CN108287415A - A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method - Google Patents
A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method Download PDFInfo
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- CN108287415A CN108287415A CN201810064609.3A CN201810064609A CN108287415A CN 108287415 A CN108287415 A CN 108287415A CN 201810064609 A CN201810064609 A CN 201810064609A CN 108287415 A CN108287415 A CN 108287415A
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- G—PHYSICS
- G02—OPTICS
- G02C—SPECTACLES; SUNGLASSES OR GOGGLES INSOFAR AS THEY HAVE THE SAME FEATURES AS SPECTACLES; CONTACT LENSES
- G02C7/00—Optical parts
- G02C7/10—Filters, e.g. for facilitating adaptation of the eyes to the dark; Sunglasses
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
- G02B1/14—Protective coatings, e.g. hard coatings
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/20—Filters
- G02B5/22—Absorbing filters
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- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Health & Medical Sciences (AREA)
- Ophthalmology & Optometry (AREA)
- General Health & Medical Sciences (AREA)
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Abstract
The invention discloses a kind of radiation protection abrasion-resistance glass spectacle lens and preparation method, the spectacle lens include following component：Silica, alundum (Al2O3), potassium oxide, cerium oxide, di-iron trioxide, diboron trioxide, boron carbide, graphene oxide, zinc oxide, silica modified polymethyl methacrylate, titanium dioxide.Preparation method includes：Molten mass first is prepared in each component mixed melting, then mixes glass melt and silica modified the polymethyl methacrylate product modified with graphene oxide；Mixed melting body is sent into molding machine again, glassware is made, then glassware is made annealing treatment, you can.Spectacle lens of the present invention not only have preferable shielding property, also have preferable crocking resistance, the service life of glasses is improved while providing safety guarantee for eyeglass wearer, have preferable application value.
Description
Technical field
The present invention relates to glassware technical fields, and in particular to a kind of radiation protection abrasion-resistance glass spectacle lens and preparation method.
Background technology
Electromagnetic radiation is formed by the electromagnetic energy for propagating and not returning field source at a distance, when electromagnetic radiation reaches certain magnitude
Or certain time will generate fuel factor and non-thermal effect to human body.Eyes are to electromagnetic radiation in human body than more sensitive device
One of official is easier to be damaged by electromagnetic radiation.The fat-free layer covering of eye, lacks blood containing the crystalline lens compared with juicy
Pipe radiates, and after by electromagnetic radiation fuel factor, crystallins solidify and generate enzyme dysbolism, so as to cause crystalline lens
Muddiness more has severe patient that can form cataract.Strong electromagnetic radiation can make the vitals cornea of human eye come to harm simultaneously, to
Cause visual fatigue, visual impairment or forfeiture.Therefore, there is the eyeglass of radiation resistance can effectively prevent for scientific and reasonable utilization
The electromagnetic radiation injury that human eye is subject to.
Targetedly have glasses of radiation protection but seldom on the market now, it is most of plated on common spectacles one layer it is anti-
It radiates film but radiation protection ability is not strong, injury of the extraneous radiation source to our glasses cannot be resisted at all.But with mobile phone electricity
The electronic products such as brain popularize this industry also slowly in most of precious screen, radiation-proof garment products of such as regarding that emerge also not from root
It is solved the problems, such as on source.In addition existing spectacle lens are careless slightly to be scratched, and very big inconvenience is brought to eyeglass wearer.
Therefore, research and development are a kind of not only having preferable radiation protection, and the glass with preferable wear-resisting property
Eyeglass is of great significance, and also complies with the demand of existing market, has preferable application prospect.
Invention content
For the defects in the prior art, the object of the present invention is to provide a kind of radiation protection abrasion-resistance glass spectacle lens and preparations
Method, the glass lens not only have preferable shielding property, also have preferable crocking resistance, are eyeglass wearer
The service life of glasses is improved while safety guarantee is provided, and there is preferable application value.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention relates to each raw materials of a kind of radiation protection abrasion-resistance glass spectacle lens, including following parts by weight：Silica 50 ~ 70
Part, 2 ~ 6 parts of alundum (Al2O3), 1.5 ~ 5 parts of potassium oxide, 1 ~ 3.5 part of cerium oxide, 5 ~ 10 parts of di-iron trioxide, diboron trioxide 3 ~ 9
Part, 0.5 ~ 2.2 part of boron carbide, 0.3 ~ 1.6 part of graphene oxide, 5 ~ 12 parts of zinc oxide, silica modified polymethylacrylic acid
8 ~ 19 parts of methyl esters, 6 ~ 15 parts of titanium dioxide.
Preferably, 67 parts of the silica, 5 parts of alundum (Al2O3), 3.2 parts of potassium oxide, 2.8 parts of cerium oxide, three oxidations
Two 7 parts of iron, 8 parts of diboron trioxide, 1.5 parts of boron carbide, 1.2 parts of graphene oxide, 8 parts of zinc oxide, silica modified poly- first
15 parts of base methyl acrylate, 9 parts of titanium dioxide.
The invention further relates to a kind of methods preparing radiation protection abrasion-resistance glass spectacle lens, include the following steps：
（1）Silica modified polymethyl methacrylate is weighed according to proportioning to be added in reaction kettle, is warming up to molten condition,
Then graphene oxide is added into reaction kettle while stirring, is stirred to react 1 ~ 2h, obtains product a1, it is spare；
（2）Silica, alundum (Al2O3), potassium oxide, cerium oxide, di-iron trioxide, three oxidations two are weighed respectively according to proportioning
Boron, boron carbide, zinc oxide, titanium dioxide, and place it in blender and blend uniformly, then mixture is placed in molten bath,
In the fusion temperature fusing corresponding to each glass formula, the glass metal of scheduled viscosity is formed；
（3）Glass metal is homogenized, is clarified, bubble is discharged, forms flowable molten mass, molten mass is then warming up to 1400 ~
1500 DEG C, keep the temperature 12 ~ 14h；
（4）Then by glass melt and step（1）In the product a1 that is prepared be uniformly mixed, obtain molten mixture a2；
（5）Then molten mixture a2 is sent into molding machine, the glass lens product of different shape and specification is made, it is then right
Glassware is made annealing treatment, you can.
Preferably, the step（1）Middle reaction temperature is 250 ~ 260 DEG C.
Preferably, the step（2）The middle blending time is 3 ~ 4h.
Preferably, the step（3）Ultrasonication is also carried out after the middle discharge bubble by molten mass, wherein supersonic frequency
Rate is 30 ~ 40kHz.
Further, the ultrasonic treatment time is 20 ~ 30min.
Preferably, the step（5）Middle annealing temperature is 1000 ~ 1100 DEG C.
Preferably, the step（5）It can be polished according to actual needs glassware after annealing, polishing treatment.
Compared with prior art, the present invention has following advantageous effect：
（1）Radiation protection abrasion-resistance glass spectacle lens of the present invention not only have preferable shielding property, also have preferable resistance to
Frictional behaviour improves the service life of glasses while providing safety guarantee for eyeglass wearer, have preferable application value.
（2）Silica modified poly-methyl methacrylate is added in radiation protection abrasion-resistance glass spectacle lens of the present invention
Ester so that eyeglass has preferable scratch-resistant, wear-resisting property and certain anti-fog performance, will be silica modified poly- in the present invention
Methyl methacrylate is modified with graphene oxide to react, can since graphene atomic weight itself is larger, property is stablized
Radioactive ray are effectively prevented, so that there is the spectacle lens that modified polymer material is prepared certain radiation protection to make
With substantially increasing the safety in utilization of spectacle lens.
（3）Di-iron trioxide and cerium oxide are added in radiation protection abrasion-resistance glass spectacle lens of the present invention so that glass
Glass material can have preferable suction-operated to the ultraviolet light and infrared ray being irradiated on glass lens, further reduced light
Radiation and injury of the line to glasses, improve the safety in utilization of eyeglass.
（4）The preparation method of radiation protection abrasion-resistance glass spectacle lens of the present invention is simple and convenient to operate, reaction condition temperature
With easy to control, suitable industrial application.
Specific implementation mode
Present invention will be further explained below with reference to specific examples.These embodiments are merely to illustrate the present invention and do not have to
In limiting the scope of the invention.In the following examples, the experimental methods for specific conditions are not specified, usually according to normal condition, such as
Sambrook equimoleculars are cloned：Laboratory manual（New York:Cold Spring Harbor Laboratory Press,
1989）Described in condition, or according to the normal condition proposed by manufacturer.
