CN108517395A - A kind of cold rolling non-oriented electrical steel band and preparation method thereof - Google Patents

A kind of cold rolling non-oriented electrical steel band and preparation method thereof Download PDF

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Publication number
CN108517395A
CN108517395A CN201810472997.9A CN201810472997A CN108517395A CN 108517395 A CN108517395 A CN 108517395A CN 201810472997 A CN201810472997 A CN 201810472997A CN 108517395 A CN108517395 A CN 108517395A
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China
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preparation
electrical steel
oriented electrical
cold rolling
steel band
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CN201810472997.9A
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Chinese (zh)
Inventor
占云高
王立涛
裴英豪
施立发
何峰
丰慧
杜军
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Maanshan Iron and Steel Co Ltd
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Maanshan Iron and Steel Co Ltd
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Priority to CN201810472997.9A priority Critical patent/CN108517395A/en
Publication of CN108517395A publication Critical patent/CN108517395A/en
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1216Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the working step(s) being of interest
    • C21D8/1222Hot rolling
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1216Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the working step(s) being of interest
    • C21D8/1233Cold rolling
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/12Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties
    • C21D8/1244Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of articles with special electromagnetic properties the heat treatment(s) being of interest
    • C21D8/1272Final recrystallisation annealing
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/14Ferrous alloys, e.g. steel alloys containing titanium or zirconium

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electromagnetism (AREA)
  • Manufacturing & Machinery (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing Of Steel Electrode Plates (AREA)

Abstract

The invention discloses a kind of cold rolling non-oriented electrical steel band and preparation method thereof, for molten steel by direct casting and wick-containing pressure at sheet billet, sheet billet is directly entered heating furnace heating and thermal insulation;Again through seven rack continuous rollings at the hot rolled plate of 2.0~2.5mm thickness;Hot rolled plate is by normalizing pickling, single stand cold mill, continuous annealing, coating and the electrical steel strip finished product that 0.5mm thickness is made.Obtained cold rolling non-oriented electrical steel band, magnetic property is excellent, the iron loss P of finished product1.5/50≤ 3.00W/Kg, magnetic strength B5000≥1.68T;And surface of steel plate is met the needs of users without flaws, excellent surface qualities such as striped, corrugation prints.

