CN108455527B - A kind of preparation facilities of ultra-high purity hydrogen - Google Patents

A kind of preparation facilities of ultra-high purity hydrogen Download PDF

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Publication number
CN108455527B
CN108455527B CN201810154394.4A CN201810154394A CN108455527B CN 108455527 B CN108455527 B CN 108455527B CN 201810154394 A CN201810154394 A CN 201810154394A CN 108455527 B CN108455527 B CN 108455527B
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chamber
communicated
pipeline
valve
cabinet
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CN108455527A (en
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王杰
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Shenzhen high gas Limited by Share Ltd
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Shenzhen High Gas Ltd By Share Ltd
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/32Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
    • C01B3/34Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/0205Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0211Processes for making hydrogen or synthesis gas containing a reforming step containing a non-catalytic reforming step
    • C01B2203/0216Processes for making hydrogen or synthesis gas containing a reforming step containing a non-catalytic reforming step containing a non-catalytic steam reforming step
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/12Feeding the process for making hydrogen or synthesis gas
    • C01B2203/1205Composition of the feed
    • C01B2203/1211Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
    • C01B2203/1235Hydrocarbons
    • C01B2203/1241Natural gas or methane

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)

Abstract

The invention discloses a kind of preparation facilities of ultra-high purity hydrogen, cabinet A including being fixedly arranged on ground, reaction chamber is provided in the cabinet A, the discharge chamber in the cabinet A is provided with below the reaction chamber, the gear cavity extended to the right is provided with and communicated in the reaction chamber right end wall, the gear cavity right side is provided with and communicated with valve A, the right side the valve A is provided with and communicated with pipeline B, the pipeline C extended to the right is provided with and communicated in the reaction chamber right end wall, the right side the pipeline C is provided with and communicated with valve B, the right side the valve B is provided with and communicated with pipeline D, the incubator for extending outward exterior space and protruding into the discharge chamber is provided in the reaction chamber, warm chamber is provided in the incubator, apparatus of the present invention structure is simple, it is easy to use, this device is using the structure that can control thermal response, and using suction Hydrogen compound is absorbed and is purified to hydrogen, and production efficiency is effectively increased.

Description

A kind of preparation facilities of ultra-high purity hydrogen
Technical field
The present invention relates to Hydrogen Energy source domains, and in particular to a kind of preparation facilities of ultra-high purity hydrogen.
Background technique
With the development of science and technology, social progress, country promotes always high-tech development, in traditional natural gas and water Steam is prepared in the technical field of hydrogen, and a relatively difficult technical problem is always existed, and is exactly the high-purity collection of hydrogen, And in the preparation process of high-purity hydrogen, the temperature of reaction more difficult to control, this device efficiently solves the problems, such as this.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation facilities of ultra-high purity hydrogen, and the above-mentioned of the prior art can be overcome to lack It falls into.
According to the present invention, the preparation facilities of a kind of ultra-high purity hydrogen of apparatus of the present invention, the cabinet including being fixedly arranged on ground It is provided with reaction chamber in A, the cabinet A, the discharge chamber in the cabinet A is provided with below the reaction chamber, it is described anti- It answers and is provided with and communicated with the gear cavity extended to the right in chamber right end wall, the gear cavity right side is provided with and communicated with valve A, the valve The right side door A is provided with and communicated with pipeline B, and the pipeline C extended to the right, the pipeline are provided with and communicated in the reaction chamber right end wall The right side C is provided with and communicated with valve B, and the right side the valve B is provided with and communicated with pipeline D, is provided in the reaction chamber outward Extend exterior space and protrude into the incubator of the discharge chamber, warm chamber is provided in the incubator, the temperature chamber upper end wall is fixed There is electrothermal tube, symmetrical stomata is provided with and communicated in the temperature chamber left hand end wall, the stomata is connected to the discharge chamber, It is provided with and communicated in the wall of temperature chamber left end and is provided with cabinet C, the case on the right side of the pipeline E, the