CN108402231A - One kind is relieved inflammation or internal heat moistening dryness for relaxing bowels health protection tea and preparation method thereof - Google Patents
One kind is relieved inflammation or internal heat moistening dryness for relaxing bowels health protection tea and preparation method thereof Download PDFInfo
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- A23F3/00—Tea; Tea substitutes; Preparations thereof
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- A61K36/185—Magnoliopsida (dicotyledons)
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Abstract
It relieves inflammation or internal heat moistening dryness for relaxing bowels health protection tea and preparation method thereof the invention discloses one kind, in terms of composition by weight, including：Big bitter sub- 30 40 parts of fruit, 30 40 parts of the sub- fruit of small hardship, 30 40 parts of dioecism momordica root, 5 10 parts of lophatherum gracile, 10 15 parts of asparagus fern, 20 25 parts of Radix Ophiopogonis, 10 15 parts of American Ginseng, 30 35 parts of radix scrophulariae, 20 25 parts of dendrobium devonianum, 10 15 parts of lily, 15 20 parts of Radix Astragali, 40 50 parts of green tea, 70 90 parts of dextrin, 210 270 parts of sucrose.The present invention is the health protection tea that constipation is treated caused by having the deficiency of Yin and yang constipation as a result,.According to clinical empirical summary and the market demand, the effect of the more preferable health protection tea for playing the moistening dryness for relaxing bowels that relieves inflammation or internal heat, the present invention uses advanced preparation process, extracts each medicine active principle to greatest extent, meanwhile, simple for process, practical, reasonable design is convenient for industrialized production.
Description
Technical field
It relieves inflammation or internal heat moistening dryness for relaxing bowels health protection tea and preparation method thereof the present invention relates to health tea technical field more particularly to one kind.
Background technology
Constipation is a kind of complicated symptom that clinic is extremely common, both can be a kind of independent disease, can also be primarily referred to as
Defecation frequency is reduced, excrement amount is reduced, excrement amount is dry and hard, defecation is laborious etc..Clinical is mainly irritant laxative, profit using drug
Slip cathartic or bulk cathartic, but be used for a long time to generate and rely on and curative effect of medication declines, can only solve it is for the moment tired, seriously
Influence the quality of life of patient.As the saying goes, Diet cures more than the doctors, accordingly, it is desirable to provide a kind of constipation-relieving tea of integration of drinking and medicinal herbs, to
Raising relieve inflammation or internal heat, moisturize, the effect of defaecation.
The daily defecation of normal person 1~2 time or 2~3 days defecations 1 time, defecation is less than 2 times constipation patient weekly, and defecation
Arduously, the scleroma of excrement matter, the few constipation of amount are the common symptoms of the elderly, and constipation occurs in about 1/3 the elderly, seriously affects life matter
Amount.Motherland's medicine is early to this disease to be recognized, and Chinese medicine thinks that this disease has the difference of body ressitance weakened while pathogenic factors prevailing.Deficiency of vital energy sun is weak, pushes powerless or cloudy
Empty blood is few, intestinal dryness constipation induced, can be described as yin constipation；Real heat phlegm wet stops up knot or the stagnation of the circulation of vital energy is not all right into constipation, can be described as yang constipation.Together
When, great mass of data proves, using the method for traditional Chinese medicine and dietotherapy, is very helpful to the improvement and treatment of constipation.But tradition
Instructions of taking is inconvenient, and drug dose is big, is not easy to be accepted by patients, and has seriously affected the performance of curative effect.Therefore, develop take,
It is easy to carry, safe and effective, have no toxic side effect, treat constipation tea bag have important value medical health care and reality anticipate
Justice.
Invention content
The present invention is directed to above-mentioned existing problem, proposes that one kind is relieved inflammation or internal heat moistening dryness for relaxing bowels health protection tea.
According to an aspect of the present invention, one kind is provided to relieve inflammation or internal heat moistening dryness for relaxing bowels health protection tea, in terms of composition by weight, including：Greatly
Bitter sub- fruit 30-40 parts, small hardship is fruit 30-40 parts sub-, 30-40 parts of dioecism momordica root, 5-10 parts of lophatherum gracile, 10-15 parts of asparagus fern, Radix Ophiopogonis 20-
25 parts, 10-15 parts of American Ginseng, 30-35 parts of radix scrophulariae, 20-25 parts of dendrobium devonianum, 10-15 parts of lily, 15-20 parts of Radix Astragali, green tea
40-50 parts, 70-90 parts of dextrin, 210-270 parts of sucrose.
In some embodiments, sub- 40 parts of the fruit of the big hardship, 40 parts of the sub- fruit of small hardship, 40 parts of dioecism momordica root, 10 parts of lophatherum gracile,
15 parts of asparagus fern, 25 parts of Radix Ophiopogonis, 15 parts of American Ginseng, 35 parts of radix scrophulariae, 25 parts of dendrobium devonianum, 15 parts of lily, 20 parts of Radix Astragali, green tea 50
Part, 90 parts of dextrin, 270 parts of sucrose.
