CN108455527A - A kind of preparation facilities of novel super-high purity hydrogen - Google Patents
A kind of preparation facilities of novel super-high purity hydrogen Download PDFInfo
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- CN108455527A CN108455527A CN201810154394.4A CN201810154394A CN108455527A CN 108455527 A CN108455527 A CN 108455527A CN 201810154394 A CN201810154394 A CN 201810154394A CN 108455527 A CN108455527 A CN 108455527A
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- end wall
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- 239000001257 hydrogen Substances 0.000 title claims abstract description 54
- 229910052739 hydrogen Inorganic materials 0.000 title claims abstract description 54
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 32
- -1 hydrogen compound Chemical class 0.000 claims abstract description 7
- 238000001179 sorption measurement Methods 0.000 claims description 33
- 239000003463 adsorbent Substances 0.000 claims description 23
- 150000002431 hydrogen Chemical class 0.000 claims description 13
- 238000010521 absorption reaction Methods 0.000 claims description 11
- 230000035939 shock Effects 0.000 claims description 7
- 238000004064 recycling Methods 0.000 claims description 6
- 230000003584 silencer Effects 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000004044 response Effects 0.000 abstract description 3
- 239000007789 gas Substances 0.000 description 14
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 14
- 239000003345 natural gas Substances 0.000 description 7
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
- 239000004236 Ponceau SX Substances 0.000 description 4
- 238000010586 diagram Methods 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 230000002146 bilateral effect Effects 0.000 description 3
- 239000000498 cooling water Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000005611 electricity Effects 0.000 description 2
- 239000008246 gaseous mixture Substances 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000008239 natural water Substances 0.000 description 2
- 230000008439 repair process Effects 0.000 description 2
- 230000004888 barrier function Effects 0.000 description 1
- 238000013016 damping Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
- C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
- C01B3/32—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air
- C01B3/34—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide, air by reaction of hydrocarbons with gasifying agents
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/02—Processes for making hydrogen or synthesis gas
- C01B2203/0205—Processes for making hydrogen or synthesis gas containing a reforming step
- C01B2203/0211—Processes for making hydrogen or synthesis gas containing a reforming step containing a non-catalytic reforming step
- C01B2203/0216—Processes for making hydrogen or synthesis gas containing a reforming step containing a non-catalytic reforming step containing a non-catalytic steam reforming step
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
- C01B2203/12—Feeding the process for making hydrogen or synthesis gas
- C01B2203/1205—Composition of the feed
- C01B2203/1211—Organic compounds or organic mixtures used in the process for making hydrogen or synthesis gas
- C01B2203/1235—Hydrocarbons
- C01B2203/1241—Natural gas or methane
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Inorganic Chemistry (AREA)
- Separation Of Gases By Adsorption (AREA)
Abstract
The invention discloses a kind of preparation facilities of novel super-high purity hydrogen,Babinet A including being fixedly arranged on ground,It is provided with reaction chamber in the babinet A,It is provided with the discharge chamber in the babinet A below the reaction chamber,It is provided with and communicated with the gear cavity extended to the right in the reaction chamber right end wall,The gear cavity right side is provided with and communicated with valve A,The right sides the valve A are provided with and communicated with pipeline B,The pipeline C extended to the right is provided with and communicated in the reaction chamber right end wall,The right sides the pipeline C are provided with and communicated with valve B,The right sides the valve B are provided with and communicated with pipeline D,The incubator for extending outward exterior space and stretching into the discharge chamber is provided in the reaction chamber,Warm chamber is provided in the incubator,Apparatus of the present invention are simple in structure,It is easy to use,This device is using the structure that can control thermal response,And hydrogen is absorbed and purified using hydrogen compound is inhaled,Effectively increase production efficiency.
Description
Technical field
The present invention relates to Hydrogen Energy source domains, and in particular to a kind of preparation facilities of novel super-high purity hydrogen.
Background technology
With the development of science and technology, social progress, country promotes always high-tech development, in traditional natural gas and water
Steam is prepared in the technical field of hydrogen, and a relatively difficult technical barrier is always existed, and is exactly the high-purity collection of hydrogen,
And in the preparation process of high-purity hydrogen, the temperature of reaction more difficult to control, this device efficiently solves the problems, such as this.
