room temperature, timber is taken out, be placed under ultraviolet lamp and be irradiated 50min, then natural drying 2 days, insect prevention timber can be obtained.
Embodiment 2
Coagulation liquid is formulated as medical PVA, water and fatty alcohol polyoxyethylene ether 3:8:0.6 in mass ratio, 40min is heated at 97 DEG C, collects heating mixture, and heating mixture is stored in 96 DEG C to get coagulation liquid.
Two stage treatment liquid is formulated as different rosemary glycoside, acetone 1:3 being in mass ratio stirred mixing to get second level Treatment fluid.
Tertiary treatment liquid is formulated as furfural, 2 hydroxy ethylamine and water 3:0.4:9 being in mass ratio uniformly mixed to get three Grade treatment fluid.
A kind of preparation method of insect prevention timber, this method comprises the following steps:
(1) it takes timber to be immersed in ammonium bicarbonate soln, and stands 70min at 23 DEG C, take out the timber after impregnating, put Enter dry 2h at 63 DEG C, the timber after drying is put into coagulation liquid and impregnates, carries out at level-one by the timber after collecting drying Manage 2h;
(2) after coagulation, timber is taken out, and natural drying 1 day, obtains coagulation timber, by coagulation wood Material is fully immersed in two stage treatment liquid, and the pH value for adjusting two stage treatment liquid is 9.0, and oscillation two stage treatment is carried out at 74 DEG C 2h;
(3) timber is taken out after vibrating two stage treatment, then be fully immersed in tertiary treatment liquid, adjust the pH for the treatment of fluid Value 4.5 is warming up to 85 DEG C, isothermal holding 1.5h, Geniposide is being added, additional amount is lumber quality in tertiary treatment liquid 0.3%, 103 DEG C are warming up to, tertiary treatment 3h is kept the temperature;
(4) it after keeping the temperature tertiary treatment, is cooled to room temperature, timber is taken out, be placed under ultraviolet lamp and be irradiated 40min, then natural drying 2 days, insect prevention timber can be obtained.
Embodiment 3
Coagulation liquid is formulated as medical PVA, water and fatty alcohol polyoxyethylene ether 3:8:0.6 in mass ratio, 40min is heated at 95 DEG C, collects heating mixture, and heating mixture is stored in 96 DEG C to get coagulation liquid.
Two stage treatment liquid is formulated as different rosemary glycoside, acetone 1:3 being in mass ratio stirred mixing to get second level Treatment fluid.
Tertiary treatment liquid is formulated as furfural, 2 hydroxy ethylamine and water 2:0.3:9 being in mass ratio uniformly mixed to get three Grade treatment fluid.
A kind of preparation method of insect prevention timber, this method comprises the following steps:
(1) it takes timber to be immersed in ammonium bicarbonate soln, and stands 70min at 20 DEG C, take out the timber after impregnating, put Enter dry 2h at 60 DEG C, the timber after drying is put into coagulation liquid and impregnates, carries out at level-one by the timber after collecting drying Manage 1h;
(2) after coagulation, timber is taken out, and natural drying 1 day, obtains coagulation timber, by coagulation wood Material is fully immersed in two stage treatment liquid, and the pH value for adjusting two stage treatment liquid is 8.5, and oscillation two stage treatment 1 is carried out at 70 DEG C ~2h;
(3) timber is taken out after vibrating two stage treatment, then be fully immersed in tertiary treatment liquid, adjust the pH for the treatment of fluid Value 4.5 is warming up to 80 DEG C, isothermal holding 1h, and Geniposide is being added, and additional amount is 0.2% of lumber quality in tertiary treatment liquid, 100 DEG C are warming up to, tertiary treatment 2h is kept the temperature;
(4) it after keeping the temperature tertiary treatment, is cooled to room temperature, timber is taken out, be placed under ultraviolet lamp and be irradiated 30min, then natural drying 2 days, insect prevention timber can be obtained.
Comparative example
Commercially available wood preservation from decay agent.
Commercially available wood preservation from decay agent in comparative example is carried out according to product description using at timber progress insect prevention Reason obtains comparison insect prevention timber.
Performance test: the comparison insect prevention timber that Examples 1 to 3 is prepared into insect prevention timber and comparative example obtains is put into and is respectively put Enter in the identical container of apparent volume, the insect prevention lumber quality being put into is equal, is put into 3g Workers of Coptotermes formosanus Shiraki into container, 2g is dwelt Northern reticulitermes flavipe, is placed in insulating box and cultivates, and observes off-test, wooden unit is cleaned out, after drying, weighing in the same way, Calculate the average intact value of wooden unit.Average intact value (I)=∑ f Y/F.Wherein, f is wooden unit number;Y is intact value (table 1);F is Hammer butt block number.
The intact value standard scale of table 1
Test time: test to all chemicals treatment group termites is all until death.
Test result such as table 2
2 test result of table
It can thus be appreciated that the present invention, which is prepared into insect prevention timber, can effectively prevent the erosion of worm, and during the preparation process simultaneously It not can cause environmental pollution.

