CN108423922A - A kind of resource recovery device for source-separated urine - Google Patents

A kind of resource recovery device for source-separated urine Download PDF

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Publication number
CN108423922A
CN108423922A CN201810114173.4A CN201810114173A CN108423922A CN 108423922 A CN108423922 A CN 108423922A CN 201810114173 A CN201810114173 A CN 201810114173A CN 108423922 A CN108423922 A CN 108423922A
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solenoid valve
water
source
pump
urine
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任武昂
金鹏康
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Shaanxi Huifeng Yueshui Circulation Technology Co., Ltd.
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Xian University of Science and Technology
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Priority to CN201810114173.4A priority Critical patent/CN108423922A/en
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/45Phosphates containing plural metal, or metal and ammonium
    • C01B25/451Phosphates containing plural metal, or metal and ammonium containing metal and ammonium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/80Compositional purity
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/001Processes for the treatment of water whereby the filtration technique is of importance
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/44Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/441Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by reverse osmosis
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/44Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis
    • C02F1/444Treatment of water, waste water, or sewage by dialysis, osmosis or reverse osmosis by ultrafiltration or microfiltration
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/50Treatment of water, waste water, or sewage by addition or application of a germicide or by oligodynamic treatment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5236Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
    • C02F1/5254Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using magnesium compounds and phosphoric acid for removing ammonia
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F1/5281Installations for water purification using chemical agents
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • C02F2001/5218Crystallization
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/10Inorganic compounds
    • C02F2101/105Phosphorus compounds
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00Nature of the contaminant
    • C02F2101/10Inorganic compounds
    • C02F2101/16Nitrogen compounds, e.g. ammonia
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/005Black water originating from toilets
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Treatment Of Water By Oxidation Or Reduction (AREA)

Abstract

A kind of resource recovery device for source-separated urine, urine passes through the Biological Pretreatment system of immobilization first, film separation system is then passed through to recycle the water resource in urine, the water source of recycling is carried out carrying out pressurization storage after ozonization, decoloration, is recycled, the treatment effect that urine minimizing can be realized while completion water resource recycling, reduces follow-up nitrogen reclamation of phosphorus resource system scale;Concentrated water caused by UF membrane enters resource recovering system, by series of steps such as depth hydrolysis, adding of agent, guanite precipitation, crystallized product dehydrations, obtains solid nitrogen and phosphorus element recovery product;Waste liquid after nutriment recycles is discharged into Slow Rate Land Treatment System, improves active microorganism quantity in water, the effect of enhanced hydrolysis rate can be realized by being transported to pretreatment system.The present invention realizes the recycling synchronous with phosphorus and nitrogen of water resource in urine, and recovery product impurity is few.

