CN108452746A - High-tower melting granulation technique under a kind of high humidity high-heat environment - Google Patents
High-tower melting granulation technique under a kind of high humidity high-heat environment Download PDFInfo
- Publication number
- CN108452746A CN108452746A CN201711380109.2A CN201711380109A CN108452746A CN 108452746 A CN108452746 A CN 108452746A CN 201711380109 A CN201711380109 A CN 201711380109A CN 108452746 A CN108452746 A CN 108452746A
- Authority
- CN
- China
- Prior art keywords
- mixing channel
- level
- phosphorus ammonium
- tower
- composite fertilizer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/02—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops
- B01J2/04—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by dividing the liquid material into drops, e.g. by spraying, and solidifying the drops in a gaseous medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/10—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic in stationary drums or troughs, provided with kneading or mixing appliances
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
Abstract
High-tower melting granulation technique under a kind of high humidity high-heat environment, is as follows：A, the phosphorus ammonium of 25 15 5 raw material total amount 23 33% of composite fertilizer is divided into three parts；It B, will be in the urea and first part of molten slot of phosphorus ammonium mixing addition urea in composite fertilizer 25 15 5；C, potash fertilizer, calcium powder and second part of phosphorus ammonium are added in level-one mixing channel, and urea is melted into the mixture in slot and is squeezed into level-one mixing channel；D, monoammonium, dry ammonium and third part phosphorus ammonium are added in two level mixing channel, and the mixture in level-one mixing channel is squeezed into two level mixing channel；E, the mixture in two level mixing channel is squeezed into sprinkling pelleting machine, is completed by high tower cooler, i.e. high-tower melting granulation after the completion of granulation.The present invention is suitable under 6 September south high humidity hot environments, by technique adjustment, so that slurry slurrying is uniformly mixed and is granulated sprinkling uniformly, improve balling ratio and cooling effect, effectively prevent fertilizer adhesion bottom of tower.
Description
Technical field
The present invention relates to fertilizer manufacture fields, and in particular to high-tower melting granulation technique under a kind of high humidity high-heat environment.
Background technology
Currently, high tower smelting process is affected by weather humidity and temperature, factory of many high tower meltings composite fertilizer is forced in
Summer stops production, and summer is the crucial moment for producing Autumn-sown wheat fertilizer.High tower melts composite fertilizer's slurry from differential comminutor spray orifice
Middle injection, under the action of gravity, surface tension, air drag, composite fertilizer's fluid column fragments into drop, drop size and spray orifice ruler
Very little, nozzle rotary speed and slurry physical property are related.Drop side contraction edge during decline cools down, and becomes approximation when dropping down onto bottom of tower
Spherical particle.On tower in descent, decline initial stage forms drop and shrinks cooled and solidified composite fertilizer's slurry, and declines the later stage
Fertiliser granulates show hygroscopicity, particle surface easily moisture absorption under high humidity hot conditions, are particularly easy to viscous bottom of tower.
Invention content
The purpose of the present invention provides high-tower melting granulation technique under a kind of high humidity high-heat environment aiming at above-mentioned deficiency.
The present invention is as follows：
A, the phosphorus ammonium of composite fertilizer 25-15-5 raw materials total amount 29% is divided into three parts, first part of phosphorus ammonium is composite fertilizer's 25-15-5 raw materials
The 5% of total amount, second part of phosphorus ammonium are the 12% of composite fertilizer 25-15-5 raw material total amounts, and third part phosphorus ammonium is composite fertilizer's 25-15-5 raw materials
The 12% of total amount；
B, by the urea and first part of molten slot of phosphorus ammonium mixing addition urea in composite fertilizer 25-15-5, urinating temperature in molten slot is
115-125℃；
C, potash fertilizer, calcium powder and second part of phosphorus ammonium being added in level-one mixing channel, temperature is 105-110 DEG C in level-one mixing channel, and
Urea is melted the mixture in slot to squeeze into level-one mixing channel；
D, monoammonium, dry ammonium and third part phosphorus ammonium are added in two level mixing channel, and temperature is 95-100 DEG C in two level mixing channel, and by one
Mixture in grade mixing channel is squeezed into two level mixing channel,
E, the mixture in two level mixing channel is squeezed into sprinkling pelleting machine, outer 29 revs/min of the rotary speed of sprinkling pelleting machine sprays simultaneously
10-20 revs/min of rotary speed in comminutor is drenched, is completed by high tower cooler, i.e. high-tower melting granulation after the completion of granulation.
The urea melts slot, level-one mixing channel and two level mixing channel and is all made of steam heating.
It is an advantage of the invention that：1, stable yields brings benefits under summer high humidity hot conditions；2, technique adjustment is simple, be not required into
Row equipment technological transformation；3, prilling temperature reduces, and fertiliser granulates is made to be easy to cooling fixed line, and granule strength improves；4, two level mixing is reduced
Slot steam consumption, effectively reduces cost；5, finished granule rate improves, and effectively prevent viscous bottom of tower.The present invention is suitable for the month south 6-9
Under high humidity hot environment, by technique adjustment, so that slurry slurrying is uniformly mixed and to be granulated sprinkling uniform, improve balling ratio and
Cooling effect effectively prevent fertilizer adhesion bottom of tower.
