CN108333333A - A kind of crude oil and heavy oil sediments measurement experimental provision - Google Patents

A kind of crude oil and heavy oil sediments measurement experimental provision Download PDF

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Publication number
CN108333333A
CN108333333A CN201810228445.3A CN201810228445A CN108333333A CN 108333333 A CN108333333 A CN 108333333A CN 201810228445 A CN201810228445 A CN 201810228445A CN 108333333 A CN108333333 A CN 108333333A
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CN
China
Prior art keywords
experimental provision
crude oil
sediments
distributor
measurement experimental
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Pending
Application number
CN201810228445.3A
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Chinese (zh)
Inventor
尹荣林
刘汗青
武梦奇
李秀林
肖荣海
白明懂
王兴艳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Inspection And Certification Group Yunnan Co Ltd Ruili Branch
Ruili Entry Exit Inspection And Quarantine Bureau Inspection And Quarantine Integrated Technology Center
Original Assignee
China Inspection And Certification Group Yunnan Co Ltd Ruili Branch
Ruili Entry Exit Inspection And Quarantine Bureau Inspection And Quarantine Integrated Technology Center
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Application filed by China Inspection And Certification Group Yunnan Co Ltd Ruili Branch, Ruili Entry Exit Inspection And Quarantine Bureau Inspection And Quarantine Integrated Technology Center filed Critical China Inspection And Certification Group Yunnan Co Ltd Ruili Branch
Priority to CN201810228445.3A priority Critical patent/CN108333333A/en
Publication of CN108333333A publication Critical patent/CN108333333A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; viscous liquids; paints; inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; viscous liquids; paints; inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2823Oils, i.e. hydrocarbon liquids raw oil, drilling fluid or polyphasic mixtures

Abstract

The present invention relates to a kind of crude oil and weight oil sediments measurement experimental provision, belong to crude oil experimental provision technical field;The crude oil and weight oil sediments measurement experimental provision includes extraction flask, distributor, hanging basket, condensing unit;The distributor is placed on the top of extraction flask, and bottom surface is equipped with distributing disc, and distributing disc inner ring is equipped with gas-guide tube, and outer ring is equipped with liquid-leaking nozzle, is welded with extended column along the outer rim of liquid-leaking nozzle, the center of distributing disc is equipped with hook;The upper weld of distributor has upper interface;The condensing unit includes shell, condenser pipe, overflow pipe, manifold and the frosted of lower part interface, is connected with upper interface by frosted interface;The configuration of the present invention is simple, convenient for disassembly and assembly, the elution of extracting sleeve edges is uniformly, fully, completely, it is fast, it can be achieved that batch detection, condensing unit are discharged after the water of generation can be collected separately to extract speed, it avoids generating bumping, while recoverable part extraction solvent when extracting, it is economic and environment-friendly.

