CN108524351A

CN108524351A - Toner and preparation method thereof

Info

Publication number: CN108524351A
Application number: CN201810349341.8A
Authority: CN
Inventors: 葛啸虎; 陈海佳; 王飞; 王一飞; 王小燕
Original assignee: Guangzhou Saliai StemCell Science and Technology Co Ltd
Current assignee: Guangzhou Saliai StemCell Science and Technology Co Ltd
Priority date: 2018-04-18
Filing date: 2018-04-18
Publication date: 2018-09-14

Abstract

The present invention relates to a kind of toners and preparation method thereof.Wherein, a kind of toner, by weight, the toner include that following raw materials are made：8 12 parts of vegetable fat；15 20 parts of moisturizer；10 20 parts of hole leaf algae extract；5 10 parts of thymopeptide-5；And 40 60 parts of deionized water.For above-mentioned toner because not adding emulsifier and surfactant, no greasy feeling non-stimulated to skin can play moisturizing, whitening effect.

Description

Toner and preparation method thereof

Technical field

The present invention relates to cosmetic technical fields, more particularly to a kind of toner and preparation method thereof.

Background technology

Existing toner, makeup breast are because containing a large amount of emulsifier, surfactant, a large amount of emulsifier, surface are lived Property agent it is big to skin irritation, especially for sensitive skin of face, dangerous property.

Invention content

Based on this, it is necessary in view of the above-mentioned problems, providing a kind of toner including hole leaf algae extract.

A kind of toner, by weight, the toner include that following raw materials are made：

8-12 parts of vegetable fat；

15-20 parts of moisturizer；

10-20 parts of hole leaf algae extract；

5-10 parts of thymopeptide-5；

And 40-60 parts of deionized water.

For above-mentioned toner because not adding emulsifier and surfactant, no greasy feeling non-stimulated to skin can play guarantor Wet, whitening effect.

In one of the embodiments, by weight, the toner further includes 4-8 parts of suspension stabilizer.

The suspension stabilizer is natural gum or sodium cellulose glycolate in one of the embodiments,.

The natural gum is at least one of Arabic gum, bassora gum, peach gum in one of the embodiments,.

In one of the embodiments, the vegetable fat be champaca flower oil, olive oil or clove bud oil at least It is a kind of.

The suspension stabilizer is on the cellulose for being loaded into grain size and being 20 μm -28 μm in one of the embodiments, Natural gum.

The moisturizer is at least one of D-sorbite, propylene glycol in one of the embodiments,.

It is 1 that the moisturizer, which includes mass ratio, in one of the embodiments,:1 D-sorbite and propylene glycol.

In one of the embodiments, by weight, the moisturizer includes D-sorbite and propylene glycol, and the mountain Pears sugar alcohol is 10 parts, and the propylene glycol is 8 parts.

Present invention also provides a kind of preparation methods of toner.

A kind of preparation method of toner as described in the present application, the preparation method of toner include the following steps：By weight Amount part weigh 8-12 parts of vegetable fat, 15-20 parts of moisturizer, 10-20 parts hole leaf algae extract, 5-10 parts of thymus gland five Peptide and 40-60 parts of deionized water are stirred and heated to 60 DEG C -70 DEG C, feed liquid are uniformly mixing to obtain, then in 3000r/ Homogeneous 10min-15min under min-3999r/min, obtains toner.

The preparation method of above-mentioned toner makeup water constituent obtained is evenly dispersed, and oil fraction will not be precipitated.Above-mentionedization Adornment water no greasy feeling non-stimulated to skin can play moisturizing, whitening effect.

The hole leaf algae extract is prepared using following technique in one of the embodiments,：

The holes 2kg leaf algae is taken, by 1:The Kong Yezao is immersed 70%-80% ethyl alcohol and impregnates 30min- by 8 solid-liquid ratio 60min；

It is subsequently placed in heating and refluxing extraction 2h-3h in water-bath, is filtered, filtrate, 6 times of amount 70%-80% second of filter residue are collected Alcohol repeats to extract once, merges filtrate twice；

The filtrate decompression twice of the merging is concentrated into no alcohol taste, concentrate is adsorbed by macroporous resin column, first With distillation water elution, then use 50% ethanol elution, collection 50% ethanol eluate, hole leaf algae extract is obtained after reduced pressure.

Specific implementation mode

In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, below in conjunction with specific implementation mode, The present invention will be described in further detail.It should be appreciated that the specific embodiments described herein are only used to explain this hair It is bright, it is not intended to limit the present invention.

