A kind of graphene finished product storage device
Technical field
The present invention relates to technical field of graphene more particularly to a kind of graphene finished product storage devices.
Background technique
Graphene be one kind by carbon atom with sp2Hybridized orbit forms the Two-dimensional Carbon nanometer material that hexangle type is in honeycomb lattice
Material, graphene have excellent optics, electricity, mechanical characteristic, pass in materialogy, micro-nano technology, the energy, biomedicine and drug
Pass etc. is with important application prospects, it is considered to be a kind of future revolutionary material.
The method of the common power production of graphene is mechanical stripping method, oxidation-reduction method, SiC epitaxial growth method, film
Production method is chemical vapour deposition technique.With the gradually breakthrough of the problems such as mass production and large scale, the production of graphene
Industryization is being accelerated using paces, is based on existing research achievement, realizes that the field of commercial applications may be mobile at first
Equipment, aerospace, new energy field of batteries.
Storage graphene is carried out using storage tank in prior art CN2047136421U, although increasing glass tank body
The intensity and hardness of wall so that glass tank body is non-friable, but take be put into when, be easy so that graphene is oxidized, simultaneously
It is easy prevent the glutinous viscous inner wall of graphene from taking out completely, to cause to waste.
Summary of the invention
The purpose of the present invention is to solve disadvantages existing in the prior art, and a kind of graphene finished product storage proposed
Cryopreservation device.
To achieve the goals above, present invention employs following technical solutions:
A kind of graphene finished product storage device, including cabinet, the side of the cabinet are connected with vacuum machine by pipeline,
The other side of cabinet is connected with defeated nitrogen machine by pipeline, and first through hole, the bottom wall of interlayer are offered in the middle part of the interlayer of cabinet bottom end
Be welded and fixed with one end of third spring, the other end of third spring and the side of fixed block are welded and fixed, fixed block it is another
Side opens up fluted, and bearing is welded in groove, plugs in the middle part of bearing and is fixed with shaft, and is welded on first through hole inner wall
Fixed set with teeth, tooth set and gear engagement are connect, is plugged in the middle part of gear and is fixed with shaft, shaft is plugged in the middle part of cabinet, and
The top of shaft is pierced by the middle part of cabinet and briquetting and is welded and fixed, and plugs in the middle part of shaft and is fixed with fixed disk, cabinet bottom end one
Hydraulic cylinder is fixed with by screw in the interlayer of side, the output end of hydraulic cylinder and one end of hydraulic stem are fixed by key pin, hydraulic
The top of bar is fixed with pallet by screw, and the middle and upper part of cabinet is fixed with sealing block by screw, the side inside sealing block
The second through-hole is offered, the inner wall of the second through-hole is connected by a hinge and has opening-closing plate.
Preferably, third through-hole, one end of the inner wall of third through-hole and the first spring are uniformly provided in the fixed disk
It is welded and fixed, the other end of the first spring and the side of fixture block are welded and fixed, the other side of fixture block and the outer wall sliding of glass tube
Connection.
Preferably, gluing is fixed with sealing strip, the middle part of sealing block between the two sides of the sealing block and the inner wall of cabinet
Sealing ring is fixed with the junction gluing of shaft.
Preferably, the pallet is located at the underface of the glass tube of the side of fixed disk.
Preferably, second through-hole is located at the surface of the side glass tube of fixed disk, and the diameter of the second through-hole is big
In the diameter of the pipe cap of glass tube and the width of tube socket.
Preferably, the bottom end of the opening-closing plate and one end of second spring are welded and fixed, the other end of second spring and
The inner wall of two through-hole sides is welded and fixed, and the outside gluing of opening-closing plate is fixed with sealing ring.
Preferably, uniform welding is fixed with sawtooth, sawtooth and gear engagement, and the top of sawtooth on the inner wall of the tooth set
It is welded with rib.
Preferably, the side on the top of the cabinet offers fourth hole, and plugs and be welded in fourth hole
Inlet/outlet pipe, the top of inlet/outlet pipe, which is connected through a screw thread, is fixed with turncap, and fourth hole is located at the surface of glass tube, and
The diameter of four through-holes is greater than the diameter of the pipe cap of glass tube and the width of tube socket.