pipeline E of exterior space Be provided in body C and push away chamber, the pipeline E is connected to the chamber that pushes away, it is described push away to be provided in chamber upper end wall communicated with exterior space Air chamber and gear transluminal, the chamber lower end wall that pushes away be installed with sliding rail, the sliding rail upper surface is slidably provided with sliding block, The upper end of slide block face is installed with slide bar, and the slide bar left side, which is installed with, pushes away what chamber or more end wall was slidably connected with described Push plate, the slide bar upper surface are installed with rack gear, and the upper surface the cabinet C is installed with cabinet, are provided in the cabinet downwards Opening and the gear cavity that communicates with the gear transluminal are installed with motor A in the gear cavity aft bulkhead, and the motor A's is defeated Shaft front end face is installed with gear, and the gear is engaged with the rack gear, is provided with and communicated with round in the discharge chamber right end wall, It is provided with the recycling bins fixed with the cabinet A on the right side of the round, is installed with reclaiming chamber, the reclaiming chamber in the recycling bins Left end wall is provided with and communicated with the port being connected to the round, and the curved tube for extending exterior space is installed in the reclaiming chamber, The curved tube right side is provided with and communicated with switch valve A, and the right side the switch valve A is provided with and communicated with communicating pipe A, the reclaiming chamber The communicating pipe B for extending exterior space to the right is provided with and communicated in right end wall, the right side the communicating pipe B is provided with and communicated with switch The right side valve B, the switch valve B is provided with and communicated with communicating pipe C, is provided with and communicated in the wall of the reaction chamber left end and extends to the left The left side pipeline F, the pipeline F of exterior space is provided with and communicated with air pump, and the air pump left side is provided with and communicated with pipeline G, It is provided with adsorption box on the left of the pipeline G, adsorbent chamber is provided in the adsorption box, the adsorbent chamber is connected to the pipeline G, The pipeline H for extending exterior space to the left, the connection setting of the left side the pipeline H are provided with and communicated in the wall of the adsorbent chamber left end There is valve C, the left side the valve C is provided with and communicated with pipeline I, is provided with and communicated in the adsorbent chamber lower end wall and extends outside The lower end surface pipeline J, the pipeline J in space is provided with and communicated with valve D, and the lower end surface the valve D is provided with and communicated with pipeline K, institute It states and is installed with gasket in adsorption box upper surface, the gasket upper surface, which offsets, is provided with backing plate, and the backing plate lower end surface is solid Equipped with the fixed block for protruding into the adsorbent chamber, the lower end of fixing block face bilateral symmetry is installed with connecting rod, consolidates between the connecting rod Equipped with several adsorption plates, described adsorption box or so end face is installed with symmetrical cabinet D, is provided with opening in the cabinet D Cunning chamber inwardly, far from the fixed block the sliding cavity wall in be installed with motor B, the output shaft outer surface of the motor B It is provided with the internal screw thread block being slidably connected with end wall above and below the sliding chamber, is provided with and is open outwardly in the internal screw thread block Thread cavity, the output shaft of the motor B is threadedly engaged with the thread cavity to be connect, and sound deadening shock absorption dress is provided on the motor B It sets.
Further technical solution, the electrothermal tube is Wave-shaped structural, to improve the heat transfer effect of device.
Further technical solution, internal screw thread block lower end surface and the adsorption box upper surface and the backing plate upper surface It flushes, to improve the running stability of device.
Further technical solution, the adsorption plate are to inhale hydrogen compound, inhale hydrogen compound and can absorb hydrogen, to improve The high-purity hydrogen absorption efficiency of device.
Further technical solution, the sound deadening shock absorption device include being fixed at disappearing for the two sides motor B or more Sound pad and the vibration damper plate for being fixed at the front and rear sides motor B face, the silencer pad are connected with the vibration damper plate.
The beneficial effects of the present invention are:
In the initial state due to apparatus of the present invention, the motor B, air pump and motor A are in stop working state, described Valve A, valve B, valve C, valve D, switch valve A and switch valve B are in close state, and the internal screw thread block is located at the backing plate Upper surface is conducive to maintenance and installation so that each bascule be made to be in original state.