Description

A kind of resource recovery device for source-separated urine
Technical field
The invention belongs to technical field of sewage, more particularly to a kind of resource recovery device for source-separated urine.
Background technology
Research data shows, the nitrogen containing 8000~10000mg/L and 700~2000mg/L P elements in urine. Think that the slops such as urine are a kind of pollutants according to current theory, needs a large amount of water source to go to rinse, water is caused to provide The huge waste in source and N, P nutriment.Since the nutriments such as nitrogen phosphorus are the important components of fertilizer, by the nutrients in urine Matter is recycled, and on the one hand can solve the problems, such as that sewage treatment plant inflow nitrogen and phosphorus load is high, improves effluent quality;Another party The product in face, recycling can be used as agricultural production fertilizer, realize recycling for resource.
Currently, in urine there are mainly three types of nutrient recovery technologies:(1) phosphorus is individually recycled, for example uses ammonium magnesium phosphate Recycling of the chemical precipitation method to phosphorus from urine;(2) nitrogen is individually recycled, for example the ammonia in sewage has been recycled using ion-exchange Nitrogen individually recycles urea in urine using isobutanediurea (IBDU);(3) the synchronous recycling of nitrogen phosphorus, for example divide completely in urea Solution generates stable fertilizer phosphorus to combine synchronous recycling nitrogen phosphorus with other methods using magnesium ammonium phosphate sediment method on the basis of ammonia nitrogen Sour ammonium magnesium (guanite), recyclable about 90% nitrogen of this method and 98% phosphorus.
It is the best choosing that nutrient recycles in urine that magnesium ammonium phosphate sediment method, which synchronizes recycling nitrogen phosphorus, in three of the above method It selects, but the application of this method must be set up on the basis of a large amount of decomposition and inversions of the urea in urine.Under natural conditions, fresh urine Quadrafos in liquid can be quickly resolve into PO (in 1 day)4 3-;When the closed placement of freshly voided urine, it is non-that urea is converted into ammonia nitrogen Often difficult, even if standing time is up to 20 days, conversion ratio is generally less than 25%.Therefore, how to accelerate urea in urine to be converted into The rate of ammonia nitrogen becomes the key factor that magnesium ammonium phosphate sediment method synchronizes recycling nitrogen phosphorus.The patent of auspicious et al. the applications of Fu Jin (CN201010168444.8) method is the pH that NaOH is added and adjusts urine, subsequent dosing, stirring precipitation;Dong Liang fly et al. application Patent (CN201110037688.7) method be can be certain by closed standing long period, these methods after urine collecting Promote the urea in urine to be converted into ammonia nitrogen in degree, but also has prodigious defect on hydrolysis rate and final effect, it is practical It is ineffective in application process.The method of the hydrolysis of urea of most effective promotion is to add urine enzyme, and research data shows to contain in urine enzyme Under conditions of amount is 50mg/l, 85% urea can be converted into ammonia nitrogen in 8 hours in urine, but since urine enzyme is very expensive, limit The large-scale application of this method is made.
Invention content
In order to overcome the disadvantages of the above prior art, the purpose of the present invention is to provide a kind of moneys for source-separated urine Source retracting device, urine by the Biological Pretreatment system of immobilization, then pass through film separation system to the water in urine first Resource is recycled, and is carried out carrying out pressurization storage after ozonization, decoloration to the water source of recycling, be recycled, completes water resource and return The treatment effect that urine minimizing can be realized while receipts reduces follow-up nitrogen reclamation of phosphorus resource system scale;Produced by UF membrane Concentrated water enter resource recovering system, by depth hydrolysis, adding of agent, guanite precipitation, crystallized product dehydration etc. it is a series of Step obtains solid nitrogen and phosphorus element recovery product;Waste liquid after nutriment recycles is discharged at slow rate soil Reason system improves active microorganism quantity in water, the effect of enhanced hydrolysis rate can be realized by being transported to pretreatment system Fruit.
