CN108308590A - A kind of edible rare sugared combinations of sweeteners low in calories - Google Patents
A kind of edible rare sugared combinations of sweeteners low in calories Download PDFInfo
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- CN108308590A CN108308590A CN201710039590.2A CN201710039590A CN108308590A CN 108308590 A CN108308590 A CN 108308590A CN 201710039590 A CN201710039590 A CN 201710039590A CN 108308590 A CN108308590 A CN 108308590A
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- trehalose
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Abstract
The present invention provides a kind of edible rare sugared combinations of sweeteners low in calories, specifically, trehalose, antierythrite, neohesperidin dihydro are looked into diketone and steviol glycoside is compounded with certain proportion, it can get the sweetener composition that homogeneity is good, heat is low, flavor is good, stability is good, and the sweetener composition of the present invention has the characteristics that pure in mouth feel, salubrious, also with low in calories, balance blood sugar, prebiotics, anti-caries, stability height and other effects.
Description
Technical field
The present invention relates to sweetener fields, in particular it relates to the rare sugared sweetener that a kind of edible is low in calories
Combination.
Background technology
Rare sugar is to exist in nature but single carbohydrates and their derivative that content is few, have extensive bioactivity and
Hypotoxicity plays an important role in fields such as food, health care and medical treatment.Because rare sugar generally has low in calories, low absorption, no
It participates in organism metabolism, balance blood sugar, cause saprodontia and other effects, substitute application of traditional carbohydrate in food, many can be solved
The health problem of today's society.
However, existing various monomer sweeteners cannot all meet peace simultaneously due to there is respective advantage and disadvantage at present
Entirely, four mouthfeel, technique, cost requirements.
And the sweetener composition provided in the market has, and homogeneity is poor, heat is high, sugariness is high, poor taste, there is bitter taste
Or the shortcomings of peculiar smell.
Therefore, there is an urgent need in the art to develop the sweet tea that a kind of homogeneity is good, heat is low, sugariness is low, flavor is good, stability is good
Taste agent composition.
Invention content
The sweet taste that the purpose of the present invention is to provide a kind of homogeneity is good, heat is low, sugariness is low, flavor is good, stability is good
Agent composition.
First aspect present invention provides a kind of sweetener composition, including following component：
Trehalose；
Antierythrite；
Neohesperidin dihydro looks into diketone；With
Steviol glycoside,
Wherein, with total restatement of the composition, the weight ratio of the trehalose and antierythrite is 0.1-80：0.5-
80, preferably, 0.5-50:1-50, more preferably, 0.8-20:5-30；The neohesperidin dihydro looks into the weight of diketone and steviol glycoside
Amount is than being 0.005-10:0.0005-4, preferably, 0.008-8:0.0008-2, more preferably, 0.001-5:0.001-1.
In another preferred example, the sweetener composition is without sucrose or containing a small amount of sucrose.
In another preferred example, in the sweetener composition, the content (wt%)≤5 of the sucrose, preferably,≤2,
More preferably ,≤1.
In another preferred example, the trehalose, the antierythrite, the neohesperidin dihydro look into diketone and stevioside
The weight ratio of glycosides is 0.1-80：0.5-80：0.005-10：0.0005-4, preferably, 0.5-50：1-50：0.008-8：
0.0008-2, more preferably, 0.8-20：5-30：0.001-5:0.001-1.
In another preferred example, with total restatement of the composition, the mass ratio of the trehalose is 5-50%, preferably
Ground, 10-40%, more preferably, 15-38%.
In another preferred example, with total restatement of the composition, the mass ratio of the antierythrite is 30-95%, compared with
Goodly, 45-90%, more preferably, 50-88%.
In another preferred example, with total restatement of the composition, the mass ratio that the neohesperidin dihydro looks into diketone is
0.01-30%, preferably, 0.05-20%, more preferably, 0.1-15%.
In another preferred example, with total restatement of the composition, the mass ratio of the steviol glycoside is 0.001-
10%, preferably, 0.005-8%, more preferably, 0.008-5%.
In another preferred example, the trehalose, the antierythrite, described with the total restatement of the sweetener composition
It is 80-100 that neohesperidin dihydro, which looks into diketone and the total content (wt%) of the steviol glycoside, preferably, 90-100, more preferably,
95-100。
In another preferred example, the composition is selected from the group：Food compositions, beverage composition for treating dental erosion, pharmaceutical composition, guarantor
Strong composition, bake class composition, dairy compositions, or combinations thereof.
Second aspect of the present invention provides a kind of product, and the product contains the sweetener group described in first aspect present invention
Close object.
In another preferred example, the product is selected from the group：Food product, beverage products, drug products, nutrition product,
Sports products, beauty product, or combinations thereof.
In another preferred example, the food product is selected from the group：Confectionary products, bread basket, bake food at confectionery products
Product, frozen milk product, meat, milk product, flavouring, snack, soup, seasoning, mixture, prepared food, baby food, diet
Type product, syrup, food covering layer, frosting, preserved fruit, tartar sauce, thick gravy, jam/jelly, or combinations thereof.
In another preferred example, the beverage products are selected from the group：Concentrate mixing drink, soda, noncarbonated beverage products,
Fruit-flavored beverage, fruit juice, tea, milk, coffee, or combinations thereof.
Third aspect present invention provides a kind of purposes of sweetener composition described in first aspect present invention, is used for (i)
Improve the homogeneity of sweetener；And/or (ii) improves the mouthfeel of sweetener.
Fourth aspect present invention provides a kind of preparation method of sweetener composition described in first aspect present invention, including step
Suddenly：
Trehalose, antierythrite, neohesperidin dihydro are looked into diketone and steviol glycoside to mix, to obtain the present invention the
Sweetener composition described in one side.
It should be understood that within the scope of the present invention, above-mentioned each technical characteristic of the invention and have in below (eg embodiment)
It can be combined with each other between each technical characteristic of body description, to form a new or preferred technical solution.As space is limited, exist
This no longer tires out one by one states.
Specific implementation mode
The present inventor's in-depth study by long-term, by largely being screened to sweetener, it has unexpectedly been found that, it uses
Trehalose, antierythrite, neohesperidin dihydro look into diketone and steviol glycoside is compounded with certain proportion, and it is good, hot to can get homogeneity
The sweetener composition that low, sugariness is low, flavor is good, stability is good is measured, and the sweetener composition of the present invention has sugariness high
In sucrose (a small amount of sweetener composition is only needed to can reach the sugariness of sucrose in actual use), pure in mouth feel, salubrious
Feature also has low in calories, balance blood sugar, prebiotics, anti-caries, stability height and other effects.On this basis, the present inventor is complete
At the present invention.
Term
As used herein, " combinations of sweeteners ", sweetener composition ", " sweet agent mixture " are used interchangeably.
Trehalose
Trehalose sugariness is the 45% of sweetness of cane sugar, also has in food applications and inhibits the flavorings such as bitter taste, fishy smell, astringent taste
Effect.
In the present invention, with total restatement of the sweetener composition, the weight ratio of the trehalose is 5-50%, compared with
Goodly, 10-40%, more preferably, 15-38%.
Antierythrite
Antierythrite is very extensive in distributed in nature, and sweet taste is pure, feels well only and without rear bitter taste, sugariness is the 70- of sucrose
80%, stability is good, crystallinity is high.Erythritol molecule after being absorbed by the body cannot be decomposed by the enzyme system in body, no
Heat is provided for body, glycometabolism is not involved in and causes change of blood sugar, is one kind that all multi-sugar alcohol sweet teas hide minimum energy in agent,
Also referred to as " zero " calorific value dispensing.In addition, antierythrite also has the biological characteristics such as tolerance is high, has no toxic side effect, it is above-mentioned
Property keeps its application field very extensive, especially in the food industry as the dilute of low calorie sweetener and high-intensity sweeteners
Agent is released, candy (including chocolate food), newborn class beverage, baked goods, soft drink etc. are widely used in.Trehalose is due to chemistry
Property stabilization, safety and stability, sweet taste are moderate, and bio-tissue can be protected in the adverse circumstances such as high temperature drying, hyperosmosis
With the vital activity of macromolecular, by people titled with the good reputation of " sugar of life ", " sugar of 21 century ".
In the present invention, with total restatement of the sweetener composition, the weight ratio of the antierythrite is 30-95%,
Preferably, 45-90%, more preferably, 50-88%.
Neohesperidin dihydro looks into diketone (NHDC)
The same neohesperidin dihydrochalcone (NHDC) with seasoning effect, feature are high (the about sucrose of sugariness
1500 times), and sweet taste is salubrious, happy, pleasant impression is lasting, can reduce people to the susceptibility of bitter taste in beverage or medicine, NHDC
When hydrolyzing in vivo, glucoside base is almost not involved in metabolism, is a kind of food additives of low energy.
In the present invention, with total restatement of the sweetener composition, the neohesperidin dihydro looks into the weight ratio of diketone
For 0.01-30%, preferably, 0.05-20%, more preferably, 0.1-15%.
Steviol glycoside
Stevioside is a kind of organic sweetener of Nantural non-toxic, and sugariness is 350-400 times of sucrose, is not joined in human body
Heat is not provided with metabolism, can replace sucrose, stevioside that also there is heat-clearing, diuresis, adjust stomach in food and medicine production
Effect of acid, also has hypertension, diabetes certain curative effect.
In the present invention, with total restatement of the sweetener composition, the weight ratio of the steviol glycoside is 0.001-
10%, preferably, 0.005-8%, more preferably, 0.008-5%.
Sweetener composition
The present invention provides a kind of sweetener compositions, including following components：Trehalose, antierythrite, neohesperidin two
Hydrogen looks into diketone and steviol glycoside.
In the preferred embodiment of the present invention, in the composition, the weight of the trehalose and antierythrite
Than for 0.1-80：0.5-80, preferably, 0.5-50:1-50, more preferably, 0.8-20:5-30；The neohesperidin dihydro looks into two
The weight ratio of ketone and steviol glycoside is 0.005-10:0.0005-4, preferably, 0.008-8:0.0008-2, more preferably, 0.001-
5:0.001-1。
In the preferred embodiment of the present invention, the trehalose, the antierythrite, the neohesperidin dihydro
The weight ratio for looking into diketone and steviol glycoside is 0.1-80：0.5-80：0.005-10：0.0005-4, preferably, 0.5-50：1-50：
0.008-8：0.0008-2, more preferably, 0.8-20：5-30：0.001-5:0.001-1.
In a preferred embodiment, the trehalose, the antierythrite, the neohesperidin dihydro look into diketone and sweet tea
The weight ratio of synanthrin glycosides is 1-10：8-18：0.03—3：0.002-0.4.
In a preferred embodiment, with the total restatement of the sweetener composition, the trehalose, the antierythrite,
It is 80-100 that the neohesperidin dihydro, which looks into diketone and the total content (wt%) of the steviol glycoside, preferably, 90-100, more preferably
Ground, 95-100.
In a preferred embodiment, the sweetener composition is free of sucrose or containing a small amount of sucrose, and described
In sweetener composition, the content (wt%)≤5 of the sucrose, preferably,≤2, more preferably ,≤1.
The trehalose, the antierythrite, the neohesperidin dihydro are looked into diketone with the steviol glycoside according to one
Certainty ratio is compounded, and the sweet taste that sugariness is higher than relatively lower sucrose, sugariness, pure in mouth feel, the salubrious present invention can be obtained
Agent composition, in addition, the sweetener composition of the present invention also has low in calories, balance blood sugar, prebiotics, anti-caries, stability
Height and other effects.
Homogeneity
For different sweeteners because of granular size difference, the ratio regular meeting added is different, if directly being mixed, the sweet tea of acquisition
Each component in taste agent composition is difficult full and uniform mixing, very poor so as to cause homogeneity.
In the present invention, the trehalose, the antierythrite, the neohesperidin dihydro are looked into diketone and the stevia rebaudianum
Glucosides is compounded according to a certain percentage, and each component in obtained sweetener composition has stable and uniform ratio.
Main advantages of the present invention include：
(1) by the trehalose, the antierythrite, the neohesperidin dihydro look into diketone and the steviol glycoside according to
Certain proportion is compounded, and the sweet tea that sugariness is higher than relatively lower sucrose, sugariness, pure in mouth feel, the salubrious present invention can be obtained
Taste agent composition, in addition, the sweetener composition of the present invention also has low in calories, balance blood sugar, prebiotics, anti-caries, stabilization
Property height and other effects.
(2) sweetener composition of the invention is with homogeneity is good, heat is low, sugariness is relatively lower, flavor is good, stability
The features such as good.
With reference to specific embodiment, the further old present invention in detail.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.The experimental method of detailed conditions is not specified in the following example, usually according to conventional strip
Part such as Sambrook et al., molecular cloning：Laboratory manual (New York:Cold Spring Harbor Laboratory
Press, 1989) condition described in, or according to the normal condition proposed by manufacturer.Unless otherwise stated, otherwise percentage and
Number is calculated by weight.
Experiment material used in following embodiment and reagent can obtain unless otherwise instructed from commercially available channel.
Universal method
The present invention provides a kind of compound schemes of low calorie sweetener composition, specifically include four kinds of sweeteners, sugariness
It it is 0.5-10 times of sucrose, specific embodiment is as follows：
1, four kinds of sweeteners are weighed by mass ratio shown in table 1
Table 1
| Ingredient | Mass ratio (wt%) |
| Trehalose | 15%-35% |
| Antierythrite | 63%-84% |
| Neohesperidin dihydrochalcone | 0.2%-10% |
| Stevioside | 0.01%-1% |
2, add water to be completely dissolved at 40-50 DEG C combinations of sweeteners, then carry out 40-50 rotary evaporations, be concentrated into precipitation
Solid is transferred in vacuum drying chamber until solid over dry by a large amount of solids after further revolving removes residual moisture, with grinding
Alms bowl grinds solid into powdered, the uniform combinations of sweeteners excessively more than 80 mesh of sieve acquisition.
3, chromatography is carried out to the homogeneity of above-mentioned gained combinations of sweeteners.
4, the sugariness of combinations of sweeteners is measured；The assay method of sugariness is in following embodiment, using sucrose as sugariness 1
Standard, prepares the aqueous sucrose solution of 10% mass concentration, then compound sweetener is formulated as to different concentration gradients, forms five people
Group carries out tasting assessment sugariness, obtains and 10% sweetness of cane sugar sweetener concentration the most similar, sugariness formula：
Sugariness=10%/formula sweetener concentration
5, the combinations of sweeteners mixed well is packed.
Efficient liquid phase chromatographic analysis condition
Trehalose and antierythrite use RID detectors, Shimadzu high performance liquid chromatograph SHIMADZU LC-20A；Chromatography
Column：Waters Sugar-Pak I, 6.5 × 300mm；Mobile phase：Ultra-pure water；Flow velocity：0.6mL/min；Column temperature：85℃；Sample introduction
Measure 40 μ L, isocratic elution time：25min.
Neohesperidin dihydrochalcone (NHDC) and stevioside use PDA detectors, Shimadzu high performance liquid chromatograph
SHIMADZU LC-20A；Chromatographic column：6L Sciences, C18 columns, 5um, 4.6 × 250mm；Mobile phase：Acetonitrile/KH2PO4Buffering
Liquid；Flow velocity：1mL/min；Column temperature：40℃；20 μ L of sample size, gradient elution time：30min.
Embodiment 1
1, it presses 2 mass ratio of table and weighs 5g sweet agent mixtures
Table 2
| Ingredient | Mass ratio (wt%) |
| Trehalose | 25% |
| Antierythrite | 74.25% |
| Neohesperidin dihydrochalcone | 0.50% |
| Stevioside | 0.25% |
2, prepared by combinations of sweeteners A：Combinations of sweeteners plus 150mL water are completely dissolved at 40-50 DEG C, then carry out 50 DEG C
Rotary evaporation is concentrated into and a large amount of solids is precipitated, and further after revolving removing residual moisture, solid is transferred in vacuum drying chamber
Until solid over dry, with mortar grinder solid at powdered, the uniform combinations of sweeteners A excessively more than 80 mesh of sieve acquisition.
3, chromatography is carried out to the homogeneity of above-mentioned gained combinations of sweeteners A
Weighing five parts of above-mentioned combinations of sweeteners A progress liquid phase analysis at random, it is formed, the combinations of sweeteners that this method obtains
With preferable homogeneity.The results are shown in Table 3.
Table 3
4, the sugariness of combinations of sweeteners A, about 2.2 times of sweetness of cane sugar are measured；
5, the combinations of sweeteners mixed well is packed.
Embodiment 2
1, it presses mass ratio shown in table 4 and weighs 5g sweet agent mixtures
Table 4
| Ingredient | Mass ratio (wt%) |
| Trehalose | 25% |
| Antierythrite | 74.25% |
| Neohesperidin dihydrochalcone | 0.25% |
| Stevioside | 0.50% |
2, prepared by combinations of sweeteners B：It is identical as the preparation method of combinations of sweeteners A.
3, chromatography is carried out to the homogeneity of above-mentioned gained combinations of sweeteners B
Weighing five parts of above-mentioned combinations of sweeteners B progress liquid phase analysis at random, it is formed, the combinations of sweeteners that this method obtains
With preferable homogeneity.The results are shown in Table 5.
Table 5
4, the sugariness of combinations of sweeteners B, about 1.75 times of sweetness of cane sugar are measured；
5, the combinations of sweeteners mixed well is packed.
It can be seen from the results above that compounding the sweetener composition of the obtained present invention with excellent with certain proportion
Homogeneity.
Embodiment 3
10 volunteers are chosen, the mouthfeel of sweetener composition of the present invention is evaluated with scoring mechanism, wherein 3-4 points are mouthfeel
Very big with sucrose difference, 5-6 points a little close with sucrose for mouthfeel, 7-8 points higher for mouthfeel and sucrose degree of closeness, 9-10 points
It is very close with sucrose for mouthfeel, almost without difference.The case where score value shown in table 6 is gives a mark for 10 people is calculated
The average mark gone out.
The results are shown in Table 6.
Table 6
| Trehalose | 7.5 point |
| Antierythrite | 7.7 point |
| Neohesperidin dihydrochalcone | 4.8 point |
| Stevioside | 5.6 point |
| The sweetener composition of embodiment 1 and embodiment 2 | 8.5 point |
| Sucrose | 10 points |
As can be seen from Table 6, sweetener composition of the invention has mouthfeel close to sucrose, pure in mouth feel, salubrious spy
Point.
Therefore, from the foregoing, the sweetness ratio sucrose of sweetener composition of the invention is high, uses in actual use very
Few dosage is that can reach the sugariness of sucrose, and the sweetener composition mouthfeel of the present invention is close to sucrose, pure in mouth feel, clear
It is refreshing, also there is excellent homogeneity.
Comparative example
1, it presses mass ratio shown in table 7 and weighs 5g sweet agent mixtures
Table 7
| Ingredient | Mass ratio (wt%) |
| Trehalose | 25% |
| Maltitol | 74.25% |
| Neohesperidin dihydrochalcone | 0.25% |
| Stevioside | 0.50% |
2, prepared by combinations of sweeteners C：Identical as the preparation method of combinations of sweeteners A, complex composition obtained is not easy powder
Broken, the easy moisture absorption, particle is relatively rough.
3, combinations of sweeteners C sugarinesses, about 2 times of sweetness of cane sugar are measured.
The result shows that with maltitol replace antierythrite, and with trehalose, neohesperidin dihydrochalcone
, steviol glycoside compounding, obtained sweetener composition grained matte, homogeneity is poor, and also have the easy moisture absorption,
The shortcomings that being not easy to crush.
Therefore, the above results fully show that sweetener composition of the invention not only has significantly excellent homogeneity, also
With extraordinary mouthfeel.
All references mentioned in the present invention is incorporated herein by reference, independent just as each document
It is incorporated as with reference to such.In addition, it should also be understood that, after reading the above teachings of the present invention, those skilled in the art can
To be made various changes or modifications to the present invention, such equivalent forms equally fall within model defined by the application the appended claims
It encloses.
Claims (10)
1. a kind of sweetener composition, which is characterized in that including following component：
Trehalose；
Antierythrite；
Neohesperidin dihydro looks into diketone；With
Steviol glycoside,
Wherein, with total restatement of the composition, the weight ratio of the trehalose and the antierythrite is 0.1-80：0.5-
80；It is 0.005-10 that the neohesperidin dihydro, which looks into diketone and the weight ratio of the steviol glycoside,:0.0005-4.
2. sweetener composition as described in claim 1, which is characterized in that the trehalose, the antierythrite, described new
It is 0.1-80 that aurantiamarin dihydro, which looks into diketone and the weight ratio of the steviol glycoside,：0.5-80：0.005-10：0.0005-4, preferably
Ground, 0.5-50：1-50：0.008-8：0.0008-2, more preferably, 0.8-20：5-30：0.001-5:0.001-1.
3. sweetener composition as described in claim 1, which is characterized in that with total restatement of the composition, the seaweed
The mass ratio of sugar is 5-50%, preferably, 10-40%, more preferably, 15-38%.
4. sweetener composition as described in claim 1, which is characterized in that with total restatement of the composition, the red moss
The mass ratio of sugar alcohol is 30-95%, preferably, 45-90%, more preferably, 50-88%.
5. sweetener composition as described in claim 1, which is characterized in that with total restatement of the composition, the new orange
The mass ratio that skin glycosides dihydro looks into diketone is 0.01-30%, preferably, 0.05-20%, more preferably, 0.1-15%.
6. sweetener composition as described in claim 1, which is characterized in that with total restatement of the composition, the stevia rebaudianum
The mass ratio of glucosides is 0.001-10%, preferably, 0.005-8%, more preferably, 0.008-5%.
7. sweetener composition as described in claim 1, which is characterized in that the composition is selected from the group：Food compositions,
Beverage composition for treating dental erosion, pharmaceutical composition, health composition, bake class composition, dairy compositions, or combinations thereof.
8. a kind of product, which is characterized in that the product contains sweetener composition described in claim 1.
9. the purposes of sweetener composition described in a kind of claim 1, which is characterized in that improve the uniform of sweetener for (i)
Property；And/or (ii) improves the mouthfeel of sweetener.
10. the preparation method of sweetener composition described in a kind of claim 1, which is characterized in that including step：
Trehalose, antierythrite, neohesperidin dihydro are looked into diketone and steviol glycoside mixes, to obtain described in claim 1
Sweetener composition.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109329864A (en) * | 2018-10-31 | 2019-02-15 | 郑书旺 | A kind of composite sweetener and preparation method |
| CN109393495A (en) * | 2018-09-30 | 2019-03-01 | 大连医诺生物股份有限公司 | A kind of taste masking amino acid granular and preparation method thereof |
| CN110200256A (en) * | 2019-06-28 | 2019-09-06 | 山东奔月生物科技股份有限公司 | The preparation method of new-type compound sweetener |
| IT202000029399A1 (en) * | 2020-12-02 | 2022-06-02 | Daniela Morandi | SWEETENER COMPOSITION FOR FOOD USE, PARTICULARLY FOR PASTRY AND ICE CREAM PRODUCTS |
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2017
- 2017-01-18 CN CN201710039590.2A patent/CN108308590A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109393495A (en) * | 2018-09-30 | 2019-03-01 | 大连医诺生物股份有限公司 | A kind of taste masking amino acid granular and preparation method thereof |
| CN109329864A (en) * | 2018-10-31 | 2019-02-15 | 郑书旺 | A kind of composite sweetener and preparation method |
| CN110200256A (en) * | 2019-06-28 | 2019-09-06 | 山东奔月生物科技股份有限公司 | The preparation method of new-type compound sweetener |
| IT202000029399A1 (en) * | 2020-12-02 | 2022-06-02 | Daniela Morandi | SWEETENER COMPOSITION FOR FOOD USE, PARTICULARLY FOR PASTRY AND ICE CREAM PRODUCTS |
| WO2022118209A1 (en) * | 2020-12-02 | 2022-06-09 | Morandi Daniela | Sweetener composition for food use, particularly for bakery and ice cream products |
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Application publication date: 20180724 |