CN108529556A - A kind of chemistry hydrogen-manufacturing reactor - Google Patents

A kind of chemistry hydrogen-manufacturing reactor Download PDF

Info

Publication number
CN108529556A
CN108529556A CN201810393982.3A CN201810393982A CN108529556A CN 108529556 A CN108529556 A CN 108529556A CN 201810393982 A CN201810393982 A CN 201810393982A CN 108529556 A CN108529556 A CN 108529556A
Authority
CN
China
Prior art keywords
medicine basket
hydrogen
guide post
compression bar
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201810393982.3A
Other languages
Chinese (zh)
Other versions
CN108529556B (en
Inventor
曹玉库
吴宝平
曹素红
李九良
刘来瑞
孔令钊
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
718th Research Institute of CSIC
Original Assignee
718th Research Institute of CSIC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 718th Research Institute of CSIC filed Critical 718th Research Institute of CSIC
Priority to CN201810393982.3A priority Critical patent/CN108529556B/en
Publication of CN108529556A publication Critical patent/CN108529556A/en
Application granted granted Critical
Publication of CN108529556B publication Critical patent/CN108529556B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Structure Of Emergency Protection For Nuclear Reactors (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The present invention discloses a kind of chemical hydrogen-manufacturing reactor, can solve security hidden trouble present in reactor operating process, and more convenient in use.The chemistry hydrogen-manufacturing reactor includes:Reaction tube, the reaction cover for sealing reaction tube and the blanking mechanism inside reaction tube and medicine basket, the medicine basket is for holding hydrogen manufacturing medicament.The blanking mechanism is used for before hydrogen production reaction, and the position of the medicine basket is locked in the top of the preset water surface inside the reaction tube;When needing hydrogen production reaction, the locking to medicine basket position is released, it is made to fall into the water in reaction tube.