To achieve the goals above, the technical solution adopted by the present invention is:
A kind of resource recovery device for source-separated urine, including:
Pretreatment system:Including packed bed 1, electric blowdown valve 3 is arranged in 1 bottom of packed bed, and source-separated urine enters filler Bed 1, then enter film separation system through 2 pressurization of Pipeline lift pump;
Film separation system:Simultaneously including sequentially connected level-one microfiltration equipment 4, two level microfiltration equipment 5, high-pressure pump 6 and two groups The entrance of the RO membrane components 7 of connection, level-one microfiltration equipment 4 is connect with the outlet of elevator pump 2;
Regenerated water utilizing system:Including the disinfecting reactor 8 that decolourizes, the water purification detached through RO membrane components 7 is anti-from decoloration disinfection It answers the lower part of device 8 to enter, is discharged, recycled water pressure vessel 10 spare into recycled water pressure vessel 10 after 9 pressurization of boosted pump On pressure sensor 11 is installed, disperser of the ozone caused by ozone generator 12 through 8 bottom of disinfecting reactor of decolourizing Mixing, disinfection, decoloring reaction are carried out with water purification;
Resource recovering system:Including having the hydrolysis reactor 15 there are two independent storage space, set in each storage space It is equipped with floating ball type liquid-level meter 16, the concentrated water detached through RO membrane components 7 is passed through respectively described in solenoid valve 1, the entrance of solenoid valve 2 14 After the dope after hydrolysis flows separately through solenoid valve 3 17, solenoid valve 4 18, belt stirrer is delivered to by pipeline pump 19 for storage space 21 struvite crystallization reactor 20, struvite crystallization reactor 20 quantify adding equipment 22 and solid phosphorus equipped with solid magnesium salts Salt quantifies adding equipment 23, and crystallized product is discharged into micropore rotary drum sieving equipment 24 to product by 20 bottom of struvite crystallization reactor It is recycled;Supernatant enters slow land treatment system 25 in struvite crystallization reactor 20, is received by 25 bottom of slow land treatment system The processing water of collection is transmitted back in the packed bed 1 of pretreatment system.
The residence time of the packed bed 1 be 12~for 24 hours, the fiberfill of built-in Wire pulling, volume accounts for the 1/3 of bed body ~1/2;The lift of Pipeline lift pump 2 is 20~30m;Electric blowdown valve 3 is set as by PLC auto-controlled timing switchs, program It is every to open 1min for 24 hours.
The precision of the level-one microfiltration equipment 4 is 5 μm, and the precision of two level microfiltration equipment 5 is 1 μm, the lift 80 of high-pressure pump 6 The producing water ratio of~120m, RO membrane component 7 is 50~70%, and desalting efficiency is not less than 90%.
The residence time of the decoloration disinfecting reactor 8 is 20~30min;Ozone dosage is 8~10mg/l, using rigid Beautiful aeration head;The lift of elevator pump 9 is 50~60m, and recycled water pressure vessel 10 uses water supply tank of atmospheric pressure, dischargeable capacity to be not less than 50L, 0.4~0.6MPa of working pressure range, 0~1MPa of range of pressure sensor 11;The air source of ozone generator 12 uses Air, yield are 1~2g/h.
The solenoid valve 1, solenoid valve 2 14, solenoid valve 3 17 and solenoid valve 4 18 are all made of normally closed solenoid valve, hydrolysis Two independent dope storage spaces total residence time is 48h in reactor 15, and the lift of pipeline pump 19 is 8~10m;Guanite The residence time of crystallization reactor 20 is 60min, and blender 21 is screw mixing paddle, the reaction that Blade height is 1/2~2/3 Device is high;Solid magnesium salts quantifies adding equipment 22 and solid microcosmic salt quantifies the metering of adding equipment 23 and adds process and be all made of direct current tune Speed motor is realized;Micropore rotary drum sieving equipment 24 selects the stainless steel mesh of 300~500 mesh to recycle product.
