CN108477148A - A kind of Lasioderma serricorne (Fabricius) repellant and preparation method thereof, application - Google Patents
A kind of Lasioderma serricorne (Fabricius) repellant and preparation method thereof, application Download PDFInfo
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- CN108477148A CN108477148A CN201810083640.1A CN201810083640A CN108477148A CN 108477148 A CN108477148 A CN 108477148A CN 201810083640 A CN201810083640 A CN 201810083640A CN 108477148 A CN108477148 A CN 108477148A
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- repellant
- fabricius
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N35/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical
- A01N35/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having two bonds to hetero atoms with at the most one bond to halogen, e.g. aldehyde radical containing aliphatically bound aldehyde or keto groups, or thio analogues thereof; Derivatives thereof, e.g. acetals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of Lasioderma serricorne (Fabricius) repellant, the Lasioderma serricorne (Fabricius) repellant is made of the component of following parts by weight：5~50 parts of nimbins, 5~50 portions of cinnamic acids, 5~50 parts of capsaicines, 1~2 part of methyl hydroxybenzoate, the agar aqueous fusion glue that 10~500 parts of agar mass percentages are 1~8%.The Lasioderma serricorne (Fabricius) repellant of the present invention it is active it is strong, the lasting period is long, the advantages that being unlikely to deteriorate, being facilitated using simple, storing, the disadvantage that chemical fumigant toxicity can be overcome big.The present invention also provides a kind of Lasioderma serricorne (Fabricius) repellant preparation methods, agar is added to the water be heated to 80~85 DEG C fusing obtain agar mass percentage be 1~8% agar aqueous fusion glue after be added methyl hydroxybenzoate stir evenly, nimbin, cinnamic acid and capsaicine is added when being cooled to 40 DEG C under stirring, stirs evenly postcooling.The Lasioderma serricorne (Fabricius) repellant preparation method processing step of the present invention is simple, and operability is strong, easily implements.
Description
Technical field
The present invention relates to tobacco-plant pest-insect Prevention Technique fields, more particularly, to a kind of Lasioderma serricorne (Fabricius) repellant and its preparation side
Method, application.
Background technology
Lasioderma serricorne Lasioderma serricorne (Fabricius) are important stored product pest, to storage tobacco leaf and
Its product is caused harm more so.This beetle belongs to coleoptera Anobiidae Anobiidae, is distributed across the whole world, and feeding habits are extremely miscellaneous.For
Prevention lasioderma serricorne, China all put into a large amount of manpowers and assets every year, and main control method has following several：(1) it fumigates：Packet
Include traditional stifling poison gas hydrogen phosphide and bromomethane and novel fumigant Ethyl formate class, carbonyl sulfide, vikane etc.；(2)
Physical control：Including leakproofness packaging material, diatomite, 60Co rays, hot air treatment and controlled atmosphere method etc.；(3) biology is anti-
It controls：Including release Lariophagus distinguensis, Greece's tyrophagus putrescentiae, using bacillus thuringiensis (Bt) preparation etc.；Lasioderma serricorne gyplure：
Such as Serrico sex pheromone insect traps；Lasioderma serricorne (Fabricius) repellant：Applied some broad spectrum activity insects repellants such as naphthalene, camphor and
The lasioderma serricorne of the preventions such as paracide moth food painting and calligraphy.
Other than fumigating system, other above control measures are all in exploration or experimental stage, the main reason is that effect is not
Ideal or benefit is not notable.Phosphine fumigation, which is used for a long time, has made lasioderma serricorne produce serious resistance, and bromomethane is because being difficult to
Degradation, can destroy ozone layer and will be eliminated；Other novel fumigant Ethyl formate class, carbonyl sulfide, vikanes etc. are in tobacco
On be not all approved to use.It is very big on tobacco quality influence that prevention lasioderma serricorne is isolated using sealing and packing material；Radiation prevention is also deposited
In the defect for influencing cigarette quality, and cost and application conditions require it is high, to the potential carcinogenic, teratogenesis of human body, mutagenic
Risk is also not yet assessed；Controlled atmosphere method is high to tabacco barn infrastructure requirements, therefore cost is very high；The season limitation of temperature control prevention
Property is too strong, and the application of biological control is still in the junior stage；Gyplure is female sex attractant, can only trap and kill male worm, therefore not have
Due control effect.Therefore, in order to effectively prevent lasioderma serricorne, it is necessary to the development of new products or new method, New Measure.