According to another aspect of the present invention, a kind of method preparing the moistening dryness for relaxing bowels health protection tea above-mentioned that relieves inflammation or internal heat is provided, is wrapped
Include following steps：
(1) the sub- fruit of load weighted big hardship, the sub- fruit of small hardship, dioecism momordica root are cleaned respectively, shredded, squeezed the juice, filtered, gained juice
Freeze-drying process is carried out, dried powder is obtained, it is spare；
(2) by load weighted lophatherum gracile, asparagus fern, Radix Ophiopogonis, American Ginseng, radix scrophulariae, dendrobium devonianum, lily, Radix Astragali, feed liquid is added
Than the water measured for 10-15 times, first impregnate, using microwave radiation exaraction, to extract power as 700W-900W, 70 DEG C of heating temperature-
90 DEG C, heating time 30-45min extract, filtering, filtrate stand for standby use；Same condition is extracted 2 times, filtrate conjunction twice
And it is 5mL crude drugs containing 1g to be concentrated into relative concentration, it is spare；
(3) ZTC1+1-III clarification process
A) ZTC1+1-III fining agent component A solution is prepared；
B) ZTC1+1-III fining agent B component solution is prepared；
C) pH value that water carries liquid is measured, it is suitable to determine that ZTC1+1-III flocculating agent As component solution and B component solution are added
Sequence；
D) liquor strength is 1.0: 5, stirring, is centrifuged after the sedimentation of ZTC1+1-III flocculants is added, obtains supernatant, supernatant
It is spare；
(4) supernatant is spray-dried；
(5) load weighted green tea crushed, be sieved, ultramicro grinding；
(6) load weighted dextrin, sucrose is added in the powder obtained by step (1), (4) and (5), 40%-60% is added
Medicinal alcohol carries out softwood making, and granulation, whole grain, pack, sterilizes, is packaged into tea bag at reduced vacuum drying.
In some embodiments, the freeze-drying step in step 1) is：
It puts gained juice into freezing chamber and carries out pre-freeze, pre-freezing temperature is set as -20 DEG C, for 24 hours, then the pre-freeze time is
Vacuum degree is set as 20Pa, with 1 DEG C of heating rate of every 1h heatings, -15 DEG C is slowly warming up to, 8h is kept the temperature, then again with 1h liters
2 DEG C of heating rate of temperature, is slowly warming up to -8 DEG C, keeps the temperature 5h, and then heated up with 1h 3 DEG C of heating rate again, is slowly warming up to
40 DEG C, 16h is kept the temperature, outlet is spare.
In some embodiments, the soaking time in step 2) is 30min.
In some embodiments, the ZTC1+1-III flocculants in step d) are B component/component A, and setting condition
For：It is calculated as (0.10g: 0.05g-0.20g: 0.10g)/10.0g by crude drug amount.
In some embodiments, the mixing speed in step d) is 400r/min, and stirs 15min under the conditions of 70 DEG C,
Sedimentation time is 30-40min, and centrifugation time 15-20min, rotating speed is that 4000-6000 turns/min.
In some embodiments, the drying process of step (4) is：Intake air temperature is 150 DEG C -180 DEG C, air outlet temperature
Degree is 60 DEG C -80 DEG C, hot air flow 0.4-0.6m3/ min, flow velocity 2mL/min-3mL/min.
Bitter sub- fruit, is a kind of distinctive edible wild herbs in Yunnan, is the fruit of plant of Solanaceae, and bitter is cool in nature, have it is clearing heat and detoxicating,
The effect of anti-inflammatory profit larynx.The southwestern band in Yunnan is originated in, because of the degree of fruit bitter, shape, the difference of size, big bitter son can be divided into
Two kinds of fruit and the sub- fruit of small hardship.Plant difference lies in the big sub- fruit of hardship is mostly purple, while leaf margin has a wavy crackle, vein and right
There is the hard thorn swung on handle.Post flowering, flower are lilac little Hua, and the one third of only eggplant flower is big.Annual spring
It blooms fruiting.Fruit is oblateness, is had compared with multiple cracks.Diameter about 3cm or so.It is bottle green when fruit prematurity, after ripe
For orange colour.Its bitter is cool, micro- after bitter to have Hui Tian, locals to love to eat very much.The small sub- fruit of hardship only has pea grain size, returns sugariness ratio
Big bitter sub- fruit is dense.
Dioecism momordica root is Curcurbitaceae dioecism momordica root category perennial root herbaceous species plant, and general south is known as balsam pear, bright and beautiful litchi
Branch, the north are known as red Miss, insane melon etc..The effect of bitter is cold in nature, has to affix one's name to clearly and washs heat, item, deciphering, for treating polydipsia
Draw drink, cute conjunctivitis mesh pain etc..Secondly be rich in vitamin C, vitamin E, amino acid and minerals, while dioecism momordica root have it is anti-mutation,
Hypoglycemic, antitumor, reduction cholesterol level and other effects.
