CN108395843A - A kind of thermal-insulating waterproof sealing compound of filleting and its preparation method and application - Google Patents
A kind of thermal-insulating waterproof sealing compound of filleting and its preparation method and application Download PDFInfo
- Publication number
- CN108395843A CN108395843A CN201810206169.0A CN201810206169A CN108395843A CN 108395843 A CN108395843 A CN 108395843A CN 201810206169 A CN201810206169 A CN 201810206169A CN 108395843 A CN108395843 A CN 108395843A
- Authority
- CN
- China
- Prior art keywords
- component
- thermal
- filleting
- sealing compound
- waterproof sealing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D195/00—Coating compositions based on bituminous materials, e.g. asphalt, tar, pitch
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2207/00—Properties characterising the ingredient of the composition
- C08L2207/10—Peculiar tacticity
- C08L2207/14—Amorphous or atactic polypropylene
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Sealing Material Composition (AREA)
Abstract
The present invention relates to thermal-insulating waterproof sealing compounds of a kind of filleting and its preparation method and application, belong to sealing waterproof technique field.Sealing compound of the present invention includes component A and B component, and by percentage to the quality, the composition and ratio of component A is：Modified pitch 0~75%, bitumen regenerant 0~80%, rapid-curing cutback creaming agent 0.01~30%, emulsion 10~70%, B component are organic or inorganic thermal insulation material.Glass microballoon, glass bead, foamed ceramic, expanded plastic particles are dispersed in by high-speed uniform in rubbery state water-repellent paint by the present invention; it prepares that a kind of rate of drying is fast, thermal coefficient is low, shrinking percentage is low and the thermal-insulating waterproof sealing compound of water-tolerant, a kind of dedicated thermal-insulating waterproof sealing material of filleting is provided for consumer.
Description
Technical field
The present invention relates to thermal-insulating waterproof sealing compound and its preparations of sealing waterproof technique field more particularly to a kind of filleting
Methods and applications.
Background technology
It is stretched caused by temperature difference and flexing, concrete construction is generally provided with seam when building.Seam is
The weak link of concrete construction hinders the normal flexible of seam first, foreign matter is easy to gather in the joint；Second is that seam can produce
Raw infiltration corrodes softening roadbed, so processing must be sealed to variator.
Filleting is mainly used in the close of the construction joints such as the expansion joint of building, deformation joint and crack repair with waterproof sealing cream
Water-proofing treatment is sealed, cardinal principle is that waterproof sealing cream pointing is formed to sealing waterproof layer barrier water edge to split in the gap of building
Stitch the channel of leakage.To adapt to the dynamic growth variation in building gap, filleting sealing compound need to meet that adhesion strength is big, elongation percentage
High, the performances requirement such as shrinking percentage is low.Filleting waterproof sealing cream mainly has oiliness and aqueous two major classes, at present existing product
The filler materials such as a large amount of dicalcium powder, talcum powder are mainly added into organic host material and compound for formula system, also
Do not occur the integrated filleting sealing compound of water-proof heat insulation.
Modified asphalt sealing material has excellent high and low temperature resistance, while resistance to ag(e)ing is good, and service life is high, is mesh
Preceding widely used construction sealing materials.But general asphalt sealant cannot meet wanting for the height displacement ability of concrete joint
It asks, a kind of crack on road sealing being exclusively used in asphalt pavement crack sealing sealing as disclosed in Chinese patent 200410050262.5
Glue, ingredient have：100 parts of asphalt, 9-15 parts of SBS, 4-10 parts of tackifying resin, 0.2-1 parts of anti-aging agent, synthetic rubber 0-4
Part, 0.15-0.45 parts of stabilizer, 2-16 parts of softening agent, 2-15 parts of viscosity modifier, 0.2-0.5 parts of antistripping agent, reinforcing agent
35-60 parts, good with the caking property of bituminous paving but poor with the adhesive property of concrete, elongation percentage is low, can not be used as building
Caulking sealing agent.Chinese patent 200710037443.8 discloses a kind of water-proofing asphalt sealing material, by pitch 40-70, ring
Alkane oil 14-20, SBS 4-12, dimethylbenzene 5-10, rosin 5-10, zinc oxide 1-7,2,4-DihydroxyBenzophenone 0.1-1,4,
4 '-thiobis (2,6- DI-tert-butylphenol compounds) 0.05-3,4- benzoyloxys -2,2,6,6- tetramethyl piperidine 0.1-1, castor oil
Surplus form, solidified after being coated in building surface or gap, 20 years or more waterproofs can be undergone, it is fast light, it is corrosion-resistant, resist cold and
Energy high temperature resistant, but its heat insulation and preservation effect is undesirable.
Glass bead is that molten molten, vitreous balling-up is again rapid cooling under certain hot conditions by nature of glass slag ore in sand form
Molding glass particles, light shell is hard, surface vitreous is closed, it is irregular spherical to be in, and inside is the inorganic of porous cavity structure
Granular materials, unit weight is light, only 100-150kg/m3, is less than 1/10th of common mineral powder, thermal coefficient only has 0.028-
0.05w/m.k is a kind of high-performance environment protection type inorganic light weight heat-insulating material.Chinese patent 201110145655.4 discloses one kind
Fill the SBS modified asphalt waterproof coiled materials and preparation method of glass bead, the raw material of the waterproof roll by 90# pitch 30-50 parts by weight,
10# pitch 10-20 parts by weight, modifying agent SBS rubber 5-8 parts by weight, acrylic resin 3-5 parts by weight, softening agent 8-12 weight
Part, rubber powder 8-10 parts by weight, hollow glass bead 5-12 parts by weight and precipitated calcium carbonate 20-30 parts by weight composition；Party's legal system
Standby waterproof roll has better high temperature resistant and thermal and insulating performance due to being added to lighter hollow glass bead.