Unless otherwise defined, all of technologies and scientific terms used here by the article and belong to the technical field of the present invention The normally understood meaning of technical staff is identical.Used term is intended merely to description tool in the description of the invention herein The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more Any and all combinations of relevant Listed Items.

Herein, term " part " is parts by weight.Unless otherwise specified, all measurements carry out at 25 DEG C.

In addition, term " first ", " second " are used for description purposes only, it is not understood to indicate or imply relative importance Or implicitly indicate the quantity of indicated technical characteristic.Define " first " as a result, the feature of " second " can be expressed or Implicitly include at least one this feature.In the description of invention, the meaning of " plurality " is at least two, such as two, three Deng unless otherwise specifically defined.In the description of the present invention, " several " are meant that at least one, such as one, two It is a etc., unless otherwise specifically defined.

The present invention provides a kind of toners, and by weight, toner includes that following raw materials are made：

8-12 parts of vegetable fat；

15-20 parts of moisturizer；

10-20 parts of hole leaf algae extract；

5-10 parts of thymopeptide-5；

And 40-60 parts of deionized water.

Wherein, leaf algae extract in hole is the algae of Phaeophyceae, Laminariales, and whitening, nti-freckle are contained in the leaf algae extract of hole Ingredient can provide sufficient water studies have shown that hole leaf algae extract is rich in a large amount of vitamin C and vitamin E for skin Point.

In a preferred embodiment, leaf algae extract in hole is 10-20 parts by weight, for example, hole leaf algae extract is 10 Part, 15 parts or 20 parts.

Wherein, the main function of vegetable fat is to releive to decompress and toner is made to have aromatic odor.

In a preferred embodiment, vegetable fat is at least one in champaca flower oil, olive oil or clove bud oil Kind.

Preferably, clove bud oil content is 8-10 parts, for example, clove bud oil content is 8 parts, 9 parts, 10 parts.

Wherein, thymopeptide-5 is N- [N- [N- [N α L- arginyl-L- lysyls [- L- α-aspartoyl]-L- figured silk fabrics ammonia Acyl]-l-tyrosine.Studies have shown that thymopeptide-5 is generally used for enhancing damnification of immunity function, the inventors of the present application found that Thymopeptide-5 plays good white-skinned face function with the hole mutual compatibility of leaf algae extract.

In a preferred embodiment, toner further includes the suspension stabilizer of 4-8 parts by weight.For example, 4 parts suspend surely Determine agent, 6 portions of suspension stabilizers, 8 portions of suspension stabilizers.

Wherein, the main function of suspension stabilizer is that water/oil is made to form uniform and stable dispersion.Make in toner Grease will not mutually sink rapidly.

In a preferred embodiment, suspension stabilizer can be selected from sodium cellulose glycolate or natural gum, it is highly preferred that Suspension stabilizer is natural gum.Most preferably, natural gum can be at least one of Arabic gum, bassora gum, peach gum.

Present inventor has found, in order to increase the effect that water/oil forms unit for uniform suspension, suspension stabilizer is loaded into In the natural gum that grain size is 20 μm -28 μm.Carrier using the cellulose of specified particle diameter as suspension stabilizer.For example, first to changing Grease is adsorbed in adornment water, recycles suspension stabilizer that cellulose is dispersed in water phase.It is highly preferred that by suspension stabilizer It is loaded into the natural gum that grain size is 25 μm.Then the natural gum for loading suspension stabilizer is mixed with other components of toner again. Wherein, it is 20-40% that suspension stabilizer, which accounts for cellulose mass fraction,.Preferably, suspension stabilizer accounts for cellulose mass fraction and is 30%.

In a preferred embodiment, by weight, toner includes that following raw materials are made：

9-10 parts of vegetable fat；

15-18 parts of moisturizer；

12-16 parts of hole leaf algae extract；

6-8 parts of thymopeptide-5；

5-7 parts of Arabic gum；

And 50-55 parts of deionized water.

In a preferred embodiment, moisturizer is at least one of D-sorbite, propylene glycol.Preferably, sorb Sugar alcohol is 10 parts by weight, and propylene glycol is 8 parts by weight.

The present invention also provides a kind of preparation methods of toner.

