CN108380166A - A kind of sodium pyrosulfate production reaction kettle with crushing function - Google Patents

A kind of sodium pyrosulfate production reaction kettle with crushing function Download PDF

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Publication number
CN108380166A
CN108380166A CN201810494596.3A CN201810494596A CN108380166A CN 108380166 A CN108380166 A CN 108380166A CN 201810494596 A CN201810494596 A CN 201810494596A CN 108380166 A CN108380166 A CN 108380166A
Authority
CN
China
Prior art keywords
main body
reactor main
drive roll
reaction kettle
driven voller
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810494596.3A
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Chinese (zh)
Inventor
张长玖
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guizhou Kaiyang Chuan Dong Chemical Co Ltd
Original Assignee
Guizhou Kaiyang Chuan Dong Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guizhou Kaiyang Chuan Dong Chemical Co Ltd filed Critical Guizhou Kaiyang Chuan Dong Chemical Co Ltd
Priority to CN201810494596.3A priority Critical patent/CN108380166A/en
Publication of CN108380166A publication Critical patent/CN108380166A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/005Feed or outlet devices as such, e.g. feeding tubes provided with baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/02Crushing or disintegrating by roller mills with two or more rollers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/28Details
    • B02C4/40Detachers, e.g. scrapers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00Sulfates or sulfites of sodium, potassium or alkali metals in general
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Food Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Crushing And Pulverization Processes (AREA)
  • Crushing And Grinding (AREA)

Abstract

The invention discloses a kind of sodium pyrosulfate production reaction kettle with crushing function, including reactor main body, driven voller, fixed plate, stirring motor, paddle, discharge port, broken motor and drive roll, it is provided with charge door above the reactor main body, and stock guide is provided with below charge door, the driven voller and drive roll are arranged by driven shaft and driving shaft in the lower section of stock guide respectively, the fixed plate is welded on the inside of reactor main body, the stirring motor is arranged in the lower end of reactor main body, the paddle is welded on the outside of agitating shaft, the discharge port is located at the lower end of reactor main body, the broken motor is arranged by driving shaft in the outside of guard shield.The sodium pyrosulfate production reaction kettle with crushing function, the lower section on the outside of driven voller and drive roll are both provided with Antisticking, play the role of striking off the raw material that driven voller and active roller surface adhere to, are conducive to the inside for falling on reactor main body under raw material.

