CN108362548A - A kind of rock sample processing unit - Google Patents

A kind of rock sample processing unit Download PDF

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Publication number
CN108362548A
CN108362548A CN201810028128.7A CN201810028128A CN108362548A CN 108362548 A CN108362548 A CN 108362548A CN 201810028128 A CN201810028128 A CN 201810028128A CN 108362548 A CN108362548 A CN 108362548A
Authority
CN
China
Prior art keywords
babinet
storage cup
pallet
rock sample
processing unit
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810028128.7A
Other languages
Chinese (zh)
Inventor
石正勇
龚炜
金芸芸
任霄宇
李小桃
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Exploration and Development Research Institute of Sinopec Henan Oilfield Branch Co
Original Assignee
China Petroleum and Chemical Corp
Exploration and Development Research Institute of Sinopec Henan Oilfield Branch Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Petroleum and Chemical Corp, Exploration and Development Research Institute of Sinopec Henan Oilfield Branch Co filed Critical China Petroleum and Chemical Corp
Priority to CN201810028128.7A priority Critical patent/CN108362548A/en
Publication of CN108362548A publication Critical patent/CN108362548A/en
Pending legal-status Critical Current

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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/44Sample treatment involving radiation, e.g. heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/34Purifying; Cleaning

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention relates to a kind of rock sample processing units.The rock sample processing unit includes babinet and pallet component, the babinet has the end face of pallet component described in support, the pallet component includes pallet and is wholely set or is embedded at least one storage cup connecting with the pallet, the lower part of the storage cup or whole stretch into the babinet when pallet described in the babinet support, and the babinet has the accommodation space for accommodating the storage cup.Storage cup is positioned by pallet, the object for the storage cup that hydrochloric acid can be added according to the location determination of storage cup, facilitate the batch processing for source rock sample and management, it avoids and is obscuring operation object due to the quantity of storage cup is excessive and floats, storage cup is limited by pallet simultaneously, is also avoided storage cup and is toppled over.

