CN108531080A - A kind of engine nano abrasion-resistant protective agent and preparation method - Google Patents
A kind of engine nano abrasion-resistant protective agent and preparation method Download PDFInfo
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- CN108531080A CN108531080A CN201810390671.1A CN201810390671A CN108531080A CN 108531080 A CN108531080 A CN 108531080A CN 201810390671 A CN201810390671 A CN 201810390671A CN 108531080 A CN108531080 A CN 108531080A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D193/00—Coating compositions based on natural resins; Coating compositions based on derivatives thereof
- C09D193/04—Rosin
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2244—Oxides; Hydroxides of metals of zirconium
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3009—Sulfides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
Abstract
The invention discloses engine nano abrasion-resistant protective agent and preparation method, the engine nano abrasion-resistant protective agent and preparation method, which is characterized in that including below according to the raw material of parts by weight：98 parts of nano zirconium dioxide, 18 parts of phosphatidase 1,158 parts of rosin, 8 parts of silane coupling agent, 78 parts of molybdenum disulfide dispersion liquid, 58 parts of silicone oil melt rosin heating, filtering；Silane coupling agent is added into the rosin of thawing, stirs evenly, obtains the first batch mixing, keeps the temperature；Nano zirconium dioxide is added into the first batch mixing, stirs evenly, obtains the second batch mixing, keeps the temperature；Silicone oil is added into the second batch mixing, stirs evenly, obtains third batch mixing, keeps the temperature；Molybdenum disulfide dispersion liquid and phosphatide are added into third batch mixing, placement is stood after stopping heat preservation.Engine nano abrasion-resistant protective agent of the present invention and preparation method can promote metal to form superpower alloy protecting film, and wear-resistant coefficient is high, and wearability is good, while having both corrosion resistance, has certain waterproof and lubricating action, and then can play the role of the prolonged mechanical service life.
Description
Technical field
The present invention relates to a kind of nano abrasion-resistant protective agent and preparation method, specifically a kind of engine nano abrasion-resistant protective agent and
Preparation method.
Background technology
Engine is the core of engine, therefore traditionally also commonly uses engine and refer to engine.The critical piece of engine is
Cylinder, and the entirely power producer of automobile.On stricti jurise engine earliest in the world by a British scientist in Christian era
One six eight zero years are invented.In the writing of game, engine refers to the main program for controlling all game functions.
Protective agent refers to the liquid substance protected to metal, nonmetallic or composite material surface, and material surface is made to have
There are certain specific functions such as acid and alkali-resistance, salt spray resistance, water-fast, wear-resistant, solvent resistant or special gas, ageing-resistant, UV resistant, resistance to height
Warm, low temperature resistant, vibration resistance, anti-skidding, antifriction, antistatic, anti-moisture, antifouling, insulation, conduction, heat conduction, thermal insulation, fire-retardant etc..
Fail to carry out wear resistence and anticorrosive and waterproof lubricating action well for the protective agent of engine at present.
Invention content
The purpose of the present invention is to provide a kind of engine nano abrasion-resistant protective agent and preparation methods, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides the following technical solutions：
A kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：80-115 parts of nano zirconium dioxide,
05-135 parts of phosphatidase 1,130-190 parts of rosin, 6-18 parts of silane coupling agent, 58-98 parts of molybdenum disulfide dispersion liquid, silicone oil 38-68
Part.
As a further solution of the present invention：The engine nano abrasion-resistant protective agent, including below according to the original of parts by weight
Material：90-105 parts of nano zirconium dioxide, 15-125 parts of phosphatidase 1,150-160 parts of rosin, 7-10 parts of silane coupling agent, molybdenum disulfide
68-88 parts of dispersion liquid, 50-65 parts of silicone oil.
As further scheme of the invention：The engine nano abrasion-resistant protective agent, which is characterized in that including pressing below
According to the raw material of parts by weight：98 parts of nano zirconium dioxide, 18 parts of phosphatidase 1,158 parts of rosin, 8 parts of silane coupling agent, molybdenum disulfide point
78 parts of dispersion liquid, 58 parts of silicone oil.