The preparation method of toner includes the following steps：8-12 parts of vegetable fat, 15-20 parts of guarantor are weighed by weight Humectant, 10-20 parts of hole leaf algae extract, 5-10 parts of thymopeptide-5 and 40-60 parts of deionized water is stirred and heated to 60 DEG C -70 DEG C, it is uniformly mixing to obtain feed liquid, then the homogeneous 10min-15min at 3000r/min-3999r/min, is changed Adornment water.

In a preferred embodiment, leaf algae extract in hole is prepared using following technique：

The holes 2kg leaf algae is taken, by 1:Kong Yezao is immersed 70%-80% ethyl alcohol and impregnates 30min-60min by 8 solid-liquid ratio；So It is placed on heating and refluxing extraction 2h-3h in water-bath, is filtered, filtrate is collected, filter residue repeats to extract with 6 times of amount 70%-80% ethyl alcohol Once, merge filtrate twice；The filtrate decompression twice of merging is concentrated into no alcohol taste, concentrate is inhaled by macroporous resin column It is attached, first with distillation water elution, then use 50% ethanol elution, collection 50% ethanol eluate, obtain Kong Yezao after reduced pressure and carry Take object.

Preferably, soaking time 50min.

Preferably, the toner further includes 5-8 parts of mangosteen extract, 2-7 parts of Honegsukle flower P.E and needle juniper extract 2-6 parts.

Present inventor is by a large amount of the study found that by mangosteen extract, Honegsukle flower P.E and needle juniper extract Toner is prepared as raw material compounding, synergistic effect well is generated between each raw material, there is significant moisturizing, anti-acne and oil-control Effect.The compatibility amount of raw material is that inventor gets by the analysis of a large amount of Research statistics, and each raw material can in the amount ranges Synergistic effect well is played, is not had any side-effects simultaneously.

Preferably, the toner further includes applicator system, for example, the applicator system includes control painting pen, the painting Pen is smeared to include cylinder, Massage Department, spring, ball and support bar, the cylinder offers accommodating cavity, the accommodating cavity it is accommodating just like Rest part of the toner other than applicator system described in upper any embodiment, in other words, the toner is in addition to applying The rest part except system is smeared to be placed in the accommodating cavity.The Massage Department connects the cylinder, and the Massage Department has Hollow structure, the Massage Department are provided with fixed link, end of the Massage Department far from the cylinder adjacent to one end of the cylinder Portion offers sample outlet hole, and the ball part is placed in the sample outlet hole, and the first end for supporting bar connects the ball, The second end for supporting bar connects the first end of the spring, and the second end of the spring connects the fixed link, the rolling Pearl supports bar and compresses the spring to open the sample outlet hole described in being used to drive when the ball is by external pressure, described Ball is additionally operable to close the sample outlet hole under the action of restoring force of the spring when external pressure disappears.In this way, above-mentioned Applicator system can preferably smear rest part of the toner other than applicator system.For another example, the sample outlet hole Shape adaptation is in the shape of the ball.For another example, the cylinder is spirally connected the Massage Department.

In order to preferably install the spring, in an embodiment, storage tank is provided in the fixed link, the spring Second end is placed in the storage tank, and for another example, the second end of the spring is abutted with the bottom wall of the storage tank.For another example, institute The second end of spring is stated in the storage tank, for another example, the second end of the spring is embedded in the storage tank and institute The second end for stating spring is abutted with the bottom wall of the storage tank.For another example, the bar that supports is provided with mounting groove, and the of the spring One end is placed in the mounting groove, and for another example, the first end of the spring is abutted with the bottom wall of the mounting groove.For another example, described The first end of spring is in the mounting groove, and for another example, the first end of the spring is in the mounting groove and described The first end of spring is abutted with the bottom wall of the mounting groove, so, it is possible preferably to install the spring.

In order to enable the ball preferably to close and open the sample outlet hole, in an embodiment, it is described go out sample Hole has circular cross-section, and for another example, the sample outlet hole has arc shaped inside wall, and for another example, the sample outlet hole is along close to the cylinder Direction gradually broadens, and for another example, the diameter in the section at the most narrow place of the sample outlet hole is less than the diameter of the ball, so, it is possible to make The ball preferably can close and open the sample outlet hole.

In order to play preferable massage effect, in an embodiment, the lateral wall of the Massage Department is provided with burr, again Such as, the lateral wall of the Massage Department is provided with several burrs, and for another example, several burrs are circularly and evenly distributed in the massage On the lateral wall in portion, it so, it is possible to make the Massage Department that can also play preferable massage effect.