When the device is running, the electrothermal tube work, which generates heat, makes institute after the motor A drives the gear rotation Rack gear bilateral reciprocation is stated, so that the push plate is pushed away intracavitary left and right push-and-pull described, by the gas of exterior space from the air Chamber pushes away intracavitary described in introducing, and enters in the discharge chamber along the pipeline E, warm chamber and stomata, and the switch valve A is opened, Enter cooling water in the curved tube by the communicating pipe A and switch valve A and form complete circulation, the switch valve B is opened, made Hot gas is entered in the communicating pipe B by the round, port and reclaiming chamber, and is discharged by the switch valve B and communicating pipe C, institute It states valve A and valve B to open, enters vapor in the reaction chamber by the pipeline B, valve A and pipeline A, and make natural Gas is entered in the reaction chamber by the pipeline D, valve B and pipeline C, what natural gas and vapor gave out in the electrothermal tube Generate reaction under temperature action and generate hydrogen, air pump work make the mixed gas containing hydrogen by the pipeline F, air pump and Pipeline G enters in the adsorbent chamber, the adsorption plate adsorbed hydrogen, and the valve C is opened, make mixed gas by the pipeline H, Valve C and pipeline I are passed into next device, to realize the function purified using the compound for absorbing hydrogen to hydrogen Can, effectively increase operating efficiency.
After adsorbing full hydrogen in the adsorption plate, the air pump stops working, and the valve C and valve D are opened, toward institute It states pipeline K to be passed through nitrogen and enter in the adsorbent chamber by the valve D and pipeline J, by the gaseous mixture in the adsorbent chamber Body is discharged by the pipeline H, valve C and pipeline I, and the valve C is closed, and the motor B drives the internal screw thread block to move outwardly It is dynamic, so that the internal screw thread block is moved to outermost extreme position, the adsorption plate is placed in hydrogen after the backing plate is proposed Collection device gives out the hydrogen in the adsorption plate, to improve the working efficiency of device.
After motor A work, the gear is engaged with the rack gear, and the gear drives described rack gear or so to move It is dynamic, then drive the slide bar to move left and right, the sliding block and the sliding rail are slidably connected, and the push plate pushes away on chamber described Lower end wall sliding, to improve the transmission stability of device.
Apparatus of the present invention structure is simple, easy to use, this device is hydrogenated using the structure that can control thermal response, and using inhaling It closes object hydrogen is absorbed and purified, effectively increases production efficiency.
The above, the specific embodiment only invented, but invent protection scope be not limited thereto, it is any without The change or replacement that creative work is expected are crossed, should all be covered within the protection scope of invention.Therefore, the protection scope of invention It should be determined by the scope of protection defined in the claims.
Detailed description of the invention
It, below will be to embodiment or existing in order to illustrate more clearly of inventive embodiments or technical solution in the prior art Attached drawing needed in technical description is briefly described, it should be apparent that, the accompanying drawings in the following description is only to invent Some embodiments for those of ordinary skill in the art without creative efforts, can also basis These attached drawings obtain other attached drawings.
Fig. 1 is a kind of overall structure diagram of the preparation facilities of ultra-high purity hydrogen of the invention;
Fig. 2 is the schematic diagram in the direction A in Fig. 1;
Fig. 3 is the schematic diagram in the direction B-B in Fig. 1;
Fig. 4 is the structural schematic diagram of motor B of the invention.
Specific embodiment
All features disclosed in this specification or disclosed all methods or in the process the step of, in addition to mutually exclusive Feature and/or step other than, can combine in any way.
Any feature disclosed in this specification (including any accessory claim, abstract and attached drawing), except non-specifically chatting It states, can be replaced by other alternative features that are equivalent or have similar purpose.That is, unless specifically stated, each feature is only It is an example in a series of equivalent or similar characteristics.