Claims (1)

1. a kind of preparation method of insect prevention timber, which is characterized in that this method comprises the following steps:
(1) it takes timber to be immersed in ammonium bicarbonate soln, and is stood at 20~25 DEG C, take out the timber after impregnating, be put into 60 Timber dry at~65 DEG C, after collecting drying, the timber after drying is put into coagulation liquid and is impregnated, and carries out coagulation 1~3h;
(2) after coagulation, timber is taken out, and natural drying obtains coagulation timber, coagulation timber is soaked completely For bubble in two stage treatment liquid, the pH value for adjusting two stage treatment liquid is 8.5~9.0, and oscillation two stage treatment 1 is carried out at 70~75 DEG C ~2h;
(3) timber is taken out after vibrating two stage treatment, then be fully immersed in tertiary treatment liquid, adjust the pH value for the treatment of fluid 4.5~5.0,80~90 DEG C, 1~2h of isothermal holding are warming up to, Geniposide is added, additional amount is timber in tertiary treatment liquid The 0.2~0.4% of quality is warming up to 100~105 DEG C, keeps the temperature 2~4h of tertiary treatment;
(4) it after keeping the temperature tertiary treatment, is cooled to room temperature, timber is taken out, be placed under ultraviolet lamp and be irradiated 30~ 50min, then natural drying can obtain insect prevention timber;
Coagulation liquid is formulated as medical PVA, water and fatty alcohol polyoxyethylene ether by quality in the step (1) It than 3:8~9:0.6, is heated at 95~98 DEG C, collects heating mixture, and heating mixture is stored in 96 DEG C, i.e., Obtain coagulation liquid;
Two stage treatment liquid is formulated as mixing different rosemary glycoside, acetone 1:3 in mass ratio in the step (2), i.e., Obtain two stage treatment liquid;
In the step (3) tertiary treatment liquid be formulated as by furfural, 2 hydroxy ethylamine and water 2~4:0.3 in mass ratio~ 0.5:9 is uniformly mixed to get tertiary treatment liquid.
CN201810290262.4A 2018-03-30 2018-03-30 A kind of preparation method of insect prevention timber Active CN108515596B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810290262.4A CN108515596B (en) 2018-03-30 2018-03-30 A kind of preparation method of insect prevention timber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810290262.4A CN108515596B (en) 2018-03-30 2018-03-30 A kind of preparation method of insect prevention timber

Publications (2)

Publication Number Publication Date
CN108515596A CN108515596A (en) 2018-09-11
CN108515596B true CN108515596B (en) 2019-11-26

Family

ID=63431118

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810290262.4A Active CN108515596B (en) 2018-03-30 2018-03-30 A kind of preparation method of insect prevention timber

Country Status (1)

Country Link
CN (1) CN108515596B (en)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113733281B (en) * 2021-10-25 2022-12-02 浙江瑞美生态建设股份有限公司 Carbonized wood and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106363731A (en) * 2016-10-11 2017-02-01 阜阳市伟叶家具有限公司 Modifying agent used for strengthening dimensional stability of compound wax emulsion of quick-growing wood
CN107116643A (en) * 2017-06-15 2017-09-01 浙江润格木业科技有限公司 A kind of health-preserving method of timber
CN107263641A (en) * 2017-07-31 2017-10-20 宿松县先盛竹业有限公司 A kind of processing method for improving bamboo product cracking resistance Anti-moth-eating
CN107671961A (en) * 2017-10-09 2018-02-09 常州琨瑶纺织品有限公司 A kind of preparation method of Wood modifier