Above system had not only facilitated toner rapid application to make up, but also can play the effect of massaging human body.

Below in conjunction with specific embodiment, the invention will be further elaborated.

Embodiment 1

A kind of precursor composition of toner includes following components by weight：

Table 1

Wherein, leaf algae extract in hole is prepared using following technique：

The holes 2kg leaf algae is taken, by 1:Kong Yezao is immersed 70% ethyl alcohol and impregnates 45min by 8 solid-liquid ratio.It is subsequently placed in water-bath Filtrate is collected in middle heating and refluxing extraction 2h, filtering, and filter residue is primary with 6 times of amount 70% ethyl alcohol repetition extractions, merges filtrate twice.

The filtrate decompression twice of merging is concentrated into no alcohol taste, concentrate is adsorbed by macroporous resin column, first with steaming Distilled water elute, then use 50% ethanol elution, collection 50% ethanol eluate, hole leaf algae extract is obtained after reduced pressure.

Component in table 1 is mixed, is stirred and heated to 70 DEG C, feed liquid is uniformly mixing to obtain, then at 3000r/min Homogeneous 14 minutes, obtains toner A1.

Embodiment 2

Table 2

Component	Content (is converted into g calculating)
		Champaca flower oil	9
D-sorbite	18
		Hole leaf algae extract	18
Deionized water	45
		Thymopeptide-5	9

Wherein, leaf algae extract in hole is prepared using following technique：

Component in table 2 is mixed, is stirred and heated to 75 DEG C, feed liquid is uniformly mixing to obtain, then at 3500r/min Homogeneous 18 minutes, obtains toner A2.

Embodiment 3

Table 3

Component	Content (is converted into g calculating)
		Champaca flower oil	6
D-sorbite	18
		Clove bud oil	6
Hole leaf algae extract	18
		Deionized water	45
Thymopeptide-5	9
		Arabic gum (is loaded into cellulose)	7

Wherein, leaf algae extract in hole is prepared using following technique：

Wherein, the treatment process of Arabic gum is：7g Arabic gums are loaded into the cellulose that grain size is 25 μm, In, it is 30% that Arabic gum, which accounts for cellulose mass fraction,.

Component in table 3 is mixed, is stirred and heated to 60 DEG C, feed liquid is uniformly mixing to obtain, then at 3800r/min Homogeneous 20 minutes, obtains toner A3.

Embodiment 4

Table 4

Component	Content (is converted into g calculating)
		Champaca flower oil	9
D-sorbite	18
		Hole leaf algae extract	18
Deionized water	45
		Thymopeptide-5	6
Arabic gum	7

Wherein, leaf algae extract in hole is prepared using the technique of embodiment 3.

Component in table 4 is mixed, is stirred and heated to 75 DEG C, feed liquid is uniformly mixing to obtain, adds 0.3 part of benzene oxygen second Alcohol, then homogeneous 18 minutes at 3500r/min, obtain toner A4.

Performance test：

1, test reagent

A1-A4 toners, commercially available certain brand toner B1 (control group)

2, tested crowd

Age:60 people of women between 30-40 Sui, is divided into 5 groups.

Health status:Subjects skin's health, no skin disease allergies meet subject and volunteer inclusion criteria.

3, test method

A1, A2, A3, A4 toner, commercially available toner B1 wiping cheek are used respectively and suitably massage 5min (continuous uses one A month), moisture when then utilizing skinanalysis apparatus test skin surface original water content and 4 hours.

4, experimental condition

Room temperature, relative humidity 40%.

5, evaluation index

Transdermal percentage of water loss=[(the initial blank value of original water content -)-(- 4 hours blank values of 4 hours moistures)]/ (the initial blank value of original water content -)

Moistening effect is weighed with transdermal percentage of water loss.

Whitening effect is evaluated

In the inboard arm of testee, ultraviolet B radiation UVB is irradiated 1 time a day with twice of minimal erythema dose, continuously Irradiation 3 days stops.To the erythema 1 day 1 time of generation, A1, A2, A3, A4 toner, toner B1 to 2 commercially available is continuously smeared Month, erythema recession situation, the i.e. index as evaluation whitening effect are observed, is measured using colour difference meter.

The measured value at position is measured before erythema measured value=continuous measured value-smearing for smearing 2 months measured positions

Wherein, each test group takes every group of average measurement.