Invention content
The purpose of the present invention is to provide a kind of preparation facilities of novel super-high purity hydrogen, can overcome the upper of the prior art
State defect.
According to the present invention, a kind of preparation facilities of novel super-high purity hydrogen of apparatus of the present invention, including it is fixedly arranged on ground
It is provided with reaction chamber in babinet A, the babinet A, the discharge chamber in the babinet A, institute are provided with below the reaction chamber
It states and is provided with and communicated with the gear cavity extended to the right in reaction chamber right end wall, the gear cavity right side is provided with and communicated with valve A, institute
It states the right sides valve A and is provided with and communicated with pipeline B, the pipeline C extended to the right is provided with and communicated in the reaction chamber right end wall, it is described
The right sides pipeline C are provided with and communicated with the right sides valve B, the valve B and are provided with and communicated with pipeline D, are provided in the reaction chamber
It extends outward exterior space and stretches into the incubator of the discharge chamber, warm chamber, the temperature chamber upper end wall are provided in the incubator
It is installed with electrothermal tube, symmetrical stomata, the stomata and the discharge chamber are provided with and communicated in the temperature chamber left hand end wall
It is connected to, is provided with and communicated in the temperature chamber left end wall and is provided with babinet C on the right side of the pipeline E, the pipeline E of exterior space,
It is provided in the babinet C and pushes away chamber, the pipeline E is connected to the chamber that pushes away, and described push away is provided with and outside sky in chamber upper end wall
Between identical air chamber and gear transluminal, the chamber lower end wall that pushes away is installed with sliding rail, and the sliding rail upper surface is slidably arranged
There is a sliding block, the upper end of slide block face is installed with slide bar, and the slide bar left side is installed with to push away the sliding of chamber or more end wall and match with described
The push plate of connection is closed, the slide bar upper surface is installed with rack, and the upper surfaces the babinet C are installed with babinet, are set in the babinet
It is equipped with gear cavity downwardly open and identical with the gear transluminal, motor A, the electricity are installed in the gear cavity aft bulkhead
The output shaft front end face of machine A is installed with gear, and the gear is engaged with the rack, connection setting in the discharge chamber right end wall
Have a round, be provided on the right side of the round with the fixed recycling bins of babinet A, be installed with reclaiming chamber in the recycling bins, institute
It states reclaiming chamber left end wall and is provided with and communicated with the port being connected to the round, be installed in the reclaiming chamber and extend exterior space
Curved tube, the curved tube right side is provided with and communicated with the right sides switch valve A, the switch valve A and is provided with and communicated with communicating pipe A, institute
The communicating pipe B for being provided with and communicated in reclaiming chamber right end wall and extending exterior space to the right is stated, the connection of the right sides the communicating pipe B is set
Be equipped with the right sides switch valve B, the switch valve B and be provided with and communicated with communicating pipe C, be provided with and communicated in the reaction chamber left end wall to
The left sides pipeline F, the pipeline F connection setting of exterior space is extended due to air pump in a left side, and the air pump left side connection is set
Be equipped with pipeline G, adsorption box be provided on the left of the pipeline G, be provided with adsorbent chamber in the adsorption box, the adsorbent chamber with it is described
Pipeline G is connected to, and the pipeline H for extending exterior space to the left, the pipeline H left ends are provided with and communicated in the adsorbent chamber left end wall
Face is provided with and communicated with the left sides valve C, the valve C and is provided with and communicated with pipeline I, is provided with and communicated in the adsorbent chamber lower end wall
The lower faces pipeline J, the pipeline J for extending exterior space are provided with and communicated with the connection setting of the lower faces valve D, the valve D
There is pipeline K, gasket is installed in the adsorption box upper surface, the gasket upper surface, which offsets, is provided with backing plate, the pad
Plate lower face is installed with the fixed block for stretching into the adsorbent chamber, and the fixed block lower face is symmetrical to be installed with connecting rod, described
It is installed with several adsorption plates between connecting rod, described adsorption box or so end face is installed with symmetrical babinet D, in the babinet D
It is provided with the cunning chamber of opening inwardly, is installed with motor B in the sliding cavity wall far from the fixed block, the motor B's is defeated
Shaft outer surface is provided with the internal thread block being slidably connected with end wall above and below the sliding chamber, is provided in the internal thread block
The thread cavity of opening outwardly, the output shaft of the motor B connect with the thread cavity screw-thread fit, are provided on the motor B
Sound deadening shock absorption device.