Description

A kind of sodium pyrosulfate production reaction kettle with crushing function
Technical field
The present invention relates to sodium pyrosulfate reaction kettle art field, specially a kind of sodium pyrosulfate production with crushing function is used Reaction kettle.
Background technology
Sodium pyrosulfate is the sodium salt of pyrosulfuric acid, can be added with niter cake in semi-transparent clear crystallization or white chunks object Thermal decomposition is made, and sulfur trioxide is generated in the reaction, then sodium pyrosulfate is obtained by the reaction with the sodium sulphate generated is decomposed.
But existing sodium pyrosulfate production reaction kettle is added in reaction kettle and reaction solution by sodium pyrosulfate raw material It when carrying out reaction production, is not easy to be crushed sodium pyrosulfate raw material, and is unfavorable for the cleaning to being crushed roller surface.
Invention content
The purpose of the present invention is to provide a kind of sodium pyrosulfate production reaction kettle with crushing function, it is above-mentioned to solve The existing sodium pyrosulfate production reaction kettle proposed in background technology, by sodium pyrosulfate raw material be added in reaction kettle with it is anti- When solution being answered to carry out reaction production, it is not easy to be crushed sodium pyrosulfate raw material, and be unfavorable for asking breaker roll removing surface Topic.
To achieve the above object, the present invention provides the following technical solutions:A kind of sodium pyrosulfate production with crushing function With reaction kettle, including reactor main body, driven voller, fixed plate, stirring motor, paddle, discharge port, broken motor and active Roller is provided with charge door above the reactor main body, and is provided with stock guide below charge door, the driven voller and master Dynamic roller is arranged by driven shaft and driving shaft in the lower section of stock guide respectively, and the rear end of driven shaft and driving shaft is respectively arranged with Driven gear and actively this wheel, the fixed plate is welded on the inside of reactor main body, and the outer end of fixed plate is by compressing bullet Spring is connected with Antisticking, and the stirring motor is arranged in the lower end of reactor main body, and in stirring motor and reactor main body The agitating shaft in portion is connected, and the paddle is welded on the outside of agitating shaft, and the discharge port is located at the lower end of reactor main body, And guard shield is provided on rear side of reactor main body, the broken motor is arranged by driving shaft in the outside of guard shield.
Preferably, the mounting structure of the stock guide is to tilt to install, and stock guide has altogether there are two settings, stock guide Between minimum range be less than minimum range between driven voller and drive roll.
Preferably, the driven voller and drive roll is relatively rotate, and parallel installation each other between driven voller and drive roll.
Preferably, the mounting structure of the fixed plate is to be horizontally mounted, and fixed plate is in about the center of reactor main body Axial symmetry is installed.
Preferably, the number of the Antisticking and the number of stock guide are identical, and Antisticking is located at driven voller and master The lower section of dynamic roller.
Preferably, the compressed spring is between Antisticking and fixed plate, and the width of Antisticking is more than drive roll Width.
Compared with prior art, the beneficial effects of the invention are as follows:The sodium pyrosulfate production reaction with crushing function Kettle is provided with stock guide below charge door, driven voller and drive roll is provided with below stock guide, plays and is carried out to raw material The effect of attrition crushing, convenient for being crushed to raw material, and the lower section on the outside of driven voller and drive roll is both provided with Antisticking, rises To the effect for striking off the raw material of driven voller and the attachment of active roller surface, be conducive to fall on the interior of reactor main body under raw material Portion, and be conducive to the cleaning of driven voller and active roller surface, by the outer end of fixed plate and Antisticking hinge connection, and in Antisticking Be provided with compressed spring between fixed plate, play the role of holding out against Antisticking, be conducive to Antisticking and driven voller and The close contact of active roller surface.
Description of the drawings
Fig. 1 is reactor main body internal structure schematic diagram of the present invention;
Fig. 2 is the portions a-a section view structure schematic diagram in Fig. 1 of the present invention;
Fig. 3 is the present invention actively this wheel and driven gear structural schematic diagram;
Fig. 4 is A point enlarged structure schematic diagrams in Fig. 1 of the present invention.
In figure:1, reactor main body;2, charge door;3, stock guide;4, driven voller;5, fixed plate;6, stirring motor;7, it stirs Mix axis;8, paddle;9, discharge port;10, guard shield;11, it is crushed motor;12, actively this takes turns;13, driving shaft;14, actively Roller;15, Antisticking;16, driven shaft;17, driven gear;18, compressed spring.
Specific implementation mode
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete Site preparation describes, it is clear that described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, it is obtained by those of ordinary skill in the art without making creative efforts every other Embodiment shall fall within the protection scope of the present invention.
- 4 are please referred to Fig.1, the present invention provides a kind of technical solution:A kind of sodium pyrosulfate production use with crushing function is anti- Answer kettle, including reactor main body 1, charge door 2, stock guide 3, driven voller 4, fixed plate 5, stirring motor 6, agitating shaft 7, paddle 8, discharge port 9, guard shield 10, broken motor 11, actively this wheel 12, driving shaft 13, drive roll 14, Antisticking 15, driven shaft 16, the top of driven gear 17 and compressed spring 18, reactor main body 1 is provided with charge door 2, and the lower section setting of charge door 2 It is to tilt to install, and stock guide 3 has altogether there are two settings, between stock guide 3 to have stock guide 3, the mounting structure of stock guide 3 Minimum range is less than the minimum range between driven voller 4 and drive roll 14, is provided with is slid into through stock guide 3 conducive to raw material in this way Between driven voller 4 and drive roll 14, driven voller 4 and drive roll 14 are arranged by driven shaft 16 and driving shaft 13 in stock guide respectively 3 lower section, and the rear end of driven shaft 16 and driving shaft 13 is respectively arranged with driven gear 17 and actively this wheel 12,4 He of driven voller Drive roll 14 is relatively rotates, and parallel installation each other between driven voller 4 and drive roll 14, is provided in this way conducive to raw material Attrition crushing, fixed plate 5 is welded on the inside of reactor main body 1, and the outer end of fixed plate 5 passes through compressed spring 18 and Antisticking 15 are connected, and the mounting structure of fixed plate 5 is to be horizontally mounted, and fixed plate 5 is axisymmetricly pacified about the center of reactor main body 1 Dress is provided in this way conducive to the fixed installation to Antisticking 15, and the number of Antisticking 15 is identical as the number of stock guide 3, and anti- Haftplatte 15 is located at the lower section of driven voller 4 and drive roll 14, and setting in this way is played driven voller 4 and the attachment of 14 surface of drive roll The effect struck off of raw material, be conducive to the inside that reactor main body 1 is fallen under raw material, and be conducive to driven voller 4 and actively The cleaning on 14 surface of roller, compressed spring 18 is between Antisticking 15 and fixed plate 5, and the width of Antisticking 15 is more than drive roll 14 width is provided with compressed spring 18 between Antisticking 15 and fixed plate 5, plays the work held out against to Antisticking 15 With being conducive to the close contact of Antisticking 15 and 14 surface of driven voller 4 and drive roll, stirring motor 6 is arranged in reactor main body 1 Lower end, and stirring motor 6 is connected with the agitating shaft 7 inside reactor main body 1, and paddle 8 is welded on the outer of agitating shaft 7 Side, discharge port 9 is located at the lower end of reactor main body 1, and the rear side of reactor main body 1 is provided with guard shield 10, is crushed motor 11 are arranged by driving shaft 13 in the outside of guard shield 10.
Operation principle:When using the sodium pyrosulfate production reaction kettle with crushing function, reaction kettle master is first checked Whether each structure of body 1 is intact, after inspection, connects the power supply of reactor main body 1, then, starts 6 He of stirring motor successively The switch of broken motor 11, stirring motor 6 drive paddle 8 to rotate by agitating shaft 7, and broken motor 11 passes through 13 band of driving shaft Dynamic actively this wheel 12 and drive roll 14 rotate, and actively this wheel 12 makes driven gear 17 under the action of being engaged with driven gear 17 It drives driven voller 4 to rotate by driven shaft 16, and then makes to relatively rotate between driven voller 4 and drive roll 14, at this point, will react molten Liquid is added from the addition mouth of 1 side wall of reactor main body, then raw material is added to the inside of reactor main body 1, raw material from charge door 2 It is slid between driven voller 4 and drive roll 14 through stock guide 3, driven voller 4 and drive roll 14 carry out attrition crushing to raw material, are crushed The lower inside of reactor main body 1 is fallen under raw material afterwards, the Antisticking 15 in fixed plate 5 can be by driven voller 4 and drive roll 14 The raw material of surface attachment strikes off, and the lower inside of reactor main body 1 is fallen under the raw material struck off, the paddle 8 on agitating shaft 7 is right Raw material and reaction solution are stirred, and when after completion of the reaction, open the valve on discharge port 9, and then reactor product is taken out, this Sample just completes the whole process of yellow phosphoric tail gas heating burner operation, and the content not being described in detail in this specification belongs to this The prior art well known to skilled artisan.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (6)

