CN108489609A - A kind of FTIR measures the wide range bearing calibration of photodetector response - Google Patents

A kind of FTIR measures the wide range bearing calibration of photodetector response Download PDF

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Publication number
CN108489609A
CN108489609A CN201810089435.6A CN201810089435A CN108489609A CN 108489609 A CN108489609 A CN 108489609A CN 201810089435 A CN201810089435 A CN 201810089435A CN 108489609 A CN108489609 A CN 108489609A
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response
spectrum
detector
photodetector
ftir
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CN108489609B (en
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张永刚
邵秀梅
张忆南
李雪
龚海梅
方家熊
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Shanghai Institute of Technical Physics of CAS
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Shanghai Institute of Technical Physics of CAS
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J3/00Spectrometry; Spectrophotometry; Monochromators; Measuring colours
    • G01J3/28Investigating the spectrum
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J3/00Spectrometry; Spectrophotometry; Monochromators; Measuring colours
    • G01J3/28Investigating the spectrum
    • G01J3/2803Investigating the spectrum using photoelectric array detector
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00Radiation pyrometry, e.g. infrared or optical thermometry
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J5/00Radiation pyrometry, e.g. infrared or optical thermometry
    • G01J5/80Calibration

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  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Spectrometry And Color Measurement (AREA)

Abstract

The invention discloses the wide range bearing calibrations that a kind of FTIR measures photodetector response, this method is using based on the pyroelectric detector with wide spectral range flat response as FTIR spectrum instrument standard configuration, it obtains the detector and amplifying circuit and the response under different scanning speed is combined to selected light and beam splitter, extract related data and fit the frequency response characteristic of the detector and amplifying circuit.The original output characteristics combined to specific light source and beam splitter using this frequency response characteristic is corrected to get to its actual output characteristics.Using this reality output characteristic after correcting as background spectrum, you can the photodetector original response spectrum to measuring gained carries out reference operation, the photodetector real response spectrum after being corrected.It is the standard configuration of FTIR spectrum instrument in view of pyroelectric detector and is responded with wide range, thus the method is pervasive and wide range, different light sources and beam splitter combination suitable for various FTIR spectrum instrument.