Specific implementation method
The present invention is as follows：
A, the phosphorus ammonium of composite fertilizer 25-15-5 raw materials total amount 29% is divided into three parts, first part of phosphorus ammonium is composite fertilizer's 25-15-5 raw materials
The 5% of total amount, second part of phosphorus ammonium are the 12% of composite fertilizer 25-15-5 raw material total amounts, and third part phosphorus ammonium is composite fertilizer's 25-15-5 raw materials
The 12% of total amount；
B, by the urea and first part of molten slot of phosphorus ammonium mixing addition urea in composite fertilizer 25-15-5, urinating temperature in molten slot is
115-125℃；
C, potash fertilizer, calcium powder and second part of phosphorus ammonium being added in level-one mixing channel, temperature is 105-110 DEG C in level-one mixing channel, and
Urea is melted the mixture in slot to squeeze into level-one mixing channel；
D, monoammonium, dry ammonium and third part phosphorus ammonium are added in two level mixing channel, and temperature is 95-100 DEG C in two level mixing channel, and by one
Mixture in grade mixing channel is squeezed into two level mixing channel,
E, the mixture in two level mixing channel is squeezed into sprinkling pelleting machine, outer 29 revs/min of the rotary speed of sprinkling pelleting machine sprays simultaneously
10-20 revs/min of rotary speed in comminutor is drenched, is completed by high tower cooler, i.e. high-tower melting granulation after the completion of granulation.
The urea melts slot, level-one mixing channel and two level mixing channel and is all made of steam heating.
Claims (2)
1. high-tower melting granulation technique under a kind of high humidity high-heat environment, it is characterised in that be as follows：
A, the phosphorus ammonium of composite fertilizer 25-15-5 raw material total amounts 23-33% is divided into three parts, first part of phosphorus ammonium is composite fertilizer 25-15-5 former
Expect that the 3-5% of total amount, second part of phosphorus ammonium are the 10-14% of composite fertilizer 25-15-5 raw material total amounts, third part phosphorus ammonium is composite fertilizer 25-
The 10-14% of 15-5 raw material total amounts；
B, by the urea and first part of molten slot of phosphorus ammonium mixing addition urea in composite fertilizer 25-15-5, urinating temperature in molten slot is
115-125℃；
C, potash fertilizer, calcium powder and second part of phosphorus ammonium being added in level-one mixing channel, temperature is 105-110 DEG C in level-one mixing channel, and
Urea is melted the mixture in slot to squeeze into level-one mixing channel；
D, monoammonium, dry ammonium and third part phosphorus ammonium are added in two level mixing channel, and temperature is 95-100 DEG C in two level mixing channel, and by one
Mixture in grade mixing channel is squeezed into two level mixing channel,
E, the mixture in two level mixing channel is squeezed into sprinkling pelleting machine, outer 29 revs/min of the rotary speed of sprinkling pelleting machine sprays simultaneously
10-20 revs/min of rotary speed in comminutor is drenched, is completed by high tower cooler, i.e. high-tower melting granulation after the completion of granulation.
2. high-tower melting granulation technique under a kind of high humidity high-heat environment according to claim 1, it is characterised in that the urine
The molten slot of element, level-one mixing channel and two level mixing channel are all made of steam heating.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711380109.2A CN108452746A (en) | 2017-12-20 | 2017-12-20 | High-tower melting granulation technique under a kind of high humidity high-heat environment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711380109.2A CN108452746A (en) | 2017-12-20 | 2017-12-20 | High-tower melting granulation technique under a kind of high humidity high-heat environment |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108452746A true CN108452746A (en) | 2018-08-28 |
Family
ID=63221202
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711380109.2A Pending CN108452746A (en) | 2017-12-20 | 2017-12-20 | High-tower melting granulation technique under a kind of high humidity high-heat environment |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108452746A (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000000452A1 (en) * | 1998-06-29 | 2000-01-06 | Kemira Agro Oy | A process for the preparation of compound fertilizer granules |
| CN100537489C (en) * | 2006-08-31 | 2009-09-09 | 广东拉多美化肥有限公司 | Method for producing compound fertilizer by high tower granulating |
| CN102432401A (en) * | 2011-09-02 | 2012-05-02 | 史丹利化肥股份有限公司 | Tower-granulated slow-release long-acting sulfenyl nitrogen and phosphorus compound fertilizer and preparation method thereof |
| CN102584395A (en) * | 2012-02-15 | 2012-07-18 | 瓮福（集团）有限责任公司 | Method for producing urea-based compound fertilizer by high tower granulation |
| CN102826889A (en) * | 2012-09-21 | 2012-12-19 | 史丹利化肥股份有限公司 | Polymorphic nitro-compound fertilizer and production method thereof |