Description

A kind of chemistry hydrogen-manufacturing reactor
Technical field
Invention is related to a kind of reactor, and in particular to a kind of reaction vessel for chemically reacting hydrogen making.
Background technology
Chemical hydrogen manufacturing cylinder or similar chemical reaction container (or reaction kettle) used at this stage, are all made of first addition system Hydrogen medicament and water, water and hydrogen manufacturing are in direct contact with medicament;Then the mode of re-closed (or closing) reactor (or reaction kettle). The basic operation flow of this kind of reactor:The water centainly matched and hydrogen manufacturing medicament are sequentially added in reactor first;Then Reactor is closed with most fast speed, it is waited for fully to be reacted.
Such reactor (or reaction kettle) has the following problems:After water and hydrogen manufacturing medicament is added, sealed in reactor Before, hydrogen manufacturing just has begun to react with medicament, especially when environment temperature is higher, due to hydrogen production reaction speed, anti- Inside has just produced a large amount of hydrogen before answering device sealing, and operating personnel's action is slightly slow, is just faced with reactor sealing not Firmly or poorly sealed situation;This kind of mode operates, and is usually present due to generating a large amount of hydrogen in the short time, and pressure is excessive to be led The too late, high pressure gas in the presence of sealing is caused to go out (or washing sealing element open), danger of hurting sb.'s feelings.
Invention content
In view of this, the present invention provide a kind of controllable hydrogen production reaction start the time, simple operation chemical hydrogen production reaction Device can not only solve security hidden trouble present in reactor operating process, and more convenient in use.
The chemical hydrogen-manufacturing reactor, including:Reaction tube and reaction cover for sealing reaction tube are set on reaction tube It is equipped with hydrogen outlet and discharge outlet;In addition, further including:Blanking mechanism inside reaction tube and medicine basket, the medicine basket are used for Hold hydrogen manufacturing medicament;
The blanking mechanism is used for before hydrogen production reaction, the position of the medicine basket is locked in preset inside the reaction tube The top of the water surface;When needing hydrogen production reaction, the locking to medicine basket position is released, it is made to fall into the water in reaction tube.
The blanking mechanism includes:Compression bar, spring, gear tongue, shaft and guide post;The guide post is co-axially located at described In reaction tube, the medicine basket is sleeved on by sleeve outside guide post;
The guide post is hollow tubular structure, and the compression bar coaxial package is in its center in hole, and at the top of the compression bar Stretch out guide post;The spring pocket outside compression bar, with the protrusion on the compression bar outer circumference surface support by the top of the spring It touches, bottom is contradicted with the guide post upper surface;
Gear tongue is provided with below compression bar in the guide post, shaft is provided in the middle part of the gear tongue and forms lever knot Structure, wherein one end of gear tongue is opposite with compression bar bottom, the other end stretches out guide post and lives medicine basket for frame, so that the medicine basket is located at pre- It sets above the water surface;When being pressed downward described gear tongue one end by the compression bar, the gear tongue other end, which rotates around the axis, to be retracted to Inside guide post.
Advantageous effect:
By the way that blanking mechanism and medicine basket is arranged so that the hydrogen production reaction startup time is controllable, can be after reactor sealing again Start hydrogen production reaction, to effectively avoid security risk present in reactor operating process.
Description of the drawings
Fig. 1 is chemical hydrogen-manufacturing reactor structural schematic diagram provided by the present invention;
Fig. 2 is the structural schematic diagram of blanking mechanism.
Wherein:1- start buttons, 2- pressure heads, 3- gasket seals, 4- springs, 5- compression bars, 6- spacer pins, 7- medicines basket, 8- gears Tongue, 9- shafts, 10- guide posts, 11- reaction tubes, 12- discharge outlet, 13- hydrogen outlets, 14- react cover
Specific implementation mode
The present invention will now be described in detail with reference to the accompanying drawings and examples.
The present embodiment provides a kind of chemical hydrogen-manufacturing reactors, can solve security risk present in reactor operating process Problem, and it is more convenient in use.
As shown in Figure 1, the hydrogen-manufacturing reactor includes:Reaction tube 11 reacts cover 14, blanking mechanism and for holding hydrogen manufacturing The medicine basket 7 of medicament.The sealing that reaction cover 14 in 11 top open part of reaction tube is used for reaction tube 11 is set, on reaction tube 11 Portion is provided with hydrogen outlet 13, and lower part is provided with discharge outlet 12.
As shown in Fig. 2, blanking mechanism includes:Start button 1, pressure head 2, compression bar 5, spring 4, gear tongue 8, turns gasket seal 3 Axis 9, spacer pin 6 and guide post 10.
Guide post 10 is coaxially arranged in reaction tube 11, medicine basket 7 is sleeved on by sleeve outside guide post 10, Neng Gouyan Guide post 10 moves axially.Guide post 10 is hollow tubular structure, and 5 coaxial package of compression bar is in its center in hole, and 5 bottom of compression bar In guide post 10, guide post 10 is stretched out at top, carries out circumferential limit to compression bar 5 by spacer pin 6, compression bar 5 is made to be merely able to It is axially moveable in the centre bore of guide post 10.Spring 4 is sleeved on outside compression bar 5, wherein on the top of spring 4 and compression bar 5 The protrusion of end face contradicts, and bottom is contradicted with 10 upper surface of guide post.The lower section of compression bar 5 is provided with gear tongue 8, gear in guide post 10 8 middle part of tongue is provided with shaft 9 and forms it into lever construction, wherein one end of gear tongue 8 is opposite with 5 bottom of compression bar, the other end stretches out 10 frame of guide post lives medicine basket 7, and medicine basket 7 is made to be located above the preset water surface;When compression bar 5 is pressed downward gear tongue end corresponding thereto, 9 rotations are retracted to inside guide post 10 8 other end of gear tongue around the shaft, so that the medicine basket 7 equipped with hydrogen production agent is moved along guide post 10 and are fallen Enter in water.
To ensure after reaction, when taking medicine basket 7 upwards gear tongue 8 can automatic retracted, gear tongue 8 lives medicine basket 7 for frame The end face of one end is inclined inclined-plane inwardly downward, and when taking medicine basket 7 upwards as a result, medicine basket 7 squeezes the inclined-plane so that gear tongue 8 around The rotation of shaft 9 is retracted to inside guide post 10, to promote medicine basket 7 directly up.
The centre bore for install pressure head 2 coaxial with compression bar 5, pressure head 2 and the centre bore are provided on reaction cover 14 Clearance fit can move axially in the centre bore, and the bottom of pressure head 2 is opposite with compression bar 5.Start button 1 is connected by screw thread It is connected on 2 top of pressure head.When the hydrogen-manufacturing reactor does not work, start button 1 and the screw thread of pressure head 2 are tightened, made under start button 1 End face is in close contact with 14 upper surface of cover is reacted, and gasket seal 3 is arranged in contact surface, to seal reaction tube 11.Start When work, start button 1 is spun up setpoint distance by rotation start button 1 upwards (makes pressure head 2 in the centre bore of reaction cover 14 Have the space of axial movement), start button 1 is then pressed, pushes compression bar 5 to be pressed downward gear tongue 8 by pressure head 2, while compressing bullet Spring 4.
Its working principle is that:When hydrogen manufacturing operates, it is first turned on reaction cover 14, into reaction tube 11 plus is filled to preset water Face;Then hydrogen manufacturing medicament is put into medicine basket 7, medicine basket 7 puts down to be lived by 8 frame of gear tongue along guide post 10, and medicine basket 7 is located at preset at this time Above the water surface, do not contacted with water.The capping reaction cover 14 at 11 upper opening of reaction tube, and make reaction cover 14 and reaction tube 11 sealings are secured.After ready, the about 10mm of start button 1 is spun up upwards, then depresses start button 1, and pressure head 2 pushes compression bar 5 are pressed downward gear tongue 8, while compressed spring 4;It keeps off tongue 8 to bounce back, releases the limit to medicine basket 7, the medicine basket 7 equipped with hydrogen production agent is made to fall Enter in water, after medicine basket 7 falls into the water, after unclamping start button 1, compression bar 5 moves up to just under the action of 4 restoring force of spring Beginning position keeps off 8 return of tongue.Hydrogen production agent in medicine basket 7 contacts generation chemical reaction with water and generates hydrogen, and passes through hydrogen outlet 13 Hydrogen is transferred out.Waste water is discharged through discharge outlet 12 after the completion of reaction, opens reaction cover 14 and takes out medicine basket 7, hydrogen manufacturing terminates. Whole operation process safety is reliable.
In conclusion the above is merely preferred embodiments of the present invention, being not intended to limit the scope of the present invention. All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in the present invention's Within protection domain.

