CN108489565A - A kind of safe and efficient gas liquid ratio accurate measuring method - Google Patents
A kind of safe and efficient gas liquid ratio accurate measuring method Download PDFInfo
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- CN108489565A CN108489565A CN201810230281.8A CN201810230281A CN108489565A CN 108489565 A CN108489565 A CN 108489565A CN 201810230281 A CN201810230281 A CN 201810230281A CN 108489565 A CN108489565 A CN 108489565A
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- liquid
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01F—MEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
- G01F5/00—Measuring a proportion of the volume flow
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- General Physics & Mathematics (AREA)
- Measuring Volume Flow (AREA)
Abstract
The present invention relates to a kind of safe and efficient accurate methods for measuring gas liquid ratio, are implemented using accurate gas liquid ratio measurement device.It is as follows:Liquid gas phase is taken after pipeline enters flow rate fine-tuning valve, can be obtained that pressure is relatively low, the slow air source of flow trim.Air source is entered by entering gas pipeline in the middle part of buffering flask after processing, is just drastically expanded wherein, abundant decrease temperature and pressure, is entered cooling liquid in gas pipeline and is directly dropped in liquid measure meter, residual fluid further cools down under the effect of peripheral cooling bath.The liquid isolated enters liquid measure meter, and gas phase enters gas gauge via outlet line.Entire agent set buffering flask, liquid measure meter, the pedestal of measuring uses integrated structure design, air source is closed after to be measured, the agent sets such as liquid measure meter are taken out from liquid nitrogen cooling bath, etc. liquid measures meter, gas gauge restore to room temperature after directly read data, you can obtain accurate gas liquid ratio.This process test is safe and convenient quick, and measuring accuracy is high, convenient for promoting the use of.
Description
Technical field
The present invention relates to the accurate measuring methods that liquid gas phase gas liquid ratio is taken in a kind of safe and efficient measurement.
Background technology
All refer to accurately measure the experiment of gas liquid ratio in fields such as chemical industry, petroleum works, such as in petroleum works field,
It is frequently necessary to know the accurate composition of underground crude oil, basic data is provided for numerical simulation.For example in condensate combine experiment, it is
Whether condensation oil ingredient has been matched in verification correct, needs to allow its gas-liquid separation again at ambient temperature, is examined again.Therefore,
A kind of method that can accurately measure gas liquid ratio is just particularly important.But when doing condensate combine experiment at present, air source is past
Quickly toward the abundant flow velocity of pressure, cause gas-liquid separation to be not thorough, influence measurement accuracy, and be easy to burst the examination for measuring liquid sample
Pipe, causes security risk.When less additionally, due to liquid phase volume, laboratory is generally sucked and is read with needle tubing with a scale, due to
Inevitably absorption remains on test tube, considers that liquid phase volume was originally smaller, and second order error is just very big.It may shape between last pipeline
At convection current, the gas phase after gas-liquid separation still may seriously take liquid, influence measuring accuracy.For above-mentioned a series of problems, have
There must be a kind of method that safety directly can accurately measure gas liquid ratio again of exploitation.
Invention content
The object of the present invention is to provide the accurate measuring methods that liquid gas phase gas liquid ratio is taken in a kind of safe and efficient measurement.
The present invention adopts the following technical scheme that:
Accurate measurement gas-liquid ratio method of the present invention is implemented using accurate gas liquid ratio measurement device.The accurate survey
Determine gas liquid ratio device, mainly by pipeline, flow rate fine-tuning valve, rubber stopper, buffering flask, liquid measure meter, liquid nitrogen cooling bath, gas gauge,
Enter gas pipeline, outlet line, pedestal composition.Come from air source to take the general pressure of liquid gas phase higher, if directly passing through pipeline
Into follow-up measuring device, it is easy to which, because the high pressure of fluid, high speed moment burst device, even if not bursting, high velocity stream also can
Seriously affect measuring accuracy.Therefore it needs to find a kind of method being substantially depressured reduction of speed, can be reached by introducing flow rate fine-tuning valve
To the effect.Air source can reduce gaseous pressure and flow velocity after flow rate fine-tuning valve regulation before measuring, obtain pressure it is relatively low,
The slow air source of flow trim increases Security of test and accuracy, therefore introduces existing flow rate fine-tuning valve.It is come out from the valve
Take liquid gas phase via rubber stopper it is fixed enter gas pipeline after, into buffering flask in the middle part of large space can drastically expand, fully
Decrease temperature and pressure, entering cooling liquid in gas pipeline can directly drop in liquid measure meter, and residual fluid can be under the effect of peripheral cooling bath
It is further cooling.Gas-liquid can be made to be completely separated by the method for this abundant decompression cooling, the liquid isolated enters liquid measure meter,
And gas phase enters gas gauge via outlet line.Entire agent set buffering flask, liquid measure meter, the pedestal of measuring is tied using integration
Structure design, close air source after to be measured, the agent sets such as liquid measure meter taken out from liquid nitrogen cooling bath, etc. liquid measures meter, gas
Gauge directly reads data after restoring to room temperature, you can obtains accurate gas liquid ratio.