Description

A kind of FTIR measures the wide range bearing calibration of photodetector response
Technical field
The invention belongs to semiconductor optoelectronic spectral ranges, specially a kind of pervasive to Fourier transform infrared (FTIR) light Spectrometer measures the method that gained photodetector response carries out broad spectral range correction.
Background technology
Semiconductor photo detector (PD) and its focal plane arrays (FPA) (FPA) device have important application in numerous areas, and Its response spectrum is all extremely paid close attention in all these applications.Conventional PD or FPA all there are one continuous response wave length scope, The size responded within this range can change namely responsiveness has a spatial distribution, this spatial distribution or response spectrum need Be obtained through actual measurement, and with series of advantages Fourier transform infrared (FTIR) spectrometer have become measure PD or The preferred instrument of FPA devices, especially in infrared band.
Although the detector optogalvanic spectra directly measured by FTIR spectrum instrument contains its spectral response information, but not The real response spectrum of detector, and greatly differ from each other in many cases with real response spectrum, this is mainly due to instruments The output characteristics (including light source and beam splitter and other component) of itself is not perfectly flat smooth, and also there are one specific spectrum for itself Caused by distribution.It is referred to as computing equipment function correction method, standard detector to solve the problems, such as that people also have been developed in this respect It transmits the correlation-correcteds method such as correction method, thus obtains the real response spectrum of detector.These all achieve certain effect, But also there is also many problems.Such as:For computing equipment function correction method, infrared light supply is simulated using Formula of the blackbody radiation Output, need set a blackbody radiation temperature, such one side infrared light supply is not the ideal black-body of single temperature, and this The setting of temperature is artificial rather than obtained by practical measurement, on the other hand the temperature of practical infrared light supply will necessarily there are one Distribution, it is difficult to single temperature simulation;In addition, the beam splitter response characteristic needed for computing equipment function correction method nor reality It surveys, these all inevitably introduce certain error.For another example:The basis that standard detector transmits correction method is based on the standard by calibration Detector, therefore correcting range can only limit within the response range of this standard detector, different wave bands needs different The continuous linking of standard detector, wave band is also had any problem, this makes application in many occasions all be very limited.Quantum type During photodetector is still evolving, some devices with wide range response have also occurred, such as respond to visible light wave range The InGaAs detectors of expansion.It is exactly that must solve the problems, such as to carry out spectral response characterization to such broad spectrum device.
Invention content
Based on problem mentioned above, innovative the proposing of the present invention provides a kind of pervasive to Fourier transform infrared (FTIR) method that photodetector response carries out broad spectral range correction obtained by spectrometer measurement, can realize to broadband range Interior photodetector carries out spectral response correction.
Bearing calibration concrete operation step of the present invention is:
1) by measuring pyroelectric detector and amplifying circuit to selected light and beam splitter combination in different scanning speed Under response, then extract related data and fit the analytic frequency response characteristic of this detector and amplifying circuit;
2) pyroelectric detector that is obtained according to step 1) and amplifying circuit analytic frequency response characteristic to specific light source and The original output characteristics of beam splitter combination is corrected, to obtain the FTIR spectrum instrument under this specific light source and beam splitter combination Reality output characteristic namely real background spectrum;
3) according to step 2) obtain using this spectrometer reality output characteristic after correcting as background spectrum, to measuring institute The original response spectrum of the photodetector obtained carries out reference operation, you can the photodetector real response light after being corrected Spectrum.
It is the standard configuration of FTIR spectrum instrument in view of pyroelectric detector and is responded with wide range, thus the method can be applied to respectively Kind of FTIR spectrum instrument, and be suitable for different light sources and the wide spectral region of beam splitter combined covering, thus be it is pervasive and Wide range.To be suitble to middle infrared band, the standard configuration pyroelectric detector of FTIR spectrum instrument is existing often to be visited for the DTGS comprising KBr windows Device is surveyed, below with regard to abbreviation DTGS detectors.DTGS detectors are flat as a kind of thermal detector, the spectral response of itself , it is unrelated with wavelength, and KBr windows infrared band and transmitance of near-infrared and visible light wave range in entire are also flat Straight, therefore DTGS detectors can consider and be in response to the device unrelated with wavelength, but its response is then straight with the frequency of optical signal Connect correlation.
To further illustrate the present invention, Fig. 1 is shown uses DTGS detectors and amplifying circuit under different scanning speed Original background spectrum of the FTIR spectrum instrument measured under specific light source and beam splitter combination, hollow square is follow-up fitting in figure Selected data point.As seen from Figure 1, with the raising of sweep speed, by DTGS detectors/amplifier combination under each wave number The output measured is all to reduce, and reality output should be constant, and here it is the frequencies by DTGS detectors and amplifying circuit Caused by response.To the measurement result of Fig. 1, for the frequency range for covering wider, in the 9000cm-1 and 3000cm- of low frequency end It is extracted relative response data on these wave number points of the 1 and 15000cm-1 of front end for being fitted, chooses this 3 wave numbers Putting has preferable representativeness, also avoids error caused by absorption band of water vapor possibility.To the data of extraction using 9000cm-1 as base Plinth makes itself and 9000cm-1 intermediate frequency models after the data of low frequency end 3000cm-1 and front end 15000cm-1 are carried out whole lifting Data trend coincidence is enclosed, using Fourier frequency fF, the linear relationship fF=2v ν between index glass sweep speed v and wave number ν are obtained The data for fitting expanded to one group of low-and high-frequency end are as shown in Figure 2.Nonlinear fitting is used to obtain the final product to this group of data To Analytic solving curve shown in Fig. 2, there can be good effect with better simply second order polynomial fit reciprocal.With Fig. 2 institutes The fitting function obtained can export (such as Fig. 1) to the instrument under a certain invisible scanning speed and be corrected, that is, do reference operation, i.e., The reality output characteristic namely real background spectrum of instrument can be obtained.
After obtaining the real background spectrum under a certain sweep speed, with this to the photoelectricity that is measured under same sweep speed herein Detector original spectrum does reference operation to get the photodetector real response spectrum to after correcting, as shown in Figure 3.It is right Routinely to be measured under wave number coordinate and operation for FTIR spectrum measures, wave number coordinate be converted into wavelength coordinate still by It is conventional to carry out.Sampling other methods are also shown in Fig. 3 and demarcate the i.e. so-called standard spectral data of detector response spectrum obtained As a means of comparing.