Invention content
In order to solve the above technical problems existing in the prior art, the present invention provides that a kind of rate of drying is fast, heat conduction system
Number is low, shrinking percentage is low and the thermal-insulating waterproof sealing compound of water-tolerant, and a kind of dedicated thermal-insulating waterproof of filleting is provided for consumer
The approach of sealing material.
The present invention is realized by following technology path：
A kind of thermal-insulating waterproof sealing compound of filleting, includes mainly component A and B component, and the component A includes modified drips
Blueness, bitumen regenerant, rapid-curing cutback creaming agent and emulsion；The B component is thermal insulation material.
The component A, by mass percentage for：
The B component is organic or inorganic thermal insulation material.
The component A further includes activator.
The weight ratio of the component A and B component is 50：1~50.
The B component be glass microballoon, glass bead, foamed ceramic, one kind in expanded plastic particles or it is a kind of with
On mixture.
The rapid-curing cutback creaming agent is inorganic creaming agent；It is preferred that in lithium magnesium silicate, aluminium-magnesium silicate, attapulgite or bentonite
One or more kinds of mixtures；It is further preferable that the rapid-curing cutback creaming agent is lithium magnesium silicate or aluminium-magnesium silicate.
The emulsion is cation, anion or nonionic colas.
The emulsion is preferably emulsifier metal carboxylate, fatty acid salt, Sulfonates, phosphates, alkyl
Amine, polyethenoxy ether class, polyoxypropylene ethers, amides or quaternary ammonium salt one or more kinds of mixtures it is water-soluble
Liquid；It is further preferable that the emulsifier is neopelex, sodium butylnaphthalenesulfonate, alkane sodium olefin sulfonate, the modified moon
One or more kinds of mixtures in cinnamic alcohol base sodium sulphate, alkyl phenol polyoxyethylene ether phosphate, loose ester acid soap.
The activator is anion or cationic activation agent；It is preferred that sodium hydroxide, sodium bicarbonate, potassium hydroxide, carbon
One or more kinds of mixtures in potassium hydrogen phthalate, hydrochloric acid, sulfuric acid, nitric acid；
The thermal-insulating waterproof sealing compound of the filleting is applied to the construction joints such as expansion joint, the deformation joint of building and crack repair
Encapsulation process.
The modified pitch is pitch and modifying agent is mixed and modified forms；
Further, the pitch is that the one or more in bitumen, coal tar asphalt or asphalt are mixed
Close object；It is preferred that asphalt, model 50#~200#.
The modifying agent is a kind of in polystyrene-type thermoplastic elastomers, polyolefins, polyvinyl chloride, polyurethanes
Or more than one mixture；The preferred SBS, SBR of the modifying agent, APP, SIS, SEBS, butyl rubber, neoprene,
One kind in butadiene rubber, isoprene rubber, EP rubbers, silicon rubber, nitrile rubber, ethylene propylene diene rubber or natural rubber or
More than one mixtures.
The SBS is to belong to styrene analog thermoplastic elastomer material, is that styrene-butadiene-styrene three is embedding
Section copolymer.
The SBR be styrene-butadiene rubber, by butadiene and it is styrene copolymerized be made.
The APP is thermoplastic resin, random polypropylene.
The SIS is thermoplastic elastic material, is styrene-isoprene-styrene block copolymer.
The SEBS is thermoplastic elastic material, is obtained by SBS Hydrogenations.
Preferably, the thermal-insulating waterproof sealing compound of a kind of filleting includes mainly component A and B component, with mass percent
Meter：
The composition and ratio of component A is：
B component is inorganic heat insulation material.
The weight ratio of the component A and B component is 50：(8-12).
It is further preferable that a kind of thermal-insulating waterproof sealing compound of filleting, includes mainly component A and B component, with matter
Measure percentages,
The composition and ratio of component A is：
The modified pitch is by 90#Asphalt with SBS modifier is mixed and modified forms.
B component is glass microballoon, glass bead.
The weight ratio of the component A and B component is 50：10.
The bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through atmospheric and vacuum distillation
At.Described 60 DEG C of rotary viscosities of bitumen regenerant are 1600~2300mPas, the needle penetration of 0 DEG C of 100g bitumen regenerant
(5s) is 19~23mm, flash-point >=210 DEG C, and loss on heating >=-1.2% meets NB/SH/T 0819-2010 requirement, has as follows
Advantage：
A, any additive is not added, and without two subharmonics, product low temperature flexibility is excellent, and performance is stablized, and has high viscous
It is low solidifying, the low feature of wax content.
B, for long-time storage without laminated segregation phenomenon, fragrance divides content high, good with SBS compatibilities.
C, without adding the softening oils such as used oil, volatile light component is free of, heavy metal is free of, has no irritating odor, is dodged
Point is high, environmentally protective.
D, product overall cost is low, cost-effective, can directly go up production line, shorten production procedure, reduce production cost.
The present invention adds bitumen regenerant in modified pitch can prevent the aging of modified pitch, in asphalt modification process
In, the reduction of each component compatibility in pitch colloidal system, solubility parameters difference increases between leading to component, if the regeneration that incorporation is certain
Agent can make the reduction of asphalitine relative amount, improve malthene to the solvability of asphalitine, improve the compatibility of pitch, carry
The needle penetration and ductility of high pitch make it restore or close to original performance.
The thermal-insulating waterproof sealing compound of filleting of the present invention can add other complementary ingredients, further change
It is apt to its performance；Also it can be directly prepared by above-mentioned formula, not increase other complementary ingredients.
