CN108467776A - Rust preventive cutting fluid preparation method - Google Patents
Rust preventive cutting fluid preparation method Download PDFInfo
- Publication number
- CN108467776A CN108467776A CN201810280902.3A CN201810280902A CN108467776A CN 108467776 A CN108467776 A CN 108467776A CN 201810280902 A CN201810280902 A CN 201810280902A CN 108467776 A CN108467776 A CN 108467776A
- Authority
- CN
- China
- Prior art keywords
- shell
- fixedly connected
- cutting fluid
- rust preventive
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M177/00—Special methods of preparation of lubricating compositions; Chemical modification by after-treatment of components or of the whole of a lubricating composition, not covered by other classes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/80—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations
- B01F31/83—Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations comprising a supplementary stirring element
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/104—Polyethers, i.e. containing di- or higher polyoxyalkylene groups of alkylene oxides containing two carbon atoms only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2209/00—Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
- C10M2209/10—Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2209/103—Polyethers, i.e. containing di- or higher polyoxyalkylene groups
- C10M2209/108—Polyethers, i.e. containing di- or higher polyoxyalkylene groups etherified
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/22—Metal working with essential removal of material, e.g. cutting, grinding or drilling
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The invention discloses rust preventive cutting fluid preparation methods comprising following steps：A, water-based antirust agent and oiliness additive are added in reaction kettle；B, mineral oil is obtained after heating 80 DEG C of carry out machineries+pulse stirring；C, emulsification antirust agent formation beam is added in mineral oil and composes reaction；D, it filters；E, it detects；F, blowing.The present invention passes through special source materials and synthesis blending technology, the service life and reduction environmental protection pressure of product can be extended again while the various performances of consideration product comprehensively, up to or over the performance of import similar product, it can be in different field of machining import substitutes simultaneously, the production cost of domestic enterprise is substantially reduced, production operation environment is improved and reduces the pressure of liquid waste processing, and product applications can be expanded, for domestic brand Branding effect, there are preferable market prospects.
Description
Technical field
The present invention relates to rust preventive cutting fluid technical fields, specially rust preventive cutting fluid preparation method.
Background technology
After liberation we gradually start to industrialize machinery production, need to carry using cutting fluid during machinery production
High processing efficiency, the abrasion for reducing cutter, the corrosion protection that equipment and workpiece are provided, and domestic chemical industry blank out, institute
To have introduced simplest saponified oil from Russia.Since China's secondary industry is started late, lathe and metal material processing phase
Larger compared with European and American developed countries' gap, mating metal working fluid is even more to prove definitely inferior.In the latest 20 years with China's machine
The continuous promotion of tool industry precise machining equipment and requirement, the requirement to metal working fluid is also higher and higher, and domestic tradition is cut
Xiao Ye manufacturing enterprises are still producing with the product in the most the fifth day of a lunar month sixties, largely use mineral oil, traditional plant grease,
The lubricant of sulfur-bearing composition, cause cutting fluid be easy smelly, service life is short, rustless property is poor, oil content is high, resource can not be again
It is raw, and be difficult to environmental protection treatment after follow-up use and corrosion generated to machine tool, and the cutting fluid performance of American-European import comprehensively,
It is environmental-friendly to operative employee, service life is long, the processing that can not meet Modern high throughput precision equipment uses, while can expire again
The demand of sufficient unlike material protection, so the market of 80% or more domestic middle and high-end market is captured by foreign capitals brand.
Continuing to bring out for China's mechanical processing especially precision machinery processing rapid development and new material, accelerates to height
A large amount of promotions of performance, the rust preventive cutting fluid demand of environmental protection, and domestic cutting fluid industry is one small point of lubricating oil industry
, all without specialized courses in university, research will be combined from principle mechanism and site of deployment to go deep into, few professions
Enterprise goes to research and develop, so causing market product very different, domestic enterprise can only sell mid and low-end products, high-end product base
This is all monopolized by foreign enterprise.
Currently, most of manufacturing enterprises, technical merit is low, also in the formula using five sixties, production equipment is simple and crude,
Product environmental performance is poor, product is lacked competitiveness, and domestic for the research use of cutting fluid raw material and new formulation at present
It is considerably less that scientific allocation mode develops the enterprise used, causes product that cannot meet client's production requirement and ecological requirements in time,
Therefore develop novel raw material and using science formula dispensing mode product can with high value added product outside surrogate, for
Domestic correspondent saves production cost, reduces environmental protection pressure with important value.
Invention content
The purpose of the present invention is to provide rust preventive cutting fluid preparation methods, to solve mentioned above in the background art ask
Topic.