Lophatherum gracile is grass family, lophatherum gracile category herbaceos perennial, root-like stock.It can be expanded for spindle-like in the middle part of fibrous root
Meat root tuber, yellow-white.Leaf lanceolar, panicle；Caryopsis ellipse.Its is cold in nature, sweet in flavor, light., can clear away heart-fire, diuresis, dispel it is tired
It is hot-tempered, there is good curative effect for swelling and aching of gum, stomatitis etc..
Asparagus fern, the root tuber of liliaceous plant lucid asparagus is cold in nature, sweet in flavor, slight bitter.With replenishing the vital essence and removing heat, the work(of moistening lung nourshing kidney
Effect.For control fever due to yin deficiency, lung carbuncle of quenching one's thirst, etc. illnesss.Lucid asparagus containing asparagine, B- sitosterols, steroid saponin, mucilaginous substance,
The ingredients such as furfural derivatives.Lucid asparagus has hemocytes increasing, enhancing reticuloendothelial system phagocytic function and extends in the presence of antibody
Between effect.
Radix Ophiopogonis, Liliaceae Ophiopogon perennial evergreen herbaceous plant, root is thicker, and intermediate or proximal end often enlarges into ellipse
Shape or fusiform small root tuber, stem are very short.The small root tuber of Radix Ophiopogonis is Chinese medicine, sweet in flavor, property slight bitter, be slightly cold, and has nourishing Yin and promoting production of body fluid, moistening lung
The benefits of clearing away heart-fire.
American Ginseng, Chinese medicine name.This product is the root of Araliaceae American Ginseng.Major function is：Beneficial lung yin, the clear fire of deficiency type,
It promotes the production of body fluid to quench thirst.It controls the deficiency syndrome of the lung to cough long, lose blood, dry throat and mouth, abnormal heat is tired of tired.
Radix scrophulariae, Chinese medicine name.Cold nature, it is sweet in flavor, bitter, at having the effect of clearing heat and cooling blood, nourishing yin and lessening fire, detoxicating and resolving a mass, cure mainly
Warm heat disease heat and ying blood；Body heat；Polydipsia；Tongue is deep red；Macular eruption；Tianjin hinder constipation.
Dendrobium devonianum, sweet in flavor, cold nature.With nourishing yin for benefiting stomach, promote the production of body fluid relieving restlessness the effect of.For consumption of body fluid caused by febrile disease, dry is tired
Yearningly, eak after being ill, tuberculosis, loss of appetite
Lily, it is sweet in flavor, it is cold in nature.With Yin nourishing and lung moistening；The effect of clearing away the heart fire and tranquillizing.The main deficiency of Yin is coughed long；The pyreticosis later stage；Waste heat is not
Clearly or feelings will it is unsuccessful caused by dysphoria palpitates with fear, insomnia and dreamful sleep, absent-minded.
Radix Astragali is the root of legume astragalus mongolicus.It is sweet in flavor, it is warm-natured.Tool：Invigorating qi for strengthening superficies, pus draining and toxin expelling, diuresis, myogenic
The effect of, it is herein supplementary inhibitory medicine, avoids the cold and cool property of drug from injuring healthy tendency, and foster healthy tendency, the effect of promoting the circulation of qi defecation.
The beneficial effects of the invention are as follows：
One kind relieving inflammation or internal heat moistening dryness for relaxing bowels tea can be in short-term suitable for acute diseases such as long-time constipation, dry feces, abdominal pains
Between be realize defecation, alleviate the pain of patient.
One kind is relieved inflammation or internal heat moistening dryness for relaxing bowels tea, and big bitter sub- fruit, the sub- fruit of small hardship and dioecism momordica root are squeezed the juice, and juice is using being freeze-dried；Its
It is secondary, active ingredient is carried out to lophatherum gracile, asparagus fern, Radix Ophiopogonis, radix scrophulariae, dendrobium devonianum, lily, Radix Astragali using microwave extraction technology and is carried
It takes, later using flocculation clarification process, clarified solution is directly spray-dried.Finally, green tea uses superfine communication technique, directly
It is mixed with above-mentioned three kinds of powder, dextrin and Icing Sugar granulation, whole grain, packaging is added.
Chinese medicine thinks that this disease has the difference of body ressitance weakened while pathogenic factors prevailing.Deficiency of vital energy sun is weak, push inability or deficiency of Yin blood is few, caused by intestinal dryness just
It is secret, it can be described as yin constipation；Real heat phlegm wet stops up knot or the stagnation of the circulation of vital energy is not all right into constipation, can be described as yang constipation.