Second object of the present invention is to provide a kind of preparation method of the thermal-insulating waterproof sealing compound of filleting, and step is such as
Under：
(1) prepared by component A rubbery states water-repellent paint：By modifying agent and pitch, bitumen regenerant and rapid-curing cutback creaming agent, input
To being modified in reaction kettle to get rubber asphalt mixture, then by emulsion by colloid mill to rubber asphalt mixture into
Up to rubbery state water-repellent paint after row emulsification, livering；
(2) component B is added to the thermal-insulating waterproof sealing compound stirred evenly in rubbery state water-repellent paint to get filleting；
(3) vacuum defoamation.
Preferably, the preparation method of the thermal-insulating waterproof sealing compound of a kind of filleting, steps are as follows：
(1) prepared by component A rubbery states water-repellent paint：The pitch and modifying agent for weighing mass percent, put into reaction kettle
In, be warming up to 140 DEG C~160 DEG C and stir evenly, under agitation be added bitumen regenerant, rapid-curing cutback creaming agent and mix 10~
20min is to slowly warm up to 180 DEG C~200 DEG C, and constant temperature stirs 2~4h to get rubber asphalt mixture；It is added into Soap liquid pot
Activator and/or emulsifier is added in the water of prescription quality percentage, and constant temperature stir-activating 20 after being heated to 40 DEG C~70 DEG C~
40min is to get emulsion；Emulsion is pumped into colloid mill, colloid mill is opened, then is pumped into rubber asphalt mixture and carries out breast
To get component A rubbery state water-repellent paints after change, livering；
(2) component B is added in rubbery state water-repellent paint in proportion and high-speed stirred is uniformly to get the heat preservation of filleting
Waterproof sealing cream；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The rapid-curing cutback creaming agent is lithium magnesium silicate or aluminium-magnesium silicate, and dosage is 0.2%~10%.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
The materials such as glass microballoon, glass bead, foamed ceramic, expanded plastic particles are by borax, silica sand, glass, ceramics
Equal raw materials are process through high-tech, and light shell is hard, grain size is small, internal mostly porous cavity structure, and surface is mostly closed pore, in not
There is low heat conduction, high intensity, heat-insulated, insulation effect, chemical property to stablize for regular shape, the substance, be a kind of high-performance ring
Guarantor's type light heat-insulating material.
Rapid-curing cutback creaming agent has unique three dimensions chain structure and special needle, rhabdolith structure, thus has not
With ordinary colloid and absorption property.Especially lithium magnesium silicate its association network knot of " card palace " formula can be formed in aqueous medium
Structure has thickening property and thixotropy, adsorption capacity is strong, it is not easy to crack, be not easy to take off.The present inventor is by lot of experiments comparison hair
Existing, after the inorganic creaming agent such as aluminium-magnesium silicate and lithium magnesium silicate, modified pitch mixture can realize good emulsifying effectiveness,
And make whole emulsion intercalation method more preferable, easily facilitate storage, and the sealant after construction is dried rapidly,
A few hours can meet the requirements after general construction, increase the facility of construction.By test analysis, rapid-curing cutback creaming agent is in sealing compound
In with the structure of " card palace " formula form and wrap up moisture, one side rapid-curing cutback creaming agent and forming for water are less than organic with active force
The Hyarogen-bonding that creaming agent is formed with water, such water are easier to from sealing compound out, still further aspect " card palace " formula
Structure form by inner and table draining gas-permeable channels, draining gas-permeable channels are like being the nose that can freely breathe one by one
Son, steam are gradually released inside sealing compound by the channel, and dry solidification is since internal entirety, in drying process
In be not in surface skining phenomenon, in sealing compound moisture volatilization reduce, draining gas-permeable channels by atmospheric pressure, gravity and
It tapers into and narrows under molecule Blang's warm-up movement influence, when sealing compound is completely solid, channel is completely closed.Sealing compound is fast
The characteristics of rapid-curing cutback dry solidification, highly shortened the construction application time, improves construction efficiency, can meet filleting thickness well
Application conditions.The present invention regard lithium magnesium silicate and/or aluminium-magnesium silicate etc. as creaming agent, glass microballoon, glass bead, foaming pottery
The materials such as porcelain, expanded plastic particles are as packing material, the unique three dimensions chain structure of britesorb and special needle, stick
Shape crystal structure is by particle studded more tight such as glass microballoon, under the promotion of the particles such as glass microballoon, modified pitch
Viscosity and compactness are increased, and since the particles such as glass microballoon are light hard, the sag for not influencing sealing compound is but promoted
The ductility of sealing compound.For modified pitch sealing compound under the function influence of the particle characteristics such as glass microballoon, stability is good, dry
Rapidly, heat preservation, heat-insulated, waterproof and adhesiving effect are enhanced so that sealing effect can be more good and lasting.By the invention
Thermal-insulating waterproof sealing compound for build seam class filleting, rate of drying is fast, and shrinking percentage is low, and thermal coefficient is low, construction is simple be easy,
Can directly pointing in wider deeper building gap still can rapid draing solidification, waterproof sealing cream after solidification is with excellent
Function of heat insulation, be excellent waterproof insulation sealed product.
Beneficial effects of the present invention：
(1) present invention uses lithium magnesium silicate and/or aluminium-magnesium silicate etc. to be used as rapid-curing cutback creaming agent, compared to organic cellulose
Ether and association type polyurethanes thickener have better thixotropy and quick dewatering drying characteristic, significantly improve waterproof
The construction application performance of sealing compound；
(2) present invention has the glass microballoon of lightweight heat-proof, glass bead, foamed ceramic, expanded plastic particles etc. more
The excellent organic of pore structure thermal and insulating performance and inorganic thermal insulation material are added what aqueous rubber state water-repellent paint was prepared
Thermal-insulating waterproof sealing compound has faster rate of drying, better caking property, high temperature resistant compared to other filletings sealed product
And thermal and insulating performance, effects of energy conservation and environmental protection protrude；
(3) thermal-insulating waterproof sealing compound of the invention can be used for building the filletings such as expansion joint, subsiding crack, and contractibility is low,
Construction is simple be easy, can directly pointing in wider deeper building gap still can rapid draing cure, well solve
The film shrinking percentage of aqueous rubber state water-repellent paint is big, is not suitable for the problem in pointing gap.