The beneficial effects of the present invention are:
1, the present invention is aspirated the air in cabinet by vacuum machine clean, defeated nitrogen machine 3 is then opened, so that filling in cabinet
If completely there is nitrogen, and filled always during glass tube of taking and set nitrogen, to guarantee that the graphene in glass tube is not oxidized.
2, the present invention drives shaft down by briquetting, and shaft presses fixed block down, and fixed block compresses third spring, from
And the gear in shaft is made to be detached from rack gear down, briquetting is then rotated, shaft drives fixed disc spins, so that in fixed disk
Through-hole alignment on through-hole and cabinet on through-hole and sealing block, thus convenient taking equipped with Graphene glass pipe, and will not
So that damaged when glass tube takes.
3, automatic open-close of the present invention by the opening-closing plate on sealing block under second spring effect, so that cabinet is being convenient for
It can guarantee certain sealing again in the case where taking, so that the intracorporal graphene of case is not oxidized.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of graphene finished product storage device proposed by the present invention;
Fig. 2 is a kind of enlarged drawing of the A of graphene finished product storage device proposed by the present invention;
Fig. 3 is a kind of enlarged drawing of the B of graphene finished product storage device proposed by the present invention;
Fig. 4 is a kind of structural schematic diagram of graphene finished product storage device fixed disk proposed by the present invention.
In figure: 1 cabinet, 2 vacuum machines, 3 defeated nitrogen machines, 4 sealing blocks, 5 fixed disks, 6 glass tubes, 7 hydraulic cylinders, 8 hydraulic stems, 9
Pallet, 10 briquettings, 11 shafts, 12 first springs, 13 fixture blocks, 14 opening-closing plates, 15 second springs, 16 gears, 17 tooth sets, 18 are fixed
Block, 19 third springs.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.
Referring to Fig.1-4, the side of a kind of graphene finished product storage device, including cabinet 1, cabinet 1 is connected by pipeline
There is vacuum machine 2, the other side of cabinet 1 is connected with defeated nitrogen machine 3 by pipeline, and it is logical that first is offered in the middle part of 1 bottom end interlayer of cabinet
Hole, the bottom wall of interlayer and one end of third spring 19 are welded and fixed, the side weldering of the other end and fixed block 18 of third spring 19
Connect fixation, the other side of fixed block 18 opens up fluted, and bearing is welded in groove, plugs to be fixed in the middle part of bearing and turns
Axis 11, and set 17 with teeth is welded and fixed on first through hole inner wall, uniform welding is fixed with sawtooth on the inner wall of tooth set 17, sawtooth and
Gear 16 engages, and the top of sawtooth is welded with rib, and the middle part of gear 16, which plugs, is fixed with shaft 11, and shaft 11 plugs
It is welded and fixed at the middle part that the top at the middle part of cabinet 1, and shaft 11 is pierced by cabinet 1 and briquetting 10, the knot of shaft 11 and cabinet 1
Gluing fixes rubber sleeve at conjunction, and the middle part of shaft 11, which plugs, is fixed with fixed disk 5, and it is logical that third is uniformly provided in fixed disk 5
One end of hole, the inner wall of third through-hole and the first spring 12 is welded and fixed, the side weldering of the other end and fixture block 13 of the first spring
Fixation is connect, the other side of fixture block 13 and the outer wall of glass tube 6 are slidably connected, solid by screw in the interlayer of 1 bottom end side of cabinet
Surely there is hydraulic cylinder 7, the output end of hydraulic cylinder 7 and one end of hydraulic stem 8 are fixed by key pin, and the top of hydraulic stem 8 passes through screw
It is fixed with pallet 9, pallet 9 is located at the underface of the glass tube 6 of the side of fixed disk 5, and the middle and upper part of cabinet 1 is fixed by screw
There is sealing block 4, gluing is fixed with sealing strip, the middle part of sealing block 4 and shaft between the two sides of sealing block 4 and the inner wall of cabinet 1
11 junction gluing fixes rubber sleeve, and the side inside sealing block 4 offers the second through-hole, and the second through-hole is located at fixed disk
The surface of 5 side glass tube 6, and the diameter of the second through-hole is greater than the diameter of the pipe cap of glass tube 6 and the width of tube socket, the
The inner wall of two through-holes, which is connected by a hinge, opening-closing plate 14, and the bottom end of opening-closing plate 14 and one end of second spring 15 are welded and fixed,
The other end of second spring 15 and the inner wall of the second through-hole side are welded and fixed, and the outside gluing of opening-closing plate 14 is fixed with sealing
Circle, the side on the top of cabinet 1 offers fourth hole, and plugs in fourth hole and be welded with inlet/outlet pipe, inlet/outlet pipe
Top, which is connected through a screw thread, is fixed with turncap, and fourth hole is located at the surface of glass tube 6, and the diameter of fourth hole is big
In the diameter of the pipe cap of glass tube 6 and the width of tube socket.