To achieve the above object, the present invention provides the following technical solutions：Rust preventive cutting fluid preparation method comprising following step
Suddenly：
A, water-based antirust agent and oiliness additive are added in reaction kettle；
B, mineral oil is obtained after heating 80 DEG C of carry out machineries+pulse stirring；
C, emulsification antirust agent formation beam is added in mineral oil and composes reaction；
D, it filters；
E, it detects；
F, blowing.
Preferably, the oiliness additive be naphthenic base white oil, and naphthenic base white oil under given conditions with cis-butenedioic anhydride, isopropyl
Alcohol reacts, and the particle generated plays charge neutrality and adsorption bridging, to make the group in system form the state of Water-In-Oil.
Preferably, the emulsification antirust agent connects the EO numbers of different number to form reticular structure, in stabilization using isomery alcohol
Colloidal dispersion system in, 1 long-chain macromolecule can adsorb 2 or several micelles or 1 micelle simultaneously can adsorb 2 simultaneously
A macromolecular chain, thus the form for forming " bridge formation " wraps up in micelle and collects to get up and form stable system.
Preferably, the detection work includes appearance, storing stability, pH value, defoaming, corrosion-resistant, antirust and maximum
No seizing load PB values detection.
Preferably, the agitating device in the step B includes shell, and the left end of case top offers feed inlet, into
Right end at the top of material mouth has been connected through hinge activity cover board, and the middle-end of case top is installed with motor, and motor is defeated
Shaft is fixedly connected with shaft, and the lower end of shaft outer surface is fixedly connected with paddle, and the upper end on the right side of shell is fixedly connected with
Controller, and the outer surface of controller be fixedly connected sequentially from front to back have motor switch, supersonic generator switch and be bubbled
Device switchs, and the lower end on the right side of shell is fixedly connected with support base, and the top of support base is installed with bubbler, bubbler
Outlet side is communicated with second pipe, and second pipe penetrates shell and is fixed on the bottom of housing cavity, second pipe end
Upper surface offers venthole, and the surrounding of housing bottom has been fixedly connected with support leg, and the bottom of support leg is fixedly connected with
Rubber pad, the bottom on the left of shell offers discharge port, and the inner surface of discharge port is movably installed with valve, upper on the left of shell
End is installed with supersonic generator, and the bottom of supersonic generator is communicated with first pipe, and the end of first pipe is worn
Enter shell and be fixed on the lower end on the left of housing cavity, and the outer surface of first pipe and second pipe is movably installed with unidirectionally
Valve.
Compared with prior art, beneficial effects of the present invention are as follows：
The present invention can be extended by special source materials and synthesis blending technology while the various performances of consideration product comprehensively again
The service life of product and reduction environmental protection pressure, up to or over the performance of import similar product, while it can be in different machines
Tool manufacture field import substitutes substantially reduce the production cost of domestic enterprise, improve production operation environment and reduce waste liquid
The pressure of processing, and product applications can be expanded, it is domestic brand Branding effect, there are preferable market prospects.
Description of the drawings
Fig. 1 is present invention process flow diagram；
Fig. 2 is agitating device structural schematic diagram of the present invention；
Fig. 3 is agitating device controller architecture schematic diagram of the present invention；
Fig. 4 is agitating device operation principle schematic diagram of the present invention.
In figure：1 shell, 2 feed inlets, 3 supersonic generators, 4 first pipes, 5 paddles, 6 ventholes, 7 discharge ports, 8
Support leg, 9 second pipes, 10 support bases, 11 bubblers, 12 shafts, 13 controllers, 131 motor switch, 132 ultrasonic waves occur
Device switch, 133 bubblers switch, 14 motors, 15 check valves.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on
Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other
Embodiment shall fall within the protection scope of the present invention.
- 4 are please referred to Fig.1, rust preventive cutting fluid preparation method comprising following steps：
A, water-based antirust agent and oiliness additive are added in reaction kettle；
B, mineral oil is obtained after heating 80 DEG C of carry out machineries+pulse stirring；
C, emulsification antirust agent formation beam is added in mineral oil and composes reaction；
D, it filters；
E, it detects；
F, blowing.
Oiliness additive is naphthenic base white oil, and naphthenic base white oil is given birth under given conditions with cis-butenedioic anhydride, isopropanol reaction
At particle play charge neutrality and adsorption bridging, to make group in system form the state of Water-In-Oil.