Invention content
The present invention is to provide a kind of tool to solve the above problem present in the lasioderma serricorne control method of the prior art
It is active it is strong, the lasting period is long, the advantages that being unlikely to deteriorate, being facilitated using simple, storing, can overcome chemical fumigant toxicity is big to lack
Point complies with the Lasioderma serricorne (Fabricius) repellant that " green tobacco " production and processing requires.
The present invention also provides a kind of Lasioderma serricorne (Fabricius) repellant preparation methods, and processing step is simple, and operability is strong, Yi Shi
It applies.
To achieve the goals above, the present invention uses following technical scheme：
A kind of Lasioderma serricorne (Fabricius) repellant of the present invention, the Lasioderma serricorne (Fabricius) repellant are made of the component of following parts by weight：5~50
Part nimbin, 5~50 portions of cinnamic acids, 5~50 parts of capsaicines, 1~2 part of methyl hydroxybenzoate, 10~500 parts of agar quality percentages contain
The agar aqueous fusion glue that amount is 1~8%.The present invention using nimbin, cinnamic acid, capsaicine, three kinds of vegetable-derived components as repellent at
Point, using methyl hydroxybenzoate as preservative, a kind of Lasioderma serricorne (Fabricius) repellant is re-dubbed using agar aqueous fusion glue as carrier, by strong
Irritation play the role of expulsion and inhibition to lasioderma serricorne, to carry out effective repellent to lasioderma serricorne, be formulated simple science, have
It is active strong, the lasting period is long, the advantages that being unlikely to deteriorate, being facilitated using simple, storing, can overcome chemical fumigant toxicity is big to lack
Point is complied with " green tobacco " production and processing and is required.
A kind of Lasioderma serricorne (Fabricius) repellant preparation method, the specific steps are：Agar is added to the water and is heated to 80~85 DEG C of fusings
Addition methyl hydroxybenzoate stirs evenly after obtaining the agar aqueous fusion glue that agar mass percentage is 1~8%, when being cooled to 40 DEG C
Nimbin, cinnamic acid and capsaicine are added under stirring, stirs evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.The present invention's
Lasioderma serricorne (Fabricius) repellant preparation method defines that the order of addition of each raw material component, each component are uniformly dispersed, and processing step is simple, can
Strong operability is easily implemented, and product obtained is in solid-state, easily storage transport.
A kind of Lasioderma serricorne (Fabricius) repellant application, concrete application method are：Lasioderma serricorne (Fabricius) repellant is placed directly in tabacco barn required
Position.
Therefore, the present invention has the advantages that：
(1) using nimbin, cinnamic acid, capsaicine, three kinds of vegetable-derived components as repellent ingredient, using methyl hydroxybenzoate as
Preservative is re-dubbed a kind of Lasioderma serricorne (Fabricius) repellant using agar aqueous fusion glue as carrier to carry out effective repellent, formula to lasioderma serricorne
Simple science, it is active it is strong, the lasting period is long, the advantages that being unlikely to deteriorate, being facilitated using simple, storing, chemical fumigation can be overcome
The big disadvantage of agent toxicity is complied with " green tobacco " production and processing and is required；
(2) defining that the order of addition of each raw material component, each component are uniformly dispersed, processing step is simple, and operability is strong,
Easily implement, product obtained is in solid-state, easily storage transport.
Specific implementation mode
Below by specific implementation mode, the present invention will be further described.
Embodiment 1
According to 5g nimbins, 5g cinnamic acids, 5g capsaicines, 1g methyl hydroxybenzoates, 10g agar mass percentages are 1%
Agar aqueous fusion glue weight proportion, first agar is added to the water and is heated to 80 DEG C of fusings and obtains agar mass percentage and be
After 1% agar aqueous fusion glue methyl hydroxybenzoate is added to stir evenly, when being cooled to 40 DEG C under stirring be added nimbin,
Cinnamic acid and capsaicine stir evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.