Compared with existing gas-oil ratio determination techniques and device, it is an advantage of the invention that:
By introducing existing flow rate fine-tuning valve in 1 present invention, it can more finely control take liquid gas by this method
The flow and pressure of phase, keep air source steadily slow, reduce security risk, increase measurement accuracy.
A kind of new method for entering gas pipeline and outlet line controlled at rubber stopper is devised in 2 present invention, is allowed into tracheae
Line extends in the middle part of buffering flask, and outlet line is just passed through rubber stopper, pulls open the vertical distance of two pipelines, this method can prevent two pipelines
Between form convection current, gas phase can be reduced to greatest extent and take liquid to outlet line, measuring accuracy can be greatly improved.
The method for buffering flask volume by expansion in 3 present invention, can drastically expand and take liquid gas phase, and liquid is taken to reduce
Gas phase temperature pressure, and liquid phase is further cooled down by peripheral liquid nitrogen cooling bath, it is convenient for gas-liquid separation, improves measuring accuracy.
Liquid measure meter just can avoid being transferred to other container measurement with scale convenient directly reading, the method in 4 present invention
When the second order error that generates, and liquid measure meter diameter is thinner, can increase liquid phase accuracy of reading, and the method is convenient and efficient and precision
It is high.
Description of the drawings
Fig. 1 is a kind of accurate measurement gas liquid ratio schematic device of the present invention.
Fig. 2 is upper figure liquid measure meter part partial enlarged view.
In figure:1. pipeline, 2. flow rate fine-tuning valves, 3. rubber stoppers, 4. buffering flasks, 5. liquid measure meters, 6. liquid nitrogen cooling baths, 7.
Gas gauge, 8. enter gas pipeline, 9. outlet lines, 10 pedestals.
Specific implementation mode
The present invention is described in detail below in conjunction with the accompanying drawings.
As shown in Figure 1 and Figure 2, gas liquid ratio measurement device of the present invention, mainly by pipeline 1, flow rate fine-tuning valve 2, rubber
Plug 3, liquid measure meter 5, liquid nitrogen cooling bath 6, gas gauge 7, enters gas pipeline 8, outlet line 9, the composition of pedestal 10 at buffering flask 4.From gas
What source came takes liquid gas phase can reduce gaseous pressure into flow rate fine-tuning valve 2 by pipeline 1 after being adjusted by flow rate fine-tuning valve 2
And flow velocity, it obtains that pressure is relatively low, the slow air source of flow trim, increases Security of test and accuracy.It is taken from what the valve came out
Liquid gas phase enters buffering flask 4 via the gas pipeline 8 that enters at rubber stopper 3, and because 4 body space of buffering flask is big, taking liquid gas phase can
Abundant decrease temperature and pressure is drastically expanded wherein, is sufficiently separated conducive to gas-liquid;The entire agent set that measures is soaked in liquid nitrogen cooling bath 6
The inside further makes fluid temperature reduction, and gas-liquid is allowed to be completely separated.This method makes gas-liquid be kept completely separate, high certainty of measurement, wherein dropping
Pressure can guarantee safety and prevent gas phase from taking liquid to greatest extent, and cooling can make liquid phase by evaporation vapor condensation to liquid phase, greatly improve
Measurement accuracy.There are two pipeline jacks on rubber stopper 3, and the jack of circle centre position is to be fixed into gas pipeline 8, face liquid measure meter 5, convenient
Liquid phase is directly dropped into meter, and another jack is and gas pipeline 8 to be allowed to extend in buffering flask 4 for fixed outlet line 9
Portion, outlet line 9 is at top.This design method ingenious can avoid forming convection current between pipeline, and outlet line 9 can be greatly decreased
Interior gas phase takes liquid.Liquid measure meter 5 measures liquid phase volume in order to directly accurate, be purposely designed to it is with a scale thin cylindric, it is this
Design method avoids second order error when transfer liquid reading.Liquid measure meter bottom is pedestal 10, to support liquid measure meter 5 gentle
Flask 4 is rushed, wherein buffering flask 4, liquid measure meter 5, pedestal 10 use integrated structure design, constitutes entire measurement agent set.
Gas enters gas gauge 7 from outlet line 9, and air source is closed after measurement, by agent sets such as liquid measure meters 5 from liquid nitrogen cooling bath
Taken out in 6, etc. liquid measures meter 5, gas gauge 7 restore to directly reading data after room temperature, you can obtain accurate gas liquid ratio.