It is a further object of the present invention to provide the protectant preparation methods of engine nano abrasion-resistant, which is characterized in that including with
Lower step：
(1) by 135 degrees Celsius of thawings of rosin heating, filtering；
(2) silane coupling agent is added into the rosin of thawing, stirs evenly, obtain the first batch mixing, keep the temperature；
(3) nano zirconium dioxide is added into the first batch mixing, stirs evenly, obtain the second batch mixing, keep the temperature；
(4) silicone oil is added into the second batch mixing, stirs evenly, obtain third batch mixing, keep the temperature；
(5) molybdenum disulfide dispersion liquid and phosphatide are added into third batch mixing, placement is stood after stopping heat preservation.
As further scheme of the invention：The step (1) uses 18 mesh screens.
As further scheme of the invention：Holding temperature setting in the step (2), step (3) and step (4)
It is 100 degrees Celsius.
As further scheme of the invention：The step (2) is stirred using the rotating speed of 80r/min.
As further scheme of the invention：The step (3) is stirred using the rotating speed of 20r/min.
As further scheme of the invention：The step (4) is stirred using the rotating speed of 28r/min.
As further scheme of the invention：It is 1.8h that the time placed is stood in the step (5).
Compared with prior art, the beneficial effects of the invention are as follows：
Engine nano abrasion-resistant protective agent of the present invention and preparation method can promote metal to form superpower alloy protecting film, wear-resistant
Coefficient is high, and wearability is good, while having both corrosion resistance, has certain waterproof and lubricating action, and then can play prolonged mechanical
The effect in service life.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：Nanometer two
80 parts of zirconium oxide, 05 part of phosphatidase 1,130 parts of rosin, 6 parts of silane coupling agent, 58 parts of molybdenum disulfide dispersion liquid, 38 parts of silicone oil.
130 parts of 135 degrees Celsius of rosin heating is melted, filtering；Into the rosin of thawing, 6 parts of addition is silane coupled
Agent is stirred evenly using the rotating speed of 80r/min, obtains the first batch mixing, 100 degrees Celsius of heat preservations；80 parts are added into the first batch mixing
Nano zirconium dioxide is stirred evenly using 20r/min, obtains the second batch mixing, 100 degrees Celsius of heat preservations；It is added 38 into the second batch mixing
The silicone oil of part, is stirred evenly using the rotating speed of 28r/min, obtains third batch mixing, 100 degrees Celsius of heat preservations；Into third batch mixing
58 parts of molybdenum disulfide dispersion liquid and 105 parts of phosphatide is added, placement 1.8h is stood after stopping heat preservation.
Embodiment 2
In the embodiment of the present invention, a kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：Nanometer two
115 parts of zirconium oxide, 35 parts of phosphatidase 1,190 parts of rosin, 18 parts of silane coupling agent, 98 parts of molybdenum disulfide dispersion liquid, 68 parts of silicone oil.
190 parts of 135 degrees Celsius of rosin heating is melted, filtering；Into the rosin of thawing, 18 parts of addition is silane coupled
Agent is stirred evenly using the rotating speed of 80r/min, obtains the first batch mixing, 100 degrees Celsius of heat preservations；115 parts are added into the first batch mixing
Nano zirconium dioxide is stirred evenly using 20r/min, obtains the second batch mixing, 100 degrees Celsius of heat preservations；It is added 68 into the second batch mixing
The silicone oil of part, is stirred evenly using the rotating speed of 28r/min, obtains third batch mixing, 100 degrees Celsius of heat preservations；Into third batch mixing
98 parts of molybdenum disulfide dispersion liquid and 135 parts of phosphatide is added, placement 1.8h is stood after stopping heat preservation.
Embodiment 3
In the embodiment of the present invention, a kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：It is described to draw
Hold up nano abrasion-resistant protective agent, which is characterized in that including below according to the raw material of parts by weight：90 parts of nano zirconium dioxide, phosphatidase 1 15
Part, 150 parts of rosin, 7 parts of silane coupling agent, 68 parts of molybdenum disulfide dispersion liquid, 50 parts of silicone oil.