Claims (6)

1. a kind of chemistry hydrogen-manufacturing reactor, including:Reaction tube (11) and reaction cover (14) for sealing reaction tube (11), instead It answers and is provided with hydrogen outlet (13) and discharge outlet (12) on cylinder (11);It is characterized in that, further including:It is internal positioned at reaction tube (11) Blanking mechanism and medicine basket (7), the medicine basket (7) is for holding hydrogen manufacturing medicament;
The blanking mechanism is used for before hydrogen production reaction, and it is internal that the position of the medicine basket (7) is locked in the reaction tube (11) The top of the preset water surface;When needing hydrogen production reaction, the locking to medicine basket (7) position is released, it is made to fall into reaction tube (11) in the water in.
2. chemistry hydrogen-manufacturing reactor as described in claim 1, which is characterized in that the blanking mechanism includes:Compression bar (5), bullet Spring (4), gear tongue (8), shaft (9) and guide post (10);The guide post (10) is co-axially located in the reaction tube (11), institute It states medicine basket (7) and guide post (10) outside is sleeved on by sleeve;
The guide post (10) is hollow tubular structure, and compression bar (5) coaxial package is in its center in hole, and the compression bar (5) guide post (10) is stretched out at top;The spring (4) is sleeved on compression bar (5) outside, top and the pressure of the spring (4) Protrusion on bar (5) outer circumference surface contradicts, and bottom is contradicted with the guide post (10) upper surface;
It is provided with gear tongue (8) below the guide post (10) interior compression bar (5), shaft (9) is provided in the middle part of the gear tongue (8) Lever construction is formed, wherein one end of gear tongue (8) is opposite with compression bar (5) bottom, the other end stretches out guide post (10) and lived for frame Medicine basket (7) makes the medicine basket (7) be located above the preset water surface;When being pressed downward described gear tongue (8) one end by the compression bar (5) When, it is internal that gear tongue (8) other end (9) rotation around the shaft is retracted to guide post (10).
3. chemistry hydrogen-manufacturing reactor as claimed in claim 2, which is characterized in that be provided with and be used on the reaction cover (14) Apply the start button (1) and pressure head (2) of downward pressure to the compression bar (5);Specially:It is set on the reaction cover (14) It is equipped with the through-hole for installing pressure head (2), the pressure head (2) can move axially in the through hole, the bottom of pressure head (2) and institute It is opposite to state compression bar (5);The start button (1) is located at the top of the pressure head (2), and is threadedly coupled with the pressure head (2).
4. as claimed in claim 2 or claim 3 chemistry hydrogen-manufacturing reactor, which is characterized in that the blanking mechanism further include for pair The spacer pin (6) that the compression bar (5) is circumferentially limited.
5. chemistry hydrogen-manufacturing reactor as claimed in claim 2 or claim 3, which is characterized in that the gear tongue (8) lives medicine basket for frame (7) end face of one end is that inclined inclined-plane squeezes this tiltedly when taking medicine basket (7) upwards by the medicine basket (7) inwardly downward Face makes the gear tongue (8) (9) rotation around the shaft be retracted to guide post (10) internal.
6. chemistry hydrogen-manufacturing reactor as claimed in claim 3, which is characterized in that in the reaction cover (14) upper surface and institute It states the opposite position of start button (1) and is provided with gasket seal (3).
CN201810393982.3A 2018-04-27 2018-04-27 Chemical hydrogen production reactor Active CN108529556B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810393982.3A CN108529556B (en) 2018-04-27 2018-04-27 Chemical hydrogen production reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810393982.3A CN108529556B (en) 2018-04-27 2018-04-27 Chemical hydrogen production reactor