As shown in Figs 1-4, the preparation facilities of a kind of ultra-high purity hydrogen of the invention, the cabinet including being fixedly arranged on ground It is provided with reaction chamber 101 in A100, the cabinet A100, is provided with below the reaction chamber 101 in the cabinet A100 Discharge chamber 102, be provided with and communicated with the gear cavity 122 extended to the right, the gear cavity 122 in the 101 right end wall of reaction chamber Right side is provided with and communicated with valve A110, and the right side the valve A110 is provided with and communicated with pipeline B111, and the reaction chamber 101 is right It is provided with and communicated with the right side pipeline C109, the pipeline C109 extended to the right in end wall and is provided with and communicated with valve B107, it is described The right side valve B107 is provided with and communicated with pipeline D108, is provided in the reaction chamber 101 and extends outward exterior space and stretch Enter the incubator 104 of the discharge chamber 102, warm chamber 105 is provided in the incubator 104,105 upper end wall of temperature chamber is installed with electricity Heat pipe 113 is provided with and communicated with symmetrical stomata 103, the stomata 103 and the row in 105 left hand end wall of temperature chamber Air cavity 102 is connected to, and pipeline E125, the pipeline E125 positioned at exterior space are provided with and communicated in the 105 left end wall of temperature chamber Right side is provided with cabinet C124, is provided in the cabinet C124 and pushes away chamber 123, and the pipeline E125 is connected to the chamber 123 that pushes away, Described push away is provided with the air chamber 160 communicated with exterior space and gear transluminal 161 in 123 upper end wall of chamber, described to push away under chamber 123 End wall is installed with sliding rail 117, and 117 upper surface of sliding rail is slidably provided with sliding block 118, and 118 upper surface of sliding block is solid Equipped with slide bar 116,116 left side of slide bar is installed with and the push plate for pushing away the sliding connection of about 123 end wall of chamber 115,116 upper surface of slide bar is installed with rack gear 119, and the upper surface the cabinet C124 is installed with cabinet 121, the cabinet It is provided with gear cavity 122 that is downwardly open and communicating with the gear transluminal 161 in 121, consolidates in 122 aft bulkhead of gear cavity Equipped with motor A300, the output shaft front end face of the motor A300 is installed with gear 120, the gear 120 and the rack gear 119 It engages, is provided with and communicated with round 106 in the 102 right end wall of discharge chamber, is provided on the right side of the round 106 and the cabinet A100 fixed recycling bins 200 are installed with reclaiming chamber 201 in the recycling bins 200, and 201 left end wall of the reclaiming chamber connection is set It is equipped with the port 210 being connected to the round 106, the curved tube 202 for extending exterior space is installed in the reclaiming chamber 201, 202 right side of curved tube is provided with and communicated with switch valve A203, and the right side the switch valve A203 is provided with and communicated with communicating pipe A204 is provided with and communicated with the communicating pipe B205 for extending exterior space to the right, the communicating pipe in the 201 right end wall of reclaiming chamber The right side B205 is provided with and communicated with switch valve B208, and the right side the switch valve B208 is provided with and communicated with communicating pipe C209, described The pipeline F126 for extending exterior space to the left is provided with and communicated in 101 left end wall of reaction chamber, the left side the pipeline F126 connects Logical to be provided with air pump 127,127 left side of air pump is provided with and communicated with pipeline G128, is provided with suction on the left of the pipeline G128 Attached case 142 is provided with adsorbent chamber 146 in the adsorption box 142, and the adsorbent chamber 146 is connected to the pipeline G128, the suction The pipeline H137 for extending exterior space to the left, the connection of the left side the pipeline H137 are provided with and communicated in attached 146 left end wall of chamber It is provided with valve C139, the left side the valve C139 is provided with and communicated with pipeline I138, connection in 146 lower end wall of adsorbent chamber It is provided with and extends the lower end surface pipeline J143, the pipeline J143 of exterior space and be provided with and communicated with valve D144, the valve The lower end surface D144 is provided with and communicated with pipeline K145, is installed with gasket 129, the gasket in 142 upper surface of adsorption box 129 upper surfaces, which offset, is provided with backing plate 131, and 131 lower end surface of backing plate is installed with the fixed block for protruding into the adsorbent chamber 146 130,130 lower end surface of the fixed block bilateral symmetry is installed with connecting rod 140, is installed with several adsorption plates between the connecting rod 140 141,142 or so the end face of adsorption box is installed with symmetrical cabinet D136, and opening court is provided in the cabinet D136 Interior cunning chamber 134, far from the fixed block 130 sliding 134 inner wall of chamber in be installed with motor B135, the motor B135's Output shaft outer surface is provided with the internal screw thread block 132 with sliding about 134 end wall of the chamber sliding connection, the internal screw thread block The thread cavity 133 of opening outwardly, the output shaft of the motor B135 and 133 company of being threadedly engaged of thread cavity are provided in 132 It connects, is provided with sound deadening shock absorption device on the motor B135.