150 parts of 135 degrees Celsius of rosin heating is melted, filtering；Into the rosin of thawing, 7 parts of addition is silane coupled
Agent is stirred evenly using the rotating speed of 80r/min, obtains the first batch mixing, 100 degrees Celsius of heat preservations；90 parts are added into the first batch mixing
Nano zirconium dioxide is stirred evenly using 20r/min, obtains the second batch mixing, 100 degrees Celsius of heat preservations；It is added 50 into the second batch mixing
The silicone oil of part, is stirred evenly using the rotating speed of 28r/min, obtains third batch mixing, 100 degrees Celsius of heat preservations；Into third batch mixing
68 parts of molybdenum disulfide dispersion liquid and 115 parts of phosphatide is added, placement 1.8h is stood after stopping heat preservation.
Embodiment 4
In the embodiment of the present invention, a kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：It is described to draw
Hold up nano abrasion-resistant protective agent, which is characterized in that including below according to the raw material of parts by weight：105 parts of nano zirconium dioxide, phosphatide
125 parts, 160 parts of rosin, 10 parts of silane coupling agent, 88 parts of molybdenum disulfide dispersion liquid, 65 parts of silicone oil.
160 parts of 135 degrees Celsius of rosin heating is melted, filtering；Into the rosin of thawing, 10 parts of addition is silane coupled
Agent is stirred evenly using the rotating speed of 80r/min, obtains the first batch mixing, 100 degrees Celsius of heat preservations；105 parts are added into the first batch mixing
Nano zirconium dioxide is stirred evenly using 20r/min, obtains the second batch mixing, 100 degrees Celsius of heat preservations；It is added 65 into the second batch mixing
The silicone oil of part, is stirred evenly using the rotating speed of 28r/min, obtains third batch mixing, 100 degrees Celsius of heat preservations；Into third batch mixing
88 parts of molybdenum disulfide dispersion liquid and 125 parts of phosphatide is added, placement 1.8h is stood after stopping heat preservation.
Embodiment 5
In the embodiment of the present invention, a kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：Nanometer two
98 parts of zirconium oxide, 18 parts of phosphatidase 1,158 parts of rosin, 8 parts of silane coupling agent, 78 parts of molybdenum disulfide dispersion liquid, 58 parts of silicone oil.
158 parts of 135 degrees Celsius of rosin heating is melted, filtering；Into the rosin of thawing, 8 parts of addition is silane coupled
Agent is stirred evenly using the rotating speed of 80r/min, obtains the first batch mixing, 100 degrees Celsius of heat preservations；98 parts are added into the first batch mixing
Nano zirconium dioxide is stirred evenly using 20r/min, obtains the second batch mixing, 100 degrees Celsius of heat preservations；It is added 58 into the second batch mixing
The silicone oil of part, is stirred evenly using the rotating speed of 28r/min, obtains third batch mixing, 100 degrees Celsius of heat preservations；Into third batch mixing
78 parts of molybdenum disulfide dispersion liquid and 118 parts of phosphatide is added, placement 1.8h is stood after stopping heat preservation.
Comparative example 1
In the embodiment of the present invention, a kind of engine nano abrasion-resistant protective agent, including below according to the raw material of parts by weight：Phosphatide
118 parts, 158 parts of rosin, 8 parts of silane coupling agent, 78 parts of molybdenum disulfide dispersion liquid, 58 parts of silicone oil.
158 parts of 135 degrees Celsius of rosin heating is melted, filtering；Into the rosin of thawing, 8 parts of addition is silane coupled
Agent is stirred evenly using the rotating speed of 80r/min, obtains the first batch mixing, 100 degrees Celsius of heat preservations；58 parts are added into the first batch mixing
Silicone oil is stirred evenly using the rotating speed of 28r/min, obtains the second batch mixing, 100 degrees Celsius of heat preservations；It is added into the second batch mixing
78 parts of molybdenum disulfide dispersion liquid and 118 parts of phosphatide stand placement 1.8h after stopping heat preservation.
The composite material that embodiment and comparative example is prepared, friction coefficient are carried out according to ASTM D1894 standards
As a result as described in Table 1, add from can be seen that in engine nano abrasion-resistant protective agent of the present invention in the experimental result of table 1
Plus nano zirconium dioxide can promote metal to form superpower alloy protecting film, and anti-friction coefficient is high, and wearability is good.
