CN108489820B - A kind of acquisition methods of high temperature tension test trus stress - Google Patents

A kind of acquisition methods of high temperature tension test trus stress Download PDF

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CN108489820B
CN108489820B CN201810147752.9A CN201810147752A CN108489820B CN 108489820 B CN108489820 B CN 108489820B CN 201810147752 A CN201810147752 A CN 201810147752A CN 108489820 B CN108489820 B CN 108489820B
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sample
formula
cross
tensile
section
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CN108489820A (en
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赵宝纯
李桂艳
王晓峰
马惠霞
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Angang Steel Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/08Investigating strength properties of solid materials by application of mechanical stress by applying steady tensile or compressive forces
    • G01N3/18Performing tests at high or low temperatures
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/02Details
    • G01N3/06Special adaptations of indicating or recording means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0016Tensile or compressive
    • G01N2203/0017Tensile
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/006Crack, flaws, fracture or rupture
    • G01N2203/0067Fracture or rupture
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/022Environment of the test
    • G01N2203/0222Temperature
    • G01N2203/0226High temperature; Heating means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/026Specifications of the specimen
    • G01N2203/0262Shape of the specimen
    • G01N2203/0266Cylindrical specimens
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/067Parameter measured for estimating the property
    • G01N2203/0676Force, weight, load, energy, speed or acceleration
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/06Indicating or recording means; Sensing means
    • G01N2203/067Parameter measured for estimating the property
    • G01N2203/0682Spatial dimension, e.g. length, area, angle

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  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
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  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The present invention relates to a kind of acquisition methods of high temperature tension test trus stress, select the tensile sample in pole shape, measure the total length and cross-sectional diameter of sample;Sample with thermocouple is mounted on hot modeling test machine, is broken sample with the tensile speed V of setting, breaked fracture surface of sample is rounded;It is projected into plane, establish coordinate system, the form fit presented according to the curve of A and B point-to-point transmission, it is indicated using functional relation, obtain the variation relation of sample cross area with tensile elongation: and then obtain the corresponding sample cross area of moment t, sample institute stress value F when then finding out moment t finally obtains the trus stress curve that sample is subject to.Advantage is: by the variation of cross-sectional area of sample during drawing by high temperature effectively being obtained, to obtain accurate trus stress curve to the rounded tensile sample analysis of rear fracture is broken.