Emulsification antirust agent connects the EO numbers of different number to form reticular structure, in stable aqueous colloidal dispersion using isomery alcohol
In system, 1 long-chain macromolecule can adsorb 2 or several micelles or 1 micelle simultaneously can adsorb 2 macromolecular chains simultaneously, because
And the form for forming " bridge formation " wraps up in micelle and collects to get up and form stable system.
It includes appearance, storing stability, pH value, defoaming, corrosion-resistant, antirust and maximum nonseizure load PB to detect work
Value detection.
Agitating device in step B includes shell 1, and the left end at 1 top of shell offers feed inlet 2,2 top of feed inlet
Right end be connected through hinge activity cover board, the middle-end at 1 top of shell is installed with motor 14, and the output shaft of motor 14
It is fixedly connected with shaft 12, the lower end of 12 outer surface of shaft is fixedly connected with paddle 5, and the upper end on 1 right side of shell is fixedly connected
There is a controller 13, and be fixedly connected sequentially from front to back motor switch 131, supersonic generator of the outer surface of controller 13 is opened
132 and bubbler switch 133 are closed, the lower end on 1 right side of shell is fixedly connected with support base 10, and peace is fixed on the top of support base 10
Equipped with bubbler 11, the outlet side of bubbler 11 is communicated with second pipe 9, and second pipe 9 penetrates shell 1 and is fixed on shell
The upper surface of the bottom of 1 inner cavity, 9 end of second pipe offers venthole 6, and the surrounding of 1 bottom of shell has been fixedly connected with branch
Support leg 8, and the bottom of support leg 8 is fixedly connected with rubber pad, the bottom in 1 left side of shell offers discharge port 7, and discharge port 7
Inner surface be movably installed with valve, the upper end in 1 left side of shell is installed with supersonic generator 3, and supersonic generator 3
Bottom be communicated with first pipe 4, the lower end that the end of first pipe 4 penetrates shell 1 and is fixed on the left of 1 inner cavity of shell, and
The outer surface of first pipe 4 and second pipe 9 is movably installed with check valve 15.
In use, by special source materials and synthesis blending technology, again may be used while the various performances of consideration product comprehensively
To extend the service life of product and reduce environmental protection pressure, up to or over the performance of import similar product, while it can be
Different field of machining import substitutes substantially reduce the production cost of domestic enterprise, improve production operation environment and drop
The pressure of low liquid waste processing, and product applications can be expanded, it is domestic brand Branding effect, before there is preferable market
Scape.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (5)
1. rust preventive cutting fluid preparation method, it is characterised in that：It includes the following steps：
A, water-based antirust agent and oiliness additive are added in reaction kettle；
B, mineral oil is obtained after heating 80 DEG C of carry out machineries+pulse stirring；
C, emulsification antirust agent formation beam is added in mineral oil and composes reaction；
D, it filters；
E, it detects；
F, blowing.
2. rust preventive cutting fluid preparation method according to claim 1, it is characterised in that：The oiliness additive is naphthenic base
White oil, and naphthenic base white oil, under given conditions with cis-butenedioic anhydride, isopropanol reaction, the particle generated plays charge neutrality and adsorption bridging
Effect, to make the group in system form the state of Water-In-Oil.
3. rust preventive cutting fluid preparation method according to claim 1, it is characterised in that：The emulsification antirust agent uses isomery
Alcohol connects the EO numbers of different number to form reticular structure, and in stable colloidal dispersion system, 1 long-chain macromolecule can be inhaled simultaneously
Attached 2 or several micelles or 1 micelle can adsorb 2 macromolecular chains simultaneously, thus the form for forming " bridge formation " wraps up in micelle
Collection gets up and forms stable system.
4. rust preventive cutting fluid preparation method according to claim 1, it is characterised in that：The detection work include appearance,
Storing stability, pH value, defoaming, corrosion-resistant, antirust and the detection of maximum nonseizure load PB values.