Further technical solution, the electrothermal tube is Wave-shaped structural, to improve the heat transfer effect of device.
Further technical solution, internal thread block lower face and the adsorption box upper surface and the backing plate upper surface
It flushes, to improve the running stability of device.
Further technical solution, the adsorption plate are to inhale hydrogen compound, inhale hydrogen compound and can absorb hydrogen, to improve
The high-purity hydrogen absorption efficiency of device.
Further technical solution, the sound deadening shock absorption device include being fixed at disappearing for the both sides motor B or more
Sound pad and the vibration damper plate for being fixed at the front and rear sides motor B face, the silencer pad are connected with the vibration damper plate.
The beneficial effects of the invention are as follows：
In the initial state due to apparatus of the present invention, the motor B, air pump and motor A are in stop working state, the valve
A, valve B, valve C, valve D, switch valve A and switch valve B are closed, and the internal thread block is located at the backing plate upper end
Face is conducive to repair and installation to make each bascule be in original state.
When device is run, the electrothermal tube work generates heat makes institute after the motor A drives the gear rotation
Rack bilateral reciprocation is stated, so that the push plate is pushed away intracavitary or so push-and-pull described, by the gas of exterior space from the air
Chamber pushes away intracavitary described in introducing, and enters in the discharge chamber along the pipeline E, warm chamber and stomata, and the switch valve A is opened,
So that cooling water is entered in the curved tube by the communicating pipe A and switch valve A and form complete cycle, the switch valve B is opened, made
Hot gas is entered by the round, port and reclaiming chamber in the communicating pipe B, and is discharged by the switch valve B and communicating pipe C, institute
It states valve A and valve B is opened, vapor is made to be entered in the reaction chamber by the pipeline B, valve A and pipeline A, and make natural
Gas is entered by the pipeline D, valve B and pipeline C in the reaction chamber, what natural gas gave out with vapor in the electrothermal tube
Generate reaction under temperature action and generate hydrogen, air pump work make the mixed gas containing hydrogen by the pipeline F, air pump and
Pipeline G enters in the adsorbent chamber, the adsorption plate adsorbed hydrogen, and the valve C is opened, make mixed gas by the pipeline H,
Valve C and pipeline I are passed into next device, to realize the work(purified to hydrogen using the compound for absorbing hydrogen
Can, effectively increase operating efficiency.
After adsorbing full hydrogen in the adsorption plate, the air pump is stopped, and the valve C and valve D are opened, toward institute
It states pipeline K to be passed through nitrogen and by the valve D and pipeline J enter in the adsorbent chamber, by the gaseous mixture in the adsorbent chamber
Body is closed by the pipeline H, valve C and pipeline I discharges, the valve C, and the motor B drives the internal thread block to move outwardly
It is dynamic, so that the internal thread block is moved to outermost extreme position, the adsorption plate is positioned over hydrogen after the backing plate is proposed
Collection device gives out the hydrogen in the adsorption plate, to improve the working efficiency of device.
After the motor A works, the gear is engaged with the rack, and the gear drives described rack or so to move
It is dynamic, then drive the slide bar to move left and right, the sliding block is slidably connected with the sliding rail, and the push plate is pushed away described on chamber
Lower end wall slides, to improve the transmission stability of device.
Apparatus of the present invention are simple in structure, easy to use, this device is hydrogenated using the structure that can control thermal response, and using inhaling
It closes object hydrogen is absorbed and purified, effectively increases production efficiency.