| CN102826890A (en) * | 2012-09-21 | 2012-12-19 | 史丹利化肥股份有限公司 | Efficient polymorphous fertilizer special for vegetables and preparation method thereof |
| CN104671948A (en) * | 2013-12-02 | 2015-06-03 | 湖北新洋丰肥业股份有限公司 | Novel prilling-tower process compound fertilizer |
| CN106008003A (en) * | 2016-05-31 | 2016-10-12 | 史丹利化肥扶余有限公司 | High tower granulation produced high concentration compound fertilizer and production method thereof |
| CN106831080A (en) * | 2015-12-04 | 2017-06-13 | 山东永大肥业有限公司 | A kind of production technology of high tower Huolisu complex fertilizer |
-
2017
- 2017-12-20 CN CN201711380109.2A patent/CN108452746A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2000000452A1 (en) * | 1998-06-29 | 2000-01-06 | Kemira Agro Oy | A process for the preparation of compound fertilizer granules |
| CN100537489C (en) * | 2006-08-31 | 2009-09-09 | 广东拉多美化肥有限公司 | Method for producing compound fertilizer by high tower granulating |
| CN102432401A (en) * | 2011-09-02 | 2012-05-02 | 史丹利化肥股份有限公司 | Tower-granulated slow-release long-acting sulfenyl nitrogen and phosphorus compound fertilizer and preparation method thereof |
| CN102584395A (en) * | 2012-02-15 | 2012-07-18 | 瓮福（集团）有限责任公司 | Method for producing urea-based compound fertilizer by high tower granulation |
| CN102826889A (en) * | 2012-09-21 | 2012-12-19 | 史丹利化肥股份有限公司 | Polymorphic nitro-compound fertilizer and production method thereof |
| CN102826890A (en) * | 2012-09-21 | 2012-12-19 | 史丹利化肥股份有限公司 | Efficient polymorphous fertilizer special for vegetables and preparation method thereof |
| CN104671948A (en) * | 2013-12-02 | 2015-06-03 | 湖北新洋丰肥业股份有限公司 | Novel prilling-tower process compound fertilizer |
| CN106831080A (en) * | 2015-12-04 | 2017-06-13 | 山东永大肥业有限公司 | A kind of production technology of high tower Huolisu complex fertilizer |
| CN106008003A (en) * | 2016-05-31 | 2016-10-12 | 史丹利化肥扶余有限公司 | High tower granulation produced high concentration compound fertilizer and production method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN100475752C (en) | Production method and equipment for highly effective slow releasing compound fertilizer and product | |
| CN104529674B (en) | A kind of humic acid special fertilizer for sweet potato and preparation method thereof | |
| CN102633553B (en) | Method for producing high-tower ammonium phosphate compound fertilizer | |
| CN102826890B (en) | Efficient polymorphous fertilizer special for vegetables and preparation method thereof | |
| CN103193533B (en) | Method for improving and stabilizing high tower nitro sulfenyl composite fertilizer product | |
| CN101367682B (en) | Method for preparing complex fertilizer with mutual solution slip tubular reactor | |
| CN104710213A (en) | Rounded grain potash fertilizer production method | |
| CN101648838B (en) | Method for producing granular ammonium sulfate by using crystalline ammonium sulfate or powdery ammonium sulfate | |
| CN104058891A (en) | Microelement-rich compound coated fertilizer for crops and preparation method of compound coated fertilizer | |
| CN101165012B (en) | High tower slow release composite fertilizer containing ureaformaldehyde and producing method thereof | |
| CN102320876B (en) | Tower granulation slow release long-acting nitrogen phosphorus potassium compound fertilizer and preparation method thereof | |
| CN107986874A (en) | A kind of method of watery fusion technique productions high tower fertilizer | |
| CN102816019B (en) | Fertilizer special for canola | |
| CN109134065A (en) | A method of granular pattern compound fertilizer is produced without steam granulation using potassium fulvate | |
| CN101768025B (en) | Method for producing sulfur fertilizer by diammonium phosphate device | |
| CN105237066A (en) | Synergistic urea ammonium nitrogen fertilizer and preparation method of same | |
| CN101439999B (en) | Apparatus for improving nitrogen content of spray granulation compound fertilizer and method for producing high-nitrogen compound fertilizer | |
| CN102267830A (en) | Method for reducing biuret content in high tower melting granulated compound fertilizer | |
| CN101125784A (en) | Fused mass granulating technique for composite fertilizer | |
| CN104387156B (en) | A kind of improvement technique producing spheric granules nitrogen-phosphorus-potassium compound fertilizer based on Nitro Phosphate Unit | |
| CN101805235B (en) | Sulfur-coated urea fertilizer and preparation method thereof | |
| CN108452746A (en) | High-tower melting granulation technique under a kind of high humidity high-heat environment | |
| CN111018627A (en) | Composite fertilizer containing polymorphic nitrogen and manufacturing method thereof | |
| CN101857476A (en) | Method for preparing compound fertilizer by adopting low-temperature fertilizer slurry pelleting | |
| CN109134134A (en) | A method of humic acid composite fertilizer granulating and forming is improved using surfactant |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180828 |
|
| WD01 | Invention patent application deemed withdrawn after publication |