Description

A kind of crude oil and heavy oil sediments measurement experimental provision
Technical field
The invention belongs to crude oil experimental provision technical fields, specifically, being related to a kind of crude oil and heavy oil sediments survey Surely experimental provision is used.
Background technology
The sediment that oil field defines refers to being present in all precipitations insoluble in regulation solvent in crude oil and heavy oil etc. Or suspended matter.Sediment in crude oil seriously affect the transport of crude oil, trade transaction, the production cost for increasing later stage product oil, And selection and the service life of the instrument and equipment of downstream user.The sediment device used in GB/T6531-86 standards is one Extracting sleeve, bottleneck condenser coil are linked into a big conical flask(Condenser)Integral structure is sealed and is cooled down.This Kind of device there are repeatability and reproducibility poor, extraction efficiency bottom, extracting and cooling velocity are slow, can not water-oil separating, operation is square Just, the disadvantages such as environmental-friendly degree is low.Publication No. CN 102338723A, a kind of entitled crude oil and fuel oil sediments The patent of invention of measurement device increases guiding device in flask, which includes that diameter is slightly less than extracting sleeve diameter Round deflector and with the connector that connect deflector and condenser coil, which is conducive to rushing for sleeve edges It washes, but since the guiding device is hung on condenser pipe lower end, the relative position between sleeve is easy offset, is still easy to cause set Cylinder rim wash is incomplete.Publication No. CN 104458479A, a kind of entitled crude oil and fuel oil sediments measurement device Patent of invention, extracting sleeve and flask separate design increase the elution that water conservancy diversion funnel is conducive to sleeve edges, but separation is set Meter makes temperature in sleeve reduce, and is unfavorable for the elution of high boiling substance, causes result higher.In addition trapezoidal condenser is leaked with water conservancy diversion Struggle against corresponding design, and room for improvement is limited, batch extraction efficiency bottom.
In view of the above the technical problems existing in the prior art, the present invention provides a kind of crude oil and heavy oil sediments measures With experimental provision, the experimental provision is simple in construction, easy to disassemble and assemble, and sediment extracting speed is fast, efficient.
Invention content
In order to solve the problems, such as background technology, the present invention provides a kind of crude oil and weight oil sediments to measure and use Experimental provision.
The crude oil and weight oil sediments measurement includes mainly extraction flask with experimental provision, distributor, hanging basket, cold Solidifying device;The distributor is hollow cone structure, and bottom surface is equipped with distributing disc, and the center weld of distributing disc has hook, point Cloth device is placed on the top of extraction flask;The top of the distributor be equipped with upper interface, the condensing unit by outer diameter with it is upper The frosted interface that interface internal diameter matches is connected with upper interface;The hanging basket is placed in extraction flask and hangs on hook On.
Further, the inner ring of the distributing disc is uniformly provided with gas-guide tube, and outer ring is uniformly provided with liquid-leaking nozzle.
Further, the condensing unit includes shell, condenser pipe, overflow pipe, manifold and the frosted of lower part interface, institute The cavity top that the shell stated is formed is equipped with condenser pipe, and cavity lower part is equipped with overflow pipe and manifold, and manifold is extended to across shell Outside, and which is provided with valve.
Further, the hanging basket lower part is uniformly provided with sleeve fixing frame, and sleeve fixing frame number is 4-6.
Further, a diameter of 0.5-1mm of the liquid-leaking nozzle.
Further, the internal diameter of the gas-guide tube is 3-4 mm, and number is 4-6.
Further, outer diameter and extraction flask are welded with along the outer rim of the liquid-leaking nozzle on distributing disc in the bottom surface of distributor The extended column that internal diameter matches.
Further, the overflow pipe height is 30-40mm.
Further, the internal diameter of the overflow pipe is 10-15mm.
Further, the outer diameter of the hanging basket and the outer diameter of extended column are consistent.
Beneficial effects of the present invention:Experimental provision overall structure of the present invention is simple, and dismounting is easy for installation, extracts sleeve edges Uniformly, fully, completely, extracting speed is fast, it can be achieved that batch detection, after the moisture content of generation can be collected separately for condensing unit for elution Discharge avoids being mixed with water generation bumping when extracting, while can recycle part extraction solvent, reduces extraction solvent waste, It is economic and environment-friendly.
Description of the drawings
Fig. 1 is that the structure of the present invention splits schematic diagram;
Fig. 2 is the combination diagram of the present invention;
Fig. 3 is the structural schematic diagram of the distributor of the present invention;
In figure, 1- condensing units, 2- condenser pipes, 3- overflow pipes, 4- shells, 5- valves, 6- manifolds, 7- frosteds interface, 8- distributions The upper interface of device, 9-, 11- extended columns, 12- hooks, 13- distributing discs, 14- gas-guide tubes, 15- liquid-leaking nozzles, 16- extraction flasks, 17- are hung Button, 18- hanging baskets, 19- sleeve fixing frames.
Specific implementation mode
In order to keep the purpose of the present invention, technical solution and advantageous effect clearer, below in conjunction with attached drawing, to the present invention Preferred embodiment be described in detail, to facilitate the technical staff to understand.
As shown in the picture, the crude oil and weight oil sediments measurement are mainly burnt including extracting with experimental provision Bottle 16, distributor 8, hanging basket 18, condensing unit 1.
