CN108283239A - A kind of soft sweets of the extract of slag containing pawpaw - Google Patents
A kind of soft sweets of the extract of slag containing pawpaw Download PDFInfo
- Publication number
- CN108283239A CN108283239A CN201710378628.9A CN201710378628A CN108283239A CN 108283239 A CN108283239 A CN 108283239A CN 201710378628 A CN201710378628 A CN 201710378628A CN 108283239 A CN108283239 A CN 108283239A
- Authority
- CN
- China
- Prior art keywords
- extract
- pawpaw
- slag
- mentioned
- carragheen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000002893 slag Substances 0.000 title claims abstract description 47
- 244000189799 Asimina triloba Species 0.000 title claims abstract description 44
- 235000006264 Asimina triloba Nutrition 0.000 title claims abstract description 44
- 235000009467 Carica papaya Nutrition 0.000 title claims abstract description 44
- 235000009508 confectionery Nutrition 0.000 title claims abstract description 24
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 33
- 241000206575 Chondrus crispus Species 0.000 claims abstract description 15
- 229920000159 gelatin Polymers 0.000 claims abstract description 14
- 235000019322 gelatine Nutrition 0.000 claims abstract description 14
- 108010010803 Gelatin Proteins 0.000 claims abstract description 13
- 239000008273 gelatin Substances 0.000 claims abstract description 13
- 235000011852 gelatine desserts Nutrition 0.000 claims abstract description 13
- 238000002360 preparation method Methods 0.000 claims abstract description 12
- 238000010521 absorption reaction Methods 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 239000003480 eluent Substances 0.000 claims description 20
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 15
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 10
- 238000002386 leaching Methods 0.000 claims description 10
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 8
- 235000019441 ethanol Nutrition 0.000 claims description 7
- 239000002994 raw material Substances 0.000 claims description 6
- 229920002538 Polyethylene Glycol 20000 Polymers 0.000 claims description 5
- 239000003463 adsorbent Substances 0.000 claims description 5
- 238000004440 column chromatography Methods 0.000 claims description 5
- 239000003208 petroleum Substances 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 244000241257 Cucumis melo Species 0.000 claims description 2
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 claims description 2
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 150000002576 ketones Chemical class 0.000 claims description 2
- 239000003643 water by type Substances 0.000 claims description 2
- 239000002023 wood Substances 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000004064 recycling Methods 0.000 abstract description 2
- 235000015110 jellies Nutrition 0.000 description 7
- 239000008274 jelly Substances 0.000 description 7
- 239000003292 glue Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- OVARTBFNCCXQKS-UHFFFAOYSA-N propan-2-one;hydrate Chemical compound O.CC(C)=O OVARTBFNCCXQKS-UHFFFAOYSA-N 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 229920001817 Agar Polymers 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 239000008272 agar Substances 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 235000013325 dietary fiber Nutrition 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 230000006641 stabilisation Effects 0.000 description 2
- 238000011105 stabilization Methods 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 244000099147 Ananas comosus Species 0.000 description 1
- 235000007119 Ananas comosus Nutrition 0.000 description 1
- 241000207199 Citrus Species 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000020971 citrus fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 235000012631 food intake Nutrition 0.000 description 1
- 239000003349 gelling agent Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/44—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/10—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing amino-acids, proteins, e.g. gelatine, peptides, polypeptides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G2200/00—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents
- A23G2200/14—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF containing organic compounds, e.g. synthetic flavouring agents containing fruits, nuts, e.g. almonds, seeds, plants, plant extracts or essential oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Botany (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Confectionery (AREA)
Abstract
The present invention relates to a kind of soft sweets manufacture field, more particularly to a kind of soft sweets of the extract of slag containing pawpaw.Preparation process be with carragheen absorption 10% ethyl acetate after, by carragheen and gelatin, pawpaw slag extract, powdered sugar mixing obtain product.The present invention can promote to research and develop soft sweets new product by preparing soft sweets, reach product diversification, and promote the effective recycling of pawpaw slag.
Description
Technical field
The present invention relates to a kind of soft sweets manufacture field, more particularly to a kind of soft sweets of the extract of slag containing pawpaw.
Background technology
Gel soft candy refers to forming network skeleton by colloid, and fill sugar containing one or more kinds of gelling agents
The glue-type candy of the stabilization of the formation such as class and moisture.Different gel soft candies can be made using different colloids, as gelatin is soft
Sugar, jelly work, carragheen soft sweets, agar fruit jelly and starch jelly etc..Due to the difference of colloidal nature, gel soft candy respectively has spy
Matter, if starch jelly is relatively viscous, carragheen soft sweets and agar fruit jelly are solid and crisp, and jelly work is tender crisp and soft, and gelatine gums is saturating
Bright and high resilience.
The domestic research for some pomace raw materials rich in dietary fiber at present has started to walk comprehensively, main research and utilization
Have apple pomace, pears slag, citrus pulp, pineapple bran etc., but yet there are no pawpaw slag converted products listing.With living standards of the people
Raising, requirement of the people to food consumption be also higher and higher.This environment is greatly promoted the prevalence of garden stuff processing product.
And during garden stuff processing, a large amount of pomace waste materials are inevitably will produce, these pomaces are dynamic except fraction roughing is used as
Outside object feed, citric acid fermented, extraction pectin, it is dropped mostly as waste, causes huge waste and environmental pollution.Its
Real, these pomaces contain abundant dietary fiber, if its performance characteristics can be directed to, production prepares pomace product, can not only reduce
The effective way of processing of agriculture product comprehensive utilization will be also opened up in environmental pollution.
But yet there are no and prepare jelly sweets using pawpaw slag extract, it is unable to reach the various of soft candy product
Property, and the effective recycling of pawpaw slag can not be promoted.
Invention content
In order to compensate for the shortcomings of the prior art, the present invention provides a kind of soft sweets of the extract of slag containing pawpaw.
The present invention is achieved through the following technical solutions：
1. a kind of soft sweets of the extract of slag containing pawpaw, preparation method are, after the ethyl acetate with carragheen absorption 10%, by OK a karaoke club
Glue and gelatin, pawpaw slag extract, powdered sugar mixing, obtain product, wherein the quality proportioning of above-mentioned each raw material is：Gelatin 10-
20 grams, 3-5 grams of pawpaw slag extract, 5-10 grams of powdered sugar, 5-10 grams of carragheen, 10% 1-2 grams of ethyl acetate；
The preparation method of above-mentioned pawpaw slag extract is as follows：
A, 10-20% ethanol waters will be added after pawpaw slag drying and crushing, ethanol water total weight is the wood after drying and crushing
2-3 times of melon slag weight is extracted 20-30 minutes in 50-60 DEG C of heat reflux, and is filtered, and obtains leaching liquor；
B, above-mentioned leaching liquor is extracted with petroleum ether, obtains extract liquor；
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is washed with the aqueous acetic acid of a concentration of 5-10%
It is de-, obtain first order eluent；
D, the Silon of 200 mesh is used to be chromatographed as adsorbent above-mentioned first order eluent, then with the third of 0.2-0.5%
Ketone aqueous solution elutes, and obtains second level eluent；
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the pawpaw slag extract after drying.
Compared with prior art, the invention has the advantages that：
(1) gelatin is added, the embedding effect of soft sweets molecule can be promoted, and reaches stabilization；
(2) pawpaw slag extract can help human body to eliminate free radical, slow down aging, and have treatment anti-inflammatory effect.
(3) present component is simple, and preparation method is easy, of low cost, and there is no the ingredients of the harm to human body, are one
The good soft sweets of kind.
Specific implementation mode
Embodiment 1:
1. a kind of soft sweets of the extract of slag containing pawpaw, preparation method are, after the ethyl acetate with carragheen absorption 10%, by OK a karaoke club
Glue and gelatin, pawpaw slag extract, powdered sugar mixing, obtain product, wherein the quality proportioning of above-mentioned each raw material is：Gelatin
10g, pawpaw slag extract 3g, powdered sugar 5g, carragheen 5g, 10% ethyl acetate 1g.