Claims (5)
1. a kind of safe and efficient gas liquid ratio accurate measuring method is implemented using accurate gas liquid ratio measurement device.The accurate survey
Gas liquid ratio device is determined mainly by pipeline (1), flow rate fine-tuning valve (2), rubber stopper (3), buffering flask (4), liquid measure meter (5), liquid nitrogen
Cooling bath (6), gas gauge (7) enter gas pipeline (8), outlet line (9), pedestal (10) composition, it is characterised in that:Air source comes
Take liquid gas phase by pipeline (1) enter flow rate fine-tuning valve (2), then via rubber stopper (3) it is fixed enter gas pipeline (8) enter
Flask (4) is buffered, liquid, which is separated, instills liquid measure meter (5), and gas phase enters gas gauge (7) via outlet line (9), entire to survey
It measures agent set buffering flask (4), liquid measure meter (5), pedestal (10) and uses integrated structure design, be put in liquid nitrogen cooling bath
(6) in, air source is closed after measurement, the agent sets such as liquid measure meter (5) are taken out from the liquid nitrogen cooling bath (6), etc. liquid measures meter
(5), gas gauge (7) restores to room temperature to directly read data, you can obtains accurate gas liquid ratio.
2. a kind of safe and efficient gas liquid ratio accurate measuring method according to claim 1, it is characterised in that:Pass through introducing
Existing flow rate fine-tuning valve (2), can more finely control the flow and pressure for taking liquid gas phase by this method, keep air source flat
It is steady slowly to reduce security risk, increase measurement accuracy.
3. a kind of safe and efficient gas liquid ratio accurate measuring method according to claim 1, it is characterised in that:Design one
The new method for entering gas pipeline (8) and outlet line (9) at kind control rubber stopper (3), allows and extends to buffering flask into gas pipeline (8)
(4) middle part, outlet line (9) are just passed through rubber stopper, pull open the vertical distance of two pipelines, and the method can prevent between two pipelines
Convection current is formed, gas phase can be reduced to greatest extent and take liquid to outlet line (9), measuring accuracy can be greatly improved.
4. a kind of safe and efficient gas liquid ratio accurate measuring method according to claim 1, it is characterised in that:Pass through expansion
The method for buffering flask (4) volume, can drastically expand and take liquid gas phase, take liquid gas phase temperature pressure to reduce, and by outer
It encloses liquid nitrogen cooling bath (6) and further cools down liquid phase, be convenient for gas-liquid separation, improve measuring accuracy.
5. a kind of safe and efficient gas liquid ratio accurate measuring method according to claim 1, it is characterised in that:Liquid measure meter
(5) scale convenient directly reading, the method are carried and can avoid being transferred to the second order error generated when other container measurement, and liquid measure
It is thinner to count diameter, liquid phase accuracy of reading can be increased, the method is convenient and efficient and precision is high.
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CN201810230281.8A CN108489565A (en) | 2018-03-20 | 2018-03-20 | A kind of safe and efficient gas liquid ratio accurate measuring method |
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CN201810230281.8A CN108489565A (en) | 2018-03-20 | 2018-03-20 | A kind of safe and efficient gas liquid ratio accurate measuring method |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110529100A (en) * | 2019-09-05 | 2019-12-03 | 西南石油大学 | High temperature and pressure pit shaft salt crust physical simulating device and its analogy method |
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CN1439448A (en) * | 2002-02-21 | 2003-09-03 | 孙永勇 | Gas-liquid separation for compressed air method and device |
US20070006640A1 (en) * | 2005-07-07 | 2007-01-11 | Gysling Daniel L | Multi-phase flow measurement system having a fluid separator |
CN201755421U (en) * | 2010-06-30 | 2011-03-09 | 安徽金鼎医药有限公司 | Gas-liquid separator |
CN202073552U (en) * | 2011-04-19 | 2011-12-14 | 克拉玛依市百口泉建筑安装有限责任公司 | Automatic oil-gas metering device |
CN102636223A (en) * | 2012-05-04 | 2012-08-15 | 宁波威瑞泰默赛多相流仪器设备有限公司 | Gas-liquid measurement method with super-small flow |
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2018
- 2018-03-20 CN CN201810230281.8A patent/CN108489565A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1439448A (en) * | 2002-02-21 | 2003-09-03 | 孙永勇 | Gas-liquid separation for compressed air method and device |
US20070006640A1 (en) * | 2005-07-07 | 2007-01-11 | Gysling Daniel L | Multi-phase flow measurement system having a fluid separator |
CN201755421U (en) * | 2010-06-30 | 2011-03-09 | 安徽金鼎医药有限公司 | Gas-liquid separator |
CN202073552U (en) * | 2011-04-19 | 2011-12-14 | 克拉玛依市百口泉建筑安装有限责任公司 | Automatic oil-gas metering device |
CN102636223A (en) * | 2012-05-04 | 2012-08-15 | 宁波威瑞泰默赛多相流仪器设备有限公司 | Gas-liquid measurement method with super-small flow |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110529100A (en) * | 2019-09-05 | 2019-12-03 | 西南石油大学 | High temperature and pressure pit shaft salt crust physical simulating device and its analogy method |
CN110529100B (en) * | 2019-09-05 | 2020-06-02 | 西南石油大学 | High-temperature high-pressure shaft salt deposition physical simulation device and simulation method thereof |
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