The above, the specific implementation mode only invented, but invent protection domain be not limited thereto, it is any without
The change or replacement that creative work is expected are crossed, should all be covered within the protection domain of invention.Therefore, the protection domain of invention
It should be determined by the scope of protection defined in the claims.
Description of the drawings
It, below will be to embodiment or existing in order to illustrate more clearly of inventive embodiments or technical solution in the prior art
Attached drawing is briefly described needed in technology description, it should be apparent that, the accompanying drawings in the following description is only to invent
Some embodiments for those of ordinary skill in the art without creative efforts, can also basis
These attached drawings obtain other attached drawings.
Fig. 1 is a kind of overall structure diagram of the preparation facilities of novel super-high purity hydrogen of the present invention；
Fig. 2 is the schematic diagram in the directions A in Fig. 1；
Fig. 3 is the schematic diagram in the directions B-B in Fig. 1；
Fig. 4 is the structural schematic diagram of the motor B of the present invention.
Specific implementation mode
All features disclosed in this specification or disclosed all methods or in the process the step of, in addition to mutually exclusive
Feature and/or step other than, can combine in any way.
This specification（Including any accessory claim, abstract and attached drawing）Disclosed in any feature, except non-specifically chatting
It states, can be replaced by other alternative features that are equivalent or have similar purpose.That is, unless specifically stated, each feature is only
It is an example in a series of equivalent or similar characteristics.
As shown in Figs 1-4, the preparation facilities of a kind of novel super-high purity hydrogen of the invention, including it is fixedly arranged on the babinet on ground
Reaction chamber 101 is provided in A100, the babinet A100,101 lower section of the reaction chamber is provided in the babinet A100
Discharge chamber 102, be provided with and communicated with the gear cavity 122 extended to the right, the gear cavity 122 in 101 right end wall of the reaction chamber
Right side is provided with and communicated with the right sides valve A110, the valve A110 and is provided with and communicated with pipeline B111, and the reaction chamber 101 is right
It is provided with and communicated with the right sides pipeline C109, the pipeline C109 extended to the right in end wall and is provided with and communicated with valve B107, it is described
The right sides valve B107 are provided with and communicated with pipeline D108, are provided in the reaction chamber 101 and extend outward exterior space and stretch
Enter the incubator 104 of the discharge chamber 102, warm chamber 105 is provided in the incubator 104,105 upper end wall of temperature chamber is installed with electricity
Heat pipe 113 is provided with and communicated with symmetrical stomata 103, the stomata 103 and the row in 105 left hand end wall of temperature chamber
Air cavity 102 is connected to, and pipeline E125, the pipeline E125 positioned at exterior space are provided with and communicated in 105 left end wall of the temperature chamber
Right side, which is provided with to be provided in babinet C124, the babinet C124, pushes away chamber 123, and the pipeline E125 is connected to the chamber 123 that pushes away,
Described push away is provided with air chamber 160 identical with exterior space and gear transluminal 161 in 123 upper end wall of chamber, described to push away under chamber 123
End wall is installed with sliding rail 117, and 117 upper surface of the sliding rail is slidably provided with sliding block 118, and 118 upper surface of the sliding block is solid
Equipped with slide bar 116,116 left side of the slide bar is installed with and the push plate for pushing away the sliding connection of about 123 end wall of chamber
115,116 upper surface of the slide bar is installed with rack 119, and the upper surfaces the babinet C124 are installed with babinet 121, the babinet
It is provided with gear cavity 122 downwardly open and identical with the gear transluminal 161 in 121, consolidates in 122 aft bulkhead of the gear cavity
Equipped with motor A300, the output shaft front end face of the motor A300 is installed with gear 120, the gear 120 and the rack 119
