CN108504466A - A kind of liquid detergent and preparation method - Google Patents
A kind of liquid detergent and preparation method Download PDFInfo
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- CN108504466A CN108504466A CN201810304067.2A CN201810304067A CN108504466A CN 108504466 A CN108504466 A CN 108504466A CN 201810304067 A CN201810304067 A CN 201810304067A CN 108504466 A CN108504466 A CN 108504466A
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- holding tray
- liquid detergent
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-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/0005—Other compounding ingredients characterised by their effect
- C11D3/0021—Dye-stain or dye-transfer inhibiting compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/1206—Water-insoluble compounds free metals, e.g. aluminium grit or flakes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
- C11D3/3773—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines in liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/667—Neutral esters, e.g. sorbitan esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Molecular Biology (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of liquid detergents, include the raw material of following parts by weight meter：30 40 parts of polyoxyethylated alkyl alcohols, 28 33 parts of stearic amides, 15 20 parts of fatty glycerides, 20 28 parts of stearic acid, 15 18 parts of polyacrylamides, 10 16 parts of glycerols, 25 30 parts of sodium xylene sulfonates, 25 30 parts of sodium carboxymethylcelluloses, 18 27 parts of triethanolamines, 16 25 parts of carboxymethyl celluloses, 16 20 parts of neopelexes, 20 29 parts of moso bamboo hemp extracts, 15 18 parts of sodium tripolyphosphates, 14 18 parts of fragrance, 18 28 parts of citric acids and 13 16 parts of nano-Ag particles；The liquid detergent process of preparing of the present invention is simply easily operated, and the liquid detergent being prepared has good effect of color protection, and has disinfection function.
Description
Technical field
The present invention relates to a kind of liquid detergent fields, and in particular to a kind of liquid detergent with color protection and disinfection function with
And preparation method.
Background technology
For clothing in washing process, dyestuff or other color dirts can lead to clothing from dye is returned in aqueous solution again to clothing
The profile of upper decorative pattern is unintelligible, and three-dimensional sense is not strong, and the background of blue, gloomy appearance occurs in clothing, and this phenomenon is known as colour contamination,
The appearance for influencing clothing, reduces the use value of clothing.Therefore, it is badly in need of a kind of washing with colour-preserving function currently on the market
Clothing liquid.
Invention content
It is an object of the present invention to provide a kind of liquid detergent and preparation methods, not only have colour-preserving function, also have
Disinfection function.
In order to realize these purposes and other advantages according to the present invention, a kind of liquid detergent, including following weight are provided
The raw material of part meter：
30-40 parts of polyoxyethylated alkyl alcohols, 28-33 parts of stearic amides, 15-20 parts of fatty glycerides, 20-28 parts
Stearic acid, 15-18 part polyacrylamide, 10-16 parts of glycerols, 25-30 parts of sodium xylene sulfonates, 25-30 parts of carboxymethyls
Sodium cellulosate, 18-27 part triethanolamine, 16-25 parts of carboxymethyl celluloses, 16-20 parts of neopelexes, 20-29 parts
Moso bamboo hemp extract, 15-18 part sodium tripolyphosphate, 14-18 parts of fragrance, 18-28 parts of citric acids and 13-16 parts of nano silvers
Grain.
The preparation method of the liquid detergent, includes the following steps：
Step 1: taking 30-34 parts of polyoxyethylated alkyl alcohols, 28-33 parts of stearic amides, 15-20 parts of fat by weight
Fatty acid glyceride, 20-28 part stearic acid, 15-18 parts of polyacrylamides and 10-16 parts of glycerols are mixed, 35 DEG C
Heating water bath obtains the first mixture；
Step 2: taking 25-30 parts of sodium xylene sulfonates, 25-30 parts of sodium carboxymethylcelluloses, 18-27 parts three by weight
Ethanol amine, 16-25 part carboxymethyl cellulose and 30-35 parts of pure water are mixed, and it is mixed to be slowly added to described first thereto
Object is closed, ultrasound environments 20min is placed in, obtains the second mixture；
Step 3: 16-20 parts of neopelexes, 20-29 portions of moso bamboos are added by weight into the second mixture
Hemp extract, 15-18 part sodium tripolyphosphate and 38-40 parts of pure water are mixed, ultrasonic vibration 30min, and in ultrasonic mistake
Journey is gradually slowly added to 14-18 parts of fragrance, 18-28 parts of citric acids and 13-16 parts of nano-Ag particles, 1200r/min thereto
Quickly stirring 2h, obtains the liquid detergent；
The extraction process of the moso bamboo hemp extract is：
Step A, it provides one and beats device comprising：
Container, cylindrical, inner wall both sides are symmetrically vertically arranged a sliding slot；The container bottom opens up liquid outlet；
Holding tray, arc-shaped, level is built in the container, and both sides are slidably fastened on two by lug respectively
Between a sliding slot, realize that the holding tray is slided up and down along two sliding slots；The holding tray is by stainless steel material
It is made, surface is covered with filter opening；When the holding tray slides to the least significant end of the sliding slot, the bottom of holding tray and the container
Bottom is in direct contact；
Multiple springs are annularly distributed in the container, and below the holding tray；Each spring one end
It is fixed on container bottom, the other end is fixed on position of the placement pan bottom close to edge；
Stick is beaten, is pumped along the short transverse of the container under motor driving；It is described to beat stick packet
It includes and circular beat plate and be vertically installed in multiple cylindrical-shaped structures on its surface, wherein beaten along radially away from described
The height in the direction at plate center, cylindrical-shaped structure gradually reduces；Multiple arc-shaped protrusions, packet is arranged in each cylindrical-shaped structure surface
It includes centrally located first protrusion and is looped around surrounding multiple second protrusions；Under the side wall of each cylindrical-shaped structure
End ring is saturated with the sponge of absolute ethyl alcohol around attaching one；
By weight 1:1 takes Moso Bamboo Leaves and sisal hemp, and be uniformly staggeredly placed in it is described beat in the holding tray of device, beat
30min must beat slurries, remove solid fiber slag, obtain liquid fiber slag, and polyvinylpyrrolidone is ground thereto, and removal is solid
Body impurity, obtains lapping liquid；
Step B, the ethyl alcohol in vacuum distillation removal lapping liquid must purify until ethanol content is less than 3% in lapping liquid
Liquid；
Step C, in mass ratio 3:5 are placed in the purification liquid and supercritical carbon dioxide in pressure vessel, adjust initial
Pressure is 7.8MPa, extracts 2h, obtains single extraction liquid；In mass ratio 2:5 by the single extraction liquid and supercritical carbon dioxide
It is placed in pressure vessel, adjusting initial pressure is 6.9MPa, extracts 3h, obtains extraction fluid, i.e., the described moso bamboo hemp extract.
Preferably, the preparation method of the liquid detergent, the sisal hemp are polished its surface using preceding with sand paper.
Preferably, the length of the preparation method of the liquid detergent, first protrusion is more than second protrusion
Length.
Preferably, the preparation method of the liquid detergent, the placement panel surface coat wear-resistant paint layer.
The present invention includes at least following advantageous effect：The liquid detergent process of preparing of the present invention is simply easily operated, tool
There is good colour-preserving function, and since its preparation process is also mixed with the nano-Ag particles with disinfection function, this is washed
Clothing liquid has good disinfection effect.
Part is illustrated to embody by further advantage, target and the feature of the present invention by following, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Description of the drawings
Fig. 1 is the structural schematic diagram for beating device of the present invention.
Specific implementation mode
Present invention will be described in further detail below with reference to the accompanying drawings, to enable those skilled in the art with reference to specification text
Word can be implemented according to this.
Embodiment 1
A kind of preparation method of liquid detergent, includes the following steps：
Step 1: taking 30 parts of polyoxyethylated alkyl alcohols, 28 parts of stearic amides, 15 parts of fatty acid glycerines by weight
Ester, 20 parts of stearic acid, 15 parts of polyacrylamides and 10 parts of glycerols are mixed, and it is mixed to obtain first for 35 DEG C of heating water baths
Close object；
Step 2: taking 25 parts of sodium xylene sulfonates, 25 parts of sodium carboxymethylcelluloses, 18 parts of triethanolamines, 16 by weight
Part carboxymethyl cellulose and 30 parts of pure water are mixed, and are slowly added to first mixture thereto, are placed in ultrasonic ring
Border 20min obtains the second mixture；
Step 3: 16 parts of neopelexes are added by weight into the second mixture, 20 parts of moso bamboo sisal hemps carry
Take object, 15 parts of sodium tripolyphosphates and 38 parts of pure water to be mixed, ultrasonic vibration 30min, and ultrasonic procedure thereto gradually
It is slowly added to 14 parts of fragrance, 18 parts of citric acids and 13 parts of nano-Ag particles, 1200r/min and quickly stirs 2h, obtain the laundry
Liquid；
The extraction process of the moso bamboo hemp extract is：
Step A, it provides one and beats device；
By weight 1:1 takes Moso Bamboo Leaves and sisal hemp, and is placed in order in the holding tray for beating device, beats 30min, obtains
Slurries are beaten, solid fiber slag is removed, obtains liquid fiber slag, polyvinylpyrrolidone is ground thereto, is removed solid impurity, is obtained
Lapping liquid；
Step B, the ethyl alcohol in vacuum distillation removal lapping liquid must purify until ethanol content is less than 3% in lapping liquid
Liquid；
Step C, in mass ratio 3:5 are placed in the purification liquid and supercritical carbon dioxide in pressure vessel, adjust initial
Pressure is 7.8MPa, extracts 2h, obtains single extraction liquid；In mass ratio 2:5 by the single extraction liquid and supercritical carbon dioxide
It is placed in pressure vessel, adjusting initial pressure is 6.9MPa, extracts 3h, obtains extraction fluid, i.e., the described moso bamboo hemp extract.
Embodiment 2
A kind of preparation method of liquid detergent, includes the following steps：
Step 1: taking 32 parts of polyoxyethylated alkyl alcohols, 29 parts of stearic amides, 17 parts of fatty acid glycerines by weight
Ester, 25 parts of stearic acid, 16 parts of polyacrylamides and 13 parts of glycerols are mixed, and it is mixed to obtain first for 35 DEG C of heating water baths
Close object；
Step 2: taking 27 parts of sodium xylene sulfonates, 28 parts of sodium carboxymethylcelluloses, 23 parts of triethanolamines, 22 by weight
Part carboxymethyl cellulose and 32 parts of pure water are mixed, and are slowly added to first mixture thereto, are placed in ultrasonic ring
Border 20min obtains the second mixture；
Step 3: 18 parts of neopelexes are added by weight into the second mixture, 25 parts of moso bamboo sisal hemps carry
Take object, 16 parts of sodium tripolyphosphates and 39 parts of pure water to be mixed, ultrasonic vibration 30min, and ultrasonic procedure thereto gradually
It is slowly added to 17 parts of fragrance, 19 parts of citric acids and 15 parts of nano-Ag particles, 1200r/min and quickly stirs 2h, obtain the laundry
Liquid；
The extraction process of the moso bamboo hemp extract is：
Step A, it provides one and beats device；
By weight 1:1 takes Moso Bamboo Leaves and sisal hemp, and is placed in order in the holding tray for beating device, beats 30min, obtains
Slurries are beaten, solid fiber slag is removed, obtains liquid fiber slag, polyvinylpyrrolidone is ground thereto, is removed solid impurity, is obtained
Lapping liquid；
Step B, the ethyl alcohol in vacuum distillation removal lapping liquid must purify until ethanol content is less than 3% in lapping liquid
Liquid；
Step C, in mass ratio 3:5 are placed in the purification liquid and supercritical carbon dioxide in pressure vessel, adjust initial
Pressure is 7.8MPa, extracts 2h, obtains single extraction liquid；In mass ratio 2:5 by the single extraction liquid and supercritical carbon dioxide
It is placed in pressure vessel, adjusting initial pressure is 6.9MPa, extracts 3h, obtains extraction fluid, i.e., the described moso bamboo hemp extract.
Embodiment 3
A kind of preparation method of liquid detergent, includes the following steps：
Step 1: taking 34 parts of polyoxyethylated alkyl alcohols, 33 parts of stearic amides, 20 parts of fatty acid glycerines by weight
Ester, 28 parts of stearic acid, 18 parts of polyacrylamides and 16 parts of glycerols are mixed, and it is mixed to obtain first for 35 DEG C of heating water baths
Close object；
Step 2: taking 30 parts of sodium xylene sulfonates, 30 parts of sodium carboxymethylcelluloses, 27 parts of triethanolamines, 25 by weight
Part carboxymethyl cellulose and 35 parts of pure water are mixed, and are slowly added to first mixture thereto, are placed in ultrasonic ring
Border 20min obtains the second mixture；
Step 3: 20 parts of neopelexes are added by weight into the second mixture, 29 parts of moso bamboo sisal hemps carry
Take object, 18 parts of sodium tripolyphosphates and 40 parts of pure water to be mixed, ultrasonic vibration 30min, and ultrasonic procedure thereto gradually
It is slowly added to 18 parts of fragrance, 28 parts of citric acids and 16 parts of nano-Ag particles, 1200r/min and quickly stirs 2h, obtain the laundry
Liquid；
The extraction process of the moso bamboo hemp extract is：
Step A, it provides one and beats device；
By weight 1:1 takes Moso Bamboo Leaves and sisal hemp, and is placed in order in the holding tray for beating device, beats 30min, obtains
Slurries are beaten, solid fiber slag is removed, obtains liquid fiber slag, polyvinylpyrrolidone is ground thereto, is removed solid impurity, is obtained
Lapping liquid；
Step B, the ethyl alcohol in vacuum distillation removal lapping liquid must purify until ethanol content is less than 3% in lapping liquid
Liquid；
Step C, in mass ratio 3:5 are placed in the purification liquid and supercritical carbon dioxide in pressure vessel, adjust initial
Pressure is 7.8MPa, extracts 2h, obtains single extraction liquid；In mass ratio 2:5 by the single extraction liquid and supercritical carbon dioxide
It is placed in pressure vessel, adjusting initial pressure is 6.9MPa, extracts 3h, obtains extraction fluid, i.e., the described moso bamboo hemp extract.
Such as Fig. 1, the invention of this reality also discloses one kind and beating device comprising：
Container 1, cylindrical, inner wall both sides are symmetrically vertically arranged a sliding slot 2；1 bottom of the container opens up liquid outlet
3；Holding tray 4, arc-shaped, level are built in the container 1, and both sides are slidably fastened on two institutes by lug respectively
Between stating sliding slot 2, realize that the holding tray 4 is slided up and down along two sliding slots 2；The holding tray 4 is by stainless steel material
It is made, surface is covered with filter opening；When the holding tray 4 slides to the least significant end of the sliding slot 2, the bottom of holding tray 4 and the appearance
The bottom of device 1 is in direct contact；Multiple springs 5 are annularly distributed in the container 1, and positioned at 4 lower section of the holding tray；Often
1 bottom of container is fixed in a 5 one end of the spring, and the other end is fixed on the position that proximal edge is leaned in 4 bottom of the holding tray；It beats
Stick pumps under the driving of motor 7 along the short transverse of the container 1；The stick of beating includes circular beats
It re-packs and 610 and is vertically installed in multiple cylindrical-shaped structures 620 on its surface, wherein beat plate 610 along radially away from described
The height in the direction at center, cylindrical-shaped structure 620 gradually reduces；It is convex that multiple arc-shapeds are arranged in each 620 surface of cylindrical-shaped structure
Rise 621, including it is centrally located first protrusion and be looped around it is surrounding it is multiple second protrusion；Each cylindrical-shaped structure
Side wall lower ends around attaching a sponge 630 for being saturated with absolute ethyl alcohol；
Moso bamboo hemp extract to be beaten when in use, is placed in tray 4 by this structure first, and the driving of motor 7 is beaten
Stick moves downward, and beats stick to push holding tray 4 to be moved downward along sliding slot 2, until the bottom of holding tray 4 touches container
Bottom, and since multiple talks being arranged between 4 bottom of container bottom and holding tray, during holding tray 4 pushes, holding tray 4
It is moved downward under the driving of motor, but spring will produce reaction force, be squeezed material to beat stick, occur to squeeze
Pressure grinding, squeezes out slurries therein, and the extreme lower position on earth of disk to be placed 4, stops the driving of motor, and spring has at this time
Greatly reaction force, by holding tray moment it is up counter push away, to shake the material on 4 surface of holding tray, keep its material loose,
Motor driving is beaten stick and is moved downward again, repeats the above process, reaches and beat effect well.
In order to prove the effect of the liquid detergent of the invention prepared, following tests is now carried out：
Detergency test
With reference to GB/T13174-2008, the experimental results showed that the liquid detergent sample of embodiment 1-3 is to edible oil soiled cotton, starch
Class soiled cotton, sebum soiled cotton detergency >=1.0, it was demonstrated that it has deoils effect well；
Color protection power is tested
The blackish green clothing of fugitive color is cut into the sample of 20 pieces of 15cm × 15cm, is acted on by identical spot, then
10 pieces of samples are washed respectively with commercial laundry liquid and the liquid detergent of embodiment 2.
Wherein, specially：
1, suitable commercial laundry liquid is taken to carry out washing sample；
2, the liquid detergent of Example 2 carries out washing sample, and dosage is commercial laundry liquid dosage 1/2.
Experimental result：It compares, the washed above-mentioned sample of the liquid detergent made from the present embodiment 2, restores with former clothing
It is original bright and new glossy；And the sample washed with commercial laundry liquid, even if greasiness removal, but gloss color is still not beautiful enough
It is beautiful.This shows that the liquid detergent of the present invention has good effect of color protection, this is because moso bamboo hemp extract therein contains certain
Kind substance, can wrap up the dye molecule in laundry water so that the dye molecule being eluted out is not easy to be adhered to clothing
On, to play good color-protecting function.
Although the embodiments of the present invention have been disclosed as above, but its is not only in the description and the implementation listed
With it can be fully applied to various fields suitable for the present invention, for those skilled in the art, can be easily
Realize other modification, therefore without departing from the general concept defined in the claims and the equivalent scope, the present invention is simultaneously unlimited
In specific details and legend shown and described herein.
Claims (5)
1. a kind of liquid detergent, which is characterized in that include the raw material of following parts by weight meter：
30-40 parts of polyoxyethylated alkyl alcohols, 28-33 parts of stearic amides, 15-20 parts of fatty glycerides, 20-28 parts of tristearin
Acid, 15-18 parts of polyacrylamides, 10-16 parts of glycerols, 25-30 parts of sodium xylene sulfonates, 25-30 parts of carboxymethyl celluloses
Plain sodium, 18-27 part triethanolamine, 16-25 parts of carboxymethyl celluloses, 16-20 parts of neopelexes, 20-29 portions of moso bamboos
Hemp extract, 15-18 part sodium tripolyphosphate, 14-18 parts of fragrance, 18-28 parts of citric acids and 13-16 parts of nano-Ag particles.
2. the preparation method of liquid detergent as described in claim 1, which is characterized in that include the following steps：
Step 1: taking 30-34 parts of polyoxyethylated alkyl alcohols, 28-33 parts of stearic amides, 15-20 parts of aliphatic acid by weight
Glyceride, 20-28 part stearic acid, 15-18 parts of polyacrylamides and 10-16 parts of glycerols are mixed, 35 DEG C of water-baths
Heating, obtains the first mixture；
Step 2: taking 25-30 parts of sodium xylene sulfonates, 25-30 parts of sodium carboxymethylcelluloses, three ethyl alcohol of 18-27 parts by weight
Amine, 16-25 part carboxymethyl cellulose and 30-35 parts of pure water are mixed, and are slowly added to first mixing thereto
Object is placed in ultrasound environments 20min, obtains the second mixture；
Step 3: 16-20 parts of neopelexes, 20-29 parts of moso bamboo sisal hemps are added by weight into the second mixture
Extract, 15-18 part sodium tripolyphosphate and 38-40 parts of pure water are mixed, ultrasonic vibration 30min, and ultrasonic procedure to
It is quick to be wherein gradually slowly added to 14-18 parts of fragrance, 18-28 parts of citric acids and 13-16 parts of nano-Ag particles, 1200r/min
2h is stirred, the liquid detergent is obtained；
The extraction process of the moso bamboo hemp extract is：
Step A, it provides one and beats device comprising：
Container, cylindrical, inner wall both sides are symmetrically vertically arranged a sliding slot；The container bottom opens up liquid outlet；
Holding tray, arc-shaped, level are built in the container, and both sides are slidably fastened on two institutes by lug respectively
Between stating sliding slot, realize that the holding tray is slided up and down along two sliding slots；The holding tray is made of stainless steel material,
Surface is covered with filter opening；When the holding tray slides to the least significant end of the sliding slot, the bottom of the bottom of holding tray and the container
It is in direct contact；
Multiple springs are annularly distributed in the container, and below the holding tray；Each spring one end is fixed
In container bottom, the other end is fixed on position of the placement pan bottom close to edge；
Stick is beaten, is pumped along the short transverse of the container under motor driving；The stick of beating includes circle
Shape beats plate and is vertically installed in multiple cylindrical-shaped structures on its surface, wherein is beaten in plate along radially away from described
The height in the direction of the heart, cylindrical-shaped structure gradually reduces；Multiple arc-shaped protrusions, including position are arranged in each cylindrical-shaped structure surface
In center first protrusion and be looped around it is surrounding it is multiple second protrusion；The side wall lower ends ring of each cylindrical-shaped structure
The sponge of absolute ethyl alcohol is saturated with around attaching one；
By weight 1:1 takes Moso Bamboo Leaves and sisal hemp, and be uniformly staggeredly placed in it is described beat in the holding tray of device, beat 30min,
Slurries must be beaten, solid fiber slag is removed, obtains liquid fiber slag, polyvinylpyrrolidone is ground thereto, removes solid again
Impurity obtains lapping liquid；
Step B, the ethyl alcohol in vacuum distillation removal lapping liquid obtains purification liquid until ethanol content is less than 3% in lapping liquid；
Step C, in mass ratio 3:5 are placed in the purification liquid and supercritical carbon dioxide in pressure vessel, adjust initial pressure
For 7.8MPa, 2h is extracted, single extraction liquid is obtained；In mass ratio 2:5 are placed in the single extraction liquid with supercritical carbon dioxide
In pressure vessel, adjusting initial pressure is 6.9MPa, extracts 3h, obtains extraction fluid, i.e., the described moso bamboo hemp extract.
3. the preparation method of liquid detergent as claimed in claim 2, which is characterized in that the sisal hemp is polished using preceding with sand paper
Its surface.
4. the preparation method of liquid detergent as claimed in claim 2, which is characterized in that the length of first protrusion is more than described
The length of second protrusion.
5. the preparation method of liquid detergent as claimed in claim 2, which is characterized in that the placement panel surface coats wear-resistant paint
Layer.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113430067A (en) * | 2021-06-24 | 2021-09-24 | 佛山菁亮日化用品有限公司 | Antibacterial mite-killing washing gel bead and preparation method thereof |
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Application publication date: 20180907 |