CN108314368A - A kind of environment-friendly light decorative insulation board and preparation method thereof - Google Patents
A kind of environment-friendly light decorative insulation board and preparation method thereof Download PDFInfo
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- CN108314368A CN108314368A CN201810336095.2A CN201810336095A CN108314368A CN 108314368 A CN108314368 A CN 108314368A CN 201810336095 A CN201810336095 A CN 201810336095A CN 108314368 A CN108314368 A CN 108314368A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B20/00—Use of materials as fillers for mortars, concrete or artificial stone according to more than one of groups C04B14/00 - C04B18/00 and characterised by shape or grain distribution; Treatment of materials according to more than one of the groups C04B14/00 - C04B18/00 specially adapted to enhance their filling properties in mortars, concrete or artificial stone; Expanding or defibrillating materials
- C04B20/02—Treatment
- C04B20/023—Chemical treatment
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/40—Porous or lightweight materials
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
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- Y02W30/91—Use of waste materials as fillers for mortars or concrete
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Abstract
The invention discloses a kind of environment-friendly light decorative insulation boards, include the raw material of following parts by weight：10~20 parts of cullet, 8~14 parts of building waste, 7~12 parts of closed perlite, 5~10 parts of polyethylene, 9~16 parts of iron tailings, 10~20 parts of cement, 5~11 parts of epoxy resin, 12~26 parts of bentonite, 6~12 parts of calcined kaolin, 3~6 parts of polyester fiber, 2~5 parts of zirconium silicate, 2~4 parts of tungsten carbide, 1~3 part of alundum (Al2O3), 2~3 parts of glass fibre, modified 4~8 parts of longan pericarp powder, 2~3 parts of foaming agent, 2~4 parts of activating agent.The environment-friendly light decorative insulation board scientific formulation, rationally, the product heat insulation effect prepared is good, and thermal coefficient is low, flexural strength, excellent in cushion effect.
Description
Technical field
The invention belongs to heat preservation plate material technical fields, and in particular to a kind of environment-friendly light decorative insulation board and its preparation side
Method.
Background technology
The heat insulation effect of plank is a key index of gauge sheet metal quality can lead to heat if heat insulation effect is poor
Loss, waste of energy do not meet energy-saving and environment-friendly demand.It is more demanding to the heat insulation effect of plank in cleaning shop, only
Have with good heat insulation effect, can just prevent scattering and disappearing for heat, improve the utilization rate of the energy.
Invention content
The present invention provides a kind of environment-friendly light decorative insulation boards and preparation method thereof, solve asking in background technology
Topic, the environment-friendly light decorative insulation board scientific formulation, rationally, the product heat insulation effect prepared is good, and thermal coefficient is low, resist
Roll over intensity, excellent in cushion effect.
It is of the existing technology in order to solve the problems, such as, it adopts the following technical scheme that：
A kind of environment-friendly light decorative insulation board, includes the raw material of following parts by weight：10~20 parts of cullet, building waste 8~
14 parts, 7~12 parts of closed perlite, 5~10 parts of polyethylene, 9~16 parts of iron tailings, 10~20 parts of cement, epoxy resin 5~11
Part, 12~26 parts of bentonite, 6~12 parts of calcined kaolin, 3~6 parts of polyester fiber, 2~5 parts of zirconium silicate, 2~4 parts of tungsten carbide,
1~3 part of alundum (Al2O3), 2~3 parts of glass fibre, modified 4~8 parts of longan pericarp powder, 2~3 parts of foaming agent, 2~4 parts of activating agent
And appropriate amount of water.
Preferably, the environment-friendly light decorative insulation board, includes the raw material of following parts by weight：15~18 parts of cullet,
10~12 parts of building waste, 9~11 parts of closed perlite, 6~10 parts of polyethylene, 10~15 parts of iron tailings, 12~18 parts of cement,
7~10 parts of epoxy resin, 15~20 parts of bentonite, 8~11 parts of calcined kaolin, 4~5 parts of polyester fiber, 3~4 parts of zirconium silicate,
2.5~3.6 parts of tungsten carbide, 1.3~2.8 parts of alundum (Al2O3), 2.2~2.7 parts of glass fibre, modified 5~7 parts of longan pericarp powder,
2.1~2.7 parts of foaming agent, 2.4~3.6 parts of activating agent and appropriate amount of water.
Preferably, the environment-friendly light decorative insulation board, includes the raw material of following parts by weight：16 parts of cullet, building
11 parts of rubbish, 10 parts of closed perlite, 8 parts of polyethylene, 13 parts of iron tailings, 17 parts of cement, 9 parts of epoxy resin, 18 parts of bentonite,
10 parts of calcined kaolin, 4.5 parts of polyester fiber, 3.4 parts of zirconium silicate, 3.2 parts of tungsten carbide, 2 parts of alundum (Al2O3), glass fibre
2.4 parts, modified 6 parts of longan pericarp powder, 2.3 parts of foaming agent, 3.1 parts of activating agent and appropriate amount of water.
Preferably, the preparation method of the modified longan pericarp powder is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 500~600r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
Preferably, the antifoaming agent is any one of calcium carbonate, magnesium carbonate, silicon carbide.
Preferably, the activating agent is succinate sulfonic acid.
A method of the environment-friendly light decorative insulation board is prepared, is included the following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 1~2 hour, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 30%~40% to make water content in material, and epoxy resin, foaming agent and activity is added
Agent is uniformly mixed, and is subsequently placed in foaming processing 10~20 hours in foaming machine, is obtained mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
Preferably, the step（2）Middle sintering temperature is 1200~1300 DEG C.
Compared with prior art, the present invention it has the advantages that：
Environment-friendly light decorative insulation board scientific formulation of the present invention, rationally, the product heat insulation effect prepared is good, heat conduction system
Number is low, flexural strength, excellent in cushion effect, specific as follows：
（1）Environment-friendly light decorative insulation board of the present invention selects closed perlite and bentonite, calcined kaolin to make
It for primary raw material, using original hole-closing structure, and adds cement and the effect of highly effective binder can be realized, while being conducive to add
Fast molding and easy mold release are used in conjunction with polyethylene, epoxy resin and also provide enhanced bentonite, calcined kaolin and other raw materials
In conjunction with, and crystallization package has been carried out to above-mentioned raw materials, enhance heat insulation effect；
（2）Environment-friendly light decorative insulation board of the present invention further increases due to adding glass fibre and polyester fiber
The compression of strong plank and tensile strength, ensure that the workability of plank；
（3）The present invention prepares environment-friendly light decorative heat-preservation plate using building waste, discarded glass, modified longan pericarp powder as raw material
Material can realize that waste resource recycles, and reduce production cost, improve product competitiveness in the market；
（4）Tungsten carbide that the present invention is added, polyethylene, epoxy resin are to improving flexural strength, the impact strength of heat preservation plate material
There is obvious action, and the heat preservation plate material prepared also has low-down thermal coefficient, greatly reduces using process
In heat energy loss.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.These embodiments are merely to illustrate the present invention and do not have to
In limiting the scope of the invention.
Embodiment 1
The present embodiment is related to a kind of environment-friendly light decorative insulation board, includes the raw material of following parts by weight：10 parts of cullet, building
8 parts of rubbish, 5 parts of polyethylene, 9 parts of iron tailings, 10 parts of cement, 5 parts of epoxy resin, 12 parts of bentonite, is forged at 7 parts of closed perlite
Burn 6 parts of kaolin, 3 parts of polyester fiber, 2 parts of zirconium silicate, 2 parts of tungsten carbide, 1 part of alundum (Al2O3), 2 parts of glass fibre, modified dragon
4 parts of eye shell powder, 2 parts of foaming agent, 2 parts of activating agent and appropriate amount of water.
Wherein, the preparation method of the modified longan pericarp powder is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 500r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
Wherein, the antifoaming agent is calcium carbonate.
Wherein, the activating agent is succinate sulfonic acid.