5. rust preventive cutting fluid preparation method according to claim 1, it is characterised in that：Agitating device in the step B
Including shell（1）, and shell（1）The left end at top offers feed inlet（2）, feed inlet（2）The right end at top is lived by hinge
It is dynamic to be connected with cover board, shell（1）The middle-end at top is installed with motor（14）, and motor（14）Output shaft be fixedly connected with
Shaft（12）, shaft（12）The lower end of outer surface is fixedly connected with paddle（5）, shell（1）The upper end on right side is fixedly connected with
Controller（13）, and controller（13）Outer surface be fixedly connected sequentially have motor switch from front to back（131）, ultrasonic wave occur
Device switchs（132）It is switched with bubbler（133）, shell（1）The lower end on right side is fixedly connected with support base（10）, and support base
（10）Top be installed with bubbler（11）, bubbler（11）Outlet side be communicated with second pipe（9）, and second pipe
（9）Penetrate shell（1）And it is fixed on shell（1）The bottom of inner cavity, second pipe（9）The upper surface of end offers venthole
（6）, shell（1）The surrounding of bottom has been fixedly connected with support leg（8）, and support leg（8）Bottom be fixedly connected with rubber pad,
Shell（1）The bottom in left side offers discharge port（7）, and discharge port（7）Inner surface be movably installed with valve, shell（1）It is left
The upper end of side is installed with supersonic generator（3）, and supersonic generator（3）Bottom be communicated with first pipe（4）, the
One pipeline（4）End penetrate shell（1）And it is fixed on shell（1）Lower end on the left of inner cavity, and first pipe（4）With the second pipe
Road（9）Outer surface be movably installed with check valve（15）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810280902.3A CN108467776A (en) | 2018-04-02 | 2018-04-02 | Rust preventive cutting fluid preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810280902.3A CN108467776A (en) | 2018-04-02 | 2018-04-02 | Rust preventive cutting fluid preparation method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108467776A true CN108467776A (en) | 2018-08-31 |
Family
ID=63262359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810280902.3A Pending CN108467776A (en) | 2018-04-02 | 2018-04-02 | Rust preventive cutting fluid preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108467776A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111088106A (en) * | 2019-11-12 | 2020-05-01 | 常州海纳金属助剂有限公司 | Formula for improving aluminum alloy protection capability of metal processing liquid and preparation method |
| CN111088107A (en) * | 2019-11-12 | 2020-05-01 | 常州海纳金属助剂有限公司 | Formula for improving antirust capacity of metal working fluid and preparation method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102787008A (en) * | 2012-08-29 | 2012-11-21 | 上海宏泽化工有限公司 | Lubricating oil for aluminum alloy sawing and preparation method of lubricating oil |
| CN202590708U (en) * | 2012-05-16 | 2012-12-12 | 浩力森涂料（上海）有限公司 | Solid-liquid two-phase stirring device |
| CN103880787A (en) * | 2014-03-12 | 2014-06-25 | 江苏大学 | Method for preparing gamma-butyrrolactone and acetone through coupling reaction |
| CN106423030A (en) * | 2016-12-12 | 2017-02-22 | 郑州搜趣信息技术有限公司 | Safe and energy-saving chemical stirring kettle |
| CN210473823U (en) * | 2019-09-02 | 2020-05-08 | 叙永县鸿艺粉业有限公司 | Powdery material vibrating and stirring device |
-
2018
- 2018-04-02 CN CN201810280902.3A patent/CN108467776A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202590708U (en) * | 2012-05-16 | 2012-12-12 | 浩力森涂料（上海）有限公司 | Solid-liquid two-phase stirring device |
| CN102787008A (en) * | 2012-08-29 | 2012-11-21 | 上海宏泽化工有限公司 | Lubricating oil for aluminum alloy sawing and preparation method of lubricating oil |
| CN103880787A (en) * | 2014-03-12 | 2014-06-25 | 江苏大学 | Method for preparing gamma-butyrrolactone and acetone through coupling reaction |
| CN106423030A (en) * | 2016-12-12 | 2017-02-22 | 郑州搜趣信息技术有限公司 | Safe and energy-saving chemical stirring kettle |
| CN210473823U (en) * | 2019-09-02 | 2020-05-08 | 叙永县鸿艺粉业有限公司 | Powdery material vibrating and stirring device |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111088106A (en) * | 2019-11-12 | 2020-05-01 | 常州海纳金属助剂有限公司 | Formula for improving aluminum alloy protection capability of metal processing liquid and preparation method |
| CN111088107A (en) * | 2019-11-12 | 2020-05-01 | 常州海纳金属助剂有限公司 | Formula for improving antirust capacity of metal working fluid and preparation method |
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| SE01 | Entry into force of request for substantive examination | ||
| CB02 | Change of applicant information | ||
| CB02 | Change of applicant information |
Address after: 213119 industrial concentration area of Hengshan Town, Wujin District, Jiangsu, Changzhou Applicant after: Changzhou Haina Environmental Protection Technology Co.,Ltd. Address before: 213119 industrial concentration area of Hengshan Town, Wujin District, Jiangsu, Changzhou Applicant before: CHANGZHOU HINAR METAL WORKING CHEMICAL Co.,Ltd. |
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Application publication date: 20180831 |