(4) present invention is prepared the dispersion of bitumen regenerant, matrix pitch and modifying agent high-speed uniform using one kettle way
Rubbery state water-repellent paint is made through high speed shear grinding emulsification, livering in rubber asphalt mixture and emulsion, then by glass microballoon,
Glass bead etc. is added in rubbery state water-repellent paint and stirs evenly, and thermal-insulating waterproof sealing compound is made, which puts into raw material letter
It is singly easy to get, without the separation of intermediate, directly obtains complicated molecule, prepare sealing compound uniform and smooth, the quality of gained
Higher；The preparation method improves production efficiency, is also beneficial to stable quality and environmental protection.
Specific implementation mode
It is limited with reference to specific embodiment technical scheme of the present invention is further, but claimed
Range describes made by being not only limited to.
Embodiment one
Component A is：
Wherein modified pitch is 90#Asphalt and SBS, SIS are modified that agent composition is mixed and modified to be formed；
Wherein rapid-curing cutback creaming agent is lithium magnesium silicate；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：Glass microballoon；
The weight ratio of component A and B component is 50：50.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 160 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix 10min,
200 DEG C are to slowly warm up to, constant temperature stirs 4h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier, heats
Constant temperature stir-activating 40min is to get emulsion blends II after to 70 DEG C；Mixture II is pumped into colloid mill, colloid is opened
Mill, then mixture I is pumped into get component A rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 50 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment two
Component A is：
Wherein modified pitch is 50#Asphalt and SBS modifier is mixed and modified forms；
Wherein rapid-curing cutback creaming agent is aluminium-magnesium silicate；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass bead and foamed ceramic；
The weight ratio of component A and B component is 50：1.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 160 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix 10min,
195 DEG C are to slowly warm up to, constant temperature stirs 3h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier, heats
Constant temperature stir-activating 40min is to get emulsion blends II after to 70 DEG C；Mixture II is pumped into colloid mill, colloid is opened
Mill, then mixture I is pumped into get component A rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 1 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment three
Component A is：
Wherein modified pitch is 200#Asphalt and SBS modifier is mixed and modified forms；
Wherein rapid-curing cutback creaming agent is the mixture of lithium magnesium silicate and aluminium-magnesium silicate；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass bead and expanded plastic particles；
The weight ratio of component A and B component is 50：50.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 150 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix 20min,
200 DEG C are to slowly warm up to, constant temperature stirs 4h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier, heats
Constant temperature stir-activating 40min is to get emulsion blends II after to 70 DEG C；Mixture II is pumped into colloid mill, colloid is opened
Mill, then mixture I is pumped into get component A rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 50 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Example IV
Component A is：
Bitumen regenerant 80%
Rapid-curing cutback creaming agent 10%
Emulsion 10%
Wherein rapid-curing cutback creaming agent is aerosil；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：Glass microballoon and glass bead, the mixture of foamed ceramic and expanded plastic particles；
The weight ratio of component A and B component is 50：10.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：The bitumen regenerant and rapid-curing cutback creaming agent of mass percent are weighed, is thrown
Enter into reaction kettle, is warming up to 140 DEG C and stirs evenly to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsification
Agent, constant temperature stir-activating 40min is to get emulsion blends II after being heated to 50 DEG C；Mixture II is pumped into colloid mill, is opened
Colloid mill is opened, then is pumped into mixture I to get rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 10 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment five
Component A is：
Modified pitch 75%
Rapid-curing cutback creaming agent 0.01%
Emulsion 24.99%
Wherein modified pitch is 90#Asphalt with APP modifying agent is mixed and modified forms；
Wherein rapid-curing cutback creaming agent is bentonite；
Wherein emulsion is the aqueous solution of emulsifier sodium butylnaphthalenesulfonate；
B component is：Foamed ceramic；
The weight ratio of component A and B component is 50：5.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 155 DEG C and stirs evenly, rapid-curing cutback creaming agent is added under agitation and mixes 20min, be to slowly warm up to
180 DEG C, constant temperature stirs 4h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier, it is permanent after being heated to 60 DEG C
Warm stir-activating 30min is to get mixture II；Mixture II is pumped into colloid mill, opens colloid mill, then be pumped into mixture I,
Up to component A rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 5 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment six
Component A is：
Wherein modified pitch is 70#Asphalt and SBR, SIS are modified that agent composition is mixed and modified to be formed；
Wherein rapid-curing cutback creaming agent is attapulgite and bentonitic mixture；
Wherein emulsion is the aqueous solution of the mixture of emulsifier neopelex and sodium butylnaphthalenesulfonate.
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass microballoon and glass bead；
The weight ratio of component A and B component is 50：20.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 160 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix 15min,
190 DEG C are to slowly warm up to, constant temperature stirs 2h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier, heats
Constant temperature stir-activating 20min is to get emulsion blends II after to 60 DEG C；Mixture II is pumped into colloid mill, colloid is opened
Mill, then be pumped into mixture I, i.e., component A obtains rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 20 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment seven
Component A is：
Wherein modified pitch is 90#Asphalt with SBS modifier is mixed and modified forms；
Wherein rapid-curing cutback creaming agent is the mixture of lithium magnesium silicate and attapulgite, and wherein lithium magnesium silicate mass percent is
4%, attapulgite mass percent is 4%.
Wherein emulsion is in emulsifier neopelex, alkyl phenol polyoxyethylene ether phosphate and loose ester acid soap
Mixture aqueous solution.
