CN108485465A - 用于高温环境的防腐蚀涂料 - Google Patents

用于高温环境的防腐蚀涂料 Download PDF

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CN108485465A
CN108485465A CN201810273091.4A CN201810273091A CN108485465A CN 108485465 A CN108485465 A CN 108485465A CN 201810273091 A CN201810273091 A CN 201810273091A CN 108485465 A CN108485465 A CN 108485465A
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汪琦
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Abstract

本发明公开了用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂38~47份、滑石粉4~8份、纳米氧化铝8~11份、纳米氧化钛1~4份、氯化铬2~5份、硅烷偶联剂2~6份、陶瓷空心微珠6~9份、丁二醇11~17份、聚酰胺树脂21~28份、羟甲基纤维素14~19份、纳米二氧化硅9~14份、磷酸三丁酯6~13份、甲醇11~19份、膨润土10~17份、聚四氟乙烯8~16份、炭黑6~11份。本发明的涂料没有刺激性气味,更有利于使用。

Description

用于高温环境的防腐蚀涂料
技术领域
本发明涉及涂料领域,具体涉及用于高温环境的防腐蚀涂料。
背景技术
随着工业技术进步,金属材料的使用越来越广泛,金属及其构件的腐蚀问题已遍及国民经济的各个领域,给人类社会造成了巨大损失。涂料防腐以其施工简便、经济适用、不受设备面积、形状的约束等特点而被广泛的应用。目前的涂料,其防腐性、耐热性差,有的会有不同程度的毒副作用及刺激气味,有害人体健康。近些年,随着科学技术的发展,对涂料的技术要求越来越高,要求在高温下漆膜不变色、不脱落、仍能保持良好的物理机械性能、隔热性能和防腐性能。
发明内容
本发明所要解决的技术问题是现有涂料在高温环境中性能较差,使用寿命效果变差,目的在于提供用于高温环境的防腐蚀涂料,解决在高温环境中涂料的使用的问题。
本发明通过下述技术方案实现:
用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂38~47份、滑石粉4~8份、纳米氧化铝8~11份、纳米氧化钛1~4份、氯化铬2~5份、硅烷偶联剂2~6份、陶瓷空心微珠6~9份、丁二醇11~17份、聚酰胺树脂21~28份、羟甲基纤维素14~19份、纳米二氧化硅9~14份、磷酸三丁酯6~13份、甲醇11~19份、膨润土10~17份、聚四氟乙烯8~16份、炭黑6~11份。
用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂40~45份、滑石粉5~7份、纳米氧化铝9~11份、纳米氧化钛1~3份、氯化铬2~4份、硅烷偶联剂3~5份、陶瓷空心微珠7~9份、丁二醇12~15份、聚酰胺树脂23~27份、羟甲基纤维素15~18份、纳米二氧化硅10~13份、磷酸三丁酯7~12份、甲醇13~18份、膨润土12~16份、聚四氟乙烯10~15份、炭黑7~10份。
用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂43份、滑石粉6份、纳米氧化铝10份、纳米氧化钛2份、氯化铬3份、硅烷偶联剂4份、陶瓷空心微珠8份、丁二醇13份、聚酰胺树脂25份、羟甲基纤维素16份、纳米二氧化硅12份、磷酸三丁酯10份、甲醇15份、膨润土14份、聚四氟乙烯14份、炭黑9份。
本发明的制作方法为:将环氧改性有机硅树脂、滑石粉、丁二醇、聚酰胺树脂、羟甲基纤维素、磷酸三丁酯、膨润土、炭黑依次加入反应容器中混合,用搅拌机以搅拌速度1800~2300r/min的速度搅拌15~20min后,在170~210℃下保温半小时;将分散后的物料混合组分加入研磨机进行研磨,研磨至粒度为3~5um,再依次加入纳米氧化铝、纳米氧化钛、纳米二氧化硅、硅烷偶联剂、陶瓷空心微珠、氯化铬、甲醇、聚四氟乙烯,以搅拌速度为1000~1300r/min的速度搅拌分散25~35min至粒度为30~45um,即可得到成品。
在本发明中环氧改性有机硅树脂的作用是提高涂料的耐高温、防腐蚀、耐溶剂性、机械性能、耐真空紫外线辐照性能;在本发明中滑石粉也可以增强涂料形状的稳定性、机械性能、降低变形性,提高粒度均匀分散性。
纳米二氧化硅可以快速形成网状结构,提高漆膜的耐老化性能、漆膜强度、光洁度等。纳米材料形成致密的涂层可以提高抗渗性及防紫外线吸收、防热老化能力,能起到增加结合强度的作用。
本发明与现有技术相比,具有如下的优点和有益效果:
1、本发明用于高温环境的防腐蚀涂料,本发明的涂料适用于高温环境中,并且在高温下也不会影响本发明涂料的性能,使用寿命更长;
2、本发明用于高温环境的防腐蚀涂料,本发明具有较好的防腐蚀效果,更便于使用;
3、本发明用于高温环境的防腐蚀涂料,本发明的涂料没有刺激性气味,更有利于使用。
具体实施方式
为使本发明的目的、技术方案和优点更加清楚明白,下面结合实施例,对本发明作进一步的详细说明,本发明的示意性实施方式及其说明仅用于解释本发明,并不作为对本发明的限定。
实施例1
本发明用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂21份、滑石粉2份、纳米氧化铝6份、纳米氧化钛1份、氯化铬1份、硅烷偶联剂1份、陶瓷空心微珠2份、丁二醇7份、聚酰胺树脂14份、羟甲基纤维素7份、纳米二氧化硅6份、磷酸三丁酯4份、甲醇8份、膨润土6份、聚四氟乙烯5份、炭黑4份。
实施例2
所述的用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂50份、滑石粉9份、纳米氧化铝26份、纳米氧化钛8份、氯化铬9份、硅烷偶联剂8份、陶瓷空心微珠16份、丁二醇21份、聚酰胺树脂34份、羟甲基纤维素21份、纳米二氧化硅18份、磷酸三丁酯24份、甲醇23份、膨润土19份、聚四氟乙烯21份、炭黑18份。
实施例3
所述的用于高温环境的防腐蚀涂料,包括以下重量份数的组分:环氧改性有机硅树脂43份、滑石粉6份、纳米氧化铝10份、纳米氧化钛2份、氯化铬3份、硅烷偶联剂4份、陶瓷空心微珠8份、丁二醇13份、聚酰胺树脂25份、羟甲基纤维素16份、纳米二氧化硅12份、磷酸三丁酯10份、甲醇15份、膨润土14份、聚四氟乙烯14份、炭黑9份。
本发明中,实施例1和实施例2在本发明的组分范围外,与实施例3相比,实施例1和实施例2所得的涂料的性能较差,并且使用寿命较短,而实施例3的性能不仅好,并且使用寿命也长,更便于使用。
以上所述的具体实施方式,对本发明的目的、技术方案和有益效果进行了进一步详细说明,所应理解的是,以上所述仅为本发明的具体实施方式而已,并不用于限定本发明的保护范围,凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。