In the present embodiment 1, when being put into graphene, the turncap on 1 top of cabinet is tightened, then opening vacuum machine 2 will
Air suction in cabinet 1 is clean, closes vacuum machine 2, then opens defeated nitrogen machine 3, completely have nitrogen so that filling and setting in cabinet 1, so
Graphene will be installed in glass tube 6 afterwards, glass tube is covered into pipe cap, continued starting defeated nitrogen machine 3, unscrew the rotation on 1 top of cabinet
Cap fills in glass tube 6 in fourth hole, and the pedestal of glass tube 6 pushes opening-closing plate 14, and opening-closing plate 14 compresses second spring 15,
Glass tube passes through the second through-hole on sealing block 4, and then glass tube 6 squeezes fixture block 13 down, so that fixture block 13 is in the first spring
Be fixedly clamped glass tube 6 under 12 restoring force, until then the top of glass tube 6 presses briquetting 10 in the lower section of sealing block 4,
Briquetting 10 drives shaft 11 down, and shaft 11 presses fixed block 18 down, and fixed block 18 compresses third spring 19, so that turning
Gear 16 on axis 11 is detached from rack gear 17 down, then rotates briquetting 10, dial is pasted on briquetting 10, rotate 30 degree, turn
Axis 11 drives fixed disk 5 to rotate 30 degree so that on the second through-hole and cabinet 1 on third through-hole and sealing block 4 in fixed disk 5
Fourth hole alignment, until fixed disk 5 on third through-hole in be respectively arranged with glass tube 6, then tighten the turncap of cabinet 1,
Defeated nitrogen machine 3 is closed, shaft 11 is under the restoring force of third spring 19, so that the gear 16 and tooth set 17 in shaft 11 continue card
Tightly, the opening-closing plate 14 on sealing plate 4 becomes horizontal under the restoring force of second spring 15, and the sealing ring in the outside of opening-closing plate 14 will
The sealing of second through-hole avoids the graphene in glass tube 6 from being oxidized, while can so that not containing oxygen inside cabinet 1
It is easily put into cabinet 1, and the glass tube 6 equipped with graphene will not be made damaged.
In the present embodiment 2, when take graphene when, open defeated nitrogen machine 3, then unscrew the turncap of 1 side of cabinet, open
Hydraulic cylinder 7, hydraulic cylinder 7 drive hydraulic stem 8 up, and hydraulic stem 8 drives pallet 9 up to move, and pallet 9 pushes glass tube 6 up,
The pipe cap of glass tube 6 opens opening-closing plate 14, and opening-closing plate 14 stretches second spring 15, until by glass tube 6 from the side of cabinet 1
It is released in fourth hole, then presses briquetting 10, briquetting 10 drives shaft 11 down, and shaft 11 presses fixed block 18 down, Gu
Determine block 18 and compress third spring 19, so that the gear 16 in shaft 11 is detached from rack gear 17 down, then rotates briquetting 10, pressure
It is pasted with dial on block 10, rotates 30 degree, shaft 11 drives 30 degree of the rotation of fixed disk 5 so that third through-hole in fixed disk 5
With the fourth hole alignment on the second through-hole and cabinet 1 on sealing block 4, then the glass tube 6 in fixed disk 5 is released one by one
Cabinet is then shut off defeated nitrogen machine 3, so that not containing oxygen inside cabinet 1, the graphene in glass tube 6 is avoided to be oxidized,
It can easily be taken out from cabinet 1 simultaneously, and the glass tube 6 equipped with graphene will not be made damaged.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.