Description

A kind of cold rolling non-oriented electrical steel band and preparation method thereof
Technical field
The invention belongs to cold rolling non-oriented electrical steel technical field more particularly to a kind of cold rolling non-oriented electrical steel band and its Preparation method.
Background technology
Cold-rolled non-oriented electrical steel is widely used in stator or rotor manufacturing of electric machines.Magnetism of the motor to electric steel plate Energy requirement is very high, while having very strict requirements to steel strip surface quality again.Using continuous casting and rolling technique of sheet bar production electricity When work steel band, when chemical composition is in a certain range, electrical sheet finished product steel belt surface will appear striped, corrugation print defect.With Electrical Steel In China market competition is growing more intense, and produces the cold rolling non-oriented electrical steel finished product steel belt of excellent surface quality just very It is necessary.
Invention content
In order to solve the above technical problems, the present invention provides a kind of cold rolling non-oriented electrical steel band and preparation method thereof, use The ingredient and preparation process for accurately controlling steel are crossed, the cold rolling non-orientation electrician for obtaining a kind of excellent surface quality, having excellent magnetic characteristics Steel band.
The technical solution that the present invention takes is:
A kind of preparation method of cold rolling non-oriented electrical steel band, includes the following steps:
(1) steel plate is casting continuously to form continuous casting billet;
(2) continuous casting billet enters heating furnace heating and thermal insulation;
(3) through seven rack tandem rollings at hot rolled plate;
(4) normalizing pickling;
(5) single stand cold mill;
(6) continuous annealing;
(7) coating, finished product.
The cold rolling non-oriented electrical steel band includes following chemical composition and weight percent:C≤0.005%, 1.5%≤ Si≤2.5%, 0.1%≤Mn≤0.5%, P≤0.04%, 0.1%≤Als≤0.4%, S≤0.007%, N≤0.005%, Ti≤0.006%, remaining is Fe and inevitable impurity.
Further, it is preferable to which it includes following chemical composition and weight percent to be::C0.0034≤C≤0.0046%, 1.7%≤Si≤2.1%, 0.2%≤Mn≤0.3%, P≤0.04%, 0.19%≤Als≤0.27%, S≤0.005%, N ≤ 0.004%, 0.003%≤Ti≤0.006%, remaining is Fe and inevitable impurity.
In the step (2), 1100~1300 DEG C of the heating temperature of heating furnace, soaking time is 0.5~1.5h.Further Ground, preferably, 1198~1252 DEG C of heating temperature, 0.8~1h of soaking time.
In the step (3), the finishing temperature of hot rolling is at 850~950 DEG C, and coiling temperature is at 650~750 DEG C.Further Ground, preferably, the finishing temperature of hot rolling is at 858~882 DEG C, and coiling temperature is at 667~693 DEG C
It in the step (4), is carried out on normalizing pickling normalizing line, normalizing temperature is 870~920 DEG C, pickling temperature 70 ~90 DEG C.Further, normalizing temperature is preferably 876~903 DEG C, and pickling temperature is preferably 78~86 DEG C.
In the step (5), single stand cold mill carries out on 6 roll reversing rollers, 5~6 passes.
In the step (6), continuous annealing carries out in continuous annealing furnace, and annealing temperature is 750~900 DEG C, when heat preservation Between be 1~3min, nitrogen hydrogen mixeding gas protection, hydrogen content percentage by volume in 20~30%, stove dew point control 20~ 30℃.Further, annealing temperature is preferably 848~862 DEG C.
The continuous casting billet, cold-reduced sheet thickness be respectively 2.0~2.5mm, 0.5mm.
The present invention is by accurately controlling the ingredient and processing parameter of electrical steel strip, obtained cold rolling non-oriented electrical steel Band, magnetic property is excellent, the iron loss P of finished product1.5/50≤ 3.00W/Kg, magnetic strength B5000≥1.68T;And surface of steel plate without striped, watt Flaws, the excellent surface qualities such as stupefied print are met the needs of users.
Specific implementation mode
The following describes the present invention in detail with reference to examples.
Embodiment 1
A kind of cold rolling non-oriented electrical steel band, chemical component weight percentage C:0.0045, Si:1.80 Mn:0.3, P:0.03, Als:0.20, S:0.0040, N:0.0030, Ti:0.0030, remaining is Fe and inevitable impurity.
The preparation method of the cold rolling non-oriented electrical steel band is:Molten steel direct casting and wick-containing pressure are at thickness 65mm's Sheet billet, sheet billet are directly entered heating furnace heating and thermal insulation, and the temperature of heating furnace is at 1200 DEG C, heating time 1h;Again through seven Rack continuous rolling at 2.2mm thickness hot rolled plate;Hot rolled plate by normalizing pickling, single stand cold mill, continuous annealing, coating and The electrical steel strip finished product of 0.5mm thickness is made.
The finishing temperature of hot rolling is 880 DEG C, and coiling temperature is 690 DEG C;Normalizing temperature is 880 DEG C, and chlorohydric acid pickling temperature is 80℃;5 passage of single stand cold mill is rolled to 0.5mm thickness;Continuous annealing carries out in continuous annealing furnace, and continuous annealing temperature is 860 DEG C, soaking time 1.5min, nitrogen hydrogen mixeding gas protection, hydrogen content percentage by volume dew point control in 30%, stove exists 30℃。
The cold rolling non-oriented electrical steel belt surface manufactured through above-mentioned technique does not have the flaws such as striped, corrugation print, surface quality It is excellent, the iron loss P of finished product1.5/50For 2.80W/Kg, magnetic strength B5000For 1.70T, magnetic property is excellent.
Embodiment 2
A kind of cold rolling non-oriented electrical steel band, chemical component weight percentage C:0.0035, Si:2.20 Mn:0.2, P:0.04, Als:0.25, S:0.0050, N:0.0040, Ti:0.0060, remaining is Fe and inevitable impurity.
The preparation method of the cold rolling non-oriented electrical steel band is:Molten steel direct casting and wick-containing pressure are at thickness 55mm's Sheet billet, sheet billet are directly entered heating furnace heating and thermal insulation, and the temperature of heating furnace is at 1250 DEG C, heating time 0.8h;It passes through again Seven rack continuous rollings at 2.5mm thickness hot rolled plate;Hot rolled plate is by normalizing pickling, single stand cold mill, continuous annealing, coating And the electrical steel strip finished product of 0.5mm thickness is made.
The finishing temperature of hot rolling is 860 DEG C, and coiling temperature is 670 DEG C;Normalizing temperature is 900 DEG C, and chlorohydric acid pickling temperature is 85℃;6 passage of single stand cold mill is rolled to 0.5mm thickness;Continuous annealing carries out in continuous annealing furnace, and continuous annealing temperature is 850 DEG C, soaking time 1.5min, nitrogen hydrogen mixeding gas protection, hydrogen content percentage by volume dew point control in 25%, stove exists 25℃。
The cold rolling non-oriented electrical steel belt surface manufactured through above-mentioned technique does not have the flaws such as striped, corrugation print, surface quality It is excellent, the iron loss P of finished product1.5/50For 2.65W/Kg, magnetic strength B5000For 1.69T, magnetic property is excellent.
The above-mentioned detailed description carried out to a kind of cold rolling non-oriented electrical steel band and preparation method thereof with reference to embodiment, is to say Bright property without being restrictive, several embodiments can be enumerated according to limited range, therefore of the invention total not departing from Change and modification under body design, should belong within protection scope of the present invention.