A method of the environment-friendly light decorative insulation board is prepared, is included the following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 1 hour, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 30% to make water content in material, and epoxy resin, foaming agent and activating agent is added, stirs
It mixes uniformly mixed, is subsequently placed in foaming machine foaming processing 10 hours, obtains mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
Wherein, the step（2）Middle sintering temperature is 1200 DEG C.
Embodiment 2
The present embodiment is related to a kind of environment-friendly light decorative insulation board, includes the raw material of following parts by weight：20 parts of cullet, building
14 parts of rubbish, 12 parts of closed perlite, 10 parts of polyethylene, 16 parts of iron tailings, 20 parts of cement, 11 parts of epoxy resin, bentonite 26
Part, 12 parts of calcined kaolin, 6 parts of polyester fiber, 5 parts of zirconium silicate, 4 parts of tungsten carbide, 3 parts of alundum (Al2O3), 3 parts of glass fibre,
Modified 8 parts of longan pericarp powder, 3 parts of foaming agent, 4 parts of activating agent and appropriate amount of water.
Wherein, the preparation method of the modified longan pericarp powder is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 600r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
Wherein, the antifoaming agent is magnesium carbonate.
Wherein, the activating agent is succinate sulfonic acid.
A method of the environment-friendly light decorative insulation board is prepared, is included the following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 2 hours, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 40% to make water content in material, and epoxy resin, foaming agent and activating agent is added, stirs
It mixes uniformly mixed, is subsequently placed in foaming machine foaming processing 20 hours, obtains mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
Wherein, the step（2）Middle sintering temperature is 1300 DEG C.
Embodiment 3
The present embodiment is related to a kind of environment-friendly light decorative insulation board, includes the raw material of following parts by weight：15 parts of cullet, building
10 parts of rubbish, 9 parts of closed perlite, 6 parts of polyethylene, 10 parts of iron tailings, 12 parts of cement, 7 parts of epoxy resin, 15 parts of bentonite,
8 parts of calcined kaolin, 4 parts of polyester fiber, 3 parts of zirconium silicate, 2.5 parts of tungsten carbide, 1.3 parts of alundum (Al2O3), glass fibre 2.2
Part, modified 5 parts of longan pericarp powder, 2.1 parts of foaming agent, 2.4 parts of activating agent and appropriate amount of water.
Wherein, the preparation method of the modified longan pericarp powder is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 520r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
Wherein, the antifoaming agent is silicon carbide.
Wherein, the activating agent is succinate sulfonic acid.
A method of the environment-friendly light decorative insulation board is prepared, is included the following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 1.2 hours, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 33% to make water content in material, and epoxy resin, foaming agent and activating agent is added, stirs
It mixes uniformly mixed, is subsequently placed in foaming machine foaming processing 12 hours, obtains mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
Wherein, the step（2）Middle sintering temperature is 1220 DEG C.
Embodiment 4
The present embodiment is related to a kind of environment-friendly light decorative insulation board, includes the raw material of following parts by weight：18 parts of cullet, building
12 parts of rubbish, 11 parts of closed perlite, 10 parts of polyethylene, 15 parts of iron tailings, 18 parts of cement, 10 parts of epoxy resin, bentonite 20
Part, 11 parts of calcined kaolin, 5 parts of polyester fiber, 4 parts of zirconium silicate, 3.6 parts of tungsten carbide, 2.8 parts of alundum (Al2O3), glass fibre
2.7 parts, modified 7 parts of longan pericarp powder, 2.7 parts of foaming agent, 3.6 parts of activating agent and appropriate amount of water.
Wherein, the preparation method of the modified longan pericarp powder is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 550r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
Wherein, the antifoaming agent is calcium carbonate.
Wherein, the activating agent is succinate sulfonic acid.
A method of the environment-friendly light decorative insulation board is prepared, is included the following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 1.5 hours, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 35% to make water content in material, and epoxy resin, foaming agent and activating agent is added, stirs
It mixes uniformly mixed, is subsequently placed in foaming machine foaming processing 15 hours, obtains mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
Wherein, the step（2）Middle sintering temperature is 1250 DEG C.