It is treated for constipation caused by the deficiency of Yin and yang constipation in the present invention, it is big bitter sub- fruit, the sub- fruit of small hardship, dioecism momordica root, light
The leaf of bamboo is monarch drug in a prescription, bitter, light, cold in nature, can clear away heart-fire, liver, lung excess fire；Radix scrophulariae, Kucheng and cool, nourishing Yin and moistening dryness are strengthened water system fire, are opened
Kidney water to grow intestinal dryness, Radix Rehmanniae, American Ginseng sweetness and bitterness and tremble with fear, clearing heat and nourishing yin strengthens aquatic Tianjin, to increase the power of radix scrophulariae nourishing Yin and moistening dryness；Lung again
With in large intestine phase table, therefore with sweet cold Radix Ophiopogonis, asparagus fern, lily, dendrobium devonianum, lung and stomach nourishing yin jin is dry with ease constipation, is altogether ministerial drug；
Radix Astragali, nature and flavor：Sweet, tepor has tonifying Qi and lifting yang, the stagnant arthritis of row, shengjin nourishing, can restrain the cold and cool property of monarch drug in a prescription, meanwhile, it adjusts
Qi-regulating machine so that drug effect up and down phase factor, fever and chills it is suitable, clearly without rushing down, be adjutant；Green tea takes it bitter cool light clear, clear upper drop
Under, to make medicine.For the formula according to " tea borrows medicine gesture, medicine to borrow tea power ", all medicines share plays clearing heat-fire, nourishing Yin and moistening dryness, defaecation
Effect.
The present invention is on the market there is not yet the health protection tea for the moistening dryness for relaxing bowels that relieves inflammation or internal heat, that is, have caused by the deficiency of Yin and yang constipation
The health protection tea that constipation is treated.According to clinical empirical summary and the market demand, the more preferable health care for playing the moistening dryness for relaxing bowels that relieves inflammation or internal heat
The effect of tea, the present invention use advanced preparation process, extract each medicine active principle to greatest extent, meanwhile, it is simple for process, it is real
With reasonable design is convenient for industrialized production.
The moistening dryness for relaxing bowels health protection tea provided by the invention that relieves inflammation or internal heat uses pure natural, pollution-free, integration of drinking and medicinal herbs raw material, greatly
Improve the effect of relieving inflammation or internal heat moistening dryness for relaxing bowels and without side-effects, be prepared into tea bag, have brew quickly, sanitation and hygiene, convenient for taking
Band adapts to the fast pace life requirement of modern.
The present invention, using domestic advanced food and pharmaceutical formulation techniques, uses food technology first in preparation process,
The juice of big bitter sub- fruit, small hardship sub- fruit and dioecism momordica root is obtained with the method squeezed the juice, then using freeze drying process, and is to have used point
Step-up temperature, by broken when vitamins and other readily oxidizable substances being avoided to be extracted using the method for the heating that directly rapidly heats up
It is bad；Secondly, using microwave extraction technology to lophatherum gracile, asparagus fern, Radix Ophiopogonis, radix scrophulariae, dendrobium devonianum, lily, Radix Astragali carry out effectively at
The extraction divided, microwave technology can destroy plant cell wall, increase the dissolution of active ingredient, and it is effective to extract each medicine to greatest extent
Substance, in the active substance in removing extracting solution, retains the work of each component to greatest extent later using flocculation clarification process
Property ingredient, extracting solution is directly spray-dried, and avoids germ contamination and liquid in long-time placement process rotten.
Flocculation clarification process therein, using ZTC1+1-III Old Regions, ZTC1+1-III natural clarifying agents are one
The novel food additives of kind, are grouped as two groups by A, B.It is after the first component is added, in different solubilities that it, which clarifies principle,
" bridge formation " connection makes molecule increase rapidly between macromolecular.Second component on the basis of the first component is formed by compound again
Add " bridge formation ", flocculate is made to form precipitation as early as possible to remove.
Finally, green tea uses superfine communication technique, is directly mixed with above-mentioned three kinds of powder, dextrin and Icing Sugar granulation is added,
Simple for process, practical, reasonable design is convenient for industrialized production.
Specific implementation mode
With reference to embodiment, invention is further described in detail.
Embodiment 1
(1) the sub- fruit 30g of big hardship, the sub- fruit 35g of small hardship, dioecism momordica root 35g are cleaned respectively, shredded, squeezed the juice, filtered, by gained
Juice puts freezing chamber into and carries out pre-freeze, and pre-freezing temperature is set as -20 DEG C, the pre-freeze time be for 24 hours, then set vacuum degree as
20Pa is heated up 1 DEG C of heating rate with every 1h, is slowly warming up to -15 DEG C, keeps the temperature 8h, and then heated up with 1h 2 DEG C of heating speed again
Rate, is slowly warming up to -8 DEG C, keeps the temperature 5h, and then heated up with 1h 3 DEG C of heating rate again, is slowly warming up to 40 DEG C, is kept the temperature 16h,
Outlet, it is spare.
(2) lophatherum gracile 10g, asparagus fern 10g, Radix Ophiopogonis 25g, American Ginseng 12g, radix scrophulariae 30g, dendrobium devonianum 25g, lily 10g, Huang
Stilbene 20g is added the water that solid-liquid ratio is 10 times of amounts, first impregnates 30min, and using microwave radiation exaraction, extraction power is 800W, heating
Temperature 70 C, heating time 35min are extracted, filtering, filtrate stand for standby use.Same condition is extracted 2 times, filtrate conjunction twice
And it is 5mL crude drugs containing 1g to be concentrated into relative concentration, it is spare.