The advantage of the invention is that:
A. bearing calibration of the invention is all based on measured data, and unique assumed condition thinks pyroelectric detector Response is unrelated with wavelength, this is also consistent with actual conditions, therefore can obtain good calibration result.
B. bearing calibration of the invention only need to carry out one group of survey to same spectrometer (the DTGS detectors for including its configuration) Amount fitting can easily obtain the frequency response characteristic of required DTGS detectors and amplifying circuit, instrumental correction step thereafter It is rapid to be all based on the background spectrum that thus characteristic obtains thus easy to operate.
C. the background spectrum after correcting also includes the interference such as water vapor absorption, therefore carries out reference with this and can substantially eliminate finally Corresponding interference in response spectrum.
D. bearing calibration of the invention is applicable since its principle combines different light sources and beam splitter, is Pervasive, wide wave-length coverage can be covered;
Description of the drawings
Fig. 1 is to be existed using the FTIR spectrum instrument that DTGS detectors and its mating amplifying circuit measure under different scanning speed Halogen tungsten lamp (white light) light source and the lower original background spectrum of quartzy beam splitter combination, in figure hollow square be subsequently be fitted selected by Data point.
Fig. 2 is the frequency of the DTGS detectors and amplifying circuit that are fitted using the data point extracted from Fig. 1 Rate response characteristic.
Fig. 3 is to measure the primary photoelectric current spectrum (fine line) of obtained Si and InGaAs detectors and using present invention side Detector real response spectrum (heavy line) after method correction;Figure orbicular spot thus the nominal data of two detectors namely for than Compared with normal data, data have been carried out normalized in figure.
Specific implementation mode
The specific implementation mode of the present invention is described in detail below in conjunction with the accompanying drawings.
Embodiment 1:Wave scalable InGaAs detector
As shown in the lower part of Figure 3, the Wave scalable InGaAs detector of an existing standard spectral data has been carried out original Optogalvanic spectra is tested, and bearing calibration using the present invention has carried out response spectrum correction.The long wave cut-off wavelength of this device is about 2.5 μm are fronts into optical detector, and the response of shortwave end is expanded to visible light wave range, therefore it is (white that halogen tungsten lamp is used in measuring Light) light source is combined with quartzy beam splitter, so that spectrometer has stronger shortwave to export, extremely may be used to cover therefrom infrared shortwave end Light-exposed wide spectral range.Changing sweep speed first under fixed aperture, gain parameter, (such as 0.1581cm/s is extremely Totally 7 grades of 1.8988cm/s) measure one group of original background spectrum (as shown in Figure 1), when measurement for ensure the quality of data can be used compared with More scanning times (such as 64 times);Due to not containing fine spectral information generally for detector measurement, can be used relatively low Resolution ratio (such as 16cm-1) to shorten time of measuring;Again with scanning constant speed (such as 0.4747cm/s, reality under identical conditions Border can be selected as needed) measure this Wave scalable InGaAs device primary photoelectric current spectrum, then from this group of original background Data needed for spectrum test extracting data carry out the frequency characteristic fitting of DTGS detectors and amplifying circuit, obtain its frequency spy The analytic parameter of property.Reference operation is done to the original background spectrum under 0.4747cm/s sweep speeds with this frequency characteristic and obtains reality Border background spectrum, then do reference operation with the original response spectrum of this real background spectrum versus wavelength extension InGaAs devices, i.e., The real response spectrum of device is obtained, finally to the spectrum under wave number coordinate is converted into wavelength coordinate to get thick to the lower parts Fig. 3 Real response spectrum after correction shown in line, filament is to measure gained original spectrum in figure, the standard spectrum of dot device thus, For comparing.The quality of data is should be noted in the process so that operation can carry out and result is reliable, to front end (and low frequency end) Due to instrument output it is too low caused by (such as 15770- near He-Ne laser wavelengths inside low quality data and spectrometer The sections 15820cm-1) on bounce data can be blocked or be deleted.Since this spectrum test all pertains only to the opposite of response Value, there is no need to the absolute figure of focused data, multiplication and division and normalization operation can at any time be carried out to facilitate data processing.
Embodiment 2:Si detectors
As shown in the tops Fig. 3, primary photoelectric current spectrum is carried out for a Si detectors of an existing standard spectral data and has been surveyed Examination, bearing calibration using the present invention have carried out response spectrum correction.The long wave cut-off wavelength of this detector is about 1 μm of front Into optical device, the response of shortwave end is expanded to visible light wave range, therefore still uses halogen tungsten lamp (white light) light source and quartz point in measuring Beam device combines, so that spectrometer has stronger shortwave to export.Change sweep speed first (such as under fixed aperture, gain parameter 0.1581cm/s to 1.8988cm/s7 grades) measure one group of original background spectrum (as shown in Figure 1), to ensure data matter when measurement More scanning times (such as 64 times) can be used in amount;Due to not containing fine spectral information generally for detector measurement, because This can be used lower resolution ratio (such as 16cm-1) to shorten time of measuring;Again under identical conditions with scanning constant speed (such as 0.4747cm/s actually can be selected as needed) the primary photoelectric current spectrum that measures this Si detector, then from this original back of the body of group Data needed for scape spectrum test extracting data carry out the frequency characteristic fitting of DTGS detectors and amplifying circuit, obtain its frequency The analytic parameter of characteristic (is noticed that this process is identical with embodiment 1, therefore need to only be carried out to same instrument primary such Operation).Reference operation is done to the original background spectrum under 0.4747cm/s sweep speeds with this frequency characteristic and obtains real background Spectrum, then reference operation is done to get to the reality of detector to the original response spectrum of Si detectors with this real background spectrum Response spectrum, finally to the spectrum under wave number coordinate is converted into wavelength coordinate to get to after being corrected shown in the thick line of the tops Fig. 3 Real response spectrum, filament is to measure gained original spectrum in figure, the standard spectrum of dot device thus, for comparing.Herein The quality of data is should be noted in the process so that operation can carry out and result is reliable, to front end (and low frequency end) since instrument exported Inside low quality data caused by low and spectrometer near He-Ne laser wavelengths on (such as sections 15770-15820cm-1) Bounce data can be blocked or be deleted.Since this spectrum test all pertains only to the relative value of response, there is no need to attention numbers According to absolute figure, multiplication and division and normalization operation can at any time carry out to facilitate data processing.