The performance test results of 1 embodiment 1-5 of table, comparative example 1
| Serial number | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example 1 |
| Friction coefficient | 0.08 | 0.06 | 0.075 | 0.07 | 0.11 | 0.01 |
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Profit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent requirements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiment being appreciated that.
Claims (10)
1. a kind of engine nanometer grinds anti-protective agent, which is characterized in that including below according to the raw material of parts by weight：Nanometer titanium dioxide
80-115 parts of zirconium, 05-135 parts of phosphatidase 1,130-190 parts of rosin, 6-18 parts of silane coupling agent, molybdenum disulfide dispersion liquid 58-98
Part, 38-68 parts of silicone oil.
2. engine nano abrasion-resistant protective agent according to claim 1, including below according to the raw material of parts by weight：Nano-silica
Change 90-105 parts of zirconium, 15-125 parts of phosphatidase 1,150-160 parts of rosin, 7-10 parts of silane coupling agent, molybdenum disulfide dispersion liquid 68-88
Part, 50-65 parts of silicone oil.
3. engine nano abrasion-resistant protective agent according to claim 1, including below according to the raw material of parts by weight：Nano-silica
Change 98 parts of zirconium, 18 parts of phosphatidase 1,158 parts of rosin, 8 parts of silane coupling agent, 78 parts of molybdenum disulfide dispersion liquid, 58 parts of silicone oil.
4. the protectant preparation method of engine nano abrasion-resistant as described in claim 1-3 is any, which is characterized in that including following step
Suddenly：
（1）By 135 degrees Celsius of thawings of rosin heating, filtering；
（2）Silane coupling agent is added into the rosin of thawing, stirs evenly, obtains the first batch mixing, keeps the temperature；
（3）Nano zirconium dioxide is added into the first batch mixing, stirs evenly, obtains the second batch mixing, keeps the temperature；
（4）Silicone oil is added into the second batch mixing, stirs evenly, obtains third batch mixing, keeps the temperature；
（5）Molybdenum disulfide dispersion liquid and phosphatide are added into third batch mixing, placement is stood after stopping heat preservation.
5. a kind of protectant preparation method of engine nano abrasion-resistant according to claim 4, which is characterized in that the step
（1）Using 18 mesh screens.
6. a kind of protectant preparation method of engine nano abrasion-resistant according to claim 4, which is characterized in that the step
（2）, step（3）And step（4）In holding temperature be set as 100 degrees Celsius.
7. a kind of protectant preparation method of engine nano abrasion-resistant according to claim 4, which is characterized in that the step
（2）It is stirred using the rotating speed of 80r/min.
8. a kind of protectant preparation method of engine nano abrasion-resistant according to claim 4, which is characterized in that the step
（3）It is stirred using the rotating speed of 20r/min.
9. a kind of protectant preparation method of engine nano abrasion-resistant according to claim 4, which is characterized in that the step
（4）It is stirred using the rotating speed of 28r/min.
10. a kind of protectant preparation method of engine nano abrasion-resistant according to claim 4, which is characterized in that the step
Suddenly（5）The middle time for standing placement is 1.8h.
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| CN201810390671.1A CN108531080A (en) | 2018-04-27 | 2018-04-27 | A kind of engine nano abrasion-resistant protective agent and preparation method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112375495A (en) * | 2020-11-30 | 2021-02-19 | 江苏科技大学 | Self-lubricating water-based environment-friendly coating and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102549282A (en) * | 2009-09-29 | 2012-07-04 | 谢夫勒科技股份两合公司 | Lubricating varnish for coating a metal component or applied to a metal component |
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2018
- 2018-04-27 CN CN201810390671.1A patent/CN108531080A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102549282A (en) * | 2009-09-29 | 2012-07-04 | 谢夫勒科技股份两合公司 | Lubricating varnish for coating a metal component or applied to a metal component |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112375495A (en) * | 2020-11-30 | 2021-02-19 | 江苏科技大学 | Self-lubricating water-based environment-friendly coating and preparation method and application thereof |
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Application publication date: 20180914 |