Description

A kind of acquisition methods of high temperature tension test trus stress
Technical field
The invention belongs to thermo dynamic analogy experimental technique field more particularly to a kind of acquisition sides of high temperature tension test trus stress Method.
Background technique
Based on high temperature tension test data research material at high temperature mechanical property and prediction of rolling force mainly using heating power Simulation test machine and material mechanical test machine.Common testing equipment embeds force sensor, can directly acquire material whole The force value that a test process is subject to, but equipment does not directly acquire material cross-sectional area situation of change during the test but Ability.During the test, the parameters such as temperature, deflection, force value and the flow stress value of material can be obtained.In high temperature One of important parameter is exactly stress value in tension test data, however, what equipment accurately collected can only be that sample is born Load force value, it is difficult to obtain the cross-sectional area that sample changes with drawing process, and stress be load force value and sample at this moment The ratio of cross-sectional area therefore be difficult to realize the precise measurement to stress value during drawing by high temperature by the prior art.
The prediction of rolling force of research material elevated temperature strength and material, one of method are obtained by the method for drawing by high temperature It to material tensile test data, and based on this data, carries out regression fit and obtains stress-strain diagram, and consider deformation speed The influence of rate and deformation temperature to flow stress needs to propose a kind of effective height to obtain high-precision draught pressure forecast value Warm tension test trus stress acquisition methods.
Summary of the invention
In order to overcome the deficiencies of the prior art, the object of the present invention is to provide a kind of acquisition sides of high temperature tension test trus stress Method, by realizing to find out the changes of section trend of sample during stretching to breaked sample analysis and effectively obtaining material The purpose of the trus stress of material during stretching.
To achieve the above object, the invention is realized by the following technical scheme:
A kind of acquisition methods of high temperature tension test trus stress, comprising the following steps:
1) tensile sample in pole shape is selected, the total length and cross-sectional diameter of sample is measured, is denoted as L, D respectively;
2) thermocouple is welded in the middle position of specimen length in step 1;
3) sample with thermocouple is mounted on hot modeling test machine, at a temperature of setting, with the stretching of setting Speed V breaks sample, and breaked fracture surface of sample is rounded;The temperature of setting, thermocouple feedback temperature are acquired in the process Degree stretches the displacement of force value and drawing process, sets data acquiring frequency as f;
4) the both ends fracture docking that will break rear sample, measures its total length L ' and fracture diameter d, obtains the elongation of sample Measure Δ L=L'-L;
5) selecting step 3) in breaked one section of sample, be projected into plane, with this section of specimen length direction, i.e., The axis of sample is y-axis, starts the vertical line for making y-axis at reduction along the length direction width of this section of sample, where vertical line section Straight line is that x-axis establishes rectangular coordinate system, is analyzed the contour line of this section of sample projection on coordinate system, contour line breaks The coordinate of terminal A is at mouthfulThe coordinate of the positive intersection points B of contour line and x-axis isAccording to A and B The form fit that the curve of point-to-point transmission is presented is indicated using functional relation (1), formula (2):
Y=ax2+c (1)
Y=ex4+f (2)
In formula (1), formula (2): a, c, e, f are undetermined coefficient;
The coordinate of A and B two o'clock is substituted into formula (1) or (2) respectively, obtains undetermined coefficient a, c, e and f, and then obtain Corresponding function expression;
6) cross-sectional diameter of the sample of function declaration obtained in step 5) with tensile elongation changing rule, it is transversal Face area S calculation formula are as follows:
S=π x2 (3)
By formula (1) or (2) and formula (3), the variation relation of sample cross area and tensile elongation is obtained:
7) t pairs of the moment is obtained by the formula (4) or formula (5) in step 6) according to the tensile speed V set in step 3) The sample cross area answered, sample institute stress value F, the then trus stress that sample is subject to when then finding out moment t
Moment, t was calculated by following formula:
In formula (6), y is the sample amount of tension calculated in step 6);
8) when finding out any time according to step 7, the cross-sectional area of stretching force value and its corresponding sample that sample is subject to It can be obtained by the trus stress curve of sample during stretching.
Compared with prior art, the beneficial effects of the present invention are:
The present invention is by effectively obtaining sample in drawing by high temperature process to the rounded tensile sample analysis of rear fracture is broken In cross-sectional area variation, it is then this value is corresponding with the stretching force value that sample in drawing process is subject to, so that it may to obtain Sample is by trus stress, to obtain accurate trus stress curve.
Detailed description of the invention
Fig. 1 is schematic diagram of the contour line in coordinate system.
In figure: the projection line of 1- contour line 2- fracture.
Specific embodiment
The present invention is described in detail with reference to the accompanying drawings of the specification, it should be noted that implementation of the invention is unlimited In the following embodiments and the accompanying drawings.
A kind of acquisition methods of high temperature tension test trus stress, comprising the following steps:
1) tensile sample in pole shape is selected, the total length and cross-sectional diameter of sample is measured, is denoted as L, D respectively;
2) thermocouple is welded in the middle position of specimen length in step 1;
3) sample with thermocouple is mounted on hot modeling test machine, according to the temperature of setting, with the stretching speed of setting Degree V breaks sample, and breaked fracture surface of sample section is rounded;The temperature of setting, thermocouple feedback are acquired in the process Temperature stretches the displacement of force value and drawing process, sets data acquiring frequency as f;
4) the both ends fracture docking that will break rear sample, measures its total length L ' and fracture diameter d, obtains the elongation of sample Measure Δ L=L'-L;
5) see Fig. 1, selecting step 3) in breaked one section of sample, be projected into plane, with this section of specimen length Direction, the i.e. axis of sample are y-axis, start the vertical line for making y-axis at reduction, along the length direction width of this section of sample with vertical line Straight line where section is that x-axis establishes rectangular coordinate system, is analyzed the contour line of this section of sample projection on coordinate system, profile The coordinate of the incision position terminal A of line isThe coordinate of the positive intersection points B of contour line and x-axis is That is B point Width starts the point at reduction on formula contour projection, according to the form fit that the curve of A and B point-to-point transmission is presented, using function Relational expression (1), formula (2) indicate:
Y=ax2+c (1)
Y=ex4+f (2)
In formula (1), formula (2): a, c, e, f are undetermined coefficient;
The coordinate of A and B two o'clock is substituted into formula (1) or (2) respectively, obtains undetermined coefficient a, c, e and f, and then obtain Corresponding function expression;
6) cross-sectional diameter of the sample of function declaration obtained in step 5) with tensile elongation changing rule, it is transversal Face area S calculation formula are as follows:
S=π x2 (3)
By formula (1) or (2) and formula (3), the variation relation of sample cross area and tensile elongation is obtained:
7) t pairs of the moment is obtained by the formula (4) or formula (5) in step 6) according to the tensile speed V set in step 3) The sample cross area answered, sample is suffered when then finding out moment t stretches force value F, then the trus stress that sample is subject to is
Moment, t was calculated by following formula:
In formula (6), y is the sample amount of tension calculated in step 6);
8) when finding out any time according to step 7, the cross-sectional area of stretching force value and its corresponding sample that sample is subject to It can be obtained by the trus stress curve of sample during stretching.
Embodiment:
The acquisition methods of high temperature tension test trus stress, comprising the following steps:
1) selecting specimen size to be tensioned is 10 × 120mm of Ф, it is known that the ingredient of the material of sample;
2) thermocouple is welded in the middle position of the specimen length in step 1);
3) sample that thermocouple is welded is installed on hot modeling test machine, and clamping;Software is controlled in test procedure Upper programming is broken sample with tensile speed 1mm/s with realizing at a temperature of 1000 DEG C;Testing acquisition parameter includes that program is set Determine temperature, thermocouple feedback temperature, the displacement for stretching force value and drawing process, the data acquiring frequency set is 20Hz; Start testing machine control program and carry out tension test, sample is broken, the breaked fracture section of sample is rounded;
4) the both ends fracture for breaking rear sample is docked, measuring its total length is 126mm and fracture diameter 4mm, is tried The elongation Δ L=6mm of sample;
5) it is (2, -3) that step 5, which obtains A point coordinate in Fig. 1, and B point coordinate is (5,0), and the unit of two reference axis is milli Rice, using formula (1), by A, B two o'clock coordinate is substituted into:
6) variation relation of sample cross area and tensile elongation is obtained are as follows:
By formula (6) and formula (8) simultaneous, it can determine that the corresponding sample cross area of moment t obtains:
7) corresponding relationship of the stretching force value and time collected according to testing machine, so that it may obtain stretching force value and examination The corresponding relationship of sample cross-sectional area, by by the ratio of two parameters of synchronization, i.e. drawing force and sample cross face Long-pending ratio, so that it may obtain the trus stress of moment sample receiving, and then obtain corresponding trus stress curve.