Embodiment 5
The present embodiment is related to a kind of environment-friendly light decorative insulation board, includes the raw material of following parts by weight：16 parts of cullet, building
11 parts of rubbish, 10 parts of closed perlite, 8 parts of polyethylene, 13 parts of iron tailings, 17 parts of cement, 9 parts of epoxy resin, 18 parts of bentonite,
10 parts of calcined kaolin, 4.5 parts of polyester fiber, 3.4 parts of zirconium silicate, 3.2 parts of tungsten carbide, 2 parts of alundum (Al2O3), glass fibre
2.4 parts, modified 6 parts of longan pericarp powder, 2.3 parts of foaming agent, 3.1 parts of activating agent and appropriate amount of water.
Wherein, the preparation method of the modified longan pericarp powder is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 570r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
Wherein, the antifoaming agent is magnesium carbonate.
Wherein, the activating agent is succinate sulfonic acid.
A method of the environment-friendly light decorative insulation board is prepared, is included the following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 1.8 hours, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 37% to make water content in material, and epoxy resin, foaming agent and activating agent is added, stirs
It mixes uniformly mixed, is subsequently placed in foaming machine foaming processing 17 hours, obtains mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
Wherein, the step（2）Middle sintering temperature is 1275 DEG C.
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (8)
1. a kind of environment-friendly light decorative insulation board, which is characterized in that include the raw material of following parts by weight：Cullet 10~20
Part, 8~14 parts of building waste, 7~12 parts of closed perlite, 5~10 parts of polyethylene, 9~16 parts of iron tailings, cement 10~20
Part, 5~11 parts of epoxy resin, 12~26 parts of bentonite, 6~12 parts of calcined kaolin, 3~6 parts of polyester fiber, zirconium silicate 2~5
Part, 2~4 parts of tungsten carbide, 1~3 part of alundum (Al2O3), 2~3 parts of glass fibre, modified 4~8 parts of longan pericarp powder, foaming agent 2~3
Part, 2~4 parts of activating agent and appropriate amount of water.
2. environment-friendly light decorative insulation board according to claim 1, which is characterized in that include the original of following parts by weight
Material：15~18 parts of cullet, 10~12 parts of building waste, 9~11 parts of closed perlite, 6~10 parts of polyethylene, iron tailings 10~
15 parts, 12~18 parts of cement, 7~10 parts of epoxy resin, 15~20 parts of bentonite, 8~11 parts of calcined kaolin, polyester fiber 4
~5 parts, 3~4 parts of zirconium silicate, 2.5~3.6 parts of tungsten carbide, 1.3~2.8 parts of alundum (Al2O3), 2.2~2.7 parts of glass fibre,
Modified 5~7 parts of longan pericarp powder, 2.1~2.7 parts of foaming agent, 2.4~3.6 parts of activating agent and appropriate amount of water.
3. environment-friendly light decorative insulation board according to claim 1, which is characterized in that include the original of following parts by weight
Material：16 parts of cullet, 11 parts of building waste, 10 parts of closed perlite, 8 parts of polyethylene, 13 parts of iron tailings, 17 parts of cement, epoxy
9 parts of resin, 18 parts of bentonite, 10 parts of calcined kaolin, 4.5 parts of polyester fiber, 3.4 parts of zirconium silicate, 3.2 parts of tungsten carbide, three oxygen
Change 2 parts of two aluminium, 2.4 parts of glass fibre, modified 6 parts of longan pericarp powder, 2.3 parts of foaming agent, 3.1 parts of activating agent and appropriate amount of water.