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass microballoon and glass bead；
The weight ratio of component A and B component is 50：10.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Weigh 50#Asphalt and modifying agent, put into reaction kettle, rise
Temperature is stirred evenly to 150 DEG C, and bitumen regenerant, rapid-curing cutback creaming agent are added under agitation and mixes 10min, is to slowly warm up to
190 DEG C, constant temperature stirs 3h to get asphalt mixture I；The water of formulation weight percentage is added into Soap liquid pot, adds emulsification
Agent, constant temperature stir-activating 30min is to get emulsion blends II after being heated to 50 DEG C；Mixture II is pumped into colloid mill, is opened
Colloid mill is opened, then is pumped into mixture I to get component A rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 10 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment eight
Component A is：
Wherein modified pitch is 200#Asphalt and SBS, SBR, APP, SIS, SEBS modification agent composition are mixed and modified
It forms；
Wherein rapid-curing cutback creaming agent is aluminium-magnesium silicate and bentonitic mixture.
Wherein emulsion is the aqueous solution of emulsifier pine ester acid soap.
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass microballoon and glass bead；
The weight ratio of component A and B component is 50：5.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Weigh the 200 of mass percent#Asphalt and modifying agent, input
It into reaction kettle, is warming up to 140 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix
20min is to slowly warm up to 180 DEG C, and constant temperature stirs 2h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsification
Agent, constant temperature stir-activating 40min is to get emulsion blends II after being heated to 40 DEG C；Mixture II is pumped into colloid mill, is opened
Colloid mill is opened, then is pumped into mixture I to get component A rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 5 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment nine
Wherein modified pitch is 50#Asphalt with SBS modifier is mixed and modified forms；
Wherein rapid-curing cutback creaming agent is lithium magnesium silicate；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein activator is sodium hydroxide；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass microballoon and glass bead；
The weight ratio of component A and B component is 50：15.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 160 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix 15min,
190 DEG C are to slowly warm up to, constant temperature stirs 3h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier and work
Agent, constant temperature stir-activating 20min is to get emulsion blends II after being heated to 60 DEG C；Mixture II is pumped into colloid mill,
Colloid mill is opened, then is pumped into mixture I, i.e., component A obtains rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 15 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Embodiment ten
Wherein modified pitch is 90#Asphalt and APP, SIS are modified that agent composition is mixed and modified to be formed；
Wherein rapid-curing cutback creaming agent is the mixture of lithium magnesium silicate, aluminium-magnesium silicate and attapulgite.
Wherein emulsion is the mixture of alkane sodium olefin sulfonate and modified bay alcohol radical sodium sulphate.
Wherein activator is the mixture of sodium hydroxide and potassium hydroxide.
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：The mixture of glass microballoon and glass bead；
The weight ratio of component A and B component is 50：25.
Preparation method：
(1) prepared by component A rubbery state water-repellent paint：Asphalt and modifying agent are weighed by mass percentage, are put into anti-
It answers in kettle, is warming up to 160 DEG C and stirs evenly, bitumen regenerant and rapid-curing cutback creaming agent are added under agitation and mix 15min,
190 DEG C are to slowly warm up to, constant temperature stirs 3h to get asphalt mixture I；Water is added into Soap liquid pot, adds emulsifier and work
Agent, constant temperature stir-activating 40min is to get emulsion blends II after being heated to 70 DEG C；Mixture II is pumped into colloid mill,
Colloid mill is opened, then is pumped into mixture I, i.e., component A obtains rubbery state water-repellent paint；
(2) weight ratio for pressing component A and B component is 50：B component is added to component A rubbery state waterproof and applied by 25 ratio
In material and high-speed stirred is uniformly to get the thermal-insulating waterproof sealing compound of filleting；
(3) vacuum defoamation：The thermal-insulating waterproof sealing compound of filleting is cooled down, vacuum defoamation is filling to get this product.
The sealing compound is applied to the encapsulation process of the construction joints such as expansion joint, the deformation joint of building and crack repair.
Comparative example 1
The composition and ratio of component is：
Wherein modified pitch is 90#Asphalt and SBS, SIS are modified that agent composition is mixed and modified to be formed；
Wherein rapid-curing cutback creaming agent is lithium magnesium silicate；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
Component ratio and preparation method are as in the first embodiment, the difference is that be not added with B component.
Comparative example 2
Component A is：
Wherein modified pitch is 90#Asphalt and SBS, SIS are modified that agent composition is mixed and modified to be formed；
Wherein creaming agent is hydroxyethyl ether cellulose；
Wherein emulsion is the aqueous solution of emulsifier neopelex；
Wherein bitumen regenerant is using the high-quality naphthenic base heavy oil of South America Venezuela as raw material, through normal pressure vacuum distillation
At.
B component is：Glass microballoon；
The weight ratio of component A and B component is 50：50.Component ratio and preparation method as in the first embodiment, the difference is that
Creaming agent is changed to organic creaming agent.
Comparative example 3
By the prescription of 201110145655.4 embodiment 1 of Chinese patent, manufactured sealing compound.
1 sealing compound Performance of test example
The adhesion strength and thermal and insulating performance of product of the present invention and comparative example product are tested, test result is shown in Table
1.Heat insulation property (β) is specifically examined and computational methods are as follows,
1. size prepares sealing compound model as required, it is placed on the face suitable for reading of thermostat after its drying, covers cover board, and
Test sensor, opening temperature instrument are inserted among cover board in hold-down support；
2. loading onto clear water in thermostat, power supply heating is opened, and record the time；
3. it is constant after 30-40 DEG C after the temperature in thermostat, start the temperature for measuring defined time interior sealing cream surface
Degree is calculated the thermal and insulating performance of sealing compound by computational methods.
4. computational methods
Parameter setting：
T0The steady temperature (DEG C) of clear water in-thermostat
T1- plus insulation particle sealing compound model surface temperature (DEG C)
T2The surface temperature (DEG C) of the sealing compound model of-present invention addition insulation particle
ΔT1- plus the temperature difference (DEG C) in sealing compound model surface and the thermostat of insulation particle
ΔT2The sealing compound model surface of the addition insulation particle of-present invention and the temperature difference (DEG C) in thermostat
β-thermal and insulating performance (temperature difference ratio between the two print)
ΔT1=(T0-T1)
ΔT2=(T0-T2)
β=(Δ T2-ΔT1)/(ΔT1+ΔT2) × 100%
1 is the results are shown in Table according to what above inspection and computational methods obtained.
1 caulking sealing cream technical indicator of table
Table 1- continues caulking sealing cream technical indicator
From the testing result of upper table 1 it is found that the thermal-insulating waterproof sealing compound of the present invention have it is splendid be bonded and sealed performance with
And preferable thermal and insulating performance, 2.0MPa or more is may be up to the drawing adhesion strength of concrete, average heat insulation property β value
80 or more.
Embodiment 1 is contrasted with comparative example 2, only changes the type of creaming agent.The embodiment of the present invention 1 (only uses silicon
Sour magnesium lithium is as creaming agent) prepared by sealing compound its be superior to performances such as concrete drawing adhesion strength and heat insulation properties
Comparative example 2 (only uses hydroxyethyl ether cellulose as creaming agent), illustrates the sealing compound for using inorganic creaming agent lithium magnesium silicate
Comprehensive performance is more excellent, illustrates that lithium magnesium silicate creaming agent has more fully played the effect of infiltration embedded structure in sealing compound system,
This be other creaming agents in pitch mill processes less than property.
Embodiment 1 is contrasted with comparative example 1, and difference lies in comparative examples 1, and B component thermal insulation material not to be added, and embodiment 1 is close
It seals the thermal and insulating performance of cream and adhesion strength is substantially better than comparative example 1, especially thermal and insulating performance in highly significant difference；
The thermal and insulating performance value and adhesion strength of embodiment 1 are in significant difference with comparative example 3 (Chinese patent 201110145655.4),
Illustrate that sealing compound prepared by inventive formulation has excellent comprehensive performance.
Show that the sealing compound of the invention pointing in filleting is closely knit compact through outdoor application experimental test result, thixotropy
Good, construction resistance is small, and constructing operation is easily easy, and rate of drying is fast, and for drying process without surface skining phenomenon, performance is complete
Expected result can be reached.The sealing compound being formulated using the embodiment of the present invention 1 and embodiment 7, pointing is in 10mm wide respectively
In the deep gaps with 5mm wide 5mm depths 10mm, it is completely dried in 68 hours, 50 hours respectively, the construction application time is short, applies
Working medium amount is guaranteed.
A kind of thermal-insulating waterproof sealing compound of filleting of the present invention can be applied to the deformation joints such as expansion joint, the subsiding crack of building and
The encapsulation process of crack repair has and adapts to the features such as expansion joint deformability is strong, and durability is high, improves conventional telescopic seam
The reliability of filleting seepage control technique, safety, which solve the shortcomings of existing concrete expansion joint repair process, improve
Repair process technology in concrete works expansion joint has good application prospect in terms of reinforcement of concrete defect.The filleting is close
Sealing cream has excellent thermal and insulating performance, there is good effects of energy conservation and environmental protection.
The above is presently preferred embodiments of the present invention, is not imposed any restrictions to the present invention that those skilled in the art are sharp
A little simple modification, equivalent variations or modification are made with the content of the disclosure above, is all fallen in protection scope of the present invention.
Claims (16)
1. a kind of thermal-insulating waterproof sealing compound of filleting, which is characterized in that include mainly component A and B component, the component A
Including modified pitch, bitumen regenerant, rapid-curing cutback creaming agent and emulsion；The B component is thermal insulation material.
2. the thermal-insulating waterproof sealing compound of filleting as described in claim 1, which is characterized in that include mainly component A and B groups
Point, by percentage to the quality,
The composition and ratio of component A is：
Modified pitch 0~75%
Bitumen regenerant 0~80%
Rapid-curing cutback creaming agent 0.01~30%
Emulsion 10~70%；
B component is organic or inorganic thermal insulation material.
3. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 1 or 2, which is characterized in that the component A further includes
Activator.
4. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 3, which is characterized in that the activator is anion
Or cationic activation agent.
5. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 4, which is characterized in that the activator is hydroxide
One or more kinds of mixtures in sodium, sodium bicarbonate, potassium hydroxide, saleratus, hydrochloric acid, sulfuric acid, nitric acid.
6. such as the thermal-insulating waterproof sealing compound of Claims 1 to 5 any one of them filleting, which is characterized in that the component A
Weight ratio with B component is 50：1~50.
7. such as the thermal-insulating waterproof sealing compound of Claims 1 to 5 any one of them filleting, which is characterized in that the B component
For one or more kinds of mixtures in glass microballoon, glass bead, foamed ceramic, expanded plastic particles.
8. such as the thermal-insulating waterproof sealing compound of Claims 1 to 5 any one of them filleting, which is characterized in that the rapid-curing cutback
Creaming agent is inorganic creaming agent.
9. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 8, which is characterized in that the rapid-curing cutback creaming agent is silicon
One or more kinds of mixtures in sour magnesium lithium, aluminium-magnesium silicate, attapulgite or bentonite.
10. such as the thermal-insulating waterproof sealing compound of Claims 1 to 5 any one of them filleting, which is characterized in that the emulsification
Liquid is cation, anion or nonionic colas.
11. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 10, which is characterized in that the emulsion is emulsification
Agent metal carboxylate, fatty acid salt, Sulfonates, phosphates, alkyl amine, polyethenoxy ether class, polyoxypropylene ethers,
The aqueous solution of one or more kinds of mixtures of amides or quaternary ammonium salt.
12. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 11, which is characterized in that the emulsifier is 12
Sodium alkyl benzene sulfonate, sodium butylnaphthalenesulfonate, alkane sodium olefin sulfonate, modified bay alcohol radical sodium sulphate, alkyl phenol polyoxyethylene ether phosphorus
One or more kinds of mixtures in acid esters, loose ester acid soap.
13. a kind of thermal-insulating waterproof sealing compound of filleting, which is characterized in that the sealing compound is applied to the expansion joint of building, becomes
The construction joints such as shape seam and the encapsulation process of crack repair.
14. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 1 or 2, which is characterized in that include mainly component A and B
Component, by percentage to the quality：
The composition and ratio of component A is：
Modified pitch 1~50%
Bitumen regenerant 15~60%
Rapid-curing cutback creaming agent 0.2~10%
Emulsion 10~45%；
B component is inorganic heat insulation material；
The weight ratio of the component A and B component is 50：(8-12).
15. the thermal-insulating waterproof sealing compound of filleting as claimed in claim 1 or 2, which is characterized in that include mainly component A and B
Component, by percentage to the quality,
The composition and ratio of component A is：
Modified pitch 10~45%
Bitumen regenerant 20~50%
Attapulgite 0.1~5%
Lithium magnesium silicate 0.1~5%
Emulsion 15~40%
The modified pitch is modified by 90# asphalt and SBS asphalt modifiers；
B component is glass microballoon, glass bead；
The weight ratio of the component A and B component is 50：10.
16. a kind of preparation method of the thermal-insulating waterproof sealing compound of filleting, which is characterized in that the thermal-insulating waterproof for preparing filleting is close
Cream is sealed, is included the following steps：
(1) prepared by component A rubbery states water-repellent paint：By modifying agent and pitch, bitumen regenerant and rapid-curing cutback creaming agent, put into anti-
It answers and is modified in kettle to get rubber asphalt mixture, then emulsion is subjected to breast by colloid mill to rubber asphalt mixture
Up to rubbery state water-repellent paint after change, livering；
(2) component B is added to the thermal-insulating waterproof sealing compound stirred evenly in rubbery state water-repellent paint to get filleting；
(3) vacuum defoamation to get.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810206169.0A CN108395843A (en) | 2018-03-13 | 2018-03-13 | A kind of thermal-insulating waterproof sealing compound of filleting and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810206169.0A CN108395843A (en) | 2018-03-13 | 2018-03-13 | A kind of thermal-insulating waterproof sealing compound of filleting and its preparation method and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108395843A true CN108395843A (en) | 2018-08-14 |
Family
ID=63091754
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810206169.0A Pending CN108395843A (en) | 2018-03-13 | 2018-03-13 | A kind of thermal-insulating waterproof sealing compound of filleting and its preparation method and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108395843A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112375540A (en) * | 2020-11-25 | 2021-02-19 | 山东省金帅防水材料有限公司 | Environment-friendly anti-aging waterproof sealant and preparation method thereof |
| CN113105843A (en) * | 2021-04-17 | 2021-07-13 | 河南阳光防水科技有限公司 | High-elasticity waterproof sealant special for deformation joint |
| CN114590010A (en) * | 2022-03-24 | 2022-06-07 | 亚士防水科技(滁州)有限公司 | Asphalt sizing material, waterproof asphalt coiled material and application |
| CN115030330A (en) * | 2022-06-14 | 2022-09-09 | 潍坊市宇虹防水材料(集团)有限公司 | SBS elastomer modified asphalt waterproof coiled material and preparation method thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4231884A (en) * | 1979-01-16 | 1980-11-04 | American Gilsonite Company | Water retardant insulation composition comprising treated low density granular mineral material and finely divided limestone or similar carbonate or silicate mineral particles and method for using same |
| CN101880139A (en) * | 2010-05-26 | 2010-11-10 | 上海大学 | Low-carbon ceramic wall body heat insulating paste and preparation method thereof |
| CN102898850A (en) * | 2012-11-10 | 2013-01-30 | 广西金雨伞防水装饰有限公司 | Modified emulsified asphalt waterproof sealant and preparation method thereof |
| CN103803850A (en) * | 2012-11-08 | 2014-05-21 | 广西启利新材料科技股份有限公司 | Thermal insulation embedded seam filling and smoothing cream and its preparation method |
| CN105238292A (en) * | 2014-07-12 | 2016-01-13 | 卢桂才 | Reactive type modified emulsified asphalt and rubber waterproof sealant, and preparation method therefor |
| CN105314999A (en) * | 2014-07-29 | 2016-02-10 | 金承黎 | Nano porous high-temperature-insulating material taking thixotropic colloid as template agent and preparation method for high-temperature-insulating material |
| CN105331126A (en) * | 2015-11-26 | 2016-02-17 | 佛山高富中石油燃料沥青有限责任公司 | No. 110 asphalt and preparation method thereof |
| CN105778533A (en) * | 2016-03-29 | 2016-07-20 | 河南省交通运输厅京珠高速公路新乡至郑州管理处 | High-permeability composite high-molecular polymer hot-melt crack filling material and preparation method |
| CN105802266A (en) * | 2016-04-25 | 2016-07-27 | 广州市市政工程维修处 | Pavement super-sticky thin adhesive cement sealing layer mixture and preparation method thereof |
-
2018
- 2018-03-13 CN CN201810206169.0A patent/CN108395843A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4231884A (en) * | 1979-01-16 | 1980-11-04 | American Gilsonite Company | Water retardant insulation composition comprising treated low density granular mineral material and finely divided limestone or similar carbonate or silicate mineral particles and method for using same |
