CN108498352A - Including inorganic alkaline powder without anti-corrosion astringent composition and preparation method - Google Patents
Including inorganic alkaline powder without anti-corrosion astringent composition and preparation method Download PDFInfo
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- CN108498352A CN108498352A CN201810475054.1A CN201810475054A CN108498352A CN 108498352 A CN108498352 A CN 108498352A CN 201810475054 A CN201810475054 A CN 201810475054A CN 108498352 A CN108498352 A CN 108498352A
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- powder
- inorganic alkaline
- corrosion
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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Abstract
The invention discloses a kind of comprising inorganic alkaline powder without anti-corrosion astringent composition and preparation method, and composition includes by mass percentage：0.01~50% moisturizer, 0.01~30% inorganic alkaline powder and 20~90% deionized water.The composition has good antibacterial bacteriostatic effect, without adding preservative, while having moisturizing, antiallergic and itching-relieving efficacies.
Description
Technical field
It a kind of not adding the present invention relates to cosmetic technical field more particularly to preservative and for skin surface includes
Inorganic alkaline powder without anti-corrosion astringent composition and preparation method.
Background technology
Since the caused by cosmetics for special use use such as present various whitening spot-removings is more and more frequently and popular, illegally add
Phenomenon remains incessant after repeated prohibition, and many crowds is caused various skin problems, if keratoderma is thinning, skin sensitivity etc. occur.In addition
The problem of environmental pollution, is increasingly severe, has aggravated the abnormal response of sensitive skin, and many consumers have to seek hospital
Treatment can just make moderate progress.
Commercially available most cosmetics all add different types of preservative, are much only added not in anti-corrosion without corrosion-resistant concept
The substance for having antisepsis of agent catalogue, the cosmetics for not adding preservative substance really are extremely a small number of.Preservative itself has latent
Or apparent irritation, the irritation being much formulated just come from preservative.For sensitive skin, no anti-corrosion addition is first
The considerations of wanting.
The commercially available cosmetics for sensitive skin, repaired with antiallergic based on, add many plant extracts or biofermentation
Raw material, these raw materials chemical composition itself is not clear enough, and there are the possibility of specified risk material.And ingredient is more complicated, more may
It will be a fashion trend to bring stimulation, simple formula combination.
Invention content
In order to solve the problems, such as the nursing of sensitive and impaired skin and repair, it is an object of the present invention to provide one kind to include
Inorganic alkaline powder without anti-corrosion astringent composition, can effectively repair problem skin, be free of preservative, it is safe and non-stimulating.This
It invents another purpose and is to provide a kind of preparation method without anti-corrosion astringent composition including inorganic alkaline powder.
To achieve the above object, the present invention provide it is a kind of comprising inorganic alkaline powder without anti-corrosion astringent composition, institute
It includes component below to state composition by mass percentage：
0.01~50% moisturizer；
0.01~30% inorganic alkaline powder；
20~90% deionized water.
As a further improvement on the present invention, the composition includes component below by mass percentage：
1~50% moisturizer；
1~30% inorganic alkaline powder；
20~90% deionized water.
As a further improvement on the present invention, the composition includes component below by mass percentage：
2~50% moisturizer；
1~30% inorganic alkaline powder；
20~90% deionized water.
As a further improvement on the present invention, the moisturizer includes propylene glycol, sorbierite, butanediol, pungent glycol, methyl
Propylene glycol, dipropylene glycol, glycerine, diglycerol, glycerin polyether, pentanediol, isoprene, polyethylene glycol, Sodium Hyaluronate, poly- paddy
It is one or more in propylhomoserin sodium；The inorganic alkaline powder includes bioactivity unorganic glass powder, bioactivity inorganic ceramic
It is one or more in powder, oyster shell whiting, pearl powder, nanometer hydroxyapatite powder.
As a further improvement on the present invention, the moisturizer selects glycerine and/or isoprene, the inorganic alkaline powder
Bioactivity unorganic glass powder and/or oyster shell whiting are selected in end.
As a further improvement on the present invention, the composition further includes essence and pigment, is not required to add in the composition
Add any preservative.
As a further improvement on the present invention, the composition includes component below by mass percentage：
2~30% glycerine；
1~20% dipropylene glycol；
1~10% bioactivity unorganic glass powder；
0~0.05% essence；
40~90% deionized water.
As a further improvement on the present invention, the composition includes component below by mass percentage：
2~10% glycerine；
1~10% isoprene；
1~10% oyster shell whiting；
70~90% deionized water.