Description

A kind of rock sample processing unit
Technical field
The present invention relates to a kind of rock sample processing units.
Background technology
Organic carbon refers to the carbon related with organic matter contained in sedimentary rock, is the important indicator for evaluating hydrocarbon source rock abundance One of.The content of organic carbon can be used for determining oil source rock, instruction abundance of organic matter in rock stratum, judge rock stratum oil generation efficiency, conversion Efficiency and differentiation degree, calculate oil generating quantity, thus it is speculated that oil primary migration direction, therefore needed to hydrocarbon source in oil drilling Rock carries out organic carbon test analysis, and the inorganic carbon component in source rock sample based on carbonate can be to organic carbon in hydrocarbon source rock Content measuring analysis have an impact, therefore need before carrying out hydrocarbon source rock organic carbon test analysis to remove hydrocarbon source rock sample in advance Inorganic carbon in product.
The method of inorganic carbon in existing removing source rock sample is that rock dust is positioned over dedicated ceramic crucible In, then ceramic crucible is put into glass beaker, then glass beaker is placed in water-bath and carries out heating water bath, keeps water Suitable dilute hydrochloric acid is added into crucible at 70 to 80 degrees Celsius for bath temperature.
When removing inorganic carbon to rock sample, more parts of source rock samples can be randomly selected, every part of source rock sample needs Add 3 to 5 dilute hydrochloric acid, needed to be added into crucible every 20 to 30 minutes primary, take or so 2 hours, this process compared with It is cumbersome time-consuming, the quantity of the beaker and crucible that use is also more, and beaker will produce floating in water-bath and leave originally Position, so that operating personnel is easy to obscure the object of beaker and crucible that hydrochloric acid is added, be not easy to carry out the sample of hydrocarbon source rock Batch processing and management.
Invention content
The purpose of the present invention is to provide a kind of convenient for carrying out the rock sample of batch processing and management to source rock sample Processing unit.
In order to solve the above-mentioned technical problem, the first technical solution of rock sample processing unit of the invention is:It is a kind of Rock sample processing unit, including babinet and pallet component, the babinet have the end face of pallet component described in support, the support Disk component includes pallet and is wholely set or is embedded at least one storage cup connecting, the babinet with the pallet The lower part of the storage cup or whole stretch into the babinet when pallet described in support, and the babinet, which has, accommodates the Sheng The accommodation space of object cup.
The advantageous effect of the technical solution is:Storage cup is positioned by pallet, it can be according to the position of storage cup The object for determining the storage cup that hydrochloric acid is added is set, the batch processing for source rock sample and management is facilitated, avoids Obscure operation object due to the quantity of storage cup is excessive and floats, while storage cup is limited by pallet, also avoids containing Object cup is toppled over.
Second of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention The first technical solution on the basis of, the storage cup and the pallet are integrated setting.Convenient for the life of pallet component Production and management, object will not occur because taking out storage cup and obscure.
The third technical solution of rock sample processing unit of the present invention is:In the rock sample processing unit of the present invention Second of technical solution on the basis of, plane where the rim of a cup of the storage cup is with the upper surface of the pallet same On horizontal plane, the storage cup all stretches into the babinet.Volume of the storage cup in babinet is increased, convenient for storage cup Interior sample is heated.
The 4th kind of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention The third technical solution on the basis of, the storage cup shares 64 and the matrix form arranged with eight rows eight is distributed in the load On object pallet.Increase the quantity of storage cup convenient for being carried out at the same time processing to a large amount of sample, distribution form is beautiful in the matrix form.
The 5th kind of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention Any one of first to fourth technical solution on the basis of, the babinet further includes and the integrally formed head cover of babinet, the top It covers to be equipped with and be adapted to the storage cup so that storage cup stretches into the relief hole of the babinet.Head cover can reduce water in babinet Temperature distributes, and reduces energy loss when carrying out heating water bath.
The 6th kind of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention The 5th kind of technical solution on the basis of, be additionally provided on the babinet for into the babinet inject water water injection hole.Pass through The water filling into babinet of dedicated water injection hole, it is convenient and efficient.
The 7th kind of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention The 6th kind of technical solution on the basis of, the water injection hole be set to the head cover corner.Avoid the water in babinet out of babinet It splashes out, while convenient for adding water into babinet.
The 8th kind of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention The 7th kind of technical solution on the basis of, the measured hole for being inserted into thermometer is additionally provided on the babinet.It is inserted by measured hole Enter thermometer convenient for grasping the water temperature in babinet in real time, water temperature is made to be maintained at the numerical value of needs.
The 9th kind of technical solution of rock sample processing unit of the present invention be:In the rock sample processing unit of the present invention The 8th kind of technical solution on the basis of, the measured hole be set to corner of the head cover far from water injection hole.Measured hole is located at remote Babinet is inserted into corner from water injection hole convenient for thermometer, while avoiding because water temperature local caused by water is newly added into babinet Variation influences the measurement to bath temperature in integrated water tank.
Description of the drawings
Fig. 1 is the structural schematic diagram of the babinet of the embodiment 1 of the rock sample processing unit of the present invention;
Fig. 2 is the babinet of Fig. 1 along line A-A sectional view;
The structural schematic diagram of the pallet component of the embodiment 1 of the rock sample processing unit of Fig. 3 present invention;
Fig. 4 is the pallet component of Fig. 3 along line B-B sectional view;
Fig. 5 is the structural schematic diagram of the pallet component of the embodiment 2 of the rock sample processing unit of the present invention.
It is respectively marked in figure:1. babinet;2. pallet;11. head cover;12. relief hole;13. water injection hole;14. measured hole; 21. storage cup.
Specific implementation mode
The embodiment 1 of the rock sample processing unit of the present invention is as shown in Fig. 1 ~ 4, including babinet 1 and pallet component, babinet 1 end face with support pallet component, the end face of support pallet component is the upper surface of head cover 11, tray set in this embodiment Part includes pallet 2 and the storage cup 21 being wholely set with pallet 2, in the present embodiment, storage cup have 64 and with The matrix form of eight rows eight row is distributed on pallet, in other embodiments, storage cup can also be 36,81 etc. its His number, can also be discrete be distributed on pallet;Plane where 21 rim of a cup of storage cup and the upper surface of pallet 2 exist In same level, storage cup 21 all stretches into babinet 1;Head cover 11 is integrally formed on babinet 1, babinet 1 and head cover 11 are equal For rectangle, head cover 11 is equipped with and is adapted to the storage cup 21 on pallet 2 so that storage cup 21 stretches into the relief hole of babinet 1 12;Water injection hole 13 is additionally provided on the head cover 11 of babinet 1, water injection hole 13 is arranged in one of head cover 11 corner, at other In embodiment, the position top in the side wall of babinet 1 can also be arranged in water injection hole 13, be additionally provided on head cover 11 for being inserted into temperature The measured hole 14 of meter, measured hole 14 are arranged far from another corner of water injection hole 13, in other embodiments, measured hole 14 It can also be arranged on the side wall of babinet 1.
When in use, the rock sample of hydrocarbon source rock is placed in crucible for the rock sample processing unit of the present invention, then will Crucible is placed on together with rock sample in storage cup, and pallet is placed on the head cover of babinet, makes storage cup by allowing Position hole is all stretched into babinet, is heated after injecting water in babinet, and water temperature in thermometer and control cabinet body is inserted into measured hole 70 to 80 degrees Celsius are maintained at, suitable dilute hydrochloric acid, each 3ml or so, per 20 ~ 30 points of minor tick is added to all rock samples Clock, the rock sample in each storage cup add 3 to 5 dilute hydrochloric acid, according to pair for the dilute hydrochloric acid that the location determination of storage cup is added dropwise As, to ensure that rock sample will not be added or leak to add dilute hydrochloric acid, the batch processing pair with rock sample and management are facilitated, Also storage cup will not topple in babinet simultaneously, and it is unrestrained to avoid rock sample.
The embodiment 2 of the rock sample processing unit of the present invention with embodiment 1 as shown in figure 5, differ only in:Storage There is cup the part beyond pallet upper surface, storage cup only partly to stretch into babinet.
The embodiment 3 of the rock sample processing unit of the present invention, with differing only in for embodiment 1:The storage cup with Pallet is split settings.
The embodiment 4 of the rock sample processing unit of the present invention, with differing only in for embodiment 1:Omit the top of babinet Lid, the pallet are directly placed on the frame of side wall formation of the babinet.
The embodiment 5 of the rock sample processing unit of the present invention, with differing only in for embodiment 1:It omits on babinet Measured hole robs the water temperature in equal device measurings babinet using thermometric.
The embodiment 6 of the rock sample processing unit of the present invention, with differing only in for embodiment 1:It omits on babinet Water injection hole directly injects water into babinet by relief hole.

