CN108300813A - A method of delay high fructose syrup from crystallizing - Google Patents
A method of delay high fructose syrup from crystallizing Download PDFInfo
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- CN108300813A CN108300813A CN201810008889.6A CN201810008889A CN108300813A CN 108300813 A CN108300813 A CN 108300813A CN 201810008889 A CN201810008889 A CN 201810008889A CN 108300813 A CN108300813 A CN 108300813A
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- fructose syrup
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
- C13K1/10—Crystallisation
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K1/00—Glucose; Glucose-containing syrups
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
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- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
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- General Health & Medical Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Jellies, Jams, And Syrups (AREA)
- Saccharide Compounds (AREA)
Abstract
The invention belongs to carbohydrate storing technology fields, and in particular to a method of delay high fructose syrup from crystallizing.The method of the delay high fructose syrup from crystallizing of the present invention, which is characterized in that finished product fructose syrup is heated, then the processing that cools down.The beneficial effects of the present invention are, the method for using the present invention, certain temperature is first heated to finished product fructose syrup, it is cooled to specific temperature again, mainly according to fructose syrup the characteristics of designed technique, make fructose syrup through heating and cooling processing after, increase its solubility, it effectively prevents fructose syrup from being crystallized under low-temperature condition, uses and sell to influence it.
Description
Technical field
The invention belongs to carbohydrate storing technology fields, and in particular to a method of delay high fructose syrup from crystallizing.
Background technology
Fructose syrup is easy to crystallization at low temperature, for example under conditions of 3-4 DEG C, fructose syrup will soon crystallize into
White particle results in whole bucket to be frozen into solid-like when serious, can not use.Its reason is mainly certain in fructose syrup
Solubility reduces a little carbohydrates at low temperature, is precipitated to crystallize, and influences its sale or normal use.
In order to solve the above technical problems, patent document or patent application document disclose the following method：
CN1974790A is disclosed, and the maltodextrin of DE values 16-18% is added into F42 fructose syrups as anti-crystal
Matter, to delaying high fructose syrup from crystallizing effect apparent, and crystallization degree is also substantially reduced, the patent No..But it is added to fructose syrup
In maltodextrin certain diluting effect can be played to the monosaccharide in syrup, make in product the total amount of fructose and glucose up to not
To requirement, the examination experiment of syrup iodine is unqualified, cannot be satisfied requirement of the application client to saccharic composition, reduces target level of product quality,
Increase enterprise's production cost.
104651540 A of CN disclose a kind of method of anti-F55 high fructose syrup from crystallizing, it is characterised in that：In F55 fruits Portugal
In the production line of syrup, after third time refining step, installation one turns brilliant tank, makes from third time refining step through third set
F55 fructose syrups after ion exchange system is refined 80 DEG C of constant temperature in the brilliant tank of this turn are kept for 20 minutes, later the F55 high fructose corns
Slurry enters third time evaporization process.
CN1974790A, which is disclosed, is added the maltodextrin of DE values 16%-18% as anti-crystal in F42 fructose syrups
Matter, although to delaying high fructose syrup from crystallizing effect apparent, and crystallization degree is also substantially reduced；But first, add in product
Add maltodextrin to reduce the purity of fructose syrup, influences product quality；Second is that crystallization degree mitigates but not from crystallization source
Thoroughly prevent the generation of crystalline polamer on head.
The method that 104651540 A of CN disclose F55 fructose syrups resistive connection crystalline substance is the installation after third time refining step
One turns brilliant tank, makes from the F55 fructose syrups in third time refining step after third set ion exchange system is refined in this turn
80 DEG C of constant temperature are kept for 20 minutes in brilliant tank, and the F55 fructose syrups enter third time evaporization process later.But the disadvantages of this method is
Although 80 DEG C of constant temperature are kept for 20 minutes in turning brilliant tank, the F55 fructose syrups enter third time evaporization process, temperature of charge later
80 DEG C or so are remained at, products molecule structure in material is not had an impact, therefore still will produce crystalline polamer；Second is that
This method does not verify F42 fructose syrups.
Invention content
For above-mentioned defect, the present invention provides a kind of methods that can postpone high fructose syrup from crystallizing, to solve high fructose corn
Slurry is easy the problem of crystallization is precipitated in a short time, and method of the invention is mainly by cooling down again to the heating of finished product fructose syrup
Mode, by above-mentioned processing, can make fructose syrup from initial after interior crystallization in 7-8 days is deferred to 1 month come what is realized
Crystallization, postpones its crystallization effect highly significant.
