CN108298537A - A kind of environment-friendlyactive active carbon binder and preparation method thereof - Google Patents
A kind of environment-friendlyactive active carbon binder and preparation method thereof Download PDFInfo
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- CN108298537A CN108298537A CN201711471108.9A CN201711471108A CN108298537A CN 108298537 A CN108298537 A CN 108298537A CN 201711471108 A CN201711471108 A CN 201711471108A CN 108298537 A CN108298537 A CN 108298537A
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- emulsifier
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- active carbon
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
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Abstract
The present invention relates to a kind of environment-friendlyactive active carbon binder, which is by mass percentage：Water 40 50%, emulsifier I 0.1 0.2%, emulsifier II 0.2 0.5%, interphase oil 15 25%, raw material 35 50%, sodium hydroxide 0.1 0.5%.The preparation method of the binder, preparation process are as follows：Material asphalt preparation, the preparation and mixing of soap lye.The present invention, which utilizes under its cryogenic conditions, still has the characteristics that mobile performance and adhesive property, can effectively solve the problem of that binder for activated carbon is seriously polluted and preheat in advance have the characteristics that pollution-free, energy saving, easy to use, can be used under 50 50 DEG C of environment.
Description
Technical field
The present invention relates to a kind of binder more particularly to a kind of binders of Environment-friendlycarbon carbon material.
Background technology
Binder for activated carbon environmental protection is increasingly becoming a kind of trend, and the existing binder with pollution can gradually be washed in a pan
It eliminates, while country increases renovation dynamics to efforts at environmental protection so that manufacturing enterprise will accomplish production environmental protection, product environmental protection.But mesh
The active carbon environmental-protection binder manufacturing enterprise of preceding China is considerably less, and there are working condition backwardness, yield for most manufacturing enterprises
Low, the problems such as poor product quality and environmental pollution are serious.It implements within 2015<<New environmental law>>Even more Activated Carbon Production is looked forward to
Industry has pushed the road of reform to.Therefore bonding is put into there is an urgent need to the production technology of a completely new environmentally friendly binder instantly
In the production industry of agent, to change existing this awkward situation.
Invention content
Present invention aim to address defects in the prior art, provide a kind of environmental pollution that can effectively reduce carbon material
Problem, and carbon material binder easy to use, at low cost.
The technical scheme is that：A kind of Environment-friendlycarbon carbon material binder, component are by mass percentage：Water
40-50%, I 0.1-0.2% of emulsifier, II 0.2-0.5% of emulsifier, interphase oil 15-25%, raw material 35-50%, sodium hydroxide
0.1-0.5%, wherein emulsifier I are lipophilic emulsifier, and emulsifier II is hydrophilic emulsifier, and interphase oil is washing oil, raw material
For pitch.
Preferably, the emulsifier I is the NP-6 in lipophilic emulsifier, and emulsifier II is in hydrophilic emulsifier
O-15, raw material are one or more arbitrary proportion mixing of low temperature coal tar pitch, medium temperature coal pitch, coal tar pitch.
A kind of preparation method of Environment-friendlycarbon carbon material environmental protection binder, preparation process is as follows：
1）The preparation of material asphalt：After interphase oil, pitch, emulsifier I are mixed according to the above ratio, heated under stirring
It is spare after stirring 5-15min under keeping warm mode after all dissolving to 80-100 DEG C；
2）The preparation of soap lye：After water, emulsifier II, sodium hydroxide are mixed according to the above ratio, all dissolved under stirring
It is spare afterwards；
3）The synthesis of binder：By above-mentioned steps 1 in the state of stirring）The material asphalt prepared is slowly added in soap lye,
Uniform black even solution to be formed is finished product after being cooled to room temperature.
Preferably, the sodium hydroxide is technical grade solid.
Beneficial effects of the present invention are as follows：Utilize the mobile performance still having under its cryogenic conditions, rapid film-forming
The characteristics of, be added into carbon material powder using itself the adhesiveness effective solution environmental issue of existing carbon material,
Have the characteristics that investment is small, at low cost, easy to use, the adhesive of such as emulsified asphalt of the present invention is environmentally safe, cost
For 1800-2000 per ton members, coal tar cost used at present is 2580-2790 per ton members, i.e., free from environmental pollution and can save
Cost.
Specific implementation mode
Below by taking double centner as an example, this technology method is described in detail as follows.
Embodiment 1：
Below by taking double centner as an example, this technology method is described in detail as follows.
A kind of Environment-friendlycarbon carbon material binder, component are by mass percentage：Water 41%, emulsifier I 0.18%, emulsification
II 0.0.47% of agent, interphase oil 25%, raw material 33%, sodium hydroxide 0.35%, wherein emulsifier I are lipophilic emulsifier, emulsification
Agent II is hydrophilic emulsifier, and interphase oil is washing oil, and raw material is pitch, and the emulsifier I is in lipophilic emulsifier
NP-6, emulsifier II are the O-15 in hydrophilic emulsifier, and raw material is medium temperature coal pitch.