(3) ZTC1+1-III clarification process
ZTC1+1-III Old Regions are added, ZTC1+1-III natural clarifying agents are a kind of novel food additives,
Commercially available acquirement.It is grouped as two groups by A, B.It is after the first component is added, in different soluble large molecules that it, which clarifies principle,
Between " bridge formation " connection so that molecule is increased rapidly.Second component adds " frame again on the basis of the first component is formed by compound
Bridge " makes flocculate form precipitation as early as possible to remove.
The preparation of ZTC1+1III fining agent component A solution：ZTC1+1-III fining agent component A 1g are weighed, are first steamed with a small amount of
Distilled water stirs into paste, and then plus distilled water is to 100mL, and swelling for 24 hours, stirs evenly, and double gauze filters to get 1%A component viscose glues
Liquid.
The preparation of ZTC1+1-III fining agent B component solution：ZTC1+1-III fining agent B component 1g are weighed, with a small amount of 1%
Acetum dissolves and stirs into paste, and then plus 1% acetic acid is to 100mL, and swelling for 24 hours, stirs evenly, and double gauze filters to get 1%
B component viscose.
A, the determination of bis- component addition sequences of B：Take the water of step (2) carry concentrated medicament be diluted with water in right amount it is dense containing crude drug
Degree 1.0: 5, measures its pH.B component is first added, A is added afterwards if pH ＞ 4.8 by ZTC1+1-III natural clarifying agent specifications
Component；If pH ＜ 4.8 are first added component A, B component are added afterwards.The pH that anti-sense spray water carries medicine is measured, determines A, B component
Addition sequence.It is 5.2 since the present embodiment water puies forward liquid pH value, it is thus determined that B component is first added, component A is added afterwards.
Liquor strength is 1.0: 5 (crude drugs g: liquid mL), mixing speed 400r/min, and 15min is stirred under the conditions of 70 DEG C,
ZTC1+1III flocculating agent Bs/A (0.10g: 0.05g)/10.0g (by crude drug amount calculate) setting condition, settle 30min after, from
Heart 15min, rotating speed are 4000 turns/min, obtain supernatant, supernatant is spare, is spray-dried in next step.
(4) supernatant is spray-dried
Liquid is spray-dried, and drying process is intake air temperature：150 DEG C, hot air flow 0.6m3/ min, outlet air
Mouth temperature：70 DEG C of flow velocitys：3mL/min.
(5) 40g green tea first carries out preliminary crushing, crosses 20 mesh sieve, then carry out ultramicro grinding, and ultramicro grinding time 30min surpasses
Crushing of Ultrafine temperature is -5.0 DEG C, and gained Ultramicro-powder size distribution is more uniform, and active ingredient result of extraction is good, and bioavilability is high.
(6) powder for making (1), (4), (5), is added dextrin 80g, cane sugar powder 250g, and 40% medicinal alcohol is added and carries out
Softwood makes, and granulation, whole grain, pack, sterilizes, is packaged into tea bag at reduced vacuum drying under the conditions of 40 DEG C.
Embodiment 2
(1) will big bitter sub- fruit 35g, the sub- fruit 30g of small hardship, dioecism momordica root 30g are cleaned, shred, squeeze the juice, are filtered respectively, by gained
Juice puts freezing chamber into and carries out pre-freeze, and pre-freezing temperature is set as -20 DEG C, the pre-freeze time be for 24 hours, then set vacuum degree as
20Pa is heated up 1 DEG C of heating rate with every 1h, is slowly warming up to -15 DEG C, keeps the temperature 8h, and then heated up with 1h 2 DEG C of heating speed again
Rate, is slowly warming up to -8 DEG C, keeps the temperature 5h, and then heated up with 1h 3 DEG C of heating rate again, is slowly warming up to 40 DEG C, is kept the temperature 16h,
Outlet, it is spare.
(2) lophatherum gracile 5g, asparagus fern 10g, Radix Ophiopogonis 20g, American Ginseng 10g, radix scrophulariae 30g, dendrobium devonianum 20g, lily 10g, Huang
Stilbene 15g is added the water that solid-liquid ratio is 10 times of amounts, first impregnates 30min, and using microwave radiation exaraction, extraction power is 900W, heating
80 DEG C of temperature, heating time 30min are extracted, filtering, filtrate stand for standby use.Same condition is extracted 2 times, filtrate conjunction twice
And it is 5mL crude drugs containing 1g to be concentrated into relative concentration, it is spare.
(3) ZTC1+1-III clarification process
ZTC1+1-III Old Regions are added, ZTC1+1-III natural clarifying agents are a kind of novel food additives,
It is grouped as two groups by A, B.It is after the first component is added that it, which clarifies principle, and " bridge formation " connects between different soluble large molecules
Molecule is set to increase rapidly.Second component adds " bridge formation " again on the basis of the first component is formed by compound, and flocculate is made to use up
It is fast to form precipitation to remove.
The preparation of ZTC1+1-III fining agent component A solution：ZTC1+1-III fining agent component A 1g are weighed, are first used a small amount of
Distilled water stirs into paste, and then plus distilled water is to 100mL, and swelling for 24 hours, stirs evenly, and double gauze filters to get 1%A component viscose glues
Liquid.