The method that the present invention postpones high fructose syrup from crystallizing, inventive concept be to be heated to finished product fructose syrup, then cool down
Processing.The temperature of heating is 50-80 DEG C, is cooled to 12-45 DEG C；Preferably, the temperature of heating is 50-70 DEG C, is cooled to 26-35
℃。
The method of the present invention is especially notable in the effect to postponing F42 high fructose syrup from crystallizing.
The mode of heating is heated using plate heat exchanger, is cooled processing to fructose syrup using condenser.
As an improvement of the present invention, it before heating to fructose syrup, first filters.
In the step of filtering：It is filtered using 0.45um filter sticks.
It is aseptic subpackaged to fructose syrup after cooling.
It is transported to glucose slurry finished pot after fructose syrup production, fructose syrup finished product is delivered to by filtering by pump 2
It is filtered in machine, filtering is carried out using 0.45 μm of filter stick, is then heated again to the fructose syrup by filtering by plate heat exchanger
The fructose syrup after heating is condensed to 12-45 DEG C to 50-80 DEG C, then by condenser, is finally existed to condensed fructose syrup
Filling or packing under aseptic condition；Preferably, 50-70 DEG C is heated to the fructose syrup by filtering by plate heat exchanger, then
The fructose syrup after heating is condensed to 26-35 DEG C by condenser, finally condensed fructose syrup is aseptically filled
Dress or packing；.
The system of delay high fructose syrup from crystallizing provided by the present invention, including：The high fructose corn connect is sequentially connected by pipeline
Starch finished pot, plate heat exchanger, condenser；Plate heat exchanger is connected with steam-heated pipe line.
Preferably, filter is provided between fructose syrup finished pot, plate heat exchanger, filter is preferably
BNA045F03BA。
There is pump between fructose syrup finished pot and filter, for conveying fructose syrup.
The beneficial effects of the present invention are the method for using the present invention is first heated to finished product fructose syrup certain
Temperature, then be cooled to specific temperature, mainly according to fructose syrup the characteristics of designed technique, make fructose syrup by plus
After heat and cooling processing, increases its solubility, effectively prevent fructose syrup from being crystallized under low-temperature condition, to influence its use
And sale.
Description of the drawings
Fig. 1 is the structural schematic diagram of the system of the present invention；
Fig. 2-Figure 17 be respectively method treated fructose syrup by the present invention in condition below (5 DEG C, 20 days),
(5 DEG C, 20 days), (10 DEG C, 20 days), (10 DEG C, 40 days), (10 DEG C, 20 days), (10 DEG C, 40 days), (10 DEG C, 20 days), (5 DEG C,
40 days), (5 DEG C, 20 days), (10 DEG C, 40 days), (10 DEG C, 20 days), (5 DEG C, 40 days), (5 DEG C, 20 days), (5 DEG C, 40 days), (5
DEG C, 20 days), (10 DEG C, 40 days) storage preserve after chromatograms；
In Fig. 1,1- fructose syrup finished pots, 2- is pumped, 3- filters, 4- plate heat exchangers, 5- condensers, and 6-steam add
Hot tank.
Specific implementation mode
The present invention is further described with reference to the accompanying drawings and detailed description, so as to the technology of this field
Personnel know more about the present invention, but do not limit the present invention with this.
Embodiment 1
Postpone the system of F42 high fructose syrup from crystallizing, including：Be sequentially connected by pipeline the fructose syrup finished pot 1 connect,
BNA045F03BA filters 3, plate heat exchanger 4, condenser 5；Plate heat exchanger is connected with steam heating tank 6, steam heating
It is the steam that plate heat exchanger 4 provides to have steam-heated pipe line, steam heating tank between tank 6 and plate heat exchanger 4, passes through steam
Steam is delivered to plate heat exchanger 4 to be heated to the fructose syrup passed through in plate heat exchanger 4 by heating pipe；In high fructose corn
Have material to be delivered to the pump 2 in filter 3 between slurry finished pot 1 and filter 3.