As a further improvement on the present invention, the composition includes component below by mass percentage：
2~10% glycerine；
1~10% butanediol；
0~10% bioactivity unorganic glass powder；
0~10% oyster shell whiting；
0~0.05% essence；
60~90% deionized water；
It is not 0 and bioactivity unorganic glass powder and shellfish that the bioactivity unorganic glass powder and oyster shell whiting are at least a kind of
The total content of shell powder is more than 0.01%.
The present invention also provides a kind of preparation method without anti-corrosion astringent composition including inorganic alkaline powder, the systems
Preparation Method includes the following steps：
Step 1 weighs glycerine, isoprene, oyster shell whiting and deionized water, and deionized water is heated to 90~95 DEG C, is protected
Temperature 15 minutes, be then cooled to 45 DEG C it is spare；
Glycerine, isoprene and oyster shell whiting is added to the deionized water after cooling in step 2, discharges after stirring；
Step 3, storage, the inspection of semifinished product, filling, product inspection and storage.
Compared with prior art, beneficial effects of the present invention are：
Composition disclosed by the invention have good antibacterial bacteriostatic effect, without adding preservative, at the same have moisturizing,
Antiallergic and itching-relieving efficacies.
Specific implementation mode
In order to make the object, technical scheme and advantages of the embodiment of the invention clearer, below in conjunction with the embodiment of the present invention
Technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described embodiment is the one of the present invention
Section Example, instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not doing
The every other embodiment obtained under the premise of going out creative work, shall fall within the protection scope of the present invention.
The present invention is described in further detail below：
The present invention provide it is a kind of comprising inorganic alkaline powder without anti-corrosion astringent composition, composition is by mass percentage
Meter includes component below：
0.01~50% moisturizer；
0.01~30% inorganic alkaline powder；
20~90% deionized water.
Preferably, composition includes component below by mass percentage：
1~50% moisturizer；
1~30% inorganic alkaline powder；
20~90% deionized water.
As further preferred, composition includes component below by mass percentage：
2~50% moisturizer；
1~30% inorganic alkaline powder；
20~90% deionized water.
Preferably, in the present invention by percentage to the quality about 0.01% to 50% moisturizer be mainly polyalcohol,
Moisturizer includes that propylene glycol, sorbierite, butanediol, pungent glycol, methyl propanediol, dipropylene glycol, glycerine, diglycerol, glycerine are poly-
It is one or more in ether, pentanediol, isoprene, polyethylene glycol, Sodium Hyaluronate, polyglutamic acid sodium, it is preferred for this group
Close object is propylene glycol and/or butanediol, and be preferred for this composition is glycerine and/or isoprene.
Preferably, inorganic alkaline powder includes bioactivity unorganic glass powder, bioactivity inorganic ceramic powder, shell
One or more in powder, pearl powder, nanometer hydroxyapatite powder, be preferable over this combination is bioactivity unorganic glass powder
And/or oyster shell whiting；Wherein：
Bioactivity unorganic glass powder is SiO2、CaO、Na2The mixture of O and MgO etc. has extremely strong absorption and filling
Effect has the effect of promoting Wound healing.Bioactivity unorganic glass powder is the silicate glass material of special construction, general logical
It crosses fusion method or sol-gel method is made.
Bioactivity inorganic ceramic powder forms gel with calcium nitrate after hydrolysis, re-sinters powder using ethyl orthosilicate as raw material
It is broken to form.It may be used as bone filling, reparation or alternative materials.With filling, antibacterial and other effects.
Oyster shell whiting is to impregnate sea shells sodium hydroxide solution using sea shells as raw material, clean, dry and powder
It is broken to obtain shell coarse powder, the shell coarse powder of a part is calcined under vacuum, obtains the first shell coarse powder, it will in addition
A part of shell coarse powder is calcined in an oxidizing atmosphere, obtains the second shell coarse powder, after mixing in proportion and is crushed,
It obtains sea shell micropowder, sodium polyacrylate solution is recycled to be embedded in antibacterial polypeptide in sea shell micropowder to obtain the final product.Oyster shell whiting has aobvious
The antibacterial bacteriostatic effect of work has repairing effect to damaged skin.
Pearl powder is to mix gained after crushing with hydrolyzed pearl extract into crossing using bivalves crushing pearl as raw material.Hydrolysis
Contain a large amount of amino acid and trace element in pearl, there is whitening and repair, pearl powder to have absorption and fungistatic effect on skin.
Nanometer hydroxyapatite powder, be using calcium hydroxide and phosphoric acid as raw material, be mixed reaction after be freeze-dried and
；Nanometer hydroxyapatite powder has inhibiting effect to microorganism, can improve skin microenvironment.
Preferably, composition includes component below by mass percentage：
2~30% glycerine；
1~20% dipropylene glycol；
1~10% bioactivity unorganic glass powder；
0~0.05% essence；
40~90% deionized water.