The preparation of ZTC1+1-III fining agent B component solution：ZTC1+1-III fining agent B component 1g are weighed, with a small amount of 1%
Acetum dissolves and stirs into paste, and then plus 1% acetic acid is to 100mL, and swelling for 24 hours, stirs evenly, and double gauze filters to get 1%
B component viscose.
A, the determination of bis- component addition sequences of B：Take in step (2) water carry concentrated medicament be diluted with water in right amount it is dense containing crude drug
Degree 1.0: 5, measures its pH.B component is first added, A is added afterwards if pH ＞ 4.8 by ZTC1+1-III natural clarifying agent specifications
Component；If pH ＜ 4.8 are first added component A, B component are added afterwards.The pH that anti-sense spray water carries medicine is measured, determines A, B component
Addition sequence.It is 5.3 since the water of the present embodiment puies forward liquid pH value, it is thus determined that B component is first added, component A is added afterwards.
Liquor strength is 1.0: 5 (crude drug g：Liquid mL), mixing speed 400r/min stirs 15min under the conditions of 70 DEG C,
ZTC1+1III flocculating agent Bs/A (0.12g: 0.06g)/10.0g (by crude drug amount calculate) setting condition, settle 30min after, from
Heart 15min, rotating speed are 4000 turns/min, obtain supernatant, supernatant is spare, is spray-dried in next step.
(4) supernatant is spray-dried
Liquid is spray-dried, and drying process is intake air temperature：160 DEG C, hot air flow 0.5m3/min, outlet air
Mouth temperature：60 DEG C of flow velocitys：2mL/min.
(5) 45g green tea first carries out preliminary crushing, crosses 20 mesh sieve, then carry out ultramicro grinding, and ultramicro grinding time 30min surpasses
Crushing of Ultrafine temperature is -10.0 DEG C, and gained Ultramicro-powder size distribution is more uniform, and active ingredient result of extraction is good, and bioavilability is high.
(6) powder for making (1), (4), (5), is added dextrin 70g, cane sugar powder 210g, and 50% medicinal alcohol is added and carries out
Softwood makes, and granulation, whole grain, pack, sterilizes, is packaged into tea bag at reduced vacuum drying under the conditions of 40 DEG C.
Embodiment 3
(1) will big bitter sub- fruit 40g, the sub- fruit 40g of small hardship, dioecism momordica root 40g are cleaned, shred, squeeze the juice, are filtered respectively, by gained
Juice puts freezing chamber into and carries out pre-freeze, and pre-freezing temperature is set as -20 DEG C, the pre-freeze time be for 24 hours, then set vacuum degree as
20Pa is heated up 1 DEG C of heating rate with every 1h, is slowly warming up to -15 DEG C, keeps the temperature 8h, and then heated up with 1h 2 DEG C of heating speed again
Rate, is slowly warming up to -8 DEG C, keeps the temperature 5h, and then heated up with 1h 3 DEG C of heating rate again, is slowly warming up to 40 DEG C, is kept the temperature 16h,
Outlet, it is spare.
(2) lophatherum gracile 10g, asparagus fern 15g, Radix Ophiopogonis 25g, American Ginseng 15g, radix scrophulariae 35g, dendrobium devonianum 25g, lily 15g, Huang
The water that solid-liquid ratio is 10 times of amounts is added in stilbene 20g, first impregnates 30min, and extraction power is 900W, 80 DEG C of heating temperature, heating time
25min is extracted, filtering, filtrate stand for standby use.Same condition is extracted 2 times, and filtrate merging, is concentrated into relative concentration twice
It is spare for 5mL crude drugs containing 1g.
(3) ZTC1+1-III clarification process
ZTC1+1-III Old Regions are added, ZTC1+1-III natural clarifying agents are a kind of novel food additives,
It is grouped as two groups by A, B.It is after the first component is added that it, which clarifies principle, and " bridge formation " connects between different soluble large molecules
Molecule is set to increase rapidly.Second component adds " bridge formation " again on the basis of the first component is formed by compound, and flocculate is made to use up
It is fast to form precipitation to remove.
The preparation of ZTC1+1-III fining agent component A solution：ZTC1+1-III fining agent component A 1g are weighed, are first used a small amount of
Distilled water stirs into paste, and then plus distilled water is to 100mL, and swelling for 24 hours, stirs evenly, and double gauze filters to get 1%A component viscose glues
Liquid.
The preparation of ZTC1+1-III fining agent B component solution：ZTC1+1-III fining agent B component 1g are weighed, with a small amount of 1%
Acetum dissolves and stirs into paste, and then plus 1% acetic acid is to 100mL, and swelling for 24 hours, stirs evenly, and double gauze filters to get 1%
B component viscose.
A, the determination of bis- component addition sequences of B：Water intaking carries concentrated medicament and is diluted with water to concentration containing crude drug 1.0 in right amount：5,
Measure its pH.B component is first added, component A is added afterwards if pH ＞ 4.8 by ZTC1+1-III natural clarifying agent specifications；If
PH ＜ 4.8 are then first added component A, B component are added afterwards.The pH that anti-sense spray water carries medicine is measured, determines the addition of A, B component
Sequentially.It is 5.2 since the water of the present embodiment puies forward liquid pH value, it is thus determined that B component is first added, component A is added afterwards.