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106363731A (en) * 2016-10-11 2017-02-01 阜阳市伟叶家具有限公司 Modifying agent used for strengthening dimensional stability of compound wax emulsion of quick-growing wood
CN107116643A (en) * 2017-06-15 2017-09-01 浙江润格木业科技有限公司 A kind of health-preserving method of timber
CN107263641A (en) * 2017-07-31 2017-10-20 宿松县先盛竹业有限公司 A kind of processing method for improving bamboo product cracking resistance Anti-moth-eating
CN107671961A (en) * 2017-10-09 2018-02-09 常州琨瑶纺织品有限公司 A kind of preparation method of Wood modifier

Also Published As

Publication number Publication date
CN108515596A (en) 2018-09-11

Similar Documents

Publication Publication Date Title
CN101716790B (en) Method for producing rubber tree carbonized wood by resin pretreatment
JP2010005875A (en) Antifungal agent for bamboo or the like and antifungal method
CN113907403A (en) Preparation method of cigar tobacco agricultural fermentation auxiliary agent and agricultural fermentation method
WO2023193740A1 (en) Outdoor high-weather-resistance bamboo scrimber, and manufacturing method therefor
CN105397892A (en) Method for producing carbonized wood through impregnation pretreatment
CN104942939A (en) Method for treating birch bark
CN104942937A (en) Mulberry bark treatment method
CN105881683A (en) Mildew preventive for environment-friendly wood composite material and preparing method of mildew preventive
CN108515596B (en) A kind of preparation method of insect prevention timber
CN109249499A (en) A kind of processing method of furniture wooden boards
CN109049222A (en) A method of improving rattan processing performance
CN108247806A (en) A kind of preparation method of the not mould non-ignitable bamboo fiberboard of no aldehyde
CN107297803A (en) A kind of softening mold-proof method of timber
CN105382893A (en) Insect preventing treatment method for wood
CN114953075B (en) Preparation method of high-color-fastness recombined decorative veneer
CN107471366B (en) A kind of redwood dehumidification process based on inhibition cell activity
CN108972769B (en) Pretreatment method for improving dyeing performance of bamboo wood
CN110271354A (en) A kind of production method of immortality lotus flower
CN104942949A (en) Lacebark pine bark treatment method
CN106142258B (en) A kind of timber modifying agent and preparation method and application
JP2022049004A (en) Wood treatment method, wood treatment agent, and wood processed product
CN111840380A (en) Treatment process for radix paeoniae alba in fresh processing of traditional Chinese medicinal materials before fresh cutting
CN109849136A (en) Natural timber modification liquid and its preparation method and application
CN111567614A (en) Grape drying accelerator and preparation method thereof
CN106863514B (en) Green persistently application and preparation method of the anticorrosive mildewproof phenolic resin on Recombined bamboo

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
TA01 Transfer of patent application right
TA01 Transfer of patent application right

Effective date of registration: 20191008

Address after: 364300 Longyan City, Fujian province Wuping County Industrial Park F-03-3

Applicant after: Wu Ping Longxing Technology Co., Ltd.

Address before: 213000 the 39 unit of Shui Mu Hua Garden, Xinbei District, Changzhou, Jiangsu, 1503

Applicant before: Lv Li

GR01 Patent grant
GR01 Patent grant
PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: A preparation method of insect resistant wood

Effective date of registration: 20201015

Granted publication date: 20191126

Pledgee: China Wuping of Longyan Branch Bank of Limited by Share Ltd.

Pledgor: Wu Ping Longxing Technology Co.,Ltd.

Registration number: Y2020980006801

CP01 Change in the name or title of a patent holder
CP01 Change in the name or title of a patent holder

Address after: 364300 F-03-3, industrial park, Longyan, Fujian

Patentee after: Fujian Longxing Jiuyuan Technology Co.,Ltd.

Address before: 364300 F-03-3, industrial park, Longyan, Fujian

Patentee before: Wu Ping Longxing Technology Co.,Ltd.