The filtering velocity of the slow land treatment system 25 is 3~5m/d, and 1.2~1.5m of thickness of filter bed, top uses perforated pipe equal Even water distribution, using the gravel layer of 30~50cm as collection water layer, the water after filter being collected into is transported to filling out for pretreatment system for bottom Expect in bed 1.
The elevator pump 9 is automatically controlled using PLC, and the method for operation is:After pressure sensor reaches setting high level, promoted It is out of service to pump 9;Pipeline lift pump 2 and high-pressure pump 6 stop after continuing to run with 5min, and ozone generator 12 continues to run with 10min After stop;After pressure sensor 11 reaches setting low value, elevator pump 9, Pipeline lift pump 2 and high-pressure pump 6 start simultaneously, ozone Generator 12 lags 5min and starts.
The independent storage space alternate run of the hydrolysis reactor 15 stores urine, and by floating ball type liquid-level meter 16 real Now automatically control:When liquid level is in low spot, corresponding solenoid valve 1 or solenoid valve 2 14 are opened, closing is corresponding to it Solenoid valve 3 17 or solenoid valve 4 18;When liquid level is in high point, corresponding solenoid valve 1 or solenoid valve two are closed 14, open corresponding solenoid valve 3 17 or solenoid valve 4 18.
The filtering layer of the slow land treatment system 25 uses fertile soil, 80~100d all to replace once, can be used for soil on the spot Earth returning to the field, greening;Water distributor of perforating uses 32 drip irrigation hoses of Φ, spacing 30cm to be improved by slow land treatment system 25 living in water The quantity of property microorganism, strenuous primary treatment system hydrolysis effect.
Compared with prior art, the beneficial effects of the invention are as follows:
1, this method realizes the recycling synchronous with phosphorus and nitrogen of water resource in urine.
2, the nutriment recovery product impurity of this method is few, quality is high.
3, this method treatment technology it is ripe, it can be achieved that different scales, occasion application.
Description of the drawings
Fig. 1 is schematic structural view of the invention.
Specific implementation mode
The embodiment that the present invention will be described in detail with reference to the accompanying drawings and examples.
As shown in Figure 1, a kind of resource recovery device for source-separated urine of the invention, including:
Pretreatment system:Including packed bed 1, electric blowdown valve 3 is arranged in 1 bottom of packed bed, and source-separated urine enters filler Bed 1, then enter film separation system through 2 pressurization of Pipeline lift pump;
Film separation system:Simultaneously including sequentially connected level-one microfiltration equipment 4, two level microfiltration equipment 5, high-pressure pump 6 and two groups The RO membrane components 7 of connection, the urine after preprocessed system pressurization sequentially enter level-one microfiltration equipment 4 and two level microfiltration equipment 5, into After the processing of row micro-filtration, then send to RO membrane components 7 and detach through high-pressure pump 6;
Regenerated water utilizing system:Including the disinfecting reactor 8 that decolourizes, the water purification detached through RO membrane components 7 is anti-from decoloration disinfection It answers the lower part of device 8 to enter, is discharged, recycled water pressure vessel 10 spare into recycled water pressure vessel 10 after 9 pressurization of boosted pump On pressure sensor 11 is installed, disperser of the ozone caused by ozone generator 12 through 8 bottom of disinfecting reactor of decolourizing Mixing, disinfection, decoloring reaction are carried out with water purification;
Resource recovering system:Including having the hydrolysis reactor 15 there are two independent storage space, set in each storage space It is equipped with floating ball type liquid-level meter 16, the concentrated water detached through RO membrane components 7 is passed through respectively described in solenoid valve 1, the entrance of solenoid valve 2 14 After the dope after hydrolysis flows separately through solenoid valve 3 17, solenoid valve 4 18, belt stirrer is delivered to by pipeline pump 19 for storage space 21 struvite crystallization reactor 20, struvite crystallization reactor 20 quantify adding equipment 22 and solid phosphorus equipped with solid magnesium salts Salt quantifies adding equipment 23, and crystallized product is discharged into micropore rotary drum sieving equipment 24 to product by 20 bottom of struvite crystallization reactor It is recycled;Supernatant enters slow land treatment system 25 in struvite crystallization reactor 20, is received by 25 bottom of slow land treatment system The processing water of collection is transmitted back in the packed bed 1 of pretreatment system.
