CN108395111A - A kind of glass surface gradual change frosting effect manufacture craft and device - Google Patents
A kind of glass surface gradual change frosting effect manufacture craft and device Download PDFInfo
- Publication number
- CN108395111A CN108395111A CN201810246818.XA CN201810246818A CN108395111A CN 108395111 A CN108395111 A CN 108395111A CN 201810246818 A CN201810246818 A CN 201810246818A CN 108395111 A CN108395111 A CN 108395111A
- Authority
- CN
- China
- Prior art keywords
- gradual change
- glass
- glass surface
- frosting
- change frosting
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000011521 glass Substances 0.000 title claims abstract description 65
- 230000008859 change Effects 0.000 title claims abstract description 43
- 230000000694 effects Effects 0.000 title claims abstract description 25
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims abstract description 22
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 10
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 8
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims abstract description 8
- 235000011130 ammonium sulphate Nutrition 0.000 claims abstract description 8
- KVBCYCWRDBDGBG-UHFFFAOYSA-N azane;dihydrofluoride Chemical compound [NH4+].F.[F-] KVBCYCWRDBDGBG-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000008155 medical solution Substances 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000004140 cleaning Methods 0.000 claims abstract description 5
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 4
- -1 calcirm-fluoride Substances 0.000 claims abstract description 4
- 230000008021 deposition Effects 0.000 claims abstract description 4
- 235000011187 glycerol Nutrition 0.000 claims abstract description 4
- 238000005507 spraying Methods 0.000 claims abstract description 4
- 239000007921 spray Substances 0.000 claims description 24
- 238000000429 assembly Methods 0.000 claims description 20
- 230000000712 assembly Effects 0.000 claims description 20
- NJPPVKZQTLUDBO-UHFFFAOYSA-N novaluron Chemical compound C1=C(Cl)C(OC(F)(F)C(OC(F)(F)F)F)=CC=C1NC(=O)NC(=O)C1=C(F)C=CC=C1F NJPPVKZQTLUDBO-UHFFFAOYSA-N 0.000 claims description 17
- 239000002518 antifoaming agent Substances 0.000 claims description 6
- 230000005540 biological transmission Effects 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 238000000151 deposition Methods 0.000 claims description 3
- 239000004576 sand Substances 0.000 claims description 2
- 238000005516 engineering process Methods 0.000 abstract description 5
- 230000007704 transition Effects 0.000 description 4
- 235000009508 confectionery Nutrition 0.000 description 3
- 230000035699 permeability Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 229920002799 BoPET Polymers 0.000 description 1
- 238000002231 Czochralski process Methods 0.000 description 1
- 206010054949 Metaplasia Diseases 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000015689 metaplastic ossification Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000007665 sagging Methods 0.000 description 1
- 238000005488 sandblasting Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C15/00—Surface treatment of glass, not in the form of fibres or filaments, by etching
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Surface Treatment Of Glass (AREA)
- Detergent Compositions (AREA)
Abstract
The invention belongs to gradual change glass technology field more particularly to a kind of glass surface gradual change frosting effect manufacture craft and devices, include the following steps：Configure gradual change frosting liquid：By water, glycerine, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent according to mass ratio be 60 70:4‑6:20‑25:2‑4：1‑3:3‑6:0.5 1 ratio is added in medical solution pool, and mixing 2 hours is stirred at room temperature, and gradual change frosting liquid is made；Make gradual change mat glass：Glass surface is cleaned, back of the body protection is carried out, the angle that the angle of inclination of frosting line is placed so as to adjust glass is adjusted, using step 1）The gradual change frosting liquid of production carries out 10 15min of spraying to glass surface, in glass surface self-assembling formation by thin to thick deposition reaction layer, remove cleaning surface, production technology provided by the invention can meet mass production requirement, and product yield is high, gradual change width and effect are controllable, and glass size is unlimited, meet the customer personalized customized demand of different field.
Description
Technical field
The invention belongs to gradual change glass technology field more particularly to a kind of glass surface gradual change frosting effect manufacture craft and
Device.
Background technology
Develop with the lasting propulsion of national urbanization process, and under the influence of land resource is increasingly limited, building is only
Can be to space to be wanted in the air, executive information systems are more and more, in new building structure, will there is several portions of working relation
Door converges in a big room, is spaced multiple partitions, has not only been conducive to inter-sectional work and has got in touch with, but also convenient for management, employee has been facilitated to do
Thing, such intensive working way of open type have become the first choice and trend of even big little company of government bodies, previous solid wall
Solid door etc. obstructs sight and the space division material of permeability is substantially unobscured, and the good glass material of daylighting is taken
Generation, gradual change glass are novel post processed glass products, can meet sight permeability and local concealment requirement, market application simultaneously
It has a extensive future.Plain mode is exactly directly to be bonded a gradual change PET film in glass surface or gradually continue sandblasting to make, product quality
It is not high, it is suitble to common place application；Chemical gradual change glass product is by carrying out technical finesse on glass surface, realizing by leading to
Impermeable natural transition is arrived thoroughly, be allowed to not only remain daylighting permeability but also has many advantages, such as certain concealment, is applied to large size more
High-end market, star office building interior trim.
Chemistry gradual change glass is completed using czochralski process at present, is operated, is realized from the lifting in liquid by glass
Different height is different from liquid reaction time length, and frosting effect is deep mixed, finally obtains from penetrating to impermeable effect mistake
It crosses, which is that by the production of batch metaplasia, but there is residual liquid medicine in the defective workmanship of glass surface sagging, causes
Product yield is relatively low and the root of existing market Difficulty.
Invention content
The object of the present invention is to provide a kind of glass surface gradual change frosting effect manufacture craft and devices.
In order to achieve the above objectives, the technical solution adopted by the present invention is：
A kind of glass surface gradual change frosting effect manufacture craft, which is characterized in that include the following steps：
1）Configure gradual change frosting liquid：By water, glycerine, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent according to mass ratio
For 60-70: 4-6 : 20-25 : 2-4：1-3 : 3-6 :The ratio of 0.5-1 is added in medical solution pool, at room temperature with
50-80 revs/min of rotating speed is stirred 2 hours, and gradual change frosting liquid is made；
2）Make gradual change mat glass：Glass surface is cleaned, carries out back of the body protection, adjust the angle of inclination of frosting line so as to adjust
The angle that glass is placed, using step 1）The gradual change frosting liquid of production carries out spraying 10-15min to glass surface, wherein glass
The speed that glass is advanced is 1-5 ms/min, and cleaning surface is removed to thick deposition reaction layer by thin in glass surface self-assembling formation
.
Further, step 1）Middle auxiliary agent is levelling agent and antifoaming agent, and the mass ratio of levelling agent and antifoaming agent is 1:1.
Further, step 2）The angle of inclination of middle automatic frosting line is 0-30 °.
A kind of glass surface gradual change frosting effect producing device, including pedestal are set to the supporting leg of pedestal lower part, are set to pedestal
The transmission component at top, the pedestal top are equipped with three groups of spray assemblies, and the distance of two neighboring spray assemblies is more than glass
Length, the spray assemblies extract liquid by water pump from medical solution pool.
Further, the supporting leg is four, wherein two height of landing leg on the inside of the spray assemblies are certain, in addition two
The height of a supporting leg is adjustable, to make the tilt adjustable of pedestal.
Further, the spray assemblies include right angle jet pipe, and the horizontal segment of the right angle jet pipe is located above pedestal, and
One group of nozzle and position sensor are additionally provided on the horizontal segment of right angle jet pipe, the vertical section of right angle jet pipe is equipped with control and switchs.
Further, the transmission component includes shaft and the runner in shaft.
Present invention has the advantage that：The production technology not only meets mass production requirement, but also product yield is high, gradually
Trapezoidal and effect are controllable, and glass size is unlimited, meet the customer personalized customized demand of different field；Since the gradual change of configuration is covered
Sand liquid contains a large amount of water, and viscosity is very low, and ammonium acid fluoride, citric acid, ammonium sulfate equal size are relatively low, and frosting reaction is relatively more slow
Slowly, frosting effect as needed, frosting time lengthening.
Description of the drawings
Fig. 1 is the glass surface gradual change frosting effect producing device structural schematic diagram of the present invention.
1, pedestal；2, supporting leg；3, spray assemblies；31, nozzle；32, jet pipe；4, transmission component；5, medical solution pool；6, glass.
Specific implementation mode
Embodiment 1
First, gradual change frosting liquid is configured：By water, glycerine, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent according to matter
Amount is than being 60: 6 : 23 : 3：1.5 : 6 :0.5 ratio is added in medical solution pool, at room temperature with 50-80 revs/min
The rotating speed of clock is stirred 2 hours, and gradual change frosting liquid is made；Auxiliary agent is levelling agent and antifoaming agent, and levelling agent and antifoaming agent
Mass ratio be 1:1, secondly, make gradual change mat glass：Glass surface is cleaned, back of the body protection is carried out, adjustment frosting line inclines
Rake angle is 5 °, so as to adjust the angle that glass is placed, using step 1）The gradual change frosting liquid of production carries out glass surface
Primary spraying 10min, wherein the speed that glass is advanced is 1-5 ms/min,（Only open one group of spray assemblies）In glass table
Face self-assembling formation, to thick deposition reaction layer, removes cleaning surface, obtained frosting effect is shallower, complete frosting portion by thin
Point very narrow, gradual transition sector width is very wide, accounts for about the 2/3 of glass surface；Wherein, glass surface gradual change frosting effect makes dress
It sets, including pedestal 1, is set to the supporting leg 2 of 1 lower part of pedestal, the supporting leg 2 is four, wherein two positioned at 3 inside of spray assemblies
2 height of supporting leg is certain, and the height of other two supporting leg 2 is adjustable, to make the tilt adjustable of pedestal 1, is set to the biography at 1 top of pedestal
Dynamic component 4,1 top of the pedestal are equipped with three groups of spray assemblies 3, and the distance of two neighboring spray assemblies 3 is more than the length of glass,
The spray assemblies 3 extract liquid by water pump from medical solution pool 5；The spray assemblies 3 include right angle jet pipe 32, the right angle
The horizontal segment of jet pipe 32 is located at 1 top of pedestal, and one group of nozzle 31 and position sensing are additionally provided on the horizontal segment of right angle jet pipe 32
Device, the vertical section of right angle jet pipe 32 are equipped with control and switch；Further, the transmission component 4 including shaft and is set to shaft
On runner.
Embodiment 2
Embodiment 2 difference from example 1 is that：Gradual change frosting liquid is carried out according to following proportioning, Jiang Shui, sweet
Oil, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent are 70 according to mass ratio: 4 : 20 : 2：1 : 3 :1 matches
It sets, adjustment frosting line side is 20 degree in the angle of inclination of horizontal plane, opens two groups of spray assemblies spray 15min successively,
Obtained frosting effect is heavier, and complete frosting part accounts for about 2/3 glass surface, and gradual transition sector width narrows, and accounts for about glass surface
1/5.
Embodiment 3
Embodiment 3 difference from example 1 is that：Gradual change frosting liquid is carried out according to following proportioning, Jiang Shui, sweet
Oil, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent are 65 according to mass ratio: 5 : 25 : 4：3 : 5 : 0.8
It configures, adjustment frosting line side is 10 degree in the angle of inclination of horizontal plane, opens three groups of spray assemblies sprays successively
10min, obtained frosting effect is moderate, and complete frosting part accounts for about 2/5 glass surface, and gradual transition sector width narrows, and accounts for about glass
The 1/3 of glass surface.
Embodiment 4
Embodiment 4 difference from example 1 is that：Gradual change frosting liquid is carried out according to following proportioning, Jiang Shui, sweet
Oil, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent are 65 according to mass ratio: 5 : 23 : 3：2: 5 :0.8 matches
It sets, opens remove cleaning frosting surface after three groups of spray assemblies spray 15min successively, substantially similar complete frosting effect,
Narrow transitional zone narrower in width accounts for about the 1/10 of glass surface.
Claims (7)
1. a kind of glass surface gradual change frosting effect manufacture craft, which is characterized in that include the following steps：
1）Configure gradual change frosting liquid：By water, glycerine, ammonium acid fluoride, citric acid, ammonium sulfate, calcirm-fluoride, auxiliary agent according to mass ratio
For 60-70: 4-6 : 20-25 : 2-4：1-3 : 3-6 :The ratio of 0.5-1 is added in medical solution pool, at room temperature with
50-80 revs/min of rotating speed is stirred 2 hours, and gradual change frosting liquid is made；
2）Make gradual change mat glass：Glass surface is cleaned, carries out back of the body protection, adjust the angle of inclination of frosting line so as to adjust
The angle that glass is placed, using step 1）The gradual change frosting liquid of production carries out spraying 10-15min to glass surface, wherein glass
The speed that glass is advanced is 1-5 ms/min, and cleaning surface is removed to thick deposition reaction layer by thin in glass surface self-assembling formation
.
2. glass surface gradual change frosting effect manufacture craft as described in claim 1, it is characterised in that：Step 1）Middle auxiliary agent is
Levelling agent and antifoaming agent, and the mass ratio of levelling agent and antifoaming agent is 1:1.
3. glass surface gradual change frosting effect manufacture craft as described in claim 1, it is characterised in that：Step 2）In cover automatically
The angle of inclination of sand line is 0-30 °.
4. glass surface gradual change frosting effect producing device as described in any one of claims 1-3, it is characterised in that：The bottom of including
Seat is set to the supporting leg of pedestal lower part, is set to the transmission component of base top, three groups of spray assemblies, phase are equipped with above the pedestal
The distance of adjacent two spray assemblies is more than the length of glass, and the spray assemblies extract liquid by water pump from medical solution pool.
5. glass surface gradual change frosting effect producing device as claimed in claim 4, it is characterised in that：The supporting leg is four
A, wherein two height of landing leg on the inside of spray assemblies are certain, the height of other two supporting leg is adjustable, to make pedestal
Tilt adjustable.
6. glass surface gradual change frosting effect producing device as claimed in claim 5, it is characterised in that：The spray assemblies packet
Right angle jet pipe is included, the horizontal segment of the right angle jet pipe is located above pedestal, and one group of spray is additionally provided on the horizontal segment of right angle jet pipe
Head and position sensor, the vertical section of right angle jet pipe are equipped with control and switch.
7. glass surface gradual change frosting effect producing device as claimed in claim 4, it is characterised in that：The transmission component packet
Include shaft and the runner in shaft.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810121324 | 2018-02-07 | ||
| CN2018101213249 | 2018-02-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108395111A true CN108395111A (en) | 2018-08-14 |
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| CN201820403307.XU Active CN208104231U (en) | 2018-02-07 | 2018-03-23 | A kind of glass surface gradual change frosting effect producing device |
| CN201810246818.XA Pending CN108395111A (en) | 2018-02-07 | 2018-03-23 | A kind of glass surface gradual change frosting effect manufacture craft and device |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201820403307.XU Active CN208104231U (en) | 2018-02-07 | 2018-03-23 | A kind of glass surface gradual change frosting effect producing device |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111302644A (en) * | 2020-03-23 | 2020-06-19 | 郑州恒昊光学科技有限公司 | Manufacturing process and system of gradually-changed frosted glass |
| CN111333341A (en) * | 2018-12-19 | 2020-06-26 | Oppo广东移动通信有限公司 | Battery cover, mobile terminal and manufacturing method of battery cover |
| CN111499213A (en) * | 2019-01-31 | 2020-08-07 | 比亚迪股份有限公司 | Gradient glass and preparation method and application thereof |
| CN112851132A (en) * | 2019-11-28 | 2021-05-28 | 比亚迪股份有限公司 | Etching solution for glass gradual-change frosting and preparation method and application thereof |
| CN113979643A (en) * | 2020-12-31 | 2022-01-28 | 安徽金龙浩光电科技有限公司 | Preparation process of glass with glittering sand effect |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111333341A (en) * | 2018-12-19 | 2020-06-26 | Oppo广东移动通信有限公司 | Battery cover, mobile terminal and manufacturing method of battery cover |
| CN111333341B (en) * | 2018-12-19 | 2022-07-12 | Oppo广东移动通信有限公司 | Battery cover, mobile terminal and manufacturing method of battery cover |
| CN111499213A (en) * | 2019-01-31 | 2020-08-07 | 比亚迪股份有限公司 | Gradient glass and preparation method and application thereof |
| CN111499213B (en) * | 2019-01-31 | 2021-09-21 | 比亚迪股份有限公司 | Gradient glass and preparation method and application thereof |
| CN112851132A (en) * | 2019-11-28 | 2021-05-28 | 比亚迪股份有限公司 | Etching solution for glass gradual-change frosting and preparation method and application thereof |
| CN112851132B (en) * | 2019-11-28 | 2022-03-15 | 比亚迪股份有限公司 | Etching solution for glass gradual-change frosting and preparation method and application thereof |
| CN111302644A (en) * | 2020-03-23 | 2020-06-19 | 郑州恒昊光学科技有限公司 | Manufacturing process and system of gradually-changed frosted glass |
| CN111302644B (en) * | 2020-03-23 | 2024-04-12 | 郑州恒昊光学科技有限公司 | Gradual change frosted glass manufacturing process and system |
| CN113979643A (en) * | 2020-12-31 | 2022-01-28 | 安徽金龙浩光电科技有限公司 | Preparation process of glass with glittering sand effect |
Also Published As
| Publication number | Publication date |
|---|---|
| CN208104231U (en) | 2018-11-16 |
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