Comparative example 1
Comparative example 1 difference from example 1 is that：By nimbin, cinnamic acid, capsaicine by etc. quality Chinese cassia tree
Sour methyl esters is replaced, remaining is identical.
Embodiment 2
According to 50g nimbins, 50g cinnamic acids, 50g capsaicines, 2g methyl hydroxybenzoates, 500g agar mass percentages are
Agar is first added to the water and is heated to 85 DEG C of fusings and obtains agar mass percentage by the weight proportion of 8% agar aqueous fusion glue
It is stirred evenly to add methyl hydroxybenzoate after 8% agar aqueous fusion glue, print chinaberry is added when being cooled to 40 DEG C under stirring
Element, cinnamic acid and capsaicine, stir evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.
Comparative example 2
Comparative example 2 and embodiment 2 the difference is that：By nimbin, cinnamic acid, capsaicine by etc. quality Chinese cassia tree
Sour methyl esters is replaced, remaining is identical.
Embodiment 3
According to 25g nimbins, 50g cinnamic acids, 25g capsaicines, 1g methyl hydroxybenzoates, 500g agar mass percentages are
Agar is first added to the water and is heated to 80~85 DEG C of fusings and obtains agar quality percentage by the weight proportion of 8% agar aqueous fusion glue
Methyl hydroxybenzoate is added after the agar aqueous fusion glue that content is 8% to stir evenly, and is added under stirring when being cooled to 40 DEG C
Nimbin, cinnamic acid and capsaicine stir evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.
Comparative example 3
Comparative example 3 and embodiment 3 the difference is that：By nimbin, cinnamic acid, capsaicine by etc. quality Chinese cassia tree
Sour methyl esters is replaced, remaining is identical.
Embodiment 4
According to 8g nimbins, 20g cinnamic acids, 10g capsaicines, 1.5g methyl hydroxybenzoates, 300g agar mass percentages
For the weight proportion of 5% agar aqueous fusion glue, first agar is added to the water and is heated to 82 DEG C of fusings and obtains agar quality percentage to contain
Amount stirs evenly to add methyl hydroxybenzoate after 5% agar aqueous fusion glue, and print is added when being cooled to 40 DEG C under stirring
Chinaberry element, cinnamic acid and capsaicine stir evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.
Comparative example 4
Comparative example 4 and embodiment 4 the difference is that：By nimbin, cinnamic acid, capsaicine by etc. quality Chinese cassia tree
Sour methyl esters is replaced, remaining is identical.
Embodiment 5
According to 50g nimbins, 20g cinnamic acids, 30g capsaicines, 1g methyl hydroxybenzoates, 500g agar mass percentages are
Agar is first added to the water and is heated to 80~85 DEG C of fusings and obtains agar quality hundred by the weight proportion of 1~8% agar aqueous fusion glue
Methyl hydroxybenzoate is added after the agar aqueous fusion glue that point content is 1~8% to stir evenly, when being cooled to 40 DEG C under stirring
Nimbin, cinnamic acid and capsaicine is added, stirs evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.
Comparative example 5
Comparative example 5 and embodiment 5 the difference is that：By nimbin, cinnamic acid, capsaicine by etc. quality Chinese cassia tree
Sour methyl esters is replaced, remaining is identical.
Embodiment 6
According to 20g nimbins, 10g cinnamic acids, 20g capsaicines, 1g methyl hydroxybenzoates, 100g agar mass percentages are
Agar is first added to the water and is heated to 82 DEG C of fusings and obtains agar mass percentage by the weight proportion of 6% agar aqueous fusion glue
It is stirred evenly to add methyl hydroxybenzoate after 1~8% agar aqueous fusion glue, print is added when being cooled to 40 DEG C under stirring
Chinaberry element, cinnamic acid and capsaicine stir evenly postcooling up to Lasioderma serricorne (Fabricius) repellant.