Claims (1)

1. a kind of acquisition methods of high temperature tension test trus stress, which comprises the following steps:
1) tensile sample in pole shape is selected, the total length and cross-sectional diameter of sample is measured, is denoted as L, D respectively;
2) thermocouple is welded in the middle position of specimen length in step 1;
3) sample with thermocouple is mounted on hot modeling test machine, at a temperature of setting, with the tensile speed V of setting Sample is broken, breaked fracture surface of sample is rounded;The temperature of setting is acquired in the process, and thermocouple feedback temperature is drawn The displacement of stretch value and drawing process sets data acquiring frequency as f;
4) the both ends fracture docking that will break rear sample, measures its total length L ' and fracture diameter d, obtains the elongation Δ of sample L=L'-L;
5) selecting step 3) in breaked one section of sample, be projected into plane, with this section of specimen length direction, i.e. sample Axis be y-axis, start the vertical line for making y-axis at reduction, along the length direction width of this section of sample with straight line where vertical line section Rectangular coordinate system is established for x-axis, the contour line of this section of sample projection on coordinate system is analyzed, the incision position of contour line The coordinate of terminal A isThe coordinate of the positive intersection points B of contour line and x-axis isAccording to A and B two o'clock Between curve present form fit, using functional relation (1), formula (2) indicate:
Y=ax2+c (1)
Y=ex4+f (2)
In formula (1), formula (2): a, c, e, f are undetermined coefficient;
The coordinate of A and B two o'clock is substituted into formula (1) or (2) respectively, obtains undetermined coefficient a, c, e and f, and then has been obtained corresponding Function expression;
6) changing rule of the cross-sectional diameter of the sample of function declaration obtained in step 5) with tensile elongation, cross section face Product S calculation formula are as follows:
S=π x2 (3)
By formula (1) or (2) and formula (3), the variation relation of sample cross area and tensile elongation is obtained:
7) it is corresponding to be obtained by the formula (4) or formula (5) in step 6) according to the tensile speed V set in step 3) by moment t Sample cross area, sample institute stress value F, the then trus stress that sample is subject to when then finding out moment t
Moment, t was calculated by following formula:
In formula (6), y is the sample amount of tension calculated in step 6);
8) when finding out any time according to step 7, the cross-sectional area of stretching force value and its corresponding sample that sample is subject to can To obtain the trus stress curve of sample during stretching.
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CN110702727B (en) * 2019-09-30 2022-02-18 鞍钢股份有限公司 Method for measuring static recrystallization volume fraction of material
CN112927185A (en) * 2021-01-19 2021-06-08 中国石油天然气集团有限公司 True stress-true strain curve test calculation method based on digital image correlation method
CN113310437B (en) * 2021-05-28 2023-05-16 广东韶钢松山股份有限公司 Method and device for automatically measuring wire rod area shrinkage

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