Claims (1)

1. a kind of FTIR measures the wide range bearing calibration of photodetector response.The wide range bearing calibration is using as FTIR light Based on the pyroelectric detector with wide spectral range flat response of spectrometer standard configuration, meter is measured and is fitted by practical It calculates to obtain the background spectrum needed for tuning detector response spectrum, then the background spectrum is utilized to obtain photodetector to be measured Real response spectrum;It is characterized in that the bearing calibration includes the following steps:
1) selected light and beam splitter are combined under different scanning speed by measuring pyroelectric detector and amplifying circuit Then the analytic frequency response characteristic that related data fits this detector and amplifying circuit is extracted in response;
2) pyroelectric detector and amplifying circuit analytic frequency response characteristic obtained according to step 1) is to specific light source and beam splitting The original output characteristics of device combination is corrected, to obtain the reality of the FTIR spectrum instrument under this specific light source and beam splitter combination Border output characteristics;
3) according to step 2) obtain using this spectrometer reality output characteristic after correcting as background spectrum, to measuring gained The original response spectrum of photodetector carries out reference operation, you can the photodetector real response spectrum after being corrected.
CN201810089435.6A 2018-01-30 2018-01-30 A kind of wide range bearing calibration of FTIR measurement photodetector response Active CN108489609B (en)

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CN109781259A (en) * 2018-12-29 2019-05-21 华中科技大学 A kind of associated method for accurately measuring aerial sports Small object infrared spectroscopy of map

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CN101520323A (en) * 2009-03-25 2009-09-02 中国科学院上海技术物理研究所 Extensive angle measuring method for inclination angle of plane moving mirror in Fourier spectrometer
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CN109781259A (en) * 2018-12-29 2019-05-21 华中科技大学 A kind of associated method for accurately measuring aerial sports Small object infrared spectroscopy of map
CN109781259B (en) * 2018-12-29 2020-05-19 华中科技大学 Method for accurately measuring infrared spectrum of small aerial moving target through spectrum correlation

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