| CN101880139A (en) * | 2010-05-26 | 2010-11-10 | 上海大学 | Low-carbon ceramic wall body heat insulating paste and preparation method thereof |
| CN103803850A (en) * | 2012-11-08 | 2014-05-21 | 广西启利新材料科技股份有限公司 | Thermal insulation embedded seam filling and smoothing cream and its preparation method |
| CN102898850A (en) * | 2012-11-10 | 2013-01-30 | 广西金雨伞防水装饰有限公司 | Modified emulsified asphalt waterproof sealant and preparation method thereof |
| CN105238292A (en) * | 2014-07-12 | 2016-01-13 | 卢桂才 | Reactive type modified emulsified asphalt and rubber waterproof sealant, and preparation method therefor |
| CN105314999A (en) * | 2014-07-29 | 2016-02-10 | 金承黎 | Nano porous high-temperature-insulating material taking thixotropic colloid as template agent and preparation method for high-temperature-insulating material |
| CN105331126A (en) * | 2015-11-26 | 2016-02-17 | 佛山高富中石油燃料沥青有限责任公司 | No. 110 asphalt and preparation method thereof |
| CN105778533A (en) * | 2016-03-29 | 2016-07-20 | 河南省交通运输厅京珠高速公路新乡至郑州管理处 | High-permeability composite high-molecular polymer hot-melt crack filling material and preparation method |
| CN105802266A (en) * | 2016-04-25 | 2016-07-27 | 广州市市政工程维修处 | Pavement super-sticky thin adhesive cement sealing layer mixture and preparation method thereof |
Non-Patent Citations (4)
| Title |
|---|
| GEORGE WYPYVH编著: "《填料手册（第二版）》", 31 October 2002, 中国石化出版社 * |
| 卢少忠编著: "《建筑涂料施工》", 31 August 2007, 中国建材工业出版社 * |
| 张晚佳: "《化工管理》", 31 December 2016 * |
| 白景瑞等: "《化妆品配方设计及应用实例》", 31 October 2001, 中国石化出版社 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112375540A (en) * | 2020-11-25 | 2021-02-19 | 山东省金帅防水材料有限公司 | Environment-friendly anti-aging waterproof sealant and preparation method thereof |
| CN113105843A (en) * | 2021-04-17 | 2021-07-13 | 河南阳光防水科技有限公司 | High-elasticity waterproof sealant special for deformation joint |
| CN114590010A (en) * | 2022-03-24 | 2022-06-07 | 亚士防水科技(滁州)有限公司 | Asphalt sizing material, waterproof asphalt coiled material and application |
| CN115030330A (en) * | 2022-06-14 | 2022-09-09 | 潍坊市宇虹防水材料(集团)有限公司 | SBS elastomer modified asphalt waterproof coiled material and preparation method thereof |
| CN115030330B (en) * | 2022-06-14 | 2022-12-09 | 潍坊市宇虹防水材料(集团)有限公司 | SBS elastomer modified asphalt waterproof coiled material and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN108395843A (en) | A kind of thermal-insulating waterproof sealing compound of filleting and its preparation method and application | |
| CA2797305C (en) | Rubber asphalt and preparation method thereof | |
| CN108395844A (en) | One-time formed rubbery state water-repellent paint of a kind of multiple tracks thickness painting and preparation method thereof | |
| CN110171942B (en) | Moisture-curing reaction type asphalt pavement cold-patch material and preparation method thereof | |
| CN107325729B (en) | A kind of uncured rubber asphalt waterproof coating and preparation method thereof | |
| KR101977583B1 (en) | Binder Compositions for Middle Temperature Asphalt Concrete Using Stylene Isoprene Stylene and Constructing Methods Using Thereof | |
| CN105408280A (en) | Room-temperature circulation asphalt composition and road paving method using the same | |
| CN106883626A (en) | A kind of modified asphalt for road and preparation method | |
| CN107384206A (en) | Rubber water-proof paint and the compound construction technology of uncured rubber asphalt waterproof coating | |
| CN108083688A (en) | Solvent-borne type cold repairing asphalt mixture and preparation method thereof | |
| KR102188825B1 (en) | Waterproof Asphalt Concrete Composition for Overlay Pavement Having Petroleum Resin Added Hydrogen, Stylene Isoprene Stylene and Aggregate-powder of Improved Grain Size and Constructing Methods Using Thereof | |
| CN107722649A (en) | A kind of modified pitch and its preparation and application | |
| CN106700009A (en) | Polyurethane composition, polyurethane water-stopping strip and steel-edged water-stopping belt comprising water-stopping strip | |
| CN109137554A (en) | A kind of anti-aging elastomer modified asphalt waterproof roll and preparation method | |
| CN106700216B (en) | It is a kind of instead to glue formula splash guard and preparation method thereof | |
| KR101100416B1 (en) | Warm-mix asphalt additive containing anti-stripping effects and manufacturing method thereof | |
| CN101423419B (en) | Concrete impervious test piece sealant | |
| CN105130256B (en) | A kind of energy-saving type asphalt concrete modifying agent and preparation method thereof | |
| CN113896487B (en) | Preparation method and application of water-curing reaction type normal-temperature liquid asphalt and mixture thereof | |
| CN110481113A (en) | A kind of environment friendly plastic rubber runway and preparation method thereof | |
| KR102207015B1 (en) | Water-Impermeable Waterproof Asphalt Concrete Compositions Comprising Urethane Resin and Constructing Methods Using Thereof | |
| Zhang et al. | An asphalt emulsion modified by compound of epoxy resin and styrene-butadiene rubber emulsion | |
| KR102207040B1 (en) | Water-Impermeable Waterproof Asphalt Concrete Compositions Comprising Low Density Polyethylene and Constructing Methods Using Thereof | |
| KR102207016B1 (en) | Modified-Asphalt Concrete Compositions for Roads Using Latex Resin and Constructing Methods Using Thereof | |
| CN108977078A (en) | A kind of buildings waterproof sealing compound and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180814 |