Claims (10)

1. a kind of preparation method of cold rolling non-oriented electrical steel band, which is characterized in that include the following steps:
(1) steel plate is casting continuously to form continuous casting billet;
(2) continuous casting billet enters heating furnace heating and thermal insulation;
(3) through seven rack tandem rollings at hot rolled plate;
(4) normalizing pickling;
(5) single stand cold mill;
(6) continuous annealing;
(7) coating, finished product.
2. preparation method according to claim 1, which is characterized in that the cold rolling non-oriented electrical steel band includes followingization It studies point and weight percent:C≤0.005%, 1.5%≤Si≤2.5%, 0.1%≤Mn≤0.5%, P≤0.04%, 0.1%≤Als≤0.4%, S≤0.007%, N≤0.005%, Ti≤0.006%, remaining is Fe and inevitable impurity.
3. preparation method according to claim 1, which is characterized in that including following chemical composition and weight percent: C0.0034≤C≤0.0046%, 1.7%≤Si≤2.3%, 0.2%≤Mn≤0.3%, P≤0.04%, 0.19%≤Als ≤ 0.27%, S≤0.005%, N≤0.004%, 0.003%≤Ti≤0.006%, remaining is Fe and inevitable impurity.
4. preparation method according to claim 1, which is characterized in that in the step (2), the heating temperature of heating furnace 1100~1300 DEG C, soaking time is 0.5~1.5h.
5. preparation method according to claim 1, which is characterized in that in the step (3), the finishing temperature of hot rolling exists 850~950 DEG C, coiling temperature is at 650~750 DEG C.
6. according to the preparation method described in claim 1-3 any one, which is characterized in that in the step (4), normalizing pickling It is carried out on normalizing line, normalizing temperature is 870~920 DEG C, and pickling temperature is 70~90 DEG C.
7. according to the preparation method described in claim 1-3 any one, which is characterized in that in the step (5), single chassis is cold It rolls and is carried out on 6 roll reversing rollers, 5~6 passes.
8. according to the preparation method described in claim 1-3 any one, which is characterized in that in the step (6), continuous annealing It is carried out in continuous annealing furnace, annealing temperature is 750~900 DEG C, and soaking time is 1~3min, nitrogen hydrogen mixeding gas protection, hydrogen Gas content percentage by volume dew point in 20~30%, stove is controlled at 20~30 DEG C.
9. according to the preparation method described in claim 1-3 any one, which is characterized in that the continuous casting billet, cold-reduced sheet thickness Degree is respectively 2.0~2.5mm, 0.5mm.
10. the cold rolling non-oriented electrical steel band that preparation method according to claim 1 is prepared, which is characterized in that institute State the iron loss P of cold rolling non-oriented electrical steel band1.5/50≤ 3.00W/Kg, magnetic strength B5000≥1.68T。
CN201810472997.9A 2018-05-17 2018-05-17 A kind of cold rolling non-oriented electrical steel band and preparation method thereof Pending CN108517395A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109822070A (en) * 2018-12-28 2019-05-31 日照钢铁控股集团有限公司 A kind of full endless rolling electric drive non-oriented electrical steel of sheet billet and preparation method
CN110106447A (en) * 2019-04-28 2019-08-09 首钢智新迁安电磁材料有限公司 A kind of high-magnetic strength non-oriented electrical steel and preparation method thereof
CN111235462A (en) * 2020-03-04 2020-06-05 马鞍山钢铁股份有限公司 Easy-blanking electrical steel for high-efficiency fixed-frequency compressor, manufacturing method of easy-blanking electrical steel, iron core prepared from easy-blanking electrical steel and heat treatment method of iron core
CN111245176A (en) * 2020-03-04 2020-06-05 马鞍山钢铁股份有限公司 Production process of cast aluminum iron core for reducing stray loss of compressor
CN112030059A (en) * 2020-08-31 2020-12-04 武汉钢铁有限公司 Short-process production method of non-oriented silicon steel
CN112063819A (en) * 2020-09-11 2020-12-11 马鞍山钢铁股份有限公司 High-yield-ratio non-oriented silicon steel and manufacturing method thereof
CN112159927A (en) * 2020-09-17 2021-01-01 马鞍山钢铁股份有限公司 Cold-rolled non-oriented silicon steel with different yield ratios and production methods of two products thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103614615A (en) * 2013-09-24 2014-03-05 马钢(集团)控股有限公司 Low cost cold rolling non-oriented electrical steel production method
CN104789860A (en) * 2015-05-07 2015-07-22 马钢(集团)控股有限公司 Electrical steel and production method thereof
CN106756522A (en) * 2017-03-21 2017-05-31 马钢(集团)控股有限公司 The low iron loss of one kind production, high-magnetic strength non-oriented electrical steel and its manufacture method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103614615A (en) * 2013-09-24 2014-03-05 马钢(集团)控股有限公司 Low cost cold rolling non-oriented electrical steel production method
CN104789860A (en) * 2015-05-07 2015-07-22 马钢(集团)控股有限公司 Electrical steel and production method thereof
CN106756522A (en) * 2017-03-21 2017-05-31 马钢(集团)控股有限公司 The low iron loss of one kind production, high-magnetic strength non-oriented electrical steel and its manufacture method