Publications (2)

Publication Number Publication Date
CN108529556A true CN108529556A (en) 2018-09-14
CN108529556B CN108529556B (en) 2021-06-15

Family

ID=63479376

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810393982.3A Active CN108529556B (en) 2018-04-27 2018-04-27 Chemical hydrogen production reactor

Country Status (1)

Country Link
CN (1) CN108529556B (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7666386B2 (en) * 2005-02-08 2010-02-23 Lynntech Power Systems, Ltd. Solid chemical hydride dispenser for generating hydrogen gas
CN202116294U (en) * 2011-07-20 2012-01-18 夏鸣 Controllable aluminum scrap hydrogen manufacturing device
CN204625175U (en) * 2015-04-14 2015-09-09 四川大学 Self-control type device for preparing hydrogen through hydrolysis
JP5909337B2 (en) * 2011-08-30 2016-04-26 セイコーインスツル株式会社 Hydrogen generator and fuel cell

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7666386B2 (en) * 2005-02-08 2010-02-23 Lynntech Power Systems, Ltd. Solid chemical hydride dispenser for generating hydrogen gas
CN202116294U (en) * 2011-07-20 2012-01-18 夏鸣 Controllable aluminum scrap hydrogen manufacturing device
JP5909337B2 (en) * 2011-08-30 2016-04-26 セイコーインスツル株式会社 Hydrogen generator and fuel cell
CN204625175U (en) * 2015-04-14 2015-09-09 四川大学 Self-control type device for preparing hydrogen through hydrolysis

Also Published As

Publication number Publication date
CN108529556B (en) 2021-06-15

Similar Documents

Publication Publication Date Title
GB1458052A (en) Method of administering securing and detaching a rinsing container
CN108529556A (en) A kind of chemistry hydrogen-manufacturing reactor
CN207500461U (en) A kind of special type pressure vessel fast and safely closing device
CN107176274B (en) Chemical gas storage type underwater life-saving equipment
CN210566478U (en) Safety valve with safety warning function
CN209080587U (en) A kind of improved combined bottle cap
CN204543341U (en) Hand fire extinguisher
KR200426428Y1 (en) Mixing vessel is capable of mixed using of materials
CN202932764U (en) Safety mechanism for soft drink manufacturing device
WO2015180220A1 (en) Portable soda machine with disposable small steel bottle, security device and dust removal device
CN208583243U (en) A kind of food inspection agitating device
CN103708095B (en) A kind of Dustproof emulsion pump mechanism
CN215981999U (en) Safety gas cylinder with slow release valve
CN112081925B (en) Sealing method for pre-ash barrel
CN110758893B (en) Locking bottle seal structure that takes off
CN215783239U (en) Mixing device
CN207187549U (en) A kind of horizontal mixer for being easy to discharging
CN220054919U (en) Vacuum bottle with locking function
CN206750493U (en) A kind of press-type bottle cover of built-in effervescent tablet
CN220616798U (en) Pressure type bath foam accommodating bottle
CN219668895U (en) Essential oil pump
CN212686416U (en) Explosion-proof chemical material barrel
CN218221904U (en) Mixing device
CN220737556U (en) Alkali washing kettle for chemical reagent production
CN219524846U (en) Container lid with screw-free quick seal and opening

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant