CN108503235A - A kind of fire-resistant fluid of flame resistant glass and its preparation and spraying method - Google Patents
A kind of fire-resistant fluid of flame resistant glass and its preparation and spraying method Download PDFInfo
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- CN108503235A CN108503235A CN201810552555.5A CN201810552555A CN108503235A CN 108503235 A CN108503235 A CN 108503235A CN 201810552555 A CN201810552555 A CN 201810552555A CN 108503235 A CN108503235 A CN 108503235A
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- resistant fluid
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Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/29—Mixtures
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/112—Deposition methods from solutions or suspensions by spraying
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/30—Aspects of methods for coating glass not covered above
- C03C2218/32—After-treatment
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Composite Materials (AREA)
- Fireproofing Substances (AREA)
Abstract
The invention discloses a kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Potassium silicate：0.02-0.10 part, potassium carbonate：10 30 parts, potassium chloride：15 45 parts, cesium chloride：28 parts, sodium tungstate：5 15 parts, deionized water：20 45 parts, antimony oxide：0.02-0.10 part, magnesium hydroxide：0.2-1.0 parts, aluminium hydroxide：0.2-1.0 parts, aluminium dihydrogen phosphate：0.4 1.5 parts, in raw material in addition to deionized water is liquid, other raw materials are solid powder.The fire-resistant fluid has very strong fire prevention effect, fire protecting performance to reach GB15763.1 2009《Safety glass flame resistant glass for building》Fire-protection standard, fire prevention temperature be up to 950 DEG C.Fire-resistant fluid is raw materials used cheap, and preparation process is simple, and odorless, has effects that environmental protection, environmental sound.And the spraying operation of the fire-resistant fluid is simple, and it is easy to use.
Description
Technical field
The present invention relates to a kind of fire-resistant fluid of flame resistant glass and its preparation and spraying methods, belong to fire-resistant fluid technology neck
Domain.
Background technology
Currently, caesium potassium fire-resistant fluid in the market is numerous, but there are expensive, of high cost, some preparation process complexity,
Some is more at being grouped as.Also some fire-resistant fluids have very strong penetrating odor, and prodigious pollution is caused to environment, this
Worker to smearing fire-resistant fluid has a huge impact, and is chronically in this environment and easily causes nausea, and vomiting etc. is bad anti-
It answers.Therefore there is an urgent need for develop a kind of low cost, high quality, the fire-resistant fluid of environmental sound.
Invention content
The object of the present invention is to provide a kind of fire-resistant fluid of flame resistant glass and its preparation and spraying methods.The fire prevention
Liquid has the advantages of low cost, high quality, environmental sound.
Technical scheme of the present invention：A kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Silicon
Sour potassium：0.02-0.10 part, potassium carbonate：10-30 parts, potassium chloride：15-45 parts, cesium chloride：2-8 parts, sodium tungstate：5-15 parts, go
Ionized water：20-45 parts, antimony oxide：0.02-0.10 part, magnesium hydroxide：0.2-1.0 parts, aluminium hydroxide：0.2—1.0
Part, aluminium dihydrogen phosphate：0.4-1.5 parts, in raw material in addition to deionized water is liquid, other raw materials are solid powder.
The fire-resistant fluid of flame resistant glass above-mentioned, with following composition by weight than raw material be made：Potassium silicate：0.04—0.07
Part, potassium carbonate：15-25 parts, potassium chloride：25-35 parts, cesium chloride：4-6 parts, sodium tungstate：8-12 parts, deionized water：28-38 parts,
Antimony oxide：0.04-0.07 part, magnesium hydroxide：0.4-0.6 part, aluminium hydroxide：0.4-0.6 part, aluminium dihydrogen phosphate：
0.7-1.2 parts.
The fire-resistant fluid of flame resistant glass above-mentioned, with following composition by weight than raw material be made：Potassium silicate：0.05 part, carbon
Sour potassium：20 parts, potassium chloride：30 parts, cesium chloride：5 parts, sodium tungstate：10 parts, deionized water：33 parts, antimony oxide：0.05 part,
Magnesium hydroxide：0.5 part, aluminium hydroxide：0.5 part, aluminium dihydrogen phosphate：0.9 part.
A kind of preparation method of the fire-resistant fluid of flame resistant glass above-mentioned, weighs various raw materials, so according to composition by weight ratio
Each raw material is put into blender afterwards after stirring 20-40min to get required fire-resistant fluid.
A kind of spraying method of the fire-resistant fluid of flame resistant glass above-mentioned, includes following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：40-50 square metres is sprayed according to per kilogram fire-resistant fluid to be sprayed, stood after the completion of spraying on original sheet glass
40-80min；
D：Glass is cleaned after the completion of standing and is dried, and tempering is carried out in annealing furnace, you can.
The spraying method of the fire-resistant fluid of flame resistant glass above-mentioned, the original sheet glass selection automobile premium grade glass are former
Piece.
Beneficial effects of the present invention：In order to test the fire-resistant fluid effect of the present invention, spy has done following tests.During experiment
It first the good edging of glass-cutting, then cleans, sprayed fire proofing liquid, then stand two hours, then washes the liquid on surface, then into
Glass is finally put into detection stove and calcines to detect its fire protecting performance by row tempering.As it can be seen from table 1 entire tempering
Process is nearly all held in 900 DEG C or more of high temperature, and the fire prevention time can reach 1 hour or more.
1 flame resistant glass fire protecting performance of table is tested
In terms of comprehensive, compared with prior art, which there is very strong fire prevention effect, fire protecting performance to reach
GB15763.1-2009《Safety glass flame resistant glass for building》Fire-protection standard, fire prevention temperature be up to 950 DEG C.Used in fire-resistant fluid
Raw material is cheap, and preparation process is simple, and odorless, has effects that environmental protection, environmental sound.And the spraying behaviour of the fire-resistant fluid
Make simply, it is easy to use.
Specific implementation mode
With reference to embodiment, the present invention is further illustrated, but is not intended as the foundation limited the present invention.
The embodiment of the present invention 1：A kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Silicon
Sour potassium：0.02kg, potassium carbonate：10kg, potassium chloride：15kg, cesium chloride：2kg, sodium tungstate：5kg, deionized water：20kg, three oxygen
Change two antimony：0.02kg, magnesium hydroxide：0.2kg, aluminium hydroxide：0.2kg, aluminium dihydrogen phosphate：0.4kg removes deionized water in raw material
Outside for liquid, other raw materials are solid powder.
The preparation method of the fire-resistant fluid of the flame resistant glass weighs various raw materials, then by each original according to composition by weight ratio
Material is put into blender after stirring 20min to get required fire-resistant fluid.
The spraying method of the fire-resistant fluid of the flame resistant glass includes following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：40 square metres are sprayed according to per kilogram fire-resistant fluid to be sprayed, stood after the completion of spraying on original sheet glass
40min；
D：Glass is cleaned after the completion of standing and is dried, and is then coated with fire prevention mark, tempering is carried out in annealing furnace, you can.
The original sheet glass selects automobile premium grade original sheet glass, and the original sheet glass intensity is higher, and fire protecting performance is more preferable.
The embodiment of the present invention 2：A kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Silicon
Sour potassium：0.10kg, potassium carbonate：30kg, potassium chloride：45kg, cesium chloride：8kg, sodium tungstate：15kg, deionized water：45kg, three oxygen
Change two antimony：0.10kg, magnesium hydroxide：1.0kg, aluminium hydroxide：1.0kg, aluminium dihydrogen phosphate：1.5kg removes deionized water in raw material
Outside for liquid, other raw materials are solid powder.
The preparation method of the fire-resistant fluid of the flame resistant glass weighs various raw materials, then by each original according to composition by weight ratio
Material is put into blender after stirring 40min to get required fire-resistant fluid.
The spraying method of the fire-resistant fluid of the flame resistant glass includes following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：50 square metres are sprayed according to per kilogram fire-resistant fluid to be sprayed, stood after the completion of spraying on original sheet glass
80min；
D：Glass is cleaned after the completion of standing and is dried, and is then coated with fire prevention mark, tempering is carried out in annealing furnace, you can.
The original sheet glass selects automobile premium grade original sheet glass, and the original sheet glass intensity is higher, and fire protecting performance is more preferable.
The embodiment of the present invention 3：A kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Silicon
Sour potassium：0.04kg, potassium carbonate：15kg, potassium chloride：25kg, cesium chloride：4kg, sodium tungstate：8kg, deionized water：28kg, three oxygen
Change two antimony：0.04kg, magnesium hydroxide：0.4kg, aluminium hydroxide：0.4kg, aluminium dihydrogen phosphate：0.7kg removes deionized water in raw material
Outside for liquid, other raw materials are solid powder.
The preparation method of the fire-resistant fluid of the flame resistant glass weighs various raw materials, then by each original according to composition by weight ratio
Material is put into blender after stirring 25min to get required fire-resistant fluid.
The spraying method of the fire-resistant fluid of the flame resistant glass includes following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：40 square metres are sprayed according to per kilogram fire-resistant fluid to be sprayed, stood after the completion of spraying on original sheet glass
50min；
D：Glass is cleaned after the completion of standing and is dried, and is then coated with fire prevention mark, tempering is carried out in annealing furnace, you can.
The original sheet glass selects automobile premium grade original sheet glass, and the original sheet glass intensity is higher, and fire protecting performance is more preferable.
The embodiment of the present invention 4：A kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Silicon
Sour potassium：0.07kg, potassium carbonate：25kg, potassium chloride：35kg, cesium chloride：6kg, sodium tungstate：12kg, deionized water：38kg, three oxygen
Change two antimony：0.07kg, magnesium hydroxide：0.6kg, aluminium hydroxide：0.6kg, aluminium dihydrogen phosphate：1.2kg removes deionized water in raw material
Outside for liquid, other raw materials are solid powder.
The preparation method of the fire-resistant fluid of the flame resistant glass weighs various raw materials, then by each original according to composition by weight ratio
Material is put into blender after stirring 35min to get required fire-resistant fluid.
The spraying method of the fire-resistant fluid of the flame resistant glass includes following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：50 square metres are sprayed according to per kilogram fire-resistant fluid to be sprayed, stood after the completion of spraying on original sheet glass
70min；
D：Glass is cleaned after the completion of standing and is dried, and is then coated with fire prevention mark, tempering is carried out in annealing furnace, you can.
The original sheet glass selects automobile premium grade original sheet glass, and the original sheet glass intensity is higher, and fire protecting performance is more preferable.
The embodiment of the present invention 5：A kind of fire-resistant fluid of flame resistant glass, with following composition by weight than raw material be made：Silicon
Sour potassium：0.05kg, potassium carbonate：20kg, potassium chloride：30kg, cesium chloride：5kg, sodium tungstate：10kg, deionized water：33kg, three oxygen
Change two antimony：0.05kg, magnesium hydroxide：0.5kg, aluminium hydroxide：0.5kg, aluminium dihydrogen phosphate：0.9kg removes deionized water in raw material
Outside for liquid, other raw materials are solid powder.
The preparation method of the fire-resistant fluid of the flame resistant glass weighs various raw materials, then by each original according to composition by weight ratio
Material is put into blender after stirring 30min to get required fire-resistant fluid.
The spraying method of the fire-resistant fluid of the flame resistant glass includes following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：45 square metres are sprayed according to per kilogram fire-resistant fluid to be sprayed, stood after the completion of spraying on original sheet glass
60min；
D：Glass is cleaned after the completion of standing and is dried, and is then coated with fire prevention mark, tempering is carried out in annealing furnace, you can.
The original sheet glass selects automobile premium grade original sheet glass, and the original sheet glass intensity is higher, and fire protecting performance is more preferable.
Claims (6)
1. a kind of fire-resistant fluid of flame resistant glass, it is characterised in that：With following composition by weight than raw material be made：Potassium silicate：
0.02-0.10 part, potassium carbonate：10-30 parts, potassium chloride：15-45 parts, cesium chloride：2-8 parts, sodium tungstate：5-15 parts, deionization
Water：20-45 parts, antimony oxide：0.02-0.10 part, magnesium hydroxide：0.2-1.0 parts, aluminium hydroxide：0.2-1.0 parts, phosphorus
Acid dihydride aluminium：0.4-1.5 parts, in raw material in addition to deionized water is liquid, other raw materials are solid powder.
2. the fire-resistant fluid of flame resistant glass according to claim 1, it is characterised in that：With following composition by weight than raw material
It is made：Potassium silicate：0.04-0.07 part, potassium carbonate：15-25 parts, potassium chloride：25-35 parts, cesium chloride：4-6 parts, sodium tungstate：8-
12 parts, deionized water：28-38 parts, antimony oxide：0.04-0.07 part, magnesium hydroxide：0.4-0.6 part, aluminium hydroxide：
0.4-0.6 part, aluminium dihydrogen phosphate：0.7-1.2 parts.
3. the fire-resistant fluid of flame resistant glass according to claim 1, it is characterised in that：With following composition by weight than raw material
It is made：Potassium silicate：0.05 part, potassium carbonate：20 parts, potassium chloride：30 parts, cesium chloride：5 parts, sodium tungstate：10 parts, deionized water：33
Part, antimony oxide：0.05 part, magnesium hydroxide：0.5 part, aluminium hydroxide：0.5 part, aluminium dihydrogen phosphate：0.9 part.
4. a kind of preparation method of the fire-resistant fluid of flame resistant glass as described in any one of claim 1-3, feature exist
In：Various raw materials are weighed according to composition by weight ratio, then each raw material are put into blender after stirring 20-40min to get required
Fire-resistant fluid.
5. a kind of spraying method of the fire-resistant fluid of flame resistant glass as described in any one of claim 1-3, feature exist
In：Include following steps：
A：Original sheet glass is selected, is cut as required, four sides are refined；
B：It is dried after original sheet glass is cleaned；
C：40-50 square metres is sprayed according to per kilogram fire-resistant fluid to be sprayed, 40- is stood after the completion of spraying on original sheet glass
80min；
D：Glass is cleaned after the completion of standing and is dried, and tempering is carried out in annealing furnace, you can.
6. the spraying method of the fire-resistant fluid of flame resistant glass according to claim 5, it is characterised in that：The original sheet glass
Select automobile premium grade original sheet glass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810552555.5A CN108503235A (en) | 2018-05-31 | 2018-05-31 | A kind of fire-resistant fluid of flame resistant glass and its preparation and spraying method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810552555.5A CN108503235A (en) | 2018-05-31 | 2018-05-31 | A kind of fire-resistant fluid of flame resistant glass and its preparation and spraying method |
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| Publication Number | Publication Date |
|---|---|
| CN108503235A true CN108503235A (en) | 2018-09-07 |
Family
ID=63402490
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810552555.5A Pending CN108503235A (en) | 2018-05-31 | 2018-05-31 | A kind of fire-resistant fluid of flame resistant glass and its preparation and spraying method |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113352730A (en) * | 2021-04-25 | 2021-09-07 | 陈练旭 | Processing method of super-thick SGP laminated glass |
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2018
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113352730A (en) * | 2021-04-25 | 2021-09-07 | 陈练旭 | Processing method of super-thick SGP laminated glass |
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Application publication date: 20180907 |