The distributor 8 is hollow conical structure, and basal diameter is more than the outer of the flask mouth of extraction flask 16 Diameter, bottom surface are equipped with distributing disc 13, and the inner ring of the distributing disc 13 is uniformly provided with gas-guide tube 14, and outer ring is uniformly provided with liquid-leaking nozzle 15, gas-guide tube 14 and the design of liquid-leaking nozzle 15 separate gas circuit and fluid path, avoid air-flow rising from being obstructed, influence experiment effect, together When liquid-leaking nozzle 15 secondary distribution is carried out to the lower condensate liquid dripped after condensation, make to carry out sleeve by 15 dripping of liquid-leaking nozzle Uniform elution.
It is welded in outer diameter and extraction flask 16 along the outer rim of the liquid-leaking nozzle 15 on distributing disc 13 in the bottom surface of distributor 8 The extended column 11 that diameter matches, when installation, go deep into extended column 11 inside extraction flask 16, and distributor 8 is placed on extraction flask 16 Top, the air-tightness when setting of extended column 11 can be worked with stiffening device.
The center weld of distributing disc 13 has hook 12, and hook 12 stretches out outside extended column 11, for fixing hanging basket 18, distributor 8 are placed on the top of extraction flask 16, realize that distributor 8 and the sealing of extraction flask 16 are detachably connected;The top of distributor 8 is same Axis is welded with interface 9.
The top of the hanging basket 18, which is equipped with, withholds 17, and hanging basket 18 is hung on by withholding 17 on hook 12;Hanging basket 18 Lower part is uniformly provided with sleeve fixing frame 19, for placing extracting sleeve.
The condensing unit 1 includes shell 4, condenser pipe 2, overflow pipe 3, manifold 6 and the frosted interface 7 of lower part, described The cavity top that is formed of shell 4 be equipped with condenser pipe 2, the inlet and outlet of condenser pipe 2 are fixed on shell 4, and cavity lower part, which is equipped with, overflows The upper surface of flow tube 3 and manifold 6, overflow pipe 3 is located at 2 lower section of condenser pipe, and manifold 6 extends to outside across shell 4, and sets thereon There is valve 5.The gas risen in experimentation is condensed into liquid, the setting of overflow pipe 3 after encountering condenser pipe 2 so that condensation The liquid of generation cannot flow directly out condensing unit 1, but be gathered in the lower part of cavity, only when the liquid level of condensate liquid is higher than excessive When flow tube 3, could toward flow down.Liquid is during being gathered in cavity lower part, since the density of water is more than extraction solvent and water It is immiscible with extraction solvent, so that water is fallen to bottom, when moisture reaches it is a certain amount of when, the valve 5 on manifold 6 can be opened, Moisture is discharged, avoiding excess water from existing causes to extract bumping;Extraction solvent can also be recycled simultaneously, reduces toxic examination The discharge of agent, it is economic and environment-friendly.
The internal diameter of the outer diameter and upper interface 9 of the frosted interface 7 of 1 lower part of condensing unit matches, when device assembles, Frosted interface 7 is inserted into upper interface 9, realizes that condensing unit 1 and the sealing of upper interface 9 are detachably connected.
Preferably, the overflow pipe height is 30-40 mm, is located at the lower section of condenser pipe 2, condensate liquid is uniformly drained To 13 top of distributing disc.
Preferably, the internal diameter of the overflow pipe 3 is 10-15 mm.
Preferably, 19 numbers of the sleeve fixing frame are 4-6, it can be achieved that Multi-example measures simultaneously, provide work and imitate Rate, Enhancement test contrast.
Preferably, a diameter of 0.5-1 mm of the liquid-leaking nozzle 15 so that condensate liquid is evenly distributed, and uniformly falls leaching Wash sleeve.
Preferably, the internal diameter of the gas-guide tube 14 is 3-4 mm, and number is 4-6.
Preferably, the outer diameter of the hanging basket 18 is consistent with the outer diameter of extended column 11.
The course of work of the present invention:
The national standard that experiment measures before starting according to sediment gets out related agents, and hanging basket 18 is hung on hook 12, will Extracting sleeve being put in sleeve fixing frame 19 symmetrically and evenly, hanging basket 18 is put in extraction flask 16,8 sealing cover of distributor is made In the top of extraction flask 16, the frosted interface 7 of 1 lower part of condensing unit is inserted into upper interface 9, the inlet and outlet point of condenser pipe 2 It is not connected with the inlet and outlet of condensed water, after experimental provision is completed, according to national standards, carries out sediment determination experiment.
In experimentation, the heated volatilization of extraction solvent, the body gas of generation is entered in condensing unit 1 by gas-guide tube 14, is met To condenser pipe 2, liquid accumulation is condensed into during the cavity lower part that the shell 4 of condensing unit 1 is formed, liquid accumulation, wherein Wet-laid in bottom, extraction solvent is cold when the liquid level of the condensate liquid of aggregation is higher than the upper surface of overflow pipe 3 on upper layer Lime set is flowed into along overflow pipe 3 on distributing disc 13, by the secondary distribution of the liquid-leaking nozzle 15 on distributing disc 13, condensate liquid is uniform Sprinkle on as the extracting sleeve in hanging basket 18, realize uniformly adequately elution, improve extraction efficiency;And it is gathered in bottom Moisture, when reaching a certain amount of, open manifold 6 on valve 5, moisture is discharged, avoid excess water exist cause to extract Bumping, while recoverable part extraction solvent, realize the recycling of extraction solvent.
Finally illustrate, preferred embodiment above is merely illustrative of the technical solution of the present invention and unrestricted, although logical It crosses above preferred embodiment the present invention is described in detail, however, those skilled in the art should understand that, can be Various changes are made to it in form and in details, without departing from claims of the present invention limited range.

Claims (9)

1. a kind of crude oil and weight oil sediments measurement experimental provision, it is characterised in that:It is precipitated in the crude oil and heavy oil Object measurement includes mainly extraction flask, distributor, hanging basket, condensing unit with experimental provision;The distributor bottom surface, which is equipped with, to be divided The center weld of cloth disk, distributing disc has hook, distributor to be placed on the top of extraction flask;The top of the distributor is equipped with and above connects Mouthful, the condensing unit is connected with the frosted interface that upper interface internal diameter matches with upper interface by outer diameter;Described hangs Basket is placed in extraction flask and hangs on hook.
2. a kind of crude oil according to claim 1 and weight oil sediments measurement experimental provision, it is characterised in that:It is described The inner ring of distributing disc be uniformly provided with gas-guide tube, outer ring is uniformly provided with liquid-leaking nozzle.
3. a kind of crude oil according to claim 1 and weight oil sediments measurement experimental provision, it is characterised in that:It is described Condensing unit include shell, condenser pipe, overflow pipe, manifold and the frosted of lower part interface, on the cavity that the shell is formed Portion is equipped with condenser pipe, and cavity lower part is equipped with overflow pipe and manifold, and manifold extends to outside across shell, and which is provided with valve.
4. a kind of crude oil according to claim 1 and weight oil sediments measurement experimental provision, it is characterised in that:It is described Hanging basket lower part be uniformly provided with sleeve fixing frame, sleeve fixing frame number is 4-6.
5. a kind of crude oil according to claim 2 and weight oil sediments measurement experimental provision, it is characterised in that:It is described Liquid-leaking nozzle a diameter of 0.5-1mm.
6. a kind of crude oil according to claim 2 and weight oil sediments measurement experimental provision, it is characterised in that:It is described The internal diameter of gas-guide tube be 3-4 mm, number is 4-6.
7. a kind of crude oil according to claim 2 and weight oil sediments measurement experimental provision, it is characterised in that:Dividing The bottom surface of cloth device is welded with the extended column that outer diameter matches with extraction flask internal diameter along the outer rim of the liquid-leaking nozzle on distributing disc.
8. a kind of crude oil according to claim 3 and weight oil sediments measurement experimental provision, it is characterised in that:It is described Overflow pipe height be 30-40mm.
9. a kind of crude oil according to claim 3 or 8 and weight oil sediments measurement experimental provision, it is characterised in that: The internal diameter of the overflow pipe is 10-15mm.
CN201810228445.3A 2018-03-20 2018-03-20 A kind of crude oil and heavy oil sediments measurement experimental provision Pending CN108333333A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810228445.3A CN108333333A (en) 2018-03-20 2018-03-20 A kind of crude oil and heavy oil sediments measurement experimental provision