1. a kind of sodium pyrosulfate production reaction kettle with crushing function, including reactor main body(1), driven voller(4), it is fixed Plate(5), stirring motor(6), paddle(8), discharge port(9), broken motor(11)And drive roll(14), it is characterised in that:Institute State reactor main body(1)Top be provided with charge door(2), and charge door(2)Lower section be provided with stock guide(3), it is described from Dynamic roller(4)And drive roll(14)Pass through driven shaft respectively(16)And driving shaft(13)It is arranged in stock guide(3)Lower section, and it is driven Axis(16)And driving shaft(13)Rear end be respectively arranged with driven gear(17)With actively this wheel(12), the fixed plate(5)Weldering It is connected on reactor main body(1)Inside, and fixed plate(5)Outer end pass through compressed spring(18)With Antisticking(15)It is connected, The stirring motor(6)It is arranged in reactor main body(1)Lower end, and stirring motor(6)With reactor main body(1)Internal stirs Mix axis(7)It is connected, the paddle(8)It is welded on agitating shaft(7)Outside, the discharge port(9)Positioned at reactor main body (1)Lower end, and reactor main body(1)Rear side be provided with guard shield(10), the broken motor(11)Pass through driving shaft (13)It is arranged in guard shield(10)Outside.
2. a kind of sodium pyrosulfate production reaction kettle with crushing function according to claim 1, it is characterised in that:Institute State stock guide(3)Mounting structure be to tilt to install, and stock guide(3)Altogether there are two setting, stock guide(3)Between most Small distance is less than driven voller(4)And drive roll(14)Between minimum range.
3. a kind of sodium pyrosulfate production reaction kettle with crushing function according to claim 1, it is characterised in that:Institute State driven voller(4)And drive roll(14)To relatively rotate, and driven voller(4)And drive roll(14)Between parallel installation each other.
4. a kind of sodium pyrosulfate production reaction kettle with crushing function according to claim 1, it is characterised in that:Institute State fixed plate(5)Mounting structure be to be horizontally mounted, and fixed plate(5)About reactor main body(1)Center axisymmetricly pacify Dress.
5. a kind of sodium pyrosulfate production reaction kettle with crushing function according to claim 1, it is characterised in that:Institute State Antisticking(15)Number and stock guide(3)Number it is identical, and Antisticking(15)It is located at driven voller(4)And drive roll (14)Lower section.
6. a kind of sodium pyrosulfate production reaction kettle with crushing function according to claim 1, it is characterised in that:Institute State compressed spring(18)Positioned at Antisticking(15)And fixed plate(5)Between, and Antisticking(15)Width be more than drive roll(14) Width.
CN201810494596.3A 2018-05-22 2018-05-22 A kind of sodium pyrosulfate production reaction kettle with crushing function Pending CN108380166A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810494596.3A CN108380166A (en) 2018-05-22 2018-05-22 A kind of sodium pyrosulfate production reaction kettle with crushing function

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810494596.3A CN108380166A (en) 2018-05-22 2018-05-22 A kind of sodium pyrosulfate production reaction kettle with crushing function

Publications (1)

Publication Number Publication Date
CN108380166A true CN108380166A (en) 2018-08-10

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Application Number Title Priority Date Filing Date
CN201810494596.3A Pending CN108380166A (en) 2018-05-22 2018-05-22 A kind of sodium pyrosulfate production reaction kettle with crushing function

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112387244A (en) * 2020-11-09 2021-02-23 马紫严 Chemical production uses high-efficient reation kettle

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112387244A (en) * 2020-11-09 2021-02-23 马紫严 Chemical production uses high-efficient reation kettle

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WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20180810

WD01 Invention patent application deemed withdrawn after publication