Liquor strength is 1.0: 5 (crude drugs g: liquid mL), mixing speed 400r/min, and 15min is stirred under the conditions of 70 DEG C,
ZTC1+1III flocculating agent Bs/A (0.12g: 0.06g)/10.0g (by crude drug amount calculate) setting condition, settle 30min after, from
Heart 15min, rotating speed are 4000 turns/min, obtain supernatant, supernatant is spare, is spray-dried in next step.
(4) supernatant is spray-dried
Liquid is spray-dried, and drying process is intake air temperature：180 DEG C, hot air flow 0.4m3/ min, outlet air
Mouth temperature：60 DEG C of flow velocitys：2mL/min.
(5) 50g green tea first carries out preliminary crushing, crosses 20 mesh sieve, then carry out ultramicro grinding, and ultramicro grinding time 30min surpasses
Crushing of Ultrafine temperature is -10.0 DEG C, and gained Ultramicro-powder size distribution is more uniform, and active ingredient result of extraction is good, and bioavilability is high.
(6) powder for making (1), (4), (5), is added dextrin 90g, cane sugar powder 270g, and 50% medicinal alcohol is added and carries out
Softwood makes, and granulation, whole grain, pack, sterilizes, is packaged into tea bag at reduced vacuum drying under the conditions of 40 DEG C.
The clinical effectiveness of the present invention
(1) patient data
180 patients of clinic of in January, 2011 Xuanwei City in January, -2015 First People's Hospital are compiled, wherein man
85 people of property, 95 people of women, the age, 6-30 Sui, 21；31-40 Sui, 40；40-60 Sui, 48；60 years old or more, 71.The course of disease
Long 20 years, shortest 1 year symptoms include mouth and nose are dry, irritated, defecation, dry and hard excrement, abdominal pain, defecation be not unsmooth etc. within 3 days or more.
Three groups are randomly divided into, every group of 60 people, there was no significant difference for three groups of data.Three groups of profits of relieving inflammation or internal heat for taking case study on implementation 1,2,3 respectively
Dry constipation-relieving tea twice a day one bag every time, even served 7 days as one therapeutic course, each course for the treatment of drug withdrawal is being taken after 2-3 days, according to patient
Constitution takes the 2-4 courses for the treatment of altogether.
(2) diagnostic criteria
The diagnostic criteria of Rome III functional consitipations
1. must include following 2 or multinomial：
A. during defecation, defecation arduously at least accounts for 25%.
B. agglomerate or hard excrement at least 25% in excrement.
C. defecation feels at least 25% not to the utmost
D. anorectal sense of obstruction at least 25%.
E. manual operations is easy to defecation at least 25%.
F. defecation ＜ 3 times weekly.
2. not having to caccagogue, seldom there is soft stool.
3. constipation type intestinal irritable syndrome diagnosis basis is insufficient.
Symptom at least occurs 6 months before diagnosis, and nearly 3 months symptoms meet the above standard.
Tcm diagnosis standard
Reference《Disease of tcm Standardization of diagnosis and curative effect》It formulates
1. defecation time extends, 2 days with last time, excrement dry, hard
It is dry such as chestnut 2. severe one difficulty in defecation, it can receive decline etc. with few abdominal distension urgency, the tired weak, stomach of god
3. excluding enteron aisle organic disease
4. criterion of therapeutical effect：
Recovery from illness：Stool is normally or horizontal, defecation ＞ 3 times weekly before recovery to disease, other symptoms whole disappear.
It is effective：Constipation is obviously improved, and interval time and just matter are close to normal, or stool is slightly dry and infrequent defecation time ＜
72h, other symptoms largely disappear.
Effectively：The infrequent defecation time shortens 1 day, or just the dry and hard improvement of matter, other symptoms take a favorable turn.
In vain：Constipation and other symptoms are without improvement.
(3) therapeutic effect
| Group | Recovery from illness | It is effective | Effectively | In vain | Total effective rate |
| Embodiment 1 | 10 | 19 | 26 | 5 | 91.7% |
| Embodiment 2 | 8 | 18 | 27 | 7 | 88.3% |
| Embodiment 3 | 10 | 19 | 27 | 4 | 93.3% |
The moistening dryness for relaxing bowels tea that relieves inflammation or internal heat of the present invention, can be short suitable for acute diseases such as long-time constipation, dry feces, abdominal pains
Time realizes defecation, alleviates the pain of patient.
Above-described is only some embodiments of the present invention.For those of ordinary skill in the art, not
Under the premise of being detached from the invention design, various modifications and improvements can be made, these belong to the protection model of the present invention
It encloses.