Preferably, composition includes component below by mass percentage：
2~10% glycerine；
1~10% isoprene；
1~10% oyster shell whiting；
70~90% deionized water.
Preferably, composition includes component below by mass percentage：
2~10% glycerine；
1~10% butanediol；
0~10% bioactivity unorganic glass powder；
0~10% oyster shell whiting；
0~0.05% essence；
60~90% deionized water；
It is not 0 and bioactivity unorganic glass powder and oyster shell whiting that bioactivity unorganic glass powder and oyster shell whiting are at least a kind of
Total content be more than 0.01%.
Preferably, composition further includes essence (daily essence) and pigment, it is additional any anti-that addition is not required in composition
Rotten agent, itself has excellent anti-corrosive antibacterial effect.Results of preservation challenge tests is as shown in table 1.
1 composition results of preservation challenge tests of table (test formulations composition contains the oyster shell whiting of 5wt%)
In preservation challenge test process：
1, mixed cell is：Escherichia coli, staphylococcus aureus, Bacillus subtilis endophyticus, bacillus subtilis
The common bacterium such as bacterium, Pseudomonas fluorescence, onion Pseudomonas alba；
2, mixing mould is：Aspergillus niger, aspergillus flavus, aspergillus ustus, Aspergillus terreus, aspergillus sydowi, Trichoderma viride, cured leaf bud branch
The common bacterium such as mould, Chaetomium globosum, paecilomyces varioti；
3, Bacteria Culture temperature is 36 ± 1 DEG C, and mycotic culture temperature is 28 ± 1 DEG C；
4, data are the bacteria containing amount in sample after cultivating certain number of days in table 1.
The present invention provides a kind of preparation method without anti-corrosion astringent composition including inorganic alkaline powder, by it is each at
It point mixes to than more uniform state, the specific steps are：Correspondence weighs moisturizer, inorganic alkaline powder and deionized water, will go
Ionized water is heated to 90~95 DEG C, keeps the temperature 15 minutes, be then cooled to 45 DEG C it is spare；Moisturizing is added to the deionized water after cooling
Agent and inorganic alkaline powder, discharge after stirring；Storage → the inspection of semifinished product → filling → product inspection → storage.
Specific embodiment：
In above-described embodiment 1-9, the moisturizer that the present invention selects is glycerine, propylene glycol, butanediol, isoprene, gathers
It is one or more in ethylene glycol -400, methyl propanediol, Sodium Hyaluronate and dipropylene glycol；Meanwhile the present invention removes above-mentioned 8 kinds
Sorbierite, pungent glycol, diglycerol, glycerin polyether, pentanediol, one kind in polyglutamic acid sodium or more also can be selected outside moisturizer
Kind；Therefore it is not elaborated in a particular embodiment to all.
In above-described embodiment 1-9, the present invention can also select that pigment is added according to actual demand.
The present invention also provides a kind of preparation method without anti-corrosion astringent composition including inorganic alkaline powder, preparation sides
Method includes the following steps：
Step 1 weighs A phases and B phases according to embodiment 1-9, and A phase deionized waters are heated to 90~95 DEG C, keep the temperature 15 points
Clock, be then cooled to 45 DEG C it is spare；
B phases are added into the A phases after cooling or the A after cooling is added in B phase mixtures for step 2, are sufficiently stirred
Discharging after uniformly；
Step 3, storage, the inspection of semifinished product, filling, product inspection and storage.
Test method
In order to test the maintenance effect and irritation to sensitive skin of the present invention, investigation experiment on probation has been carried out：
1, respondent：100 people of each department sensitivity skin consumer, 86 parts of the trial state feedback form finally withdrawn.
2, control time：On March 2, -2018 years on the 3rd January in 2018.
3, test uses product：The composition being formulated according to embodiment 1 of the present invention.
4, test method：After daily morning and evening face cleaning cleaning, take this product appropriate, uniformly in smearing and skin, observation and experience
Use feeling.
5, test result table is as follows：
2 product of table uses 60 days feedback summary tables
Feed back conclusion
Test crowd is all sensibility skin, and only people feedback has minimal irritation, other people all nonirritant reactions,
This test is fed back without allergy implementations, shows that this product is used suitable for sensibility skin.Smearing use feeling and sticky sense side
Face, this product also show well, obtain public receive.In terms of to the maintenance effect of skin and antipruritic and antiallergic, this product has pole
Good effect absolutely proves that this product can be used for maintenance sensitive question skin.This product also has good moistening effect simultaneously, can
Toner as daily indispensability uses.
It these are only the preferred embodiment of the present invention, be not intended to restrict the invention, for those skilled in the art
For member, the invention may be variously modified and varied.Any modification made by all within the spirits and principles of the present invention,
Equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. it is a kind of comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that the composition presses quality hundred
It includes component below to divide than meter：
0.01~50% moisturizer；
0.01~30% inorganic alkaline powder；
20~90% deionized water.