It is transported to glucose slurry finished pot 1 after fructose syrup production, fructose syrup finished product is delivered to by filtering by pump 2
It is filtered in machine 3,60 DEG C or so then is heated to the fructose syrup by filtering by plate heat exchanger 4 again, then will by condenser 5
Fructose syrup after heating is condensed to 35 DEG C, finally aseptically filling to condensed fructose syrup or packing.
It is 300-350L/min that fructose syrup, which is delivered to the flow velocity in filter,；It is sent immediately after being heated to 60 DEG C or so
Into being condensed in condenser 5.
In contrast to the method for storing fructose syrup before improving directly in fructose syrup finished pot, the two is compared as follows：
(improve before with improve after using same fructose syrup)；
| Temperature | Before improvement (crystallization time/day) | Embodiment 1 (crystallization time/day) |
| 5℃ | 7 days | 60 |
| 10℃ | 12 days | 75 |
| 15℃ | 17 days | 90 |
Note：Crystallization time refers to by how many days starting to crystallize.
For example, before the present invention improves, store at 5 DEG C, same fructose syrup only passes through 7 days and begins to tie
It is brilliant；It is stored at 10 DEG C, began to crystallize by 12 days；It is stored at 15 DEG C, began to crystallize by 17 days；As it can be seen that without
The fructose syrup for crossing processing is easy for crystallizing within the very short time limit；
And after method using the present invention handles same a collection of fructose syrup, it stores at 5 DEG C, fructose syrup exists
Storage just starts to crystallize after 60 days；It is stored at 10 DEG C, starts to crystallize by 75 talentes；It is stored at 15 DEG C, by 90 talentes
Start to crystallize；Before improvement, method of the invention greatly delays the time of high fructose syrup from crystallizing, and effect is very
It is notable.
The method and apparatus of embodiment of learning from else's experience 1 treated fructose syrup, does experiment below：
Take the fructose syrup of different volumes, number 1,2,3,4；
Set respectively it is below under the conditions of place, the result observed is as follows：
Note：Number 1 is sampling 50ml, observes the result of gained；Number 2 is sampling 200ml, observes the result of gained；It compiles
Numbers 3 be sampling 500ml, observes the result of gained；Number 4 is sampling 1L, observes the result of gained；
Comparative example 1
It is transported to fructose syrup finished pot after fructose syrup production, then was delivered to fructose syrup finished product by pumping
It is filtered in filter, 70 DEG C then is heated to the fructose syrup by filtering by plate heat exchanger again, cooled to room temperature, most
Aseptically filling to condensed fructose syrup afterwards or packing.
Comparative example 2
It is transported to glucose slurry finished pot after fructose syrup production, fructose syrup finished product is delivered to filter by pumping
Then middle filtering is heated to 90 DEG C by plate heat exchanger to the fructose syrup by filtering again, then will be after heating by condenser
Fructose syrup is condensed to 35 DEG C, finally aseptically filling to condensed fructose syrup or packing.
Comparative example 3
It is transported to glucose slurry finished pot after fructose syrup production, fructose syrup finished product is delivered to filter by pumping
Then middle filtering is heated to 80 DEG C by plate heat exchanger to the fructose syrup by filtering again, then will be after heating by condenser
Fructose syrup is condensed to 35 DEG C, finally aseptically filling to condensed fructose syrup or packing.
Comparative example 4
It is transported to glucose slurry finished pot after fructose syrup production, fructose syrup finished product is delivered to board-like change by pumping
Hot device is heated to 45 DEG C to the fructose syrup by filtering, then is condensed the fructose syrup after heating to 35 DEG C, most by condenser
Aseptically filling to condensed fructose syrup afterwards or packing.
Comparative example 5
It is transported to glucose slurry finished pot after fructose syrup production, fructose syrup finished product is delivered to filter by pumping
Then middle filtering is heated to 60 DEG C by plate heat exchanger to the fructose syrup by filtering again, then will be after heating by condenser
Fructose syrup is condensed to 10 DEG C, finally aseptically filling to condensed fructose syrup or packing.
It can be seen that in comparative example 1 from the result in above table, natural cooling, although fructose syrup can also be made to reach
To the purpose of delayed crystallisation, but the time of natural cooling its consumption is long, is unfavorable for industrialized production；
In comparative example 2, fructose syrup is heated to 90 DEG C, then be cooled to 35 DEG C, although can also reach makes fructose syrup
Achieve the purpose that delayed crystallisation, but after fructose syrup is heated to excessively high temperature, darkening for syrup can be made, influence it
Appearance luster, the reason is that fructose syrup is heat-sensitive substance, it is more sensitive to temperature；And fructose syrup can under excessive temperature
It can be gelatinized and generate slightly bitter taste, influence its mouthfeel；Increase in addition, being heated to excessively high temperature its energy consumption, cost is big
It is big to improve, also it is unfavorable for industrialized production；
Equally, it also will appear the defects of comparative example 2 in comparative example 3；
In comparative example 4, since the temperature of heating is relatively low, in actual treatment, it is possible to it will appear the phenomenon that slightly crystallizing,
Effect is not heated to 50-70 DEG C good as provided by the present invention；
In comparative example 5, when cooling, its temperature is down to 10 DEG C, cooling is relatively low, although can also reach the present invention's
Purpose, but its energy consumption is high, should not use in actual production.
Table 1- tables 16 are after the glucose syrup after method processing using the present invention stores under the following conditions respectively
By the chromatogram of detection；
Table 1：(5 DEG C, 20 days)；Table 2 (5 DEG C, 20 days)；Table 3 (10 DEG C, 20 days)；Table 4 (10 DEG C, 40 days)；Table 5 (10 DEG C,
20 days)；Table 6 (10 DEG C, 40 days)；Table 7 (10 DEG C, 20 days)；Table 8 (5 DEG C, 40 days)；Table 9 (5 DEG C, 20 days)；Table 10 (10 DEG C, 40
It)；Table 11 (10 DEG C, 20 days)；Table 12 (5 DEG C, 40 days)；Table 13 (5 DEG C, 20 days)；Table 14 (5 DEG C, 40 days)；Table 15 (5 DEG C, 20
It)；Table 16 (10 DEG C, 40 days)；
Table 1
Table 2
Table 3
Table 4
Table 5
Table 6
Table 7
Table 8
Table 9
Table 10
Table 11
Table 12
Table 13
Table 14
Table 15
Table 16
From in above table data and in conjunction with collection of illustrative plates can be seen that method through the invention treated fructose syrup
Longer time can be preserved in low temperature without crystallizing, and what effective solution fructose syrup was easy that crystallization is precipitated in a short time asks
Topic.
Embodiment 2
In embodiment 2 using with 1 identical equipment of embodiment, fructose syrup is handled；
It is transported to glucose slurry finished pot 1 after fructose syrup production, fructose syrup finished product is delivered to by filtering by pump 2
It is filtered in machine 3,55 DEG C or so then is heated to the fructose syrup by filtering by plate heat exchanger 4 again, then will by condenser 5
Fructose syrup after heating is condensed to 26 DEG C, finally aseptically filling to condensed fructose syrup or packing.
It is 300-350L/min that fructose syrup, which is delivered to the flow velocity in filter,；It is sent immediately after being heated to 55 DEG C or so
Into being condensed in condenser 5.
The method and apparatus of embodiment of learning from else's experience 2 treated fructose syrup, does experiment below：
Take the fructose syrup of different volumes, number 1,2,3,4；
Set respectively it is below under the conditions of place, the result observed is as follows：
| Number | 10 DEG C, 30 days | 10 DEG C, 30 days | 5 DEG C, 30 days | 5 DEG C, 30 days |
| 1 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
| 2 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
| 3 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
| 4 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
Note：Number 1 is sampling 50ml, observes the result of gained；Number 2 is sampling 200ml, observes the result of gained；It compiles
Numbers 3 be sampling 500ml, observes the result of gained；Number 4 is sampling 1L, observes the result of gained.
Embodiment 3
In embodiment 3 using with 1 identical equipment of embodiment, fructose syrup is handled；
It is transported to glucose slurry finished pot 1 after fructose syrup production, fructose syrup finished product is delivered to by filtering by pump 2
It is filtered in machine 3,50 DEG C or so then is heated to the fructose syrup by filtering by plate heat exchanger 4 again, then will by condenser 5
Fructose syrup after heating is condensed to 12 DEG C or so, finally aseptically filling to condensed fructose syrup or packing.
It is 300-350L/min that fructose syrup, which is delivered to the flow velocity in filter,；It is sent immediately after being heated to 50 DEG C or so
Into being condensed in condenser 5.
The method and apparatus of embodiment of learning from else's experience 3 treated fructose syrup, does experiment below：
Take the fructose syrup of different volumes, number 1,2,3,4；
Set respectively it is below under the conditions of place, the result observed is as follows：
Note：Number 1 is sampling 50ml, observes the result of gained；Number 2 is sampling 200ml, observes the result of gained；It compiles
Numbers 3 be sampling 500ml, observes the result of gained；Number 4 is sampling 1L, observes the result of gained.
Embodiment 4
In embodiment 4 using with 1 identical equipment of embodiment, fructose syrup is handled；
It is transported to glucose slurry finished pot 1 after fructose syrup production, fructose syrup finished product is delivered to by filtering by pump 2
It is filtered in machine 3,70 DEG C or so then is heated to the fructose syrup by filtering by plate heat exchanger 4 again, then will by condenser 5
Fructose syrup after heating is condensed to 45 DEG C or so, finally aseptically filling to condensed fructose syrup or packing.
It is 330L/min or so that fructose syrup, which is delivered to the flow velocity in filter,；It is sent immediately after being heated to 70 DEG C or so
Into being condensed in condenser 5.
The method and apparatus of embodiment of learning from else's experience 4 treated fructose syrup, does experiment below：
Take the fructose syrup of different volumes, number 1,2,3,4；
Set respectively it is below under the conditions of place, the result observed is as follows：
Note：Number 1 is sampling 50ml, observes the result of gained；Number 2 is sampling 200ml, observes the result of gained；It compiles
Numbers 3 be sampling 500ml, observes the result of gained；Number 4 is sampling 1L, observes the result of gained.
Embodiment 5
In embodiment 5 using with 1 identical equipment of embodiment, fructose syrup is handled；
It is transported to glucose slurry finished pot 1 after fructose syrup production, fructose syrup finished product is delivered to by filtering by pump 2
It is filtered in machine 3,65 DEG C or so then is heated to the fructose syrup by filtering by plate heat exchanger 4 again, then will by condenser 5
Fructose syrup after heating is condensed to 33 DEG C or so, finally aseptically filling to condensed fructose syrup or packing.
It is 350L/min or so that fructose syrup, which is delivered to the flow velocity in filter,；It is sent immediately after being heated to 65 DEG C or so
Into being condensed in condenser 5.
The method and apparatus of embodiment of learning from else's experience 5 treated fructose syrup, does experiment below：
Take the fructose syrup of different volumes, number 1,2,3,4；
Set respectively it is below under the conditions of place, the result observed is as follows：
| Number | 10 DEG C, 30 days | 10 DEG C, 30 days | 5 DEG C, 30 days | 5 DEG C, 30 days |
| 1 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
| 2 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
| 3 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
| 4 | Nodeless mesh | Nodeless mesh | Nodeless mesh | Nodeless mesh |
Note：Number 1 is sampling 50ml, observes the result of gained；Number 2 is sampling 200ml, observes the result of gained；It compiles
Numbers 3 be sampling 500ml, observes the result of gained；Number 4 is sampling 1L, observes the result of gained.
It can be seen that from the experiment in embodiment 2- embodiments when fructose syrup is heated to 50-70 DEG C, then by condenser
Fructose syrup after heating is condensed to 12-45 DEG C, finally aseptically filling to condensed fructose syrup or packing,
Its shelf life pass through 20 days after, will not crystallize, and the present inventor it was proved that, the fructose syrup even having
Storage will not crystallize after 40 days.Therefore, method of the invention is relative to the mode directly stored before improving, greatly
Delay the crystallization time of product.
Claims (10)
1. a kind of method of delay high fructose syrup from crystallizing, which is characterized in that heated to finished product fructose syrup, then the place that cools
Reason.
2. a kind of method of delay high fructose syrup from crystallizing as described in claim 1, which is characterized in that fructose syrup is F42 fruits
Glucose is starched.
3. a kind of method of delay high fructose syrup from crystallizing as described in claim 1, which is characterized in that the temperature of heating is 50-
80 DEG C, it is cooled to 12-45 DEG C；Preferably, the temperature of heating is 50-70 DEG C, is cooled to 26-35 DEG C.
4. a kind of method of delay high fructose syrup from crystallizing as described in claim 1, which is characterized in that the mode of heating uses plate
Formula heat exchanger heats, and is cooled processing to fructose syrup using condenser.
5. a kind of method of delay high fructose syrup from crystallizing as described in claim 1, which is characterized in that heated to fructose syrup
Before processing, first filter.
6. a kind of method of delay high fructose syrup from crystallizing as claimed in claim 5, which is characterized in that filtering uses 0.45 μm
Filter stick, it is aseptic subpackaged to fructose syrup after cooling.
7. a kind of method of delay high fructose syrup from crystallizing as described in claim 1, includes the following steps：
Glucose slurry finished pot is transported to after fructose syrup production（1）, pass through pump（2）Fructose syrup finished product is delivered to filtering
Machine（3）Middle filtering, then again by plate heat exchanger（4）50-80 DEG C is heated to the fructose syrup by filtering, then by condenser
（5）Fructose syrup after heating is condensed to 12-45 DEG C, it is finally aseptically filling to condensed fructose syrup or point
Dress；Preferably, the fructose syrup of filtering is heated to 50-70 DEG C, and the fructose syrup after heating is condensed to 26-35 DEG C.
8. a kind of method of delay high fructose syrup from crystallizing as described in claim 1, includes the following steps：
Glucose slurry finished pot is transported to after fructose syrup production（1）, pass through pump（2）Fructose syrup finished product is delivered to filtering
Machine（3）Middle filtering, filtering is carried out using 0.45 μm of filter stick, then again by plate heat exchanger（4）To the high fructose corn by filtering
Slurry is heated to 50-80 DEG C, then by condenser（5）Fructose syrup after heating is condensed to 12-45 DEG C, finally to condensed fruit
Glucose slurry is aseptically filling or dispenses.
9. a kind of system of delay high fructose syrup from crystallizing, including：The fructose syrup finished pot connect is sequentially connected by pipeline（1）、
Plate heat exchanger（4）, condenser（5）；Plate heat exchanger（4）It is connected with steam heating tank by pipeline（6）.
10. a kind of system of delay high fructose syrup from crystallizing as claimed in claim 8, which is characterized in that fructose syrup finished pot,
Plate heat exchanger（4）Between have filter（3）.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810008889.6A CN108300813A (en) | 2018-01-04 | 2018-01-04 | A method of delay high fructose syrup from crystallizing |
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| CN201810008889.6A CN108300813A (en) | 2018-01-04 | 2018-01-04 | A method of delay high fructose syrup from crystallizing |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110551776A (en) * | 2019-10-10 | 2019-12-10 | 中粮融氏生物科技有限公司 | anti-crystallization fructose-glucose syrup and preparation method thereof |
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| GB2105337A (en) * | 1981-08-26 | 1983-03-23 | Hydrocarbon Research Inc | Process for making l-sugars and d-fructose |
| CN1974790A (en) * | 2006-12-27 | 2007-06-06 | 王德友 | Method of preventing high fructose syrup from crystallizing |
| CN104651540A (en) * | 2014-12-31 | 2015-05-27 | 吉林中粮生化有限公司 | Crystallization resisting method for F55 high fructose corn syrup |
| CN107475322A (en) * | 2017-07-25 | 2017-12-15 | 安徽万德生物科技有限公司 | A kind of technique for preparing fructose syrup |
-
2018
- 2018-01-04 CN CN201810008889.6A patent/CN108300813A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2105337A (en) * | 1981-08-26 | 1983-03-23 | Hydrocarbon Research Inc | Process for making l-sugars and d-fructose |
| CN1974790A (en) * | 2006-12-27 | 2007-06-06 | 王德友 | Method of preventing high fructose syrup from crystallizing |
| CN104651540A (en) * | 2014-12-31 | 2015-05-27 | 吉林中粮生化有限公司 | Crystallization resisting method for F55 high fructose corn syrup |
| CN107475322A (en) * | 2017-07-25 | 2017-12-15 | 安徽万德生物科技有限公司 | A kind of technique for preparing fructose syrup |
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| 尤新: "《淀粉衍生物》", 30 April 2001, 北京：中国物资出版社 * |
| 杨婀娜: "《淀粉糖浆生产技术》", 30 June 1984, 黑龙江科学技术出版社 * |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110551776A (en) * | 2019-10-10 | 2019-12-10 | 中粮融氏生物科技有限公司 | anti-crystallization fructose-glucose syrup and preparation method thereof |
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