The preparation method of above-mentioned pawpaw slag extract is as follows：
A, 10% ethanol water will be added after pawpaw slag drying and crushing, ethanol water total weight is the pawpaw after drying and crushing
2 times of slag weight are extracted 20 minutes in 50 DEG C of heat reflux, and are filtered, and obtain leaching liquor；
B, above-mentioned leaching liquor is extracted with petroleum ether, obtains extract liquor；
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is eluted with a concentration of 10% aqueous acetic acid,
Obtain first order eluent；
D, the Silon of 200 mesh is used to be chromatographed as adsorbent above-mentioned first order eluent, then with 0.2% acetone water
Solution elutes, and obtains second level eluent；
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the pawpaw slag extract after drying.
Embodiment 2:
1. a kind of soft sweets of the extract of slag containing pawpaw, preparation method are, after the ethyl acetate with carragheen absorption 10%, by OK a karaoke club
Glue and gelatin, pawpaw slag extract, powdered sugar mixing, obtain product, wherein the quality proportioning of above-mentioned each raw material is：Gelatin
15g, pawpaw slag extract 4g, powdered sugar 7.5g, carragheen 7.5g, 10% ethyl acetate 1.5g.
The preparation method of above-mentioned pawpaw slag extract is as follows：
A, 15% ethanol water will be added after pawpaw slag drying and crushing, ethanol water total weight is the pawpaw after drying and crushing
2.5 times of slag weight are extracted 25 minutes in 55 DEG C of heat reflux, and are filtered, and obtain leaching liquor；
B, above-mentioned leaching liquor is extracted with petroleum ether, obtains extract liquor；
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is eluted with a concentration of 5% aqueous acetic acid, obtained
First order eluent；
D, the Silon of 200 mesh is used to be chromatographed as adsorbent above-mentioned first order eluent, then with 0.35% acetone water
Solution elutes, and obtains second level eluent；
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the pawpaw slag extract after drying.
Embodiment 3：
1. a kind of soft sweets of the extract of slag containing pawpaw, preparation method are, after the ethyl acetate with carragheen absorption 10%, by OK a karaoke club
Glue and gelatin, pawpaw slag extract, powdered sugar mixing, obtain product, wherein the quality proportioning of above-mentioned each raw material is：Gelatin
20g, pawpaw slag extract 5g, powdered sugar 10g, carragheen 10g, 10% ethyl acetate 2g.
The preparation method of above-mentioned pawpaw slag extract is as follows：
A, 20% ethanol water will be added after pawpaw slag drying and crushing, ethanol water total weight is the pawpaw after drying and crushing
3 times of slag weight are extracted 30 minutes in 60 DEG C of heat reflux, and are filtered, and obtain leaching liquor；
B, above-mentioned leaching liquor is extracted with petroleum ether, obtains extract liquor；
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is eluted with a concentration of 8% aqueous acetic acid, obtained
First order eluent；
D, the Silon of 200 mesh is used to be chromatographed as adsorbent above-mentioned first order eluent, then with 0.5% acetone water
Solution elutes, and obtains second level eluent；
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the pawpaw slag extract after drying.
Claims (1)
1. a kind of soft sweets of the extract of slag containing pawpaw, it is characterised in that preparation method is：With the ethyl acetate of carragheen absorption 10%
Afterwards, by carragheen and gelatin, pawpaw slag extract, powdered sugar mixing, product is obtained, wherein the quality proportioning of above-mentioned each raw material
For：10-20 grams of gelatin, 3-5 grams of pawpaw slag extract, 5-10 grams of powdered sugar, 5-10 grams of carragheen, 10% ethyl acetate 1-2
Gram；
The preparation method of above-mentioned pawpaw slag extract is as follows：
A, 10-20% ethanol waters will be added after pawpaw slag drying and crushing, ethanol water total weight is the wood after drying and crushing
2-3 times of melon slag weight is extracted 20-30 minutes in 50-60 DEG C of heat reflux, and is filtered, and obtains leaching liquor；
B, above-mentioned leaching liquor is extracted with petroleum ether, obtains extract liquor；
C, above-mentioned extract liquor is subjected to column chromatography with PEG 20000 column, then is washed with the aqueous acetic acid of a concentration of 5-10%
It is de-, obtain first order eluent；
D, the Silon of 200 mesh is used to be chromatographed as adsorbent above-mentioned first order eluent, then with the third of 0.2-0.5%
Ketone aqueous solution elutes, and obtains second level eluent；
E, above-mentioned second level eluent is recrystallized with ethyl alcohol, to get the pawpaw slag extract after drying.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710378628.9A CN108283239A (en) | 2017-05-25 | 2017-05-25 | A kind of soft sweets of the extract of slag containing pawpaw |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710378628.9A CN108283239A (en) | 2017-05-25 | 2017-05-25 | A kind of soft sweets of the extract of slag containing pawpaw |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108283239A true CN108283239A (en) | 2018-07-17 |
Family
ID=62831311
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710378628.9A Pending CN108283239A (en) | 2017-05-25 | 2017-05-25 | A kind of soft sweets of the extract of slag containing pawpaw |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108283239A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115109170A (en) * | 2022-08-05 | 2022-09-27 | 十堰风神汽车橡塑制品有限公司 | Environment-friendly plasticizer, nitrile rubber and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101978848A (en) * | 2010-11-12 | 2011-02-23 | 盐城工学院 | Functional soft sweets rich in polysaccharides of phizoma phragmitis and preparation method thereof |
| CN105146023A (en) * | 2015-07-31 | 2015-12-16 | 青岛文创科技有限公司 | Papaya soft sweets and making method thereof |
| CN105166280A (en) * | 2015-09-23 | 2015-12-23 | 华南农业大学 | Mulberry soft sweets and preparing method thereof |
| CN106107957A (en) * | 2016-05-31 | 2016-11-16 | 湖北文理学院 | A kind of mangosteen skin gingerol antioxidant and preparation method thereof |
| CN106387254A (en) * | 2016-08-30 | 2017-02-15 | 桂林实力科技有限公司 | Siraitia grosvenorii soft sweets and preparation method thereof |
-
2017
- 2017-05-25 CN CN201710378628.9A patent/CN108283239A/en active Pending
Patent Citations (5)
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|---|---|---|---|---|
| CN101978848A (en) * | 2010-11-12 | 2011-02-23 | 盐城工学院 | Functional soft sweets rich in polysaccharides of phizoma phragmitis and preparation method thereof |
| CN105146023A (en) * | 2015-07-31 | 2015-12-16 | 青岛文创科技有限公司 | Papaya soft sweets and making method thereof |
| CN105166280A (en) * | 2015-09-23 | 2015-12-23 | 华南农业大学 | Mulberry soft sweets and preparing method thereof |
| CN106107957A (en) * | 2016-05-31 | 2016-11-16 | 湖北文理学院 | A kind of mangosteen skin gingerol antioxidant and preparation method thereof |
| CN106387254A (en) * | 2016-08-30 | 2017-02-15 | 桂林实力科技有限公司 | Siraitia grosvenorii soft sweets and preparation method thereof |
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| Title |
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| 李小鑫等: ""刺梨果渣软糖配方工艺优化研究"", 《食品科技》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115109170A (en) * | 2022-08-05 | 2022-09-27 | 十堰风神汽车橡塑制品有限公司 | Environment-friendly plasticizer, nitrile rubber and preparation method thereof |
| CN115109170B (en) * | 2022-08-05 | 2023-11-21 | 十堰风神汽车橡塑制品有限公司 | Environment-friendly plasticizer, nitrile rubber and preparation method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20180717 |