It engages, round 106 is provided with and communicated in 102 right end wall of the discharge chamber, 106 right side of the round is provided with and the babinet
The fixed recycling bins 200 of A100, reclaiming chamber 201 is installed in the recycling bins 200, and the connection of 201 left end wall of the reclaiming chamber is set
It is equipped with the port 210 being connected to the round 106, the curved tube 202 for extending exterior space is installed in the reclaiming chamber 201,
202 right side of the curved tube is provided with and communicated with the right sides switch valve A203, the switch valve A203 and is provided with and communicated with communicating pipe
A204 is provided with and communicated with the communicating pipe B205 for extending exterior space to the right, the communicating pipe in 201 right end wall of the reclaiming chamber
The right sides B205 are provided with and communicated with the right sides switch valve B208, the switch valve B208 and are provided with and communicated with communicating pipe C209, described
The left sides pipeline F126, the pipeline F126 company for extending exterior space to the left is provided with and communicated in 101 left end wall of reaction chamber
Logical to be arranged due to air pump 127,127 left side of the air pump is provided with and communicated on the left of pipeline G128, the pipeline G128 and is provided with
Adsorption box 142 is provided with adsorbent chamber 146 in the adsorption box 142, and the adsorbent chamber 146 is connected to the pipeline G128, described
The left sides pipeline H137, the pipeline H137 company for extending exterior space to the left is provided with and communicated in 146 left end wall of adsorbent chamber
It is logical to be provided with the left sides valve C139, the valve C139 and be provided with and communicated with pipeline I138, connect in 146 lower end wall of the adsorbent chamber
Logical be provided with extends the lower faces pipeline J143, the pipeline J143 of exterior space and is provided with and communicated with valve D144, the valve
The lower faces door D144 are provided with and communicated with pipeline K145, and gasket 129, the sealing are installed in 142 upper surface of the adsorption box
It pads 129 upper surfaces and offsets and be provided with backing plate 131,131 lower face of the backing plate is installed with the fixed block for stretching into the adsorbent chamber 146
130,130 lower face of the fixed block is symmetrical to be installed with connecting rod 140, and several adsorption plates are installed between the connecting rod 140
141,142 or so end face of the adsorption box is installed with symmetrical babinet D136, and opening court is provided in the babinet D136
Interior cunning chamber 134 is installed with motor B135 in 134 inner wall of sliding chamber far from the fixed block 130, the motor B135's
Output shaft outer surface is provided with the internal thread block 132 being slidably connected with about 134 end wall of the sliding chamber, the internal thread block
The thread cavity 133 of opening outwardly is provided in 132, output shaft and 133 screw-thread fit of the thread cavity of the motor B135 connect
It connects, sound deadening shock absorption device is provided on the motor B135.
Valuably, wherein the electrothermal tube 113 is Wave-shaped structural, to improve the heat transfer effect of device.
Valuably, wherein on 132 lower face of internal thread block and 142 upper surface of the adsorption box and the backing plate 131
End face, to improve the running stability of device.
Valuably, wherein the adsorption plate 141 is to inhale hydrogen compound, inhales hydrogen compound and can absorb hydrogen, to improve
The high-purity hydrogen absorption efficiency of device.
Valuably, wherein the sound deadening shock absorption device includes the noise elimination for being fixed at the both sides motor B135 or more
Pad 1351 and the vibration damper plate 1352 for being fixed at the front and rear sides motor B135 face, the silencer pad 1351 and the damping
Plate 1352 is connected, and the sound deadening shock absorption device can reduce the noise and vibrations that the motor B135 work generates.
In the initial state, the motor B135, air pump 127 and motor A300 are in the shape that is stopped to apparatus of the present invention
State, the valve A110, valve B107, valve C139, valve D144, switch valve A203 and switch valve B208, which are in, closes shape
State, the internal thread block 132 are located at 131 upper surface of the backing plate.