4. environment-friendly light decorative insulation board according to claim 1, which is characterized in that the system of the modified longan pericarp powder
Preparation Method is as follows：
（1）Pulverizer is added after longan pericarp is air-dried to crush, is then added in agate jar, adds a diameter of 5mm
Zirconia ball longan pericarp powder is obtained with the rotating speed ball milling 5 hours of 500~600r/min after taking-up；
（2）By step（1）Gained longan pericarp powder is added in the sodium hydroxide solution that mass concentration is 16%, is heated to 45 DEG C of stirrings
It 1 hour, is subsequently placed in ultrasonic stirrer, ultrasound 15 minutes, drains after taking-up, with distillation under the conditions of supersonic frequency is 90Hz
Water washing obtains alkalization longan pericarp powder to neutrality after drying；
（3）By step（2）Gained alkalizes in longan pericarp powder addition dimethyl sulfoxide (DMSO), 45 DEG C is fully heated to after infiltration, stirring 2 is small
When after in being added dropwise to perchloric acid, acetic anhydride in 1 hour, take out, staticly settle after continuing stirring 3 hours, distilled water is used after filtering
It is 6 to wash to the pH value of filtrate, is placed in baking oven drying at 100 DEG C and obtains modified longan pericarp powder after 10 hours, wherein alkalization dragon
Eye shell powder, dimethyl sulfoxide (DMSO), perchloric acid, acetic anhydride weight ratio be 8:65:1:33.
5. environment-friendly light decorative insulation board according to claim 1, which is characterized in that the antifoaming agent be calcium carbonate,
Any one of magnesium carbonate, silicon carbide.
6. environment-friendly light decorative insulation board according to claim 1, which is characterized in that the activating agent is succinate
Sulfonic acid.
7. a kind of method preparing any one of claim 1~6 environment-friendly light decorative insulation board, which is characterized in that packet
Include following steps：
（1）By above-mentioned formula weigh cullet, building waste, closed perlite, polyethylene, iron tailings, cement, epoxy resin,
Bentonite, calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder, hair
Infusion, activating agent and water, it is spare；
（2）Discarded glass is cleaned, powder is ground into, is subsequently placed in sintering furnace and is sintered 1~2 hour, obtain sintered glass powder；
（3）By building waste removal of impurities, grind into powder, then with closed perlite, polyethylene, iron tailings, cement, bentonite,
Calcined kaolin, polyester fiber, zirconium silicate, tungsten carbide, alundum (Al2O3), glass fibre, modified longan pericarp powder mixing, set together
The grind into powder in ball mill, then ultrasonic wave be uniformly dispersed, obtain mixed-powder；
（4）Water is added into mixed-powder, it is 30%~40% to make water content in material, and epoxy resin, foaming agent and activity is added
Agent is uniformly mixed, and is subsequently placed in foaming processing 10~20 hours in foaming machine, is obtained mixed slurry；
（5）Mixed slurry is poured into mold, hot-forming, demoulding is placed in fog room and conserves to get environment-friendly light dress
Adorn heat preservation plate material.
8. preparation method according to claim 7, which is characterized in that the step（2）Middle sintering temperature be 1200~
1300℃。
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| CN109809790A (en) * | 2019-04-01 | 2019-05-28 | 浙江工业大学 | A kind of insulating brick and preparation method thereof prepared using silica hydrogel as raw material |
| CN109809789A (en) * | 2019-04-01 | 2019-05-28 | 浙江工业大学 | A method of construction wall thermal insulation clamp central layer is prepared by raw material of silica hydrogel |
| CN111499205A (en) * | 2020-04-14 | 2020-08-07 | 江西鼎盛新材料科技有限公司 | Microcrystalline foam heat-insulation and decoration integrated board sintered by lepidolite tailings at one time |
| CN111995423A (en) * | 2019-05-26 | 2020-11-27 | 广东罕王石和陶绿色建材科技有限公司 | Foamed ceramic terrazzo composite board and preparation method thereof |
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| CN109809790A (en) * | 2019-04-01 | 2019-05-28 | 浙江工业大学 | A kind of insulating brick and preparation method thereof prepared using silica hydrogel as raw material |
| CN109809789A (en) * | 2019-04-01 | 2019-05-28 | 浙江工业大学 | A method of construction wall thermal insulation clamp central layer is prepared by raw material of silica hydrogel |
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| CN111499205A (en) * | 2020-04-14 | 2020-08-07 | 江西鼎盛新材料科技有限公司 | Microcrystalline foam heat-insulation and decoration integrated board sintered by lepidolite tailings at one time |
| CN111499205B (en) * | 2020-04-14 | 2022-05-17 | 江西鼎盛新材料科技有限公司 | Microcrystalline foam heat-insulation and decoration integrated board sintered by lepidolite tailings at one time |
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