CN108338216A - A method of preparing sugarcane wax cold press soybean oil grease gel - Google Patents

A method of preparing sugarcane wax cold press soybean oil grease gel Download PDF

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Publication number
CN108338216A
CN108338216A CN201810082861.7A CN201810082861A CN108338216A CN 108338216 A CN108338216 A CN 108338216A CN 201810082861 A CN201810082861 A CN 201810082861A CN 108338216 A CN108338216 A CN 108338216A
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CN
China
Prior art keywords
soybean oil
cold press
sugarcane wax
gel
press soybean
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810082861.7A
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Chinese (zh)
Inventor
于殿宇
江连洲
李丹
张如春
王立琦
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Northeast Agricultural University
Original Assignee
Northeast Agricultural University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Northeast Agricultural University filed Critical Northeast Agricultural University
Priority to CN201810082861.7A priority Critical patent/CN108338216A/en
Publication of CN108338216A publication Critical patent/CN108338216A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23DEDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
    • A23D7/00Edible oil or fat compositions containing an aqueous phase, e.g. margarines
    • A23D7/01Other fatty acid esters, e.g. phosphatides

Abstract

Sugarcane wax cold press soybean oil grease gel is prepared the invention discloses a kind of, primary raw material is sugarcane wax, cold press soybean oil.Grease gel is the organogel using liquid vegetable oil as continuous phase, is not generate that trans-fatty acid, saturated fatty acid be relatively low, a kind of substance rich in mono-/multi- unsaturated fatty acid, can substitute tradition and plastic fat is prepared by method for hydrogenation.Show that the optimum condition for preparing sugarcane wax cold press soybean oil grease gel be sugarcane wax mass fraction 9%, 90 DEG C of bath temperature and cooling temperature is 20 DEG C by research, the holding oiliness of grease gel is up to that 89.8%, fusing point is up to 44.3 DEG C, solid fats content is minimum 0.7%, hardness is up to 99g at this time.The present invention obtains a kind of hydrophobicity and the stronger grease gel of mechanicalness, and a more healthy new road is opened up in the production for margarine etc..

Description

A method of preparing sugarcane wax cold press soybean oil grease gel
Technical field
The invention belongs to food margarine production technical fields, and in particular to a kind of to prepare sugarcane wax cold press soybean oil oil The method of fat gel.
Background technology
Currently, food special fat is mostly shortening and universal margarine, source can be divided mainly into hydrogenated vegetable The mixture of oil and refining animal grease and said two devices, wherein hydrogenated vegetable oil contain trans-fatty acid, Excess free enthalpy meeting Cause people to suffer from multiclass disease, increases and suffer from risk of cardiovascular diseases, the incidence of type-2 diabetes mellitus, inhibition infant's growth hair The incidence etc. for educating, increasing inflammation, it is totally unfavorable to the health of human body, it is also very desirable to find a kind of replacement plasticity completely or partially Liquid vegetable oil progress gelation is obtained grease gel as plasticity fat by the new way of fat based on the agent of edibility waxy gel The potential substitute of fat increasingly attracts attention.
Grease gel is a kind of using liquid vegetable oil as the supramolecular organogel of continuous phase, is that grease field is ground in recent years Study carefully comparison it is popular do not generate trans-fatty acid, saturated fatty acid it is relatively low and rich in mono-/multi- unsaturated fatty acid a kind of object Matter can substitute the plastic fat that tradition is prepared by method for hydrogenation completely or partially.
Sugarcane wax referred to as " cerosin ", is attached to the wax of sugarcane epidermis, and main component is 16 carbon fatty acids and 30 carbon fat The ester that fat alcohol or stigmasterol are constituted, for brown-green to auburn solid, matter is hard and crisp, is the byproduct of sugar industry, for making Standby floor wax, shoe polish and carbon paper etc..Sugarcane wax is a kind of wax gellike agent, and it is solidifying that grease can be formed with cold press soybean oil Glue.
Invention content
The present invention is a kind of grease gel developed as main component using sugarcane wax, cold press soybean oil, and sugarcane wax is in cold press The crystal network structure that is formed is more organized when forming grease gel in soybean oil and compactness, can hold onto more liquid State oil, therefore have stronger hydrophobicity and mechanicalness compared with other grease gels, the technical solution adopted by the present invention is cold Squeeze the sugarcane wax gelling agent that certain mass score is added in soybean oil, the temperature of regulating thermostatic magnetic agitation water-bath to 80 DEG C~ 100 DEG C, stirring switch is opened, the dissolving of gelling agent is accelerated, stirred after object to be mixed is completely dissolved, not heating stirring 5min, it will The mixture of heat is placed at 10 DEG C~30 DEG C, is stood for 24 hours, is obtained sugarcane wax cold press soybean oil grease gel.It utilizes with wax The grease gel that gelling agent sugarcane wax is formed prepares novel artificial cream as raw material, and one is opened up more for the production of margarine For the new road of health.
Specific implementation mode
Specific implementation mode one:One, by mass fraction it is respectively first 3%, 6%, 9%, 12%, 15% to be added separately to In the cold press soybean oil of equal quality;Secondly respectively regulating thermostatic magnetic stirring apparatus water-bath temperature to 80 DEG C, 85 DEG C, 90 DEG C, 95 DEG C, 100 DEG C, then open stirring switch, accelerate the dissolving of gelling agent, stir after object to be mixed is completely dissolved, do not heat 5min is stirred, the sugarcane wax of heat and the mixture of cold press soybean oil are individually positioned in 10 DEG C, 15 DEG C, 20 DEG C, 25 DEG C, 30 DEG C Under, it stands for 24 hours, obtains sugarcane wax cold press soybean oil grease gel, the holding oiliness, fusing point, hard fat of its grease gel are contained Amount, hardness are analyzed.
Specific implementation mode two:Present embodiment is sugarcane wax gel in step 1 with one difference of specific implementation mode The difference of the additive amount of agent, respectively 6%, 9%, 12%, it obtains the holding oiliness to sugarcane wax cold press soybean oil grease gel, melt The influence of point, solid fats content, hardness, other steps are same as the specific embodiment one.
Specific implementation mode three:Present embodiment is in step 1 that constant temperature magnetic force stirs with one difference of specific implementation mode Mix the temperature of water-bath be respectively 85 DEG C, 90 DEG C, 95 DEG C, obtain the holding oiliness to sugarcane wax cold press soybean oil grease gel, The influence of fusing point, solid fats content, hardness, other steps are same as the specific embodiment one.
Specific implementation mode four:Present embodiment and one difference of specific implementation mode are in step 1 to heat Sugarcane wax cold press soybean oil blend object is placed at 15 DEG C, 20 DEG C, 25 DEG C, is stood for 24 hours, is obtained to sugarcane wax cold press soybean oil The influence of the holding oiliness, fusing point, solid fats content, hardness of grease gel, other steps are same as the specific embodiment one.