When device is run, the work of the electrothermal tube 113 generates heat, and the motor A300 drives 120 turns of the gear
After dynamic, make 119 bilateral reciprocation of the rack, the push plate 115 is made to push away left and right push-and-pull in chamber 123 described, it will be external empty
Between gas from the air chamber 160 introduce it is described push away in chamber 123, and along the pipeline E125, warm chamber 105 and stomata 103
Into in the discharge chamber 102, the switch valve A203 is opened, make cooling water by the communicating pipe A204 and switch valve A203 into
Enter and form complete cycle in the curved tube 202, the switch valve B208 is opened, and makes hot gas by the round 106, port 210
Enter in the communicating pipe B205 with reclaiming chamber 201, and is discharged by the switch valve B208 and communicating pipe C209, the valve
A110 and valve B107 are opened, and vapor is made to enter the reaction chamber 101 by the pipeline B111, valve A110 and pipeline A112
It is interior, and natural gas is made to be entered in the reaction chamber 101 by the pipeline D108, valve B107 and pipeline C109, natural gas and water
Steam generates reaction under the temperature action that the electrothermal tube 113 gives out and generates hydrogen, and the work of the air pump 127 makes containing hydrogen
The mixed gas of gas is entered by the pipeline F126, air pump 127 and pipeline G128 in the adsorbent chamber 146, the adsorption plate 141
Adsorbed hydrogen, the valve C139 are opened, and mixed gas is made to be passed into down by the pipeline H137, valve C139 and pipeline I138
One device.
After absorption completely hydrogen in the adsorption plate 141, the air pump 127 is stopped, the valve C139 and valve
D144 is opened, and is passed through nitrogen toward the pipeline K145 and is entered the adsorbent chamber 146 by the valve D144 and pipeline J143
It is interior, by the mixed gas in the adsorbent chamber 146 by the pipeline H137, valve C139 and pipeline I138 discharges, the valve
C139 is closed, and the motor B135 drives the internal thread block 132 to move outwardly, so that the internal thread block 132 is moved to outermost
The adsorption plate 141 is positioned over Hydrogen collection device, by the adsorption plate by side pole extreme position after proposing the backing plate 131
Hydrogen in 141 gives out.
After the motor A300 works, the gear 120 is engaged with the rack 119, and the gear 120 drives described
Rack 119 moves left and right, then the slide bar 116 is driven to move left and right, the sliding block 118 and 117 company of being slidably matched of the sliding rail
It connects, the push plate 115 pushes away the sliding of about 123 end wall of chamber described.
The beneficial effects of the invention are as follows：In the initial state due to apparatus of the present invention, at the motor B, air pump and motor A
In stop working state, the valve A, valve B, valve C, valve D, switch valve A and switch valve B are closed, described
Internal thread block is located at the backing plate upper surface, to make each bascule be in original state, is conducive to repair and installation.
When device is run, the electrothermal tube work generates heat makes institute after the motor A drives the gear rotation
Rack bilateral reciprocation is stated, so that the push plate is pushed away intracavitary or so push-and-pull described, by the gas of exterior space from the air
Chamber pushes away intracavitary described in introducing, and enters in the discharge chamber along the pipeline E, warm chamber and stomata, and the switch valve A is opened,
So that cooling water is entered in the curved tube by the communicating pipe A and switch valve A and form complete cycle, the switch valve B is opened, made
Hot gas is entered by the round, port and reclaiming chamber in the communicating pipe B, and is discharged by the switch valve B and communicating pipe C, institute
It states valve A and valve B is opened, vapor is made to be entered in the reaction chamber by the pipeline B, valve A and pipeline A, and make natural
Gas is entered by the pipeline D, valve B and pipeline C in the reaction chamber, what natural gas gave out with vapor in the electrothermal tube
Generate reaction under temperature action and generate hydrogen, air pump work make the mixed gas containing hydrogen by the pipeline F, air pump and
Pipeline G enters in the adsorbent chamber, the adsorption plate adsorbed hydrogen, and the valve C is opened, make mixed gas by the pipeline H,
Valve C and pipeline I are passed into next device, to realize the work(purified to hydrogen using the compound for absorbing hydrogen
Can, effectively increase operating efficiency.
After adsorbing full hydrogen in the adsorption plate, the air pump is stopped, and the valve C and valve D are opened, toward institute
It states pipeline K to be passed through nitrogen and by the valve D and pipeline J enter in the adsorbent chamber, by the gaseous mixture in the adsorbent chamber
Body is closed by the pipeline H, valve C and pipeline I discharges, the valve C, and the motor B drives the internal thread block to move outwardly
It is dynamic, so that the internal thread block is moved to outermost extreme position, the adsorption plate is positioned over hydrogen after the backing plate is proposed
Collection device gives out the hydrogen in the adsorption plate, to improve the working efficiency of device.