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Application Number Priority Date Filing Date Title
CN201810228445.3A CN108333333A (en) 2018-03-20 2018-03-20 A kind of crude oil and heavy oil sediments measurement experimental provision

Publications (1)

Publication Number Publication Date
CN108333333A true CN108333333A (en) 2018-07-27

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Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2296754Y (en) * 1997-06-17 1998-11-11 朱华结 Three in one reflux condensation distillation water separator
CN201470403U (en) * 2009-08-11 2010-05-19 李刚 Reflux condenser
CN101856567A (en) * 2010-05-26 2010-10-13 重庆大学 Clapboard structure of extracting tank
CN202015512U (en) * 2011-03-08 2011-10-26 南京师范大学 Packing tower grid plate and vapour-liquid distributor integrated device
CN102455346A (en) * 2010-10-15 2012-05-16 中国石油化工股份有限公司 Asphalt analysis apparatus and use of the asphalt analysis apparatus in asphalt determination
CN202983717U (en) * 2012-11-30 2013-06-12 江苏省原子医学研究所 Liquid separation instrument and liquid separation device
CN103191578A (en) * 2013-04-27 2013-07-10 温州市天龙轻工设备有限公司 Extracting pot with homogenization baffle plate
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CN105699245A (en) * 2016-04-07 2016-06-22 中国石油化工股份有限公司 Oil field sludge multicomponent testing method
CN206474188U (en) * 2017-01-26 2017-09-08 佟宇婷 Vertical type separation water glass apparatus and vertical type separation water system
CN207012591U (en) * 2017-07-03 2018-02-16 无锡科伦达化工热力装备有限公司 A kind of de-heavy oil column
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2296754Y (en) * 1997-06-17 1998-11-11 朱华结 Three in one reflux condensation distillation water separator
CN201470403U (en) * 2009-08-11 2010-05-19 李刚 Reflux condenser
CN101856567A (en) * 2010-05-26 2010-10-13 重庆大学 Clapboard structure of extracting tank
CN102455346A (en) * 2010-10-15 2012-05-16 中国石油化工股份有限公司 Asphalt analysis apparatus and use of the asphalt analysis apparatus in asphalt determination
CN202015512U (en) * 2011-03-08 2011-10-26 南京师范大学 Packing tower grid plate and vapour-liquid distributor integrated device
CN202983717U (en) * 2012-11-30 2013-06-12 江苏省原子医学研究所 Liquid separation instrument and liquid separation device
CN103191578A (en) * 2013-04-27 2013-07-10 温州市天龙轻工设备有限公司 Extracting pot with homogenization baffle plate
CN203954716U (en) * 2014-06-06 2014-11-26 宜宾石平香料有限公司 Condenser in a kind of tower of rectifying column
CN204121804U (en) * 2014-08-26 2015-01-28 中华人民共和国大榭出入境检验检疫局 A kind of extracting is with dripping shower device
CN105699245A (en) * 2016-04-07 2016-06-22 中国石油化工股份有限公司 Oil field sludge multicomponent testing method
CN206474188U (en) * 2017-01-26 2017-09-08 佟宇婷 Vertical type separation water glass apparatus and vertical type separation water system
CN207012591U (en) * 2017-07-03 2018-02-16 无锡科伦达化工热力装备有限公司 A kind of de-heavy oil column
CN207964822U (en) * 2018-03-20 2018-10-12 瑞丽出入境检验检疫局检验检疫综合技术中心 A kind of crude oil and heavy oil sediments measurement experimental provision

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《石油工业常用国家标准汇编》编委会: "《石油工业常用国家标准汇编 油气田产品、试验方法和储运》", 中国标准出版社, pages: 78 - 81 *

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