Claims (4)

1. a kind of method preparing sugarcane wax cold press soybean oil grease gel, characterization step are as follows:
Step 1:It is respectively first 3%, 6%, 9%, 12%, 15% cold press for being added separately to equal quality by mass fraction In soybean oil;Secondly the temperature of regulating thermostatic magnetic stirring apparatus water-bath is to 80 DEG C, 85 DEG C, 90 DEG C, 95 DEG C, 100 DEG C respectively, so Stirring switch is opened afterwards, accelerates the dissolving of gelling agent, is stirred after object to be mixed is completely dissolved, not heating stirring 5min, by heat The mixture of sugarcane wax and cold press soybean oil is individually positioned at 10 DEG C, 15 DEG C, 20 DEG C, 25 DEG C, 30 DEG C, is stood for 24 hours, is obtained sweet Cerosin cold press soybean oil grease gel, analyzes the holding oiliness of its grease gel, fusing point, solid fats content, hardness.
2. the research method according to claim 1 for preparing sugarcane wax cold press soybean oil grease gel, it is characterised in that step The difference of the additive amount of sugarcane wax gelling agent in rapid one, respectively 6%, 9%, 12%, it obtains to sugarcane wax cold press soybean oil oil The influence of the holding oiliness, fusing point, solid fats content, hardness of fat gel, other same step 1 of process.
3. the research method according to claim 1 for preparing sugarcane wax cold press soybean oil grease gel, it is characterised in that step The temperature of temperature constant magnetic stirring water-bath is respectively 85 DEG C, 90 DEG C, 95 DEG C in rapid one, is obtained to sugarcane wax cold press soybean oil oil The influence of the holding oiliness, fusing point, solid fats content, hardness of fat gel, other same step 1 of process.
4. the research method according to claim 1 for preparing sugarcane wax cold press soybean oil grease gel, it is characterised in that step The sugarcane wax cold press soybean oil blend object heated is placed at 15 DEG C, 20 DEG C, 25 DEG C in rapid one, stands for 24 hours, obtains pair The influence of the holding oiliness, fusing point, solid fats content, hardness of sugarcane wax cold press soybean oil grease gel, other same steps of process One.
CN201810082861.7A 2018-01-29 2018-01-29 A method of preparing sugarcane wax cold press soybean oil grease gel Pending CN108338216A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810082861.7A CN108338216A (en) 2018-01-29 2018-01-29 A method of preparing sugarcane wax cold press soybean oil grease gel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810082861.7A CN108338216A (en) 2018-01-29 2018-01-29 A method of preparing sugarcane wax cold press soybean oil grease gel

Publications (1)

Publication Number Publication Date
CN108338216A true CN108338216A (en) 2018-07-31

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CN201810082861.7A Pending CN108338216A (en) 2018-01-29 2018-01-29 A method of preparing sugarcane wax cold press soybean oil grease gel

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111418665A (en) * 2020-03-30 2020-07-17 天津科技大学 Preparation and application of cocoa butter low-melting-point fraction organic oleogel
CN114009763A (en) * 2021-11-03 2022-02-08 上海应用技术大学 Fructus cannabis oil gel and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102510725A (en) * 2009-06-12 2012-06-20 玛尔斯有限公司 Polymer gelation of oils
CN105145869A (en) * 2015-06-26 2015-12-16 江西农业大学 Soybean oil and thymus mongolicus oil based gel oil and preparation method thereof
CN105341186A (en) * 2015-12-05 2016-02-24 福州大学 Method for processing grease added with organic gel

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102510725A (en) * 2009-06-12 2012-06-20 玛尔斯有限公司 Polymer gelation of oils
CN105145869A (en) * 2015-06-26 2015-12-16 江西农业大学 Soybean oil and thymus mongolicus oil based gel oil and preparation method thereof
CN105341186A (en) * 2015-12-05 2016-02-24 福州大学 Method for processing grease added with organic gel

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
JULIO CESAR BARBOSA ROCHA等: "Thermal and rheological properties of organogels formed by sugarcane or candelilla wax in soybean oil", 《FOOD RESEARCH INTERNATIONAL》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111418665A (en) * 2020-03-30 2020-07-17 天津科技大学 Preparation and application of cocoa butter low-melting-point fraction organic oleogel
CN114009763A (en) * 2021-11-03 2022-02-08 上海应用技术大学 Fructus cannabis oil gel and preparation method thereof

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Application publication date: 20180731