After the motor A works, the gear is engaged with the rack, and the gear drives described rack or so to move
It is dynamic, then drive the slide bar to move left and right, the sliding block is slidably connected with the sliding rail, and the push plate is pushed away described on chamber
Lower end wall slides, to improve the transmission stability of device.
Apparatus of the present invention are simple in structure, easy to use, this device is hydrogenated using the structure that can control thermal response, and using inhaling
It closes object hydrogen is absorbed and purified, effectively increases production efficiency.
The above, the specific implementation mode only invented, but invent protection domain be not limited thereto, it is any without
The change or replacement that creative work is expected are crossed, should all be covered within the protection domain of invention.Therefore, the protection domain of invention
It should be determined by the scope of protection defined in the claims.
Claims (5)
1. a kind of preparation facilities of novel super-high purity hydrogen, including be fixedly arranged in the babinet A, the babinet A on ground and be provided with instead
Chamber is answered, the discharge chamber in the babinet A is provided with below the reaction chamber, is provided with and communicated in the reaction chamber right end wall
The gear cavity extended to the right, the gear cavity right side are provided with and communicated with the right sides valve A, the valve A and are provided with and communicated with pipe
Road B is provided with and communicated with the right sides pipeline C, the pipeline C extended to the right in the reaction chamber right end wall and is provided with and communicated with valve
The right side B, the valve B is provided with and communicated with pipeline D, is provided in the reaction chamber and extends outward exterior space and stretch into institute
The incubator of discharge chamber is stated, warm chamber is provided in the incubator, the temperature chamber upper end wall is installed with electrothermal tube, described temperature chamber or so end
Symmetrical stomata is provided with and communicated in wall, the stomata is connected to the discharge chamber, is connected to and is set in the temperature chamber left end wall
It is equipped with to be provided with to be provided in babinet C, the babinet C on the right side of the pipeline E, the pipeline E of exterior space and pushes away chamber, the pipe
Road E is connected to the chamber that pushes away, and described push away is provided with air chamber identical with exterior space and gear transluminal in chamber upper end wall, described
It pushes away chamber lower end wall and is installed with sliding rail, the sliding rail upper surface is slidably provided with sliding block, and the upper end of slide block face is installed with cunning
Bar, the slide bar left side be installed with the push plate for pushing away the sliding connection of chamber or more end wall, the slide bar upper surface is solid
Equipped with rack, the upper surfaces the babinet C are installed with babinet, be provided in the babinet it is downwardly open and with the gear transluminal phase
With gear cavity, be installed with motor A in the gear cavity aft bulkhead, the output shaft front end face of the motor A is installed with gear, institute
It states gear to engage with the rack, round is provided with and communicated in the discharge chamber right end wall, the round right side is provided with and institute
State the fixed recycling bins of babinet A, be installed with reclaiming chamber in the recycling bins, the reclaiming chamber left end wall be provided with and communicated with it is described
The port of round connection is installed with the curved tube for extending exterior space, the curved tube right side connection setting in the reclaiming chamber
There are the right sides switch valve A, the switch valve A to be provided with and communicated with communicating pipe A, is provided with and communicated with to the right in the reclaiming chamber right end wall
Extend the communicating pipe B of exterior space, the right sides the communicating pipe B are provided with and communicated with the right sides switch valve B, the switch valve B
It is provided with and communicated with communicating pipe C, the pipeline F for extending exterior space to the left is provided with and communicated in the reaction chamber left end wall, it is described
The connection of the left sides pipeline F is arranged due to air pump, and the air pump left side is provided with and communicated on the left of pipeline G, the pipeline G and is provided with
Adsorption box is provided with adsorbent chamber in the adsorption box, and the adsorbent chamber is connected to the pipeline G, in the adsorbent chamber left end wall
It is provided with and communicated with and extends the left sides pipeline H, the pipeline H of exterior space to the left and be provided with and communicated with valve C, the valve C
Left side is provided with and communicated with pipeline I, and the pipeline J for extending exterior space is provided with and communicated in the adsorbent chamber lower end wall, described
The lower faces pipeline J are provided with and communicated with the lower faces valve D, the valve D and are provided with and communicated with pipeline K, in the adsorption box upper surface
It is installed with gasket, the gasket upper surface, which offsets, is provided with backing plate, and the backing plate lower face, which is installed with, stretches into the absorption
The fixed block of chamber, the fixed block lower face is symmetrical to be installed with connecting rod, and several adsorption plates, institute are installed between the connecting rod
It states adsorption box or so end face and is installed with symmetrical babinet D, the cunning chamber of opening inwardly is provided in the babinet D, far from institute
State be installed in the sliding cavity wall of fixed block motor B, the motor B output shaft outer surface be provided with on the sliding chamber
The internal thread block of lower end wall sliding connection is provided with the thread cavity of opening outwardly in the internal thread block, the motor B's
Output shaft is connect with the thread cavity screw-thread fit, and sound deadening shock absorption device is provided on the motor B.