A kind of preparation method of Environment-friendlycarbon carbon material environmental protection binder, preparation process are as follows：
1）The preparation of material asphalt：0.18 kilogram of 33 kilograms of mid temperature pitch, 25 kilograms of washing oil and NP-6 are weighed under stirring
It carries out being mixed and heated to 80-100 DEG C, kept the temperature after all dissolving, it is spare：
2）It is prepared by soap lye：0.35 kilogram of industrial sodium hydroxide, 0.47 kilogram of O-15 and 41 kilogram of water are weighed under stirring
Mixing, and 40 DEG C or so are heated to, after all dissolving,
3）By above-mentioned steps 2）The soap lye prepared is slowly added into the state of stirring by above-mentioned steps 1）, the raw material for preparing
In asphaltic liquid, it is stirred at room temperature, after at homogeneous liquid, natural cooling, as finished product.
It is stirred at room temperature, after at homogeneous liquid, natural cooling, as finished product.
Embodiment 2-5.
On the basis of embodiment 1, change the proportion relation of each material, remaining condition is constant.
Based on any of the above embodiments, change technological parameter, remaining condition is constant.
Claims (4)
1. a kind of environment-friendlyactive active carbon binder, component are by mass percentage：Water 40-50%, I 0.1-0.2% of emulsifier,
II 0.2-0.5% of emulsifier, interphase oil 15-25%, raw material 35-50%, sodium hydroxide 0.1-0.5%.
2. a kind of environment-friendlyactive active carbon binder as described in claim 1, which is characterized in that the emulsifier I is oleophylic
Property emulsifier in NP-6, emulsifier II be hydrophilic emulsifier in 0-15, raw material be low temperature coal tar pitch, medium temperature coal pitch,
The one or more arbitrary proportion mixing of coal tar pitch.
3. a kind of preparation method of environment-friendlyactive active carbon binder as described in claim 1, preparation process are as follows：
1）The preparation of material asphalt：After interphase oil, pitch, emulsifier I are mixed according to the above ratio, heated under stirring
It is spare after stirring 5-10min under keeping warm mode after all dissolving to 80-100 DEG C；
2）The preparation of soap lye：After water, emulsifier II, sodium hydroxide are mixed according to the above ratio, all dissolved under stirring
It is spare afterwards；
3）The synthesis of binder：By above-mentioned steps 1 in the state of stirring）The material asphalt prepared is slowly added in soap lye,
Uniform black even solution to be formed is finished product after being cooled to room temperature.
4. the preparation method of binder as claimed in claim 3, which is characterized in that the sodium hydroxide is solid for technical grade
Body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711471108.9A CN108298537A (en) | 2017-12-29 | 2017-12-29 | A kind of environment-friendlyactive active carbon binder and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711471108.9A CN108298537A (en) | 2017-12-29 | 2017-12-29 | A kind of environment-friendlyactive active carbon binder and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN108298537A true CN108298537A (en) | 2018-07-20 |
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| CN201711471108.9A Pending CN108298537A (en) | 2017-12-29 | 2017-12-29 | A kind of environment-friendlyactive active carbon binder and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113816376A (en) * | 2021-09-30 | 2021-12-21 | 国家能源集团宁夏煤业有限责任公司 | Binder special for coal-based activated carbon and preparation method thereof |
| CN114752349A (en) * | 2022-04-18 | 2022-07-15 | 宁夏西泰煤化工有限公司 | Coal-based activated carbon binder based on high-temperature coal tar and modified asphalt, and production method and system thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60168759A (en) * | 1984-02-13 | 1985-09-02 | Toa Doro Kogyo Kk | W/o bituminous emulsion |
| CN105580814A (en) * | 2016-03-30 | 2016-05-18 | 吴美燕 | Preparation method of water-based epoxy coal tar pitch multifunctional emulsion |
-
2017
- 2017-12-29 CN CN201711471108.9A patent/CN108298537A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60168759A (en) * | 1984-02-13 | 1985-09-02 | Toa Doro Kogyo Kk | W/o bituminous emulsion |
| CN105580814A (en) * | 2016-03-30 | 2016-05-18 | 吴美燕 | Preparation method of water-based epoxy coal tar pitch multifunctional emulsion |
Non-Patent Citations (2)
| Title |
|---|
| 刘尚乐: "《乳化沥青及其在道路、建筑工程中的应用》", 31 July 2008, 中国建材工业出版社 * |
| 朱洪法 朱玉霞: "《工业助剂手册》", 30 June 2007, 金盾出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113816376A (en) * | 2021-09-30 | 2021-12-21 | 国家能源集团宁夏煤业有限责任公司 | Binder special for coal-based activated carbon and preparation method thereof |
| CN114752349A (en) * | 2022-04-18 | 2022-07-15 | 宁夏西泰煤化工有限公司 | Coal-based activated carbon binder based on high-temperature coal tar and modified asphalt, and production method and system thereof |
| CN114752349B (en) * | 2022-04-18 | 2023-09-26 | 宁夏西泰煤化工有限公司 | Coal-based activated carbon binder based on high-temperature coal tar and modified asphalt, and production method and system thereof |
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Application publication date: 20180720 |