Embodiment 1：
A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method of the preferred embodiment of the present invention；
The radiation protection abrasion-resistance glass spectacle lens are prepared by each raw material of each component of following parts by weight：
67 parts of silica；
5 parts of alundum (Al2O3)；
3.2 parts of potassium oxide；
2.8 parts of cerium oxide；
7 parts of di-iron trioxide；
8 parts of diboron trioxide；
1.5 parts of boron carbide；
1.2 parts of graphene oxide；
8 parts of zinc oxide；
15 parts of silica modified polymethyl methacrylate；
9 parts of titanium dioxide.
The method that the present invention prepares radiation protection abrasion-resistance glass spectacle lens, includes the following steps：
（1）Silica modified polymethyl methacrylate is weighed according to proportioning to be added in reaction kettle, is warming up to molten condition,
Then graphene oxide is added into reaction kettle while stirring, is stirred to react 2h, obtains product a1, it is spare；
（2）Silica, alundum (Al2O3), potassium oxide, cerium oxide, di-iron trioxide, three oxidations two are weighed respectively according to proportioning
Boron, boron carbide, zinc oxide, titanium dioxide, and place it in blender and blend uniformly, then mixture is placed in molten bath,
In the fusion temperature fusing corresponding to each glass formula, the glass metal of scheduled viscosity is formed；
（3）Glass metal is homogenized, is clarified, bubble is discharged, forms flowable molten mass, molten mass is then warming up to 1460
DEG C, keep the temperature 14h；
（4）Then by glass melt and step（1）In the product a1 that is prepared be uniformly mixed, obtain molten mixture a2；
（5）Then molten mixture a2 is sent into molding machine, the glass lens product of different shape and specification is made, it is then right
Glassware is made annealing treatment, you can.
Wherein, the step（1）Middle reaction temperature is 260 DEG C.
Wherein, the step（2）The middle blending time is 4h.
Wherein, the step（3）Ultrasonication is also carried out after the middle discharge bubble by molten mass, wherein supersonic frequency
For 35kHz.
Further, the ultrasonic treatment time is 30min.
Wherein, the step（5）Middle annealing temperature is 1000 DEG C.
Wherein, the step（5）It can be polished according to actual needs glassware after annealing, polishing treatment.
Embodiment 2：
A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method of the preferred embodiment of the present invention；
The radiation protection abrasion-resistance glass spectacle lens are prepared by each raw material of following parts by weight：
50 parts of silica；
2 parts of alundum (Al2O3)；
1.5 parts of potassium oxide；
1 part of cerium oxide；
5 parts of di-iron trioxide；
3 parts of diboron trioxide；
0.5 part of boron carbide；
0.3 part of graphene oxide；
5 parts of zinc oxide；
8 parts of silica modified polymethyl methacrylate；
6 parts of titanium dioxide.
The method that the present invention prepares radiation protection abrasion-resistance glass spectacle lens, includes the following steps：
（1）Silica modified polymethyl methacrylate is weighed according to proportioning to be added in reaction kettle, is warming up to molten condition,
Then graphene oxide is added into reaction kettle while stirring, is stirred to react 1h, obtains product a1, it is spare；
（2）Silica, alundum (Al2O3), potassium oxide, cerium oxide, di-iron trioxide, three oxidations two are weighed respectively according to proportioning
Boron, boron carbide, zinc oxide, titanium dioxide, and place it in blender and blend uniformly, then mixture is placed in molten bath,
In the fusion temperature fusing corresponding to each glass formula, the glass metal of scheduled viscosity is formed；
（3）Glass metal is homogenized, is clarified, bubble is discharged, forms flowable molten mass, molten mass is then warming up to 1400
DEG C, keep the temperature 14h；
（4）Then by glass melt and step（1）In the product a1 that is prepared be uniformly mixed, obtain molten mixture a2；
（5）Then molten mixture a2 is sent into molding machine, the glass lens product of different shape and specification is made, it is then right
Glassware is made annealing treatment, you can.
Wherein, the step（1）Middle reaction temperature is 250 DEG C.
Wherein, the step（2）The middle blending time is 3h.
Wherein, the step（3）Ultrasonication is also carried out after the middle discharge bubble by molten mass, wherein supersonic frequency
For 30kHz.
Further, the ultrasonic treatment time is 30min.
Wherein, the step（5）Middle annealing temperature is 1000 DEG C.
Wherein, the step（5）It can be polished according to actual needs glassware after annealing, polishing treatment.