2. as described in claim 1 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that described group
It includes component below to close object by mass percentage：
1~50% moisturizer；
1~30% inorganic alkaline powder；
20~90% deionized water.
3. as claimed in claim 2 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that described group
It includes component below to close object by mass percentage：
2~50% moisturizer；
1~30% inorganic alkaline powder；
20~90% deionized water.
4. it is as claimed in any one of claims 1-3 comprising inorganic alkaline powder without anti-corrosion astringent composition, feature
It is, the moisturizer includes propylene glycol, sorbierite, butanediol, pungent glycol, methyl propanediol, dipropylene glycol, glycerine, double sweet
It is one or more in oil, glycerin polyether, pentanediol, isoprene, polyethylene glycol, Sodium Hyaluronate, polyglutamic acid sodium；It is described
Inorganic alkaline powder includes bioactivity unorganic glass powder, bioactivity inorganic ceramic powder, oyster shell whiting, pearl powder, nano-hydroxy
It is one or more in apatite powder.
5. as claimed in claim 4 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that the guarantor
Humectant selects glycerine and/or isoprene, the inorganic alkaline powder to select bioactivity unorganic glass powder and/or oyster shell whiting.
6. as claimed in claim 4 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that described group
It further includes essence and pigment to close object, is not required to add any preservative in the composition.
7. as claimed in claim 6 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that described group
It includes component below to close object by mass percentage：
2~30% glycerine；
1~20% dipropylene glycol；
1~10% bioactivity unorganic glass powder；
0~0.05% essence；
40~90% deionized water.
8. as claimed in claim 6 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that described group
It includes component below to close object by mass percentage：
2~10% glycerine；
1~10% isoprene；
1~10% oyster shell whiting；
70~90% deionized water.
9. as claimed in claim 6 comprising inorganic alkaline powder without anti-corrosion astringent composition, which is characterized in that described group
It includes component below to close object by mass percentage：
2~10% glycerine；
1~10% butanediol；
0~10% bioactivity unorganic glass powder；
0~10% oyster shell whiting；
0~0.05% essence；
60~90% deionized water；
It is not 0 and bioactivity unorganic glass powder and oyster shell whiting that the bioactivity unorganic glass powder and oyster shell whiting are at least a kind of
Total content be more than 0.01%.
10. a kind of preparation method without anti-corrosion astringent composition as claimed in claim 8 including inorganic alkaline powder,
It is characterized in that, the preparation method includes the following steps：
Step 1 weighs glycerine, isoprene, oyster shell whiting and deionized water, deionized water is heated to 90~95 DEG C, heat preservation 15
Minute, be then cooled to 45 DEG C it is spare；
Glycerine, isoprene and oyster shell whiting is added to the deionized water after cooling in step 2, discharges after stirring；
Step 3, storage, the inspection of semifinished product, filling, product inspection and storage.
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| CN201810475054.1A CN108498352A (en) | 2018-05-17 | 2018-05-17 | Including inorganic alkaline powder without anti-corrosion astringent composition and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810475054.1A CN108498352A (en) | 2018-05-17 | 2018-05-17 | Including inorganic alkaline powder without anti-corrosion astringent composition and preparation method |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199471A (en) * | 2007-12-28 | 2008-06-18 | 浙江长生鸟珍珠生物科技有限公司 | Pearl whitening moisturizing astringent and process for preparing same |
| CN103284930A (en) * | 2013-05-10 | 2013-09-11 | 周卫忠 | Preparation method of pure natural talcum powder |
| CN103462872A (en) * | 2013-09-26 | 2013-12-25 | 陈理敬 | Whitening moisturizing make-up lotion and preparation method thereof |
| CN105560147A (en) * | 2015-12-29 | 2016-05-11 | 青岛拓联信息技术有限公司 | Whitening toning lotion |
-
2018
- 2018-05-17 CN CN201810475054.1A patent/CN108498352A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101199471A (en) * | 2007-12-28 | 2008-06-18 | 浙江长生鸟珍珠生物科技有限公司 | Pearl whitening moisturizing astringent and process for preparing same |
| CN103284930A (en) * | 2013-05-10 | 2013-09-11 | 周卫忠 | Preparation method of pure natural talcum powder |
| CN103462872A (en) * | 2013-09-26 | 2013-12-25 | 陈理敬 | Whitening moisturizing make-up lotion and preparation method thereof |
| CN105560147A (en) * | 2015-12-29 | 2016-05-11 | 青岛拓联信息技术有限公司 | Whitening toning lotion |
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Application publication date: 20180907 |