During present invention process, following parameter and specific setting can be taken:
The residence time of packed bed 1 be 12~for 24 hours, the fiberfill of built-in Wire pulling, volume accounts for the 1/3~1/ of bed body 2;The lift of Pipeline lift pump 2 is 20~30m;By PLC auto-controlled timing switchs, program is set as per for 24 hours electric blowdown valve 3 Open 1min.
The precision of level-one microfiltration equipment 4 is 5 μm, and the precision of two level microfiltration equipment 5 is 1 μm, the lift 80 of high-pressure pump 6~ The producing water ratio of 120m, RO membrane component 7 is 50~70%, and desalting efficiency is not less than 90%.
The residence time of decoloration disinfecting reactor 8 is 20~30min;Ozone dosage is 8~10mg/l, is exposed using corundum Gas head;The lift of elevator pump 9 is 50~60m, and recycled water pressure vessel 10 uses water supply tank of atmospheric pressure, dischargeable capacity to be not less than 50L, 0.4~0.6MPa of working pressure range, 0~1MPa of range of pressure sensor 11;The air source of ozone generator 12 uses air, Yield is 1~2g/h.
Solenoid valve 1, solenoid valve 2 14, solenoid valve 3 17 and solenoid valve 4 18 are all made of normally closed solenoid valve, hydrolysis Two independent dope storage spaces total residence time is 48h in device 15, and the lift of pipeline pump 19 is 8~10m;Struvite crystallization The residence time of reactor 20 is 60min, and blender 21 is screw mixing paddle, the reactor that Blade height is 1/2~2/3 It is high;Solid magnesium salts quantifies adding equipment 22 and solid microcosmic salt quantifies the metering of adding equipment 23 and adds process and be all made of DC speed regulation Motor is realized;Micropore rotary drum sieving equipment 24 selects the stainless steel mesh of 300~500 mesh to recycle product.
The filtering velocity of slow land treatment system 25 is 3~5m/d, and 1.2~1.5m of thickness of filter bed, top uses the uniform cloth of perforated pipe Water, using the gravel layer of 30~50cm as collection water layer, the water after filter being collected into is transported to the packed bed 1 of pretreatment system for bottom It is interior.
Elevator pump 9 is automatically controlled using PLC, and the method for operation is:After pressure sensor reaches setting high level, elevator pump 9 It is out of service;Pipeline lift pump 2 and high-pressure pump 6 stop after continuing to run with 5min, and ozone generator 12 stops after continuing to run with 10min Only;After pressure sensor 11 reaches setting low value, elevator pump 9, Pipeline lift pump 2 and high-pressure pump 6 start simultaneously, and ozone occurs Device 12 lags 5min and starts.
The independent storage space alternate run of hydrolysis reactor 15 stores urine, and is realized certainly by floating ball type liquid-level meter 16 Dynamic control:When liquid level is in low spot, corresponding solenoid valve 1 or solenoid valve 2 14 are opened, corresponding electricity is closed Magnet valve 3 17 or solenoid valve 4 18;When liquid level is in high point, corresponding solenoid valve 1 or solenoid valve 2 14 are closed, is opened Open corresponding solenoid valve 3 17 or solenoid valve 4 18.
The filtering layer of slow land treatment system 25 uses fertile soil, 80~100d all to replace once, can be used for soil on the spot also Field, greening;Water distributor of perforating uses 32 drip irrigation hoses of Φ, spacing 30cm that it is micro- to improve activity in water by slow land treatment system 25 Biomass, strenuous primary treatment system hydrolysis effect.
Specific embodiment:By the 400L urines being collected into be delivered to processing capacity be 50L/h invention device in, obtain as Lower result:
To sum up, the present invention realizes the recycling synchronous with phosphorus and nitrogen of water resource in urine, and recovery product is miscellaneous Matter is few.In addition, the automatic control level of the present apparatus is high, it is aided with automatic program appropriate and can reach unattended operation.