Embodiment 3：
A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method of the preferred embodiment of the present invention；
The radiation protection abrasion-resistance glass spectacle lens are prepared by each raw material of following parts by weight：
70 parts of silica；
6 parts of alundum (Al2O3)；
5 parts of potassium oxide；
3.5 parts of cerium oxide；
10 parts of di-iron trioxide；
9 parts of diboron trioxide；
2.2 parts of boron carbide；
1.6 parts of graphene oxide；
12 parts of zinc oxide；
19 parts of silica modified polymethyl methacrylate；
15 parts of titanium dioxide.
The method that the present invention prepares radiation protection abrasion-resistance glass spectacle lens, includes the following steps：
（1）Silica modified polymethyl methacrylate is weighed according to proportioning to be added in reaction kettle, is warming up to molten condition,
Then graphene oxide is added into reaction kettle while stirring, is stirred to react 2h, obtains product a1, it is spare；
（2）Silica, alundum (Al2O3), potassium oxide, cerium oxide, di-iron trioxide, three oxidations two are weighed respectively according to proportioning
Boron, boron carbide, zinc oxide, titanium dioxide, and place it in blender and blend uniformly, then mixture is placed in molten bath,
In the fusion temperature fusing corresponding to each glass formula, the glass metal of scheduled viscosity is formed；
（3）Glass metal is homogenized, is clarified, bubble is discharged, forms flowable molten mass, molten mass is then warming up to 1500
DEG C, keep the temperature 12h；
（4）Then by glass melt and step（1）In the product a1 that is prepared be uniformly mixed, obtain molten mixture a2；
（5）Then molten mixture a2 is sent into molding machine, the glass lens product of different shape and specification is made, it is then right
Glassware is made annealing treatment, you can.
Wherein, the step（1）Middle reaction temperature is 260 DEG C.
Wherein, the step（2）The middle blending time is 4h.
Wherein, the step（3）Ultrasonication is also carried out after the middle discharge bubble by molten mass, wherein supersonic frequency
For 40kHz.
Further, the ultrasonic treatment time is 20min.
Wherein, the step（5）Middle annealing temperature is 1100 DEG C.
Wherein, the step（5）It can be polished according to actual needs glassware after annealing, polishing treatment.
In conclusion radiation protection abrasion-resistance glass spectacle lens of the present invention, not only have preferable shielding property, also
With preferable crocking resistance, the service life of glasses is improved while providing safety guarantee for eyeglass wearer, is had
Preferable application value.The preparation method of radiation protection abrasion-resistance glass spectacle lens of the present invention is simple and convenient to operate, reacts item
Part is mildly easy to control, is suitble to industrial application
Specific embodiments of the present invention are described above.It is to be appreciated that the invention is not limited in above-mentioned specific
Embodiment, those skilled in the art can make various deformations or amendments within the scope of the claims, this has no effect on this
The substantive content of invention.
Claims (9)
1. a kind of radiation protection abrasion-resistance glass spectacle lens, which is characterized in that each raw material including following parts by weight：Silica 50 ~
70 parts, 2 ~ 6 parts of alundum (Al2O3), 1.5 ~ 5 parts of potassium oxide, 1 ~ 3.5 part of cerium oxide, 5 ~ 10 parts of di-iron trioxide, diboron trioxide 3
~ 9 parts, 0.5 ~ 2.2 part of boron carbide, 0.3 ~ 1.6 part of graphene oxide, 5 ~ 12 parts of zinc oxide, silica modified polymethyl
8 ~ 19 parts of sour methyl esters, 6 ~ 15 parts of titanium dioxide.
2. radiation protection abrasion-resistance glass spectacle lens according to claim 1, which is characterized in that 67 parts of the silica, three
5 parts of Al 2 O, 3.2 parts of potassium oxide, 2.8 parts of cerium oxide, 7 parts of di-iron trioxide, 8 parts of diboron trioxide, 1.5 parts of boron carbide,
1.2 parts of graphene oxide, 8 parts of zinc oxide, 15 parts of silica modified polymethyl methacrylate, 9 parts of titanium dioxide.
3. a kind of method preparing radiation protection abrasion-resistance glass spectacle lens as claimed in claim 1 or 2, which is characterized in that including
Following steps：
（1）Silica modified polymethyl methacrylate is weighed according to proportioning to be added in reaction kettle, is warming up to molten condition,
Then graphene oxide is added into reaction kettle while stirring, is stirred to react 1 ~ 2h, obtains product a1, it is spare；
（2）Silica, alundum (Al2O3), potassium oxide, cerium oxide, di-iron trioxide, three oxidations two are weighed respectively according to proportioning
Boron, boron carbide, zinc oxide, titanium dioxide, and place it in blender and blend uniformly, then mixture is placed in molten bath,
In the fusion temperature fusing corresponding to each glass formula, the glass metal of scheduled viscosity is formed；
（3）Glass metal is homogenized, is clarified, bubble is discharged, forms flowable molten mass, molten mass is then warming up to 1400 ~
1500 DEG C, keep the temperature 12 ~ 14h；
（4）Then by glass melt and step（1）In the product a1 that is prepared be uniformly mixed, obtain molten mixture a2；
（5）Then molten mixture a2 is sent into molding machine, the glass lens product of different shape and specification is made, it is then right
Glassware is made annealing treatment, you can.
4. the preparation method of radiation protection abrasion-resistance glass spectacle lens according to claim 3, which is characterized in that the step
（1）Middle reaction temperature is 250 ~ 260 DEG C.
5. the preparation method of radiation protection abrasion-resistance glass spectacle lens according to claim 3, which is characterized in that the step
（2）The middle blending time is 3 ~ 4h.
6. the preparation method of radiation protection abrasion-resistance glass spectacle lens according to claim 3, which is characterized in that the step
（3）Ultrasonication is also carried out after the middle discharge bubble by molten mass, wherein supersonic frequency is 30 ~ 40kHz.
7. the preparation method of radiation protection abrasion-resistance glass spectacle lens according to claim 6, which is characterized in that the ultrasonic wave
Processing time is 20 ~ 30min.
8. the preparation method of radiation protection abrasion-resistance glass spectacle lens according to claim 3, which is characterized in that the step
（5）Middle annealing temperature is 1000 ~ 1100 DEG C.
9. the preparation method of radiation protection abrasion-resistance glass spectacle lens according to claim 3, which is characterized in that the step
（5）It can be polished according to actual needs glassware after annealing, polishing treatment.
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| CN201810064609.3A CN108287415A (en) | 2018-01-23 | 2018-01-23 | A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method |
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| CN201810064609.3A CN108287415A (en) | 2018-01-23 | 2018-01-23 | A kind of radiation protection abrasion-resistance glass spectacle lens and preparation method |
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ID=62835881
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109188718A (en) * | 2018-09-27 | 2019-01-11 | 镇江奥视达光学有限公司 | A kind of lightweight myopia-proof lens and its production method |
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| JP2009197155A (en) * | 2008-02-22 | 2009-09-03 | Bridgestone Corp | Photocurable composition, antireflection film having antireflection membrane of the composition, and optical filter for display having the same |
| CN101708954A (en) * | 2009-11-30 | 2010-05-19 | 蔡绪忠 | Ultraviolet ray and infrared ray adsorption blue transparent glass |
| CN107399907A (en) * | 2017-08-01 | 2017-11-28 | 合肥利裕泰玻璃制品有限公司 | A kind of shatter-resistant glass of resistance to the temperature difference |
| CN108676477A (en) * | 2018-06-04 | 2018-10-19 | 合肥钢骨玻璃制品有限公司 | A kind of coating and preparation method thereof improving glass transmission rate |
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2018
- 2018-01-23 CN CN201810064609.3A patent/CN108287415A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2009197155A (en) * | 2008-02-22 | 2009-09-03 | Bridgestone Corp | Photocurable composition, antireflection film having antireflection membrane of the composition, and optical filter for display having the same |
| CN101708954A (en) * | 2009-11-30 | 2010-05-19 | 蔡绪忠 | Ultraviolet ray and infrared ray adsorption blue transparent glass |
| CN107399907A (en) * | 2017-08-01 | 2017-11-28 | 合肥利裕泰玻璃制品有限公司 | A kind of shatter-resistant glass of resistance to the temperature difference |
| CN108676477A (en) * | 2018-06-04 | 2018-10-19 | 合肥钢骨玻璃制品有限公司 | A kind of coating and preparation method thereof improving glass transmission rate |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109188718A (en) * | 2018-09-27 | 2019-01-11 | 镇江奥视达光学有限公司 | A kind of lightweight myopia-proof lens and its production method |
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