Valuably, wherein the electrothermal tube 113 is Wave-shaped structural, to improve the heat transfer effect of device.
Valuably, wherein on 132 lower end surface of internal screw thread block and 142 upper surface of adsorption box and the backing plate 131 End face, to improve the running stability of device.
Valuably, wherein the adsorption plate 141 is to inhale hydrogen compound, inhales hydrogen compound and can absorb hydrogen, to improve The high-purity hydrogen absorption efficiency of device.
Valuably, wherein the sound deadening shock absorption device includes the noise elimination for being fixed at the two sides motor B135 or more Pad 1351 and the vibration damper plate 1352 for being fixed at the front and rear sides motor B135 face, the silencer pad 1351 and the damping Plate 1352 is connected, and the sound deadening shock absorption device can reduce the noise and vibration that the motor B135 work generates.
In the initial state, the motor B135, air pump 127 and motor A300 are in the shape that stops working to apparatus of the present invention State, the valve A110, valve B107, valve C139, valve D144, switch valve A203 and switch valve B208, which are in, closes shape State, the internal screw thread block 132 are located at 131 upper surface of backing plate.
When the device is running, the work of electrothermal tube 113 generates heat, and the motor A300 drives described 120 turns of gear After dynamic, make 119 bilateral reciprocation of rack gear, the push plate 115 is made to push away left and right push-and-pull in chamber 123 described, it will be external empty Between gas from the air chamber 160 introduce it is described push away in chamber 123, and along the pipeline E125, warm chamber 105 and stomata 103 Into in the discharge chamber 102, the switch valve A203 is opened, make cooling water by the communicating pipe A204 and switch valve A203 into Enter and form complete circulation in the curved tube 202, the switch valve B208 is opened, and makes hot gas by the round 106, port 210 Enter in the communicating pipe B205 with reclaiming chamber 201, and is discharged by the switch valve B208 and communicating pipe C209, the valve A110 and valve B107 is opened, and vapor is made to enter the reaction chamber 101 by the pipeline B111, valve A110 and pipeline A112 It is interior, and enter natural gas in the reaction chamber 101 by the pipeline D108, valve B107 and pipeline C109, natural gas and water Steam generates reaction under the temperature action that the electrothermal tube 113 gives out and generates hydrogen, and the work of air pump 127 makes containing hydrogen The mixed gas of gas is entered in the adsorbent chamber 146 by the pipeline F126, air pump 127 and pipeline G128, the adsorption plate 141 Adsorbed hydrogen, the valve C139 are opened, and are passed into down mixed gas by the pipeline H137, valve C139 and pipeline I138 One device.
After adsorbing full hydrogen in the adsorption plate 141, the air pump 127 stops working, the valve C139 and valve D144 is opened, and is passed through nitrogen toward the pipeline K145 and is entered the adsorbent chamber 146 by the valve D144 and pipeline J143 It is interior, the mixed gas in the adsorbent chamber 146 is discharged by the pipeline H137, valve C139 and pipeline I138, the valve C139 is closed, and the motor B135 drives the internal screw thread block 132 to move outwardly, is moved to the internal screw thread block 132 outermost The adsorption plate 141 is placed in Hydrogen collection device after proposing the backing plate 131, by the adsorption plate by side pole extreme position Hydrogen in 141 gives out.
After motor A300 work, the gear 120 is engaged with the rack gear 119, and the gear 120 drives described Rack gear 119 moves left and right, then the slide bar 116 is driven to move left and right, the sliding block 118 and 117 company of being slidably matched of sliding rail It connects, the push plate 115 pushes away the sliding of about 123 end wall of chamber described.
