CN108278894A - A kind of vacuum sintering furnace making self-lubricating workpiece - Google Patents

A kind of vacuum sintering furnace making self-lubricating workpiece Download PDF

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Publication number
CN108278894A
CN108278894A CN201810122033.1A CN201810122033A CN108278894A CN 108278894 A CN108278894 A CN 108278894A CN 201810122033 A CN201810122033 A CN 201810122033A CN 108278894 A CN108278894 A CN 108278894A
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CN
China
Prior art keywords
vacuum
self
flue
furnace body
workpiece
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Pending
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CN201810122033.1A
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Chinese (zh)
Inventor
李荣华
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Suzhou Golden Small New Mstar Technology Ltd
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Suzhou Golden Small New Mstar Technology Ltd
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Application filed by Suzhou Golden Small New Mstar Technology Ltd filed Critical Suzhou Golden Small New Mstar Technology Ltd
Priority to CN201810122033.1A priority Critical patent/CN108278894A/en
Publication of CN108278894A publication Critical patent/CN108278894A/en
Pending legal-status Critical Current

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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS, OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B21/00Open or uncovered sintering apparatus; Other heat-treatment apparatus of like construction
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D19/00Arrangements of controlling devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D7/00Forming, maintaining, or circulating atmospheres in heating chambers
    • F27D7/06Forming or maintaining special atmospheres or vacuum within heating chambers
    • F27D2007/066Vacuum
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • F27D2009/0002Cooling of furnaces
    • F27D2009/0005Cooling of furnaces the cooling medium being a gas
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D9/00Cooling of furnaces or of charges therein
    • F27D2009/0002Cooling of furnaces
    • F27D2009/001Cooling of furnaces the cooling medium being a fluid other than a gas
    • F27D2009/0013Cooling of furnaces the cooling medium being a fluid other than a gas the fluid being water
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D19/00Arrangements of controlling devices
    • F27D2019/0003Monitoring the temperature or a characteristic of the charge and using it as a controlling value

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Powder Metallurgy (AREA)

Abstract

The present invention discloses a kind of vacuum sintering furnace making self-lubricating workpiece, including:Vacuum furnace body;The vacuum furnace body is communicated with exhaust equipment;Flue in the vacuum furnace body, the flue are equipped with the heating element for sintered self-lubricated workpiece;The pressure exerting arrangement being connect with the flue;The pressure exerting arrangement can apply pressure to the surface of the self-lubricating workpiece.The support base for being used to support self-lubricating workpiece lower surface is additionally provided in the flue;The pressure exerting arrangement includes in the flue and the pressure head that can be pushed to the self-lubricating workpiece surface, the pushing component being connect with the pressure head;The pushing component includes:The lifting cylinder sleeve and the cylinder outside the vacuum furnace body being threaded through on the courage wall of the flue and the chamber wall of the vacuum furnace body.The vacuum sintering furnace of the making self-lubricating workpiece realizes the technique of once sintered completion, reduces the cumbersome technique of repeatedly rolling sintering.

Description

A kind of vacuum sintering furnace making self-lubricating workpiece
Technical field
The invention belongs to self-lubricating workpiece to make industry field more particularly to a kind of vacuum-sintering making self-lubricating workpiece Stove, it is a kind of in the alloy powders such as steel plate or steel shaft set sintered copper, iron and containing the compound of solid lubricant especially suitable for making The two-sided workpiece of type, sinter layer thickness is generally between 1-5mm.
Background technology
Current bimetal self-lubricating bearing using various ways manufacture, such as normal melt casting method, centrifugal casting, Guipure continous way sintering process etc..
Common fusion-cast be usually steel plate surface casting melt after tin bronze 663, the fusion-cast method compared with To be common, but he the shortcomings that be that double-deck adhesion strength is poor, the material molecule of casting is loosely organized, and wearability is poor, and nothing Method forms porous organization in surface wear-resistant layer, makes interior surface oil-containing, auto-supply is realized when so cannot reach both surface friction Purpose.
Centrifugal casting is also in surface casting tin bronze 663, and centrifugal casting is more common, is generally used for shaft sleeve zero The making of component, product limitation is poor, and for the compactness for the product that centrifugal casting is cast than more consistent, molecular structure is close, But due to the left and right of rotation, loss is bigger, and production cost is relatively high, and also has no idea to realize that the inside realization of casting is porous Tissue, while can not achieve the purpose that friction level auto-supply.
Guipure continous way sintering process mainly has a disadvantage that:
1, since the workpiece of meshbeltfurnace is to remain at operating status, the powder of sintered surface remains at loose state It has no idea to give pressure compaction on top, so the molecular structure of sinter layer is loose, cannot be densified, therefore being made in sintering should It also needs to carry out cold rolling process during product, and be repeatedly sintered and roll, so one side technique is cumbersome, another party Face also wastes energy consumption significantly, increases production cost.
When 2, due to sintering realized under high temperature workpiece free state, all be sintered products include base material and sintering Layer often will produce prodigious deflection, and prodigious trouble is brought to metalworking, and due to the increase of deflection loss also with Increasing.
3, due to sintered rolling, lead to internal oil-containing blockage of the micro orifice, oil can not be penetrated into wherein, therefore transported in slide plate It there will not be oil in row friction process to ooze out from surface layer, therefore increase the probability of the occlusion in operational process and locking.
4, making being not only for anti-attrition self-lubricating slide board needs the wear-resisting of sinter layer to also need to that sinter layer is made to become microcosmic More dummy status, the sinter layer for being sintered completion handles the automatic oil-containing of realization by vacuum oil immersion, when anti-attrition self-lubricating plate is rubbing Certain negative pressure can be generated on surface when wiping movement, be that the inside of oil-containing is precipitated automatically.
Based on above-mentioned sintering requirement, when sintering the control of sintering surface pressure be strict.Therefore it on the one hand needs to burn Knot layer gives certain pressure, and the pressure control of sintering layer surface has no that it has the report of this respect at present, and due to more Secondary sintering and rolling, production cost is quite high, and the market competitiveness is poor.
Invention content
In view of the deficiencies in the prior art, the present invention is to provide a kind of vacuum sintering furnace making self-lubricating workpiece, makes to moisten certainly The surface of sliding