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109822070A (en) * 2018-12-28 2019-05-31 日照钢铁控股集团有限公司 A kind of full endless rolling electric drive non-oriented electrical steel of sheet billet and preparation method
CN110106447A (en) * 2019-04-28 2019-08-09 首钢智新迁安电磁材料有限公司 A kind of high-magnetic strength non-oriented electrical steel and preparation method thereof
CN111235462A (en) * 2020-03-04 2020-06-05 马鞍山钢铁股份有限公司 Easy-blanking electrical steel for high-efficiency fixed-frequency compressor, manufacturing method of easy-blanking electrical steel, iron core prepared from easy-blanking electrical steel and heat treatment method of iron core
CN111245176A (en) * 2020-03-04 2020-06-05 马鞍山钢铁股份有限公司 Production process of cast aluminum iron core for reducing stray loss of compressor
CN111235462B (en) * 2020-03-04 2021-12-24 马鞍山钢铁股份有限公司 Easy-blanking electrical steel for high-efficiency fixed-frequency compressor, manufacturing method of easy-blanking electrical steel, iron core prepared from easy-blanking electrical steel and heat treatment method of iron core
CN112030059A (en) * 2020-08-31 2020-12-04 武汉钢铁有限公司 Short-process production method of non-oriented silicon steel
CN112030059B (en) * 2020-08-31 2021-08-03 武汉钢铁有限公司 Short-process production method of non-oriented silicon steel
CN112063819A (en) * 2020-09-11 2020-12-11 马鞍山钢铁股份有限公司 High-yield-ratio non-oriented silicon steel and manufacturing method thereof
CN112159927A (en) * 2020-09-17 2021-01-01 马鞍山钢铁股份有限公司 Cold-rolled non-oriented silicon steel with different yield ratios and production methods of two products thereof

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Application publication date: 20180911