Comparative example 6
Comparative example 6 and embodiment 6 the difference is that：By nimbin, cinnamic acid, capsaicine by etc. quality Chinese cassia tree
Sour methyl esters is replaced, remaining is identical.
Lasioderma serricorne repellency test is carried out to the Lasioderma serricorne (Fabricius) repellant that the various embodiments described above and comparative example obtain.Experimental rig is
C4 type packed in cases, 1098X672X705 millimeters of carton interior diameter, 1115X690X725 millimeters of outer diameter；Testing specific method is：
The diagonal both ends of carton bottom are respectively put into flue-cured tobacco (kind：Zhongyan-100) blade 100g and it is put into each reality in processing end middle part of blade
The Lasioderma serricorne (Fabricius) repellant that example obtains is applied, it is random to launch lasioderma serricorne adult 50, it is used in combination the plate glass cover of 150cm × 120cm to exist
It prevents lasioderma serricorne from escaping on carton, is 30 days during experiment, daily the lasioderma serricorne work borer population amount on timing statistics Flue-cured, system
Lasioderma serricorne adult is re-replaced after meter, calculates separately the average scattering ratio of each formula as the following formula：
Average scattering ratio (%)=(lasioderma serricorne quantity/experiment lasioderma serricorne sum on 1- Σ flue-cured tobaccos), scattering ratio is bigger, obtains
The test result arrived is as shown in table 1.
1 lasioderma serricorne repellency test test result of table
It can be seen from Table 1 that the scattering ratio that generates to lasioderma serricorne of the obtained Lasioderma serricorne (Fabricius) repellant of each embodiment is up to 96%
More than, hence it is evident that scattering ratio caused by the repellant obtained higher than each comparative example illustrates the Lasioderma serricorne (Fabricius) repellant repellent of the present invention
Effect highly significant, and using 30 days when, still have good repellent effect.
Above-mentioned embodiment is only a preferred solution of the present invention, not the present invention is made in any form
Limitation, on the premise of not exceeding the technical scheme recorded in the claims also other variations and modifications.
Claims (3)
1. a kind of Lasioderma serricorne (Fabricius) repellant, which is characterized in that the Lasioderma serricorne (Fabricius) repellant is made of the component of following parts by weight：5~
50 parts of nimbins, 5~50 portions of cinnamic acids, 5~50 parts of capsaicines, 1~2 part of methyl hydroxybenzoate, 10~500 parts of agar quality percentages
The agar aqueous fusion glue that content is 1~8%.
2. a kind of Lasioderma serricorne (Fabricius) repellant preparation method as described in claim 1, which is characterized in that the specific steps are：By agar
It is added to the water and is heated to that Ni Bo is added after 80~85 DEG C of fusings obtain the agar aqueous fusion glue that agar mass percentage is 1~8%
Tortoise beetle ester stirs evenly, and nimbin, cinnamic acid and capsaicine is added when being cooled to 40 DEG C under stirring, stirs evenly rear cold
But up to Lasioderma serricorne (Fabricius) repellant.
3. a kind of Lasioderma serricorne (Fabricius) repellant application as described in claim 1, which is characterized in that concrete application method is：By tobacco
First repellant is placed directly within required position in tabacco barn.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810083640.1A CN108477148A (en) | 2018-01-29 | 2018-01-29 | A kind of Lasioderma serricorne (Fabricius) repellant and preparation method thereof, application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810083640.1A CN108477148A (en) | 2018-01-29 | 2018-01-29 | A kind of Lasioderma serricorne (Fabricius) repellant and preparation method thereof, application |
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| CN108477148A true CN108477148A (en) | 2018-09-04 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114467963A (en) * | 2021-07-01 | 2022-05-13 | 山东中医药大学 | Pesticide compound drug-loaded microsphere for honeysuckle and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114467963A (en) * | 2021-07-01 | 2022-05-13 | 山东中医药大学 | Pesticide compound drug-loaded microsphere for honeysuckle and preparation method thereof |
| CN114467963B (en) * | 2021-07-01 | 2024-02-13 | 山东中医药大学 | Pesticide compound drug-loaded microsphere for honeysuckle and preparation method thereof |
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