2. a kind of preparation facilities of novel super-high purity hydrogen as described in claim 1, it is characterised in that：The electrothermal tube is wave
Wave type structure.
3. a kind of preparation facilities of novel super-high purity hydrogen as described in claim 1, it is characterised in that：Under the internal thread block
End face is flushed with the adsorption box upper surface and the backing plate upper surface.
4. a kind of preparation facilities of novel super-high purity hydrogen as described in claim 1, it is characterised in that：The adsorption plate is to inhale
Hydrogen compound inhales hydrogen compound and can absorb hydrogen.
5. a kind of preparation facilities of novel super-high purity hydrogen as described in claim 1, it is characterised in that：The sound deadening shock absorption dress
It sets the silencer pad including being fixed at the both sides motor B or more and is fixed at subtracting for the front and rear sides motor B face
Plate is shaken, the silencer pad is connected with the vibration damper plate.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810154394.4A CN108455527B (en) | 2018-02-23 | 2018-02-23 | A kind of preparation facilities of ultra-high purity hydrogen |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810154394.4A CN108455527B (en) | 2018-02-23 | 2018-02-23 | A kind of preparation facilities of ultra-high purity hydrogen |
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| CN108455527B CN108455527B (en) | 2019-03-08 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1186769A (en) * | 1996-12-23 | 1998-07-08 | 株式会社油公 | Natural gas-using hydrogen generator |
| US5932181A (en) * | 1996-12-23 | 1999-08-03 | Yukong Limited | Natural gas-using hydrogen generator |
| US20030092780A1 (en) * | 1999-12-28 | 2003-05-15 | Jostein Sogge | Method and plant for production of oxygenated hydrocarbons |
| CN206069359U (en) * | 2016-08-31 | 2017-04-05 | 四川北方红光特种化工有限公司 | A kind of middle pressure cabinet of natural gas hydrogen preparation |
-
2018
- 2018-02-23 CN CN201810154394.4A patent/CN108455527B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1186769A (en) * | 1996-12-23 | 1998-07-08 | 株式会社油公 | Natural gas-using hydrogen generator |
| US5932181A (en) * | 1996-12-23 | 1999-08-03 | Yukong Limited | Natural gas-using hydrogen generator |
| US20030092780A1 (en) * | 1999-12-28 | 2003-05-15 | Jostein Sogge | Method and plant for production of oxygenated hydrocarbons |
| CN206069359U (en) * | 2016-08-31 | 2017-04-05 | 四川北方红光特种化工有限公司 | A kind of middle pressure cabinet of natural gas hydrogen preparation |
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|---|---|
| CN108455527B (en) | 2019-03-08 |
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Effective date of registration: 20190202 Address after: 518118 No.9A Niusheng Road, Xiuxin Industrial Zone, Kengzi Street, Pingshan New District, Shenzhen City, Guangdong Province Applicant after: Shenzhen high gas Limited by Share Ltd Address before: 321300 No. 865 Huajie Town, Yongkang City, Jinhua City, Zhejiang Province Applicant before: Wang Jie |
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