CN108333637A - A method of it improving geochemical well logging technology and determines constituent content accuracy - Google Patents

A method of it improving geochemical well logging technology and determines constituent content accuracy Download PDF

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Publication number
CN108333637A
CN108333637A CN201711338259.7A CN201711338259A CN108333637A CN 108333637 A CN108333637 A CN 108333637A CN 201711338259 A CN201711338259 A CN 201711338259A CN 108333637 A CN108333637 A CN 108333637A
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well logging
geochemical well
constituent content
geochemical
scale tank
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CN108333637B (en
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刘军涛
刘树才
张锋
李福生
苗彬
杨传乐
张泉滢
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Lanzhou University
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China University of Mining and Technology CUMT
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01VGEOPHYSICS; GRAVITATIONAL MEASUREMENTS; DETECTING MASSES OR OBJECTS; TAGS
    • G01V5/00Prospecting or detecting by the use of nuclear radiation, e.g. of natural or induced radioactivity
    • G01V5/04Prospecting or detecting by the use of nuclear radiation, e.g. of natural or induced radioactivity specially adapted for well-logging
    • G01V5/08Prospecting or detecting by the use of nuclear radiation, e.g. of natural or induced radioactivity specially adapted for well-logging using primary nuclear radiation sources or X-rays
    • G01V5/10Prospecting or detecting by the use of nuclear radiation, e.g. of natural or induced radioactivity specially adapted for well-logging using primary nuclear radiation sources or X-rays using neutron sources
    • G01V5/101Prospecting or detecting by the use of nuclear radiation, e.g. of natural or induced radioactivity specially adapted for well-logging using primary nuclear radiation sources or X-rays using neutron sources and detecting the secondary Y-rays produced in the surrounding layers of the bore hole

Abstract

The invention discloses a kind of methods that raising geochemical well logging technology determines constituent content accuracy, and in particular to petroleum and natural gas logging technique field.When determining constituent content which solve existing geochemical well logging technology, fixed a set of elemental standards spectrum, the affected deficiency of constituent content accuracy is utilized.This method specifically includes:Build geochemical well logging instrument scale tank;Mathematical calculation model is set up using method for numerical simulation;Numerical Simulation Program is improved, the reaction type for being able to record neutron and having an effect with stratum element, position, time and the program of numerical calculation for discharging gamma energy are obtained;It is measured in scale tank using geochemical well logging instrument, benchmark verification is carried out using gamma-spectrometric data logarithm calculation procedure is measured;More set elemental standards spectrum library under different well logging conditions is established for field data processing;Using the method for loop iteration, the error of fitting of various criterion spectrum is calculated, selects a set of standard spectrum of error of fitting minimum, calculates backbone element.