Claims (3)

1.用于高温环境的防腐蚀涂料,其特征在于,包括以下重量份数的组分:环氧改性有机硅树脂38~47份、滑石粉4~8份、纳米氧化铝8~11份、纳米氧化钛1~4份、氯化铬2~5份、硅烷偶联剂2~6份、陶瓷空心微珠6~9份、丁二醇11~17份、聚酰胺树脂21~28份、羟甲基纤维素14~19份、纳米二氧化硅9~14份、磷酸三丁酯6~13份、甲醇11~19份、膨润土10~17份、聚四氟乙烯8~16份、炭黑6~11份。
2.根据权利要求1所述的用于高温环境的防腐蚀涂料,其特征在于,包括以下重量份数的组分:环氧改性有机硅树脂40~45份、滑石粉5~7份、纳米氧化铝9~11份、纳米氧化钛1~3份、氯化铬2~4份、硅烷偶联剂3~5份、陶瓷空心微珠7~9份、丁二醇12~15份、聚酰胺树脂23~27份、羟甲基纤维素15~18份、纳米二氧化硅10~13份、磷酸三丁酯7~12份、甲醇13~18份、膨润土12~16份、聚四氟乙烯10~15份、炭黑7~10份。
3.根据权利要求1所述的用于高温环境的防腐蚀涂料,其特征在于,包括以下重量份数的组分:环氧改性有机硅树脂43份、滑石粉6份、纳米氧化铝10份、纳米氧化钛2份、氯化铬3份、硅烷偶联剂4份、陶瓷空心微珠8份、丁二醇13份、聚酰胺树脂25份、羟甲基纤维素16份、纳米二氧化硅12份、磷酸三丁酯10份、甲醇15份、膨润土14份、聚四氟乙烯14份、炭黑9份。
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Cited By (1)

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Publication number Priority date Publication date Assignee Title
CN112177480A (zh) * 2019-07-01 2021-01-05 金鹏节能科技有限公司 一种耐腐蚀铝合金门窗及其制备方法

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103965776A (zh) * 2013-01-29 2014-08-06 惠州市华昱美实业有限公司 一种耐高温隔热防腐蚀涂料
CN105440934A (zh) * 2015-12-11 2016-03-30 青岛唐鹏钢结构工程有限公司 一种彩钢板耐高温防腐蚀涂料

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103965776A (zh) * 2013-01-29 2014-08-06 惠州市华昱美实业有限公司 一种耐高温隔热防腐蚀涂料
CN105440934A (zh) * 2015-12-11 2016-03-30 青岛唐鹏钢结构工程有限公司 一种彩钢板耐高温防腐蚀涂料

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112177480A (zh) * 2019-07-01 2021-01-05 金鹏节能科技有限公司 一种耐腐蚀铝合金门窗及其制备方法

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