Claims (8)
- The moistening dryness for relaxing bowels health protection tea 1. one kind is relieved inflammation or internal heat, which is characterized in that in terms of composition by weight, including：Big bitter sub- fruit 30-40 parts, small hardship is fruit 30-40 parts sub-, 30-40 parts of dioecism momordica root, 5-10 parts of lophatherum gracile, 10-15 parts of asparagus fern, wheat Winter 20-25 part, 10-15 parts of American Ginseng, 30-35 parts of radix scrophulariae, 20-25 parts of dendrobium devonianum, 10-15 parts of lily, 15-20 parts of Radix Astragali, 40-50 parts of green tea, 70-90 parts of dextrin, 210-270 parts of sucrose.
- The moistening dryness for relaxing bowels health protection tea 2. one kind according to claim 1 is relieved inflammation or internal heat, which is characterized in that sub- 40 parts of the fruit of the big hardship, Sub- 40 parts of the fruit of small hardship, 40 parts of dioecism momordica root, 10 parts of lophatherum gracile, 15 parts of asparagus fern, 25 parts of Radix Ophiopogonis, 15 parts of American Ginseng, 35 parts of radix scrophulariae, tooth valve 25 parts of the stem of noble dendrobium, 15 parts of lily, 20 parts of Radix Astragali, 50 parts of green tea, 90 parts of dextrin, 270 parts of sucrose.
- 3. a kind of method for the moistening dryness for relaxing bowels health protection tea that relieves inflammation or internal heat preparing claims 1 or 2, which is characterized in that include the following steps：(1) the sub- fruit of load weighted big hardship, the sub- fruit of small hardship, dioecism momordica root are cleaned respectively, shredded, squeezed the juice, filtered, gained juice carries out Freeze-drying process obtains dried powder, spare；(2) by load weighted lophatherum gracile, asparagus fern, Radix Ophiopogonis, American Ginseng, radix scrophulariae, dendrobium devonianum, lily, Radix Astragali, solid-liquid ratio, which is added, is The 10-15 times of water measured, first impregnates, using microwave radiation exaraction, to extract power as 700W-900W, and 70 DEG C -90 of heating temperature DEG C, heating time 30-45min extract, filtering, filtrate stand for standby use；Same condition is extracted 2 times, filtrate merging twice, It is 5mL crude drugs containing 1g to be concentrated into relative concentration, spare；(3) ZTC1+1-III clarification processA) ZTC1+1-III fining agent component A solution is prepared；B) ZTC1+1-III fining agent B component solution is prepared；C) pH value that water carries liquid is measured, determines ZTC1+1-III flocculating agent As component solution and B component solution addition sequence；D) liquor strength is 1.0: 5 (g/mL), and stirring centrifuges after the sedimentation of ZTC1+1-III flocculants is added, obtains supernatant, supernatant Liquid is spare；(4) supernatant is spray-dried；(5) load weighted green tea crushed, be sieved, ultramicro grinding；(6) load weighted dextrin, sucrose is added in the powder obtained by step (1), (4) and (5), it is medicinal that 40%-60% is added Ethyl alcohol carries out softwood making, and granulation, whole grain, pack, sterilizes, is packaged into tea bag at reduced vacuum drying.
- 4. a kind of method preparing the moistening dryness for relaxing bowels health protection tea that relieves inflammation or internal heat according to claim 3, which is characterized in that the step 1) the freeze-drying process step in is：It puts gained juice into freezing chamber and carries out pre-freeze, pre-freezing temperature is set as -20 DEG C, the pre-freeze time is for 24 hours, then to set Vacuum degree is 20Pa, with 1 DEG C of heating rate of every 1h heatings, is slowly warming up to -15 DEG C, keeps the temperature 8h, then heated up 2 DEG C with 1h again Heating rate, be slowly warming up to -8 DEG C, keep the temperature 5h, then heated up with 1h 3 DEG C of heating rate again, is slowly warming up to 40 DEG C, 16h is kept the temperature, outlet is spare.
- 5. a kind of method preparing the moistening dryness for relaxing bowels health protection tea that relieves inflammation or internal heat according to claim 3, which is characterized in that the step 2) soaking time in is 30min.
- 6. a kind of method preparing the moistening dryness for relaxing bowels health protection tea that relieves inflammation or internal heat according to claim 3, which is characterized in that the step D) the ZTC1+1-III flocculants in are B component/component A, and setting condition is：It is calculated as (0.10g: 0.05g- by crude drug amount 0.20g∶0.10g)/10.0g。
- 7. a kind of method preparing the moistening dryness for relaxing bowels health protection tea that relieves inflammation or internal heat according to claim 3, which is characterized in that the step D) mixing speed in is 400r/min, and 15min is stirred under the conditions of 70 DEG C, sedimentation time 30-40min, and centrifugation time is 15-20min, rotating speed are that 4000-6000 turns/min.
- 8. a kind of method preparing the moistening dryness for relaxing bowels health protection tea that relieves inflammation or internal heat according to claim 3, which is characterized in that the step (4) drying process is：Intake air temperature is 150 DEG C -180 DEG C, air outlet temperature is 60 DEG C -80 DEG C, hot air flow 0.4- 0.6m3/ min, flow velocity 2mL/min-3mL/min.
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