Claims (9)

1. a kind of rock sample processing unit, it is characterised in that:Including babinet and pallet component, the babinet has described in support The end face of pallet component, the pallet component include pallet and be wholely set or be embedded in the pallet connect to A few storage cup lower part of the storage cup or is all stretched into the babinet when pallet described in the babinet support, The babinet has the accommodation space for accommodating the storage cup.
2. rock sample processing unit according to claim 1, it is characterised in that:The storage cup and the pallet It is integrated setting.
3. rock sample processing unit according to claim 2, it is characterised in that:Plane where the rim of a cup of the storage cup In same level, the storage cup all stretches into the babinet for upper surface with the pallet.
4. rock sample processing unit according to claim 3, it is characterised in that:The storage cup shares 64 and with eight The matrix form of eight row of row is distributed on the pallet.
5. according to claim 1 ~ 4 any one of them rock sample processing unit, it is characterised in that:The babinet further include with The integrally formed head cover of babinet, the head cover are equipped with and are adapted to the storage cup so that storage cup stretches into the resigning of the babinet Hole.
6. rock sample processing unit according to claim 5, it is characterised in that:It is additionally provided on the babinet for institute State the water injection hole of injection water in babinet.
7. rock sample processing unit according to claim 6, it is characterised in that:The water injection hole is set to the head cover Corner.
8. rock sample processing unit according to claim 7, it is characterised in that:It is additionally provided on the babinet for being inserted into The measured hole of thermometer.
9. rock sample processing unit according to claim 8, it is characterised in that:It is remote that the measured hole is set to the head cover Corner from water injection hole.
CN201810028128.7A 2018-01-11 2018-01-11 A kind of rock sample processing unit Pending CN108362548A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810028128.7A CN108362548A (en) 2018-01-11 2018-01-11 A kind of rock sample processing unit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810028128.7A CN108362548A (en) 2018-01-11 2018-01-11 A kind of rock sample processing unit

Publications (1)

Publication Number Publication Date
CN108362548A true CN108362548A (en) 2018-08-03

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CN201810028128.7A Pending CN108362548A (en) 2018-01-11 2018-01-11 A kind of rock sample processing unit

Country Status (1)

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CN (1) CN108362548A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111595879A (en) * 2019-02-21 2020-08-28 中国石油化工股份有限公司 Multi-sample preparation device and method suitable for argon ion polishing

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204255716U (en) * 2014-11-17 2015-04-08 中国石油天然气股份有限公司 A kind of pretreating device analyzed for total content of organic carbon in sedimentogeneous rock
CN105606432A (en) * 2016-03-17 2016-05-25 中国石油大学(北京) Pretreatment device for organic carbon content analysis
CN107132098A (en) * 2017-07-11 2017-09-05 国家地质实验测试中心 A kind of automatic pretreating device of rock total organic carbon test sample and method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204255716U (en) * 2014-11-17 2015-04-08 中国石油天然气股份有限公司 A kind of pretreating device analyzed for total content of organic carbon in sedimentogeneous rock
CN105606432A (en) * 2016-03-17 2016-05-25 中国石油大学(北京) Pretreatment device for organic carbon content analysis
CN107132098A (en) * 2017-07-11 2017-09-05 国家地质实验测试中心 A kind of automatic pretreating device of rock total organic carbon test sample and method

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
蒋有录 等: "《油气地质与勘探实验、习题及课程设计》", 30 April 2013, 中国石油大学出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111595879A (en) * 2019-02-21 2020-08-28 中国石油化工股份有限公司 Multi-sample preparation device and method suitable for argon ion polishing
CN111595879B (en) * 2019-02-21 2023-02-10 中国石油化工股份有限公司 Multi-sample preparation device and method suitable for argon ion polishing

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Application publication date: 20180803

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