The beneficial effects of the present invention are: in the initial state due to apparatus of the present invention, at the motor B, air pump and motor A In stop working state, the valve A, valve B, valve C, valve D, switch valve A and switch valve B are in close state, described Internal screw thread block is located at the backing plate upper surface, so that each bascule be made to be in original state, is conducive to maintenance and installation.
When the device is running, the electrothermal tube work, which generates heat, makes institute after the motor A drives the gear rotation Rack gear bilateral reciprocation is stated, so that the push plate is pushed away intracavitary left and right push-and-pull described, by the gas of exterior space from the air Chamber pushes away intracavitary described in introducing, and enters in the discharge chamber along the pipeline E, warm chamber and stomata, and the switch valve A is opened, Enter cooling water in the curved tube by the communicating pipe A and switch valve A and form complete circulation, the switch valve B is opened, made Hot gas is entered in the communicating pipe B by the round, port and reclaiming chamber, and is discharged by the switch valve B and communicating pipe C, institute It states valve A and valve B to open, enters vapor in the reaction chamber by the pipeline B, valve A and pipeline A, and make natural Gas is entered in the reaction chamber by the pipeline D, valve B and pipeline C, what natural gas and vapor gave out in the electrothermal tube Generate reaction under temperature action and generate hydrogen, air pump work make the mixed gas containing hydrogen by the pipeline F, air pump and Pipeline G enters in the adsorbent chamber, the adsorption plate adsorbed hydrogen, and the valve C is opened, make mixed gas by the pipeline H, Valve C and pipeline I are passed into next device, to realize the function purified using the compound for absorbing hydrogen to hydrogen Can, effectively increase operating efficiency.
After adsorbing full hydrogen in the adsorption plate, the air pump stops working, and the valve C and valve D are opened, toward institute It states pipeline K to be passed through nitrogen and enter in the adsorbent chamber by the valve D and pipeline J, by the gaseous mixture in the adsorbent chamber Body is discharged by the pipeline H, valve C and pipeline I, and the valve C is closed, and the motor B drives the internal screw thread block to move outwardly It is dynamic, so that the internal screw thread block is moved to outermost extreme position, the adsorption plate is placed in hydrogen after the backing plate is proposed Collection device gives out the hydrogen in the adsorption plate, to improve the working efficiency of device.
After motor A work, the gear is engaged with the rack gear, and the gear drives described rack gear or so to move It is dynamic, then drive the slide bar to move left and right, the sliding block and the sliding rail are slidably connected, and the push plate pushes away on chamber described Lower end wall sliding, to improve the transmission stability of device.
Apparatus of the present invention structure is simple, easy to use, this device is hydrogenated using the structure that can control thermal response, and using inhaling It closes object hydrogen is absorbed and purified, effectively increases production efficiency.
The above, the specific embodiment only invented, but invent protection scope be not limited thereto, it is any without The change or replacement that creative work is expected are crossed, should all be covered within the protection scope of invention.Therefore, the protection scope of invention It should be determined by the scope of protection defined in the claims.

Claims (5)

1. a kind of preparation facilities of ultra-high purity hydrogen is provided with reaction chamber including being fixedly arranged in the cabinet A, the cabinet A on ground, It is provided with the discharge chamber in the cabinet A below the reaction chamber, is provided with and communicated with to the right in the reaction chamber right end wall The gear cavity of extension, the gear cavity right side are provided with and communicated with valve A, and the right side the valve A is provided with and communicated with pipeline B, It is provided with and communicated with the right side pipeline C, the pipeline C extended to the right in the reaction chamber right end wall and is provided with and communicated with valve B, institute It states the right side valve B and is provided with and communicated with pipeline D, be provided in the reaction chamber and extend outward exterior space and protrude into the row The incubator of air cavity, is provided with warm chamber in the incubator, and the temperature chamber upper end wall is installed with electrothermal tube, in the temperature chamber left hand end wall It is provided with and communicated with symmetrical stomata, the stomata is connected to the discharge chamber, is provided with and communicated in the wall of temperature chamber left end It is provided with cabinet C on the right side of the pipeline E, the pipeline E of exterior space, is provided in the cabinet C and pushes away chamber, the pipeline E It is connected to the chamber that pushes away, described push away