6, test result

Table 5

	Moistening effect (transdermal percentage of water loss)	Erythema measured value
			A1	33.53%	0.65
A2	30.13%	0.78
			A3	28.84%	0.34
A4	29.72%	0.45
			B1	36.33%	0.79

As shown in Table 5, for each test group (A1, A2, A3, A4) is compared with B1 groups, transdermal percentage of water loss is relatively low, erythema measured value compared with It is low.And then show that the moistening effect of the toner of test group and whitening effect are preferable.Wherein, A3, A4 group are containing suspending stabilized Agent, each component in toner are uniformly mixed.And the guarantor of A3 (containing the Arabic gum for being loaded into the cellulose that grain size is 25 μm) group Wet effect and whitening effect are best, and in subjective appreciation test, A3 group toners are homogeneous, no water-oil separating phenomenon, in half Flow-like.Skin sense after smearing is salubrious, soft, to skin without obvious stimulation.

It should be noted that the parts by weight in each embodiment, i.e. mass parts, that is, mass fraction, Ke Yili Xie Weike, milligram, kilogram, jin, kilogram, pound, ton etc..By gram for, for example, 1 parts by weight be 0.0001 to 10000 gram in A certain quality；For example, 1 parts by weight can be 0.001g, 0.01g, 0.02g, 0.05g, 0.1g, 0.2g, 0.5g, 1g, 2g, 3g, 4g, 5g, 10g, 15g, 20g, 30g, 50g, 80g, 100g, 500g, 1000g, 5000g, 10000g or 50000g etc., and be not limited to This, manufactures according to actual production and selects, each embodiment and so on.For example, 1 parts by weight are 1 gram, 0.1 parts by weight are 0.1 gram, and so on.

Each technical characteristic of embodiment described above can be combined arbitrarily, to keep description succinct, not to above-mentioned reality It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited In contradiction, it is all considered to be the range of this specification record.

Several embodiments of the invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the protection of the present invention Range.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.

Claims

1. a kind of toner, which is characterized in that by weight, the toner includes that following raw materials are made：

8-12 parts of vegetable fat；

15-20 parts of moisturizer；

10-20 parts of hole leaf algae extract；

5-10 parts of thymopeptide-5；

And 40-60 parts of deionized water.

2. toner according to claim 1, which is characterized in that by weight, the toner further includes 4-8 parts Suspension stabilizer.

3. toner according to claim 2, which is characterized in that the suspension stabilizer is natural gum or hydroxymethyl cellulose Sodium.

4. toner according to claim 1, which is characterized in that the natural gum is Arabic gum, bassora gum, in peach gum extremely Few one kind.

5. toner according to claim 1, which is characterized in that the vegetable fat is champaca flower oil, olive oil or fourth At least one of fragrant flower bud oil.

6. toner according to claim 3, which is characterized in that the suspension stabilizer be loaded into grain size be 20 μm- Natural gum on 28 μm of cellulose.

7. toner according to claim 1, which is characterized in that the moisturizer is D-sorbite, in propylene glycol extremely Few one kind.

8. toner according to claim 7, which is characterized in that the moisturizer includes that mass ratio is 1:1 sorb Sugar alcohol and propylene glycol.

9. a kind of preparation method of toner, which is characterized in that the preparation method of the toner includes the following steps：By weight Part weigh 8-12 parts of vegetable fat, 15-20 parts of moisturizer, 10-20 parts hole leaf algae extract, 5-10 parts of thymus gland five Peptide and 40-60 parts of deionized water；60 DEG C -70 DEG C are stirred and heated to, feed liquid is uniformly mixing to obtain, then in 3000r/ Homogeneous 10min-15min under min-3999r/min, obtains toner.

10. the preparation method of toner according to claim 9, which is characterized in that the hole leaf algae extract is using such as It is prepared by lower technique：

The holes 2kg leaf algae is taken, by 1:The Kong Yezao is immersed 70%-80% ethyl alcohol and impregnates 30-60min by 8 solid-liquid ratio；Then It is placed in heating and refluxing extraction 2-3h in water-bath, is filtered, filtrate is collected, filter residue repeats extraction one with 6 times of amount 70%-80% ethyl alcohol It is secondary, merge filtrate twice；

The filtrate decompression twice of the merging is concentrated into no alcohol taste, concentrate is adsorbed by macroporous resin column, first with steaming Distilled water elute, then use 50% ethanol elution, collection 50% ethanol eluate, hole leaf algae extract is obtained after reduced pressure.