Claims (9)

1. a kind of resource recovery device for source-separated urine, which is characterized in that including:
Pretreatment system:Including packed bed (1), electric blowdown valve (3) is arranged in packed bed (1) bottom, and source-separated urine, which enters, to be filled out Expect bed (1), then enters film separation system through Pipeline lift pump (2) pressurization;
Film separation system:Including sequentially connected level-one microfiltration equipment (4), two level microfiltration equipment (5), high-pressure pump (6) and two groups RO membrane components (7) in parallel, the entrance of level-one microfiltration equipment (4) are connect with the outlet of elevator pump (2);
Regenerated water utilizing system:Including decoloration disinfecting reactor (8), the water purification through RO membrane components (7) separation is anti-from decoloration disinfection It answers the lower part of device (8) to enter, is discharged, regeneration water pressure spare into recycled water pressure vessel (10) after boosted pump (9) pressurization Pressure sensor (11) is installed, ozone is through the disinfecting reactor (8) that decolourizes caused by ozone generator (12) on storage tank (10) The disperser of bottom carries out mixing, disinfection, decoloring reaction with water purification;
Resource recovering system:Including having the hydrolysis reactor (15) there are two independent storage space, it is arranged in each storage space Have floating ball type liquid-level meter (16), through RO membrane components (7) separation concentrated water respectively pass through solenoid valve one (13), solenoid valve two (14) into Enter the storage space, it is defeated by pipeline pump (19) after the dope after hydrolysis flows separately through solenoid valve three (17), solenoid valve four (18) It send to the struvite crystallization reactor (20) of belt stirrer (21), struvite crystallization reactor (20) is quantitative equipped with solid magnesium salts Adding equipment (22) and solid microcosmic salt quantify adding equipment (23), and crystallized product is discharged by struvite crystallization reactor (20) bottom Micropore rotary drum sieving equipment (24) recycles product;Struvite crystallization reactor (20) interior supernatant enters slow rate system It unites (25), is transmitted back to by the processing water of slow land treatment system (25) bottom collection in the packed bed (1) of pretreatment system.
2. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the packed bed (1) Residence time be 12~for 24 hours, the fiberfill of built-in Wire pulling, volume accounts for the 1/3~1/2 of bed body;Pipeline lift pumps (2) Lift be 20~30m;By PLC auto-controlled timing switchs, program is set as every and opens 1min for 24 hours electric blowdown valve (3).
3. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the level-one micro-filtration is set The precision of standby (4) is 5 μm, and the precision of two level microfiltration equipment (5) is 1 μm, lift 80~120m, the RO membrane component of high-pressure pump (6) (7) producing water ratio is 50~70%, and desalting efficiency is not less than 90%.
4. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the decoloration disinfection is anti- It is 20~30min to answer the residence time of device (8);Ozone dosage is 8~10mg/l, using corundum aeration head;Elevator pump (9) Lift is 50~60m, and recycled water pressure vessel (10) uses water supply tank of atmospheric pressure, dischargeable capacity to be not less than 50L, working pressure range 0.4~0.6MPa, 0~1MPa of range of pressure sensor (11);The air source of ozone generator (12) uses air, yield 1 ~2g/h.
5. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the solenoid valve one (13), solenoid valve two (14), solenoid valve three (17) and solenoid valve four (18) are all made of normally closed solenoid valve, in hydrolysis reactor (15) Two independent dope storage spaces total residence time is 48h, and the lift of pipeline pump (19) is 8~10m;Struvite crystallization is reacted The residence time of device (20) is 60min, and blender (21) is screw mixing paddle, the reactor that Blade height is 1/2~2/3 It is high;Solid magnesium salts quantifies adding equipment (22) and solid microcosmic salt quantifies the metering of adding equipment (23) and adds process and be all made of direct current Speed regulating motor is realized;Micropore rotary drum sieving equipment (24) selects the stainless steel mesh of 300~500 mesh to recycle product.
6. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the slow rate system The filtering velocity of (25) of uniting is 3~5m/d, 1.2~1.5m of thickness of filter bed, and top uses perforated pipe water distribution uniformity, bottom using 30~ As collection water layer, the water after filter being collected into is transported in the packed bed (1) of pretreatment system the gravel layer of 50cm.
7. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the elevator pump (9) It is automatically controlled using PLC, the method for operation is:After pressure sensor reaches setting high level, elevator pump (9) is out of service;Pipeline Elevator pump (2) and high-pressure pump (6) stop after continuing to run with 5min, and ozone generator (12) stops after continuing to run with 10min;Work as pressure After force snesor (11) reaches setting low value, elevator pump (9), Pipeline lift pump (2) and high-pressure pump (6) start simultaneously, ozone hair Raw device (12) lags 5min and starts.
8. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the hydrolysis reactor (15) independent storage space alternate run stores urine, and is automatically controlled by floating ball type liquid-level meter (16) to realize:Work as liquid level When in low spot, corresponding solenoid valve one (13) or solenoid valve two (14) are opened, corresponding solenoid valve three is closed (17) or solenoid valve four (18);When liquid level is in high point, corresponding solenoid valve one (13) or solenoid valve two (14) are closed, Open corresponding solenoid valve three (17) or solenoid valve four (18).
9. being used for the resource recovery device of source-separated urine according to claim 1, which is characterized in that the slow rate system The filtering layer of system (25) uses fertile soil, 80~100d all to replace once, can be used for soil returning to the field on the spot, afforest;Perforation water distribution Pipe uses 32 drip irrigation hoses of Φ, spacing 30cm to improve the quantity of active microorganism in water by slow land treatment system (25), strengthens Pretreatment system hydrolysis effect.
CN201810114173.4A 2018-02-05 2018-02-05 A kind of resource recovery device for source-separated urine Pending CN108423922A (en)

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CN109912155A (en) * 2019-03-20 2019-06-21 中国农业大学 A kind of integrated technology and application method of livestock and poultry liquid dung harmless treatment
CN111453800A (en) * 2020-04-10 2020-07-28 北京交通大学 Membrane distillation system and method for urine resource recovery
CN113023817A (en) * 2021-03-08 2021-06-25 北京林业大学 Reactor, system and method for urine in-situ resource recovery

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CN109912155A (en) * 2019-03-20 2019-06-21 中国农业大学 A kind of integrated technology and application method of livestock and poultry liquid dung harmless treatment
CN111453800A (en) * 2020-04-10 2020-07-28 北京交通大学 Membrane distillation system and method for urine resource recovery
CN113023817A (en) * 2021-03-08 2021-06-25 北京林业大学 Reactor, system and method for urine in-situ resource recovery
CN113023817B (en) * 2021-03-08 2022-06-24 北京林业大学 Reactor, system and method for urine in-situ resource recovery

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