is provided with the air chamber communicated with exterior space and gear transluminal in chamber upper end wall, described to push away Chamber lower end wall is installed with sliding rail, and the sliding rail upper surface is slidably provided with sliding block, and the upper end of slide block face is installed with slide bar, The slide bar left side be installed with it is described push away chamber or more end wall sliding connection push plate, the slide bar upper surface is installed with Rack gear, the upper surface the cabinet C are installed with cabinet, are provided with downwardly open in the cabinet and communicate with the gear transluminal Gear cavity is installed with motor A in the gear cavity aft bulkhead, and the output shaft front end face of the motor A is installed with gear, the tooth Wheel is engaged with the rack gear, and round is provided with and communicated in the discharge chamber right end wall, is provided with and the case on the right side of the round Body A fixed recycling bins are installed with reclaiming chamber in the recycling bins, and reclaiming chamber left end wall is provided with and communicated with and the round The port of connection is installed with the curved tube for extending exterior space in the reclaiming chamber, and the curved tube right side is provided with and communicated with out Valve A is closed, the right side the switch valve A is provided with and communicated with communicating pipe A, is provided with and communicated in the reclaiming chamber right end wall and extends to the right The right side the communicating pipe B of exterior space out, the communicating pipe B is provided with and communicated with switch valve B, the connection of the right side the switch valve B It is provided with communicating pipe C, the pipeline F, the pipeline F for extending exterior space to the left are provided with and communicated in the wall of the reaction chamber left end Left side is provided with and communicated with air pump, and the air pump left side is provided with and communicated with pipeline G, is provided with adsorption box on the left of the pipeline G, Adsorbent chamber is provided in the adsorption box, the adsorbent chamber is connected to the pipeline G, connection setting in the wall of the adsorbent chamber left end There is the left side pipeline H, the pipeline H for extending exterior space to be to the left provided with and communicated with valve C, the left side the valve C connects It is logical to be provided with pipeline I, the lower end pipeline J, the pipeline J for extending exterior space is provided with and communicated in the adsorbent chamber lower end wall Face is provided with and communicated with valve D, and the lower end surface the valve D is provided with and communicated with pipeline K, is installed with sealing in the adsorption box upper surface Pad, the gasket upper surface, which offsets, is provided with backing plate, and the backing plate lower end surface is installed with the fixed block for protruding into the adsorbent chamber, The lower end of fixing block face bilateral symmetry is installed with connecting rod, and several adsorption plates are installed between the connecting rod, and the adsorption box is left Right side is installed with symmetrical cabinet D, and the cunning chamber of opening inwardly is provided in the cabinet D, far from the fixed block Motor B is installed in the sliding cavity wall, the output shaft outer surface of the motor B is provided with to be slided with end wall above and below the sliding chamber The internal screw thread block of mating connection is provided with the thread cavity of opening outwardly, the output shaft of the motor B and institute in the internal screw thread block It states thread cavity and is threadedly engaged connection, be provided with sound deadening shock absorption device on the motor B.
2. a kind of preparation facilities of ultra-high purity hydrogen as described in claim 1, it is characterised in that: the electrothermal tube is undaform Structure.
3. a kind of preparation facilities of ultra-high purity hydrogen as described in claim 1, it is characterised in that: internal screw thread block lower end surface It is flushed with the adsorption box upper surface and the backing plate upper surface.
4. a kind of preparation facilities of ultra-high purity hydrogen as described in claim 1, it is characterised in that: the adsorption plate is to inhale hydrogenation Object is closed, hydrogen compound is inhaled and can absorb hydrogen.
5. a kind of preparation facilities of ultra-high purity hydrogen as described in claim 1, it is characterised in that: the sound deadening shock absorption device packet The vibration damper plate for including the silencer pad for being fixed at the two sides motor B or more and being fixed at the front and rear sides motor B face, The silencer pad is connected with the vibration damper plate.
CN201810154394.4A 2018-02-23 2018-02-23 A kind of preparation facilities of ultra-high purity hydrogen Active CN108455527B (en)

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CN201810154394.4A CN108455527B (en) 2018-02-23 2018-02-23 A kind of preparation facilities of ultra-high purity hydrogen

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