Description

A method of it improving geochemical well logging technology and determines constituent content accuracy
Technical field
The present invention relates to petroleum and natural gas logging technique fields, and in particular to a kind of raising geochemical well logging technology determination member The method of cellulose content accuracy.
Background technology
Geochemical well logging technology is that by neutron source neutron occurs for one kind, utilizes neutron and formation material that inelastic scattering occurs And radiation capture effect, the gamma spectra data that acquisition effect generates, and then determine the logging method of stratum backbone element content. Current main geochemical well logging instrument mainly has the ECS of Schlumberger, the GEM of Halliburton, the FleX of Bake Hughes and this human relations The FEM of Lith Scanner, petrochina Logging Company that shellfish is thanked, the PNST etc. of Daqing oil field testing service company.Geochemical well logging Instrument is measured in underground, by acquiring non-ballistic and capture gamma spectra, is handled and is surveyed using the standard gamma power spectrum library of element Power spectrum is measured, and then formation skeleton element yield and content is calculated.Generally by scale tank or the method for numerical simulation, establish The standard gamma power spectrum library of a set of stratum element.Schlumberger, Bake Hughes, petrochina Logging Company are formed by building SiO2、CaCO3, the substances such as S scale bucket, obtain the standard power spectrum library of the elements such as Si, Ca.It can also be by numerical simulation side Method establishes the stratigraphic model that stratum group corresponds to oxide as element, establishes a set of elemental standards gal for field data processing Ma Nengpuku.
But in well logging, it can change such as formation porosity, density, well under the well logging condition of different depth points Eye size, drilling fluid types etc..When above-mentioned well logging condition changes, the spatial flux distribution that neutron occurs for neutron source can be sent out Changing.Therefore the generation position of inelastic scattering and capture gamma ray can change, and influence gamma ray and reach detection The path of device.The shape of the standard gamma power spectrum of single element can be affected.If utilizing fixed a set of elemental standards gamma Power spectrum library has handled actual measurement gamma spectra, can fix exactness really to constituent content and have an impact.
Patent No. US7366615 (04/2008), US5471057 (11/1995), US20110218735 (09/2011) United States Patent (USP), Patent No. CN103696765 (11/2013), CN102084271 (06/2009), CN102518431 (06/ 2012), the Chinese patent of CN104329075 (09/2014), CN105182422 (09/2015), CN105629319A.
The .PNST-E pulsed neutron formation element logging technology researchs such as Zheng Hua《Logging technique》.2015, volume 39 the (the 4th Phase)
Geochemical well logging development course and technique prospects of the superfine of Yuan based on gamma spectra《Advances in Geophysics》 .2014, volume 29 (the 4th phase)
The shale gas-bearing formation pulsed neutron geochemical well logging Monte Carlo studies such as Liu Juntao《Logging technique》.2015, volume 39 (volume 5).
The such as Liu Juntao pulsed neutron geochemical well logging instrument MC benchmarks and standard of instruments spectrum analog [C] // China's nuclear science Technical progress report .2013.
Above-mentioned patent or document describe the method that existing some elemental standards spectrum obtains and constituent content determines, wherein He Biao, Liu Juntao et al. introduce a kind of method for establishing fixed a set of stratum element standard spectrum;In terms of constituent content determination, all It is that fixed a set of elemental standards spectrum is utilized, but when well logging condition changes, such as borehole size, drilling mud type are not Meanwhile the shape of elemental standards spectrum can change.Gamma-spectrometric data is measured using a set of elemental standards spectrum processing of fixation, element contains Amount accuracy in computation can be affected.
Deficiency existing for constituent content is determined for above-mentioned existing geochemical well logging, is passed through invention describes one kind and being established more sets It is true to improve geochemical well logging technology for elemental standards gamma spectra library under the conditions of Different Strata, the method calculated using loop iteration Determine a kind of method of constituent content accuracy.
Invention content
The purpose of the present invention is against the above deficiency, it is proposed that a kind of element by establishing under the conditions of more covering Different Stratas Standard gamma power spectrum library, the method calculated using loop iteration improve the side that geochemical well logging technology determines constituent content accuracy Method.
The present invention specifically adopts the following technical scheme that:
A method of it improving geochemical well logging technology and determines constituent content accuracy, specifically include:
A. the scale tank of geochemical well logging instrument is built, is annulus type wherein among scale tank, Known Elements is added in scale tank The packing material of element composition;
B. geochemical well logging instrument, packing material and scale tank is used to set up mathematical calculation model, wherein packing material is filled into In scale tank, geochemical well logging instrument is inserted into packing material;
C. Numerical Simulation Program is improved, the reaction type for recording neutron and having an effect with stratum element, position, time are obtained And generate the program of numerical calculation of the energy of inelastic scattering and radiation capture gamma ray;
D. it is measured in scale tank using geochemical well logging instrument, journey is calculated using obtained gamma-spectrometric data logarithm is measured Sequence carries out benchmark verification;
E. establish Different porosities, borehole size, drilling mud type or oil-gas possibility stratigraphic model, skeleton is respectively The correspondence oxide of different elements is used to survey after obtaining more set leading element gamma spectra library storages under different well logging conditions Data processing;
F. the method for using loop iteration is utilized respectively and covers different leading element gamma spectra library processing element well loggings more Instrument measured spectrum data calculates the error of fitting iterated to calculate every time, selects a set of leading element gamma of error of fitting minimum Power spectrum library is calculated each element yield of stratum, backbone element content is finally calculated.
Preferably, the geochemical well logging instrument includes shell and ground control system, in being sequentially connected with from bottom to top in shell Component, Neutron shielding body, gamma crystal counter, photomultiplier, underground control and Acquisition Circuit and ground control system.
Preferably, leading element gamma spectra library includes Si, Ca, S, Fe, S, Ti, Gd, Cl, H, K and Al.
Preferably, the scale tank is horizontal, and outer shroud radius is more than 80cm, and inner ring radius is 10cm.
Preferably, the spectrum of the elemental standards under different well logging conditions can be calculated in the program of numerical calculation.
The present invention has the advantages that:
By this method, overcomes elemental standards spectral shape under different well logging conditions and change the shadow calculated constituent content It rings, improves the accuracy that geochemical well logging technology determines constituent content.
Description of the drawings
Fig. 1 is the method flow schematic diagram for improving geochemical well logging technology and determining constituent content accuracy;
Fig. 2 is typical stratum geochemical well logging apparatus structure schematic diagram;
Fig. 3 is geochemical well logging instrument test graduation apparatus structural schematic diagram;
Fig. 4 is the Si elemental standards spectrum comparison under different well logging conditions.
Wherein, 1 is neutron source, and 2 be Neutron shielding body, and 3 be gamma crystal counter, and 4 be photomultiplier, and 5 be underground Control and Acquisition Circuit, 6 be ground control system, and 7 be scale tank.
Specific implementation mode
The specific implementation mode of the present invention is described further in the following with reference to the drawings and specific embodiments:
As shown in Figure 1-Figure 3, a method of improving geochemical well logging technology and determine constituent content accuracy, specifically include:
Wherein, skeleton and packing material are the composed structure of simulated formation, and the stratum of skeleton simulation is more rich, fills material Expect that the stratum of simulation is relatively easy.
A. the scale tank of geochemical well logging instrument is built, is annulus type wherein among scale tank, Known Elements is added in scale tank The packing material of element composition, packing material can be quartz sand, and quartz sand group becomes quartz 99%, feldspar 1%.
B. the parameter of geochemical well logging instrument, packing material and scale tank 7 is used to set up mathematical calculation model, wherein packing material It is filled into scale tank, packing material can be above-mentioned quartz sand, and geochemical well logging instrument is inserted into packing material;
Wherein, geochemical well logging instrument includes shell and ground control system, be sequentially connected with from bottom to top in shell neutron source 1, Neutron shielding body 2, gamma crystal counter 3, photomultiplier 4, underground control and Acquisition Circuit 5 and ground control system 6.
C. it improves Numerical Simulation Program, obtains and be able to record reaction type when neutron is had an effect with stratum element, position Set, the time and generate inelastic scattering and radiation capture gamma ray energy program of numerical calculation;
D. it is measured in scale tank using geochemical well logging instrument, journey is calculated using obtained gamma-spectrometric data logarithm is measured Sequence carries out benchmark verification;
E. establish Different porosities, borehole size, drilling mud type or oil-gas possibility stratigraphic model (stratigraphic model Porosity can take 0% respectively, 5%, 10%, 15%, 20%, 30%, 40%), skeleton is respectively the correspondence oxygen of different elements Compound establishes the stratigraphic model that wellbore radius is respectively 6cm, 8cm, 10cm, 12cm, 16cm;Establish drilling fluid be respectively fresh water, The stratigraphic model of barite mud (water, barite, bentonite);Finally obtain more set leading element gals under different well logging conditions For real after Ma Nengpuku (leading element gamma spectra library includes Si, Ca, S, Fe, S, Ti, Gd, Cl, H, K and Al) storage The processing of survey data;It is respectively the Si elemental standards spectrum obtained under the conditions of fresh water and barite mud to be illustrated in figure 4 wellbore fluid, It can be seen that well logging condition difference produces influence to elemental standards spectral shape.
F. the method for using loop iteration is utilized respectively and covers different leading element gamma spectra library processing element well loggings more Instrument measured spectrum data calculates the error of fitting iterated to calculate every time, selects a set of leading element gamma of error of fitting minimum Power spectrum library is calculated each element yield of stratum, backbone element content is finally calculated.
It is utilized respectively the present invention and current geochemical well logging processing method (is based on a set of fixed element standard spectrum and oxide Model carries out constituent content conversion), processing formation skeleton group becomes SiO2、Al2O3, MgO and FeO, drilling mud it is respectively light When water and barite mud, the capture gamma spectra data that the apparatus measures on stratum obtain, and calculate formation skeleton constituent content. During calculating elements content, existing constituent content is respectively adopted and determines that method and the method for the present invention, the element of the two contain It measures result of calculation and actual comparison is as shown in table 1.
Table 1
As can be seen from Table 1, the geochemical well logging apparatus measures power spectrum number under different well logging conditions is handled using existing method According to the accuracy in computation of constituent content is impacted.Formation skeleton constituent content accuracy is calculated using the method for the present invention to be carried It is high.
Certainly, above description is not limitation of the present invention, and the present invention is also not limited to the example above, this technology neck The variations, modifications, additions or substitutions that the technical staff in domain is made in the essential scope of the present invention should also belong to the present invention's Protection domain.

Claims (5)

1. a kind of method for improving geochemical well logging technology and determining constituent content accuracy, which is characterized in that specifically include:
A. the scale tank of geochemical well logging instrument is built, is annulus type wherein among scale tank, known element group is added in scale tank At packing material;
B. geochemical well logging instrument, packing material and scale tank parameter is used to set up mathematical calculation model, wherein packing material is filled into In scale tank, geochemical well logging instrument is inserted into packing material;
C. improve Numerical Simulation Program, obtain be able to record reaction type when neutron is had an effect with stratum element, position, when Between and generate inelastic scattering and radiation capture gamma ray energy program of numerical calculation;
D. measured in scale tank using geochemical well logging instrument, using measure obtained gamma-spectrometric data logarithm calculation procedure into Row benchmark is verified;
E. establish Different porosities, borehole size, drilling mud type or oil-gas possibility stratigraphic model, skeleton be respectively difference The correspondence oxide of element is used for field data after obtaining more set leading element gamma spectra library storages under different well logging conditions Processing;
F. the method for using loop iteration is utilized respectively and covers different leading element gamma spectra library processing element logging instrument realities more Power spectrum data is surveyed, the error of fitting iterated to calculate every time is calculated, selects a set of leading element gamma spectra of error of fitting minimum Library is calculated each element yield of stratum, backbone element content is finally calculated.
2. a kind of method for improving geochemical well logging technology and determining constituent content accuracy as described in claim 1, feature exist In the geochemical well logging instrument includes shell and ground control system, and neutron source, neutron shield are sequentially connected with from bottom to top in shell Body, gamma crystal counter, photomultiplier, underground control and Acquisition Circuit and ground control system.
3. a kind of method for improving geochemical well logging technology and determining constituent content accuracy as claimed in claim 1 or 2, feature It is, leading element gamma spectra library includes Si, Ca, S, Fe, S, Ti, Gd, Cl, H, K and Al.
4. a kind of method for improving geochemical well logging technology and determining constituent content accuracy as described in claim 1, feature exist In the scale tank is horizontal, and outer shroud radius is more than 80cm, and inner ring radius is 10cm.
5. a kind of method for improving geochemical well logging technology and determining constituent content accuracy as described in claim 1, feature exist In the spectrum of the elemental standards under different well logging conditions can be calculated in the program of numerical calculation.
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109241644A (en) * 2018-09-19 2019-01-18 中国矿业大学 A kind of element yield calculation method for stratum element well logging
CN109740279A (en) * 2019-01-14 2019-05-10 东华理工大学 A kind of electrically controllable neutron Analysis of Gamma Energy Spectrum method in characteristic frequency spectrum library
CN109814147A (en) * 2019-01-01 2019-05-28 中国人民解放军63653部队 Use the method for gamma activity Nuclear analysis around detector plus decaying bulk measurement aperture
CN115267928A (en) * 2022-09-28 2022-11-01 中石化经纬有限公司 Intelligent energy spectrum processing method for logging while drilling element

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201763313U (en) * 2010-07-23 2011-03-16 中国石油化工集团公司 Calibrating device for pulsed neutron logging tool
CN104329075A (en) * 2014-09-05 2015-02-04 西安奥华电子仪器有限责任公司 Obtaining method of element capture normal spectroscopy in elemental logging
CN105182422A (en) * 2015-09-02 2015-12-23 中国石油天然气集团公司 Stratum element logging element standard spectrum making and application method
CN107229080A (en) * 2017-05-23 2017-10-03 兰州大学 A kind of acquisition methods of geochemical well logging neutron absorption gamma spectra

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201763313U (en) * 2010-07-23 2011-03-16 中国石油化工集团公司 Calibrating device for pulsed neutron logging tool
CN104329075A (en) * 2014-09-05 2015-02-04 西安奥华电子仪器有限责任公司 Obtaining method of element capture normal spectroscopy in elemental logging
CN105182422A (en) * 2015-09-02 2015-12-23 中国石油天然气集团公司 Stratum element logging element standard spectrum making and application method
CN107229080A (en) * 2017-05-23 2017-10-03 兰州大学 A kind of acquisition methods of geochemical well logging neutron absorption gamma spectra

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
刘军涛 等: "脉冲中子元素测井仪MC基准实验及仪器标准谱模拟", 《中国核科学技术进展报告》 *
向威 等: "地层元素测井中元素标准谱的数值模拟及影响因素研究", 《中国地球科学联合学术年会2014》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109241644A (en) * 2018-09-19 2019-01-18 中国矿业大学 A kind of element yield calculation method for stratum element well logging
CN109814147A (en) * 2019-01-01 2019-05-28 中国人民解放军63653部队 Use the method for gamma activity Nuclear analysis around detector plus decaying bulk measurement aperture
CN109740279A (en) * 2019-01-14 2019-05-10 东华理工大学 A kind of electrically controllable neutron Analysis of Gamma Energy Spectrum method in characteristic frequency spectrum library
CN115267928A (en) * 2022-09-28 2022-11-01 中石化经纬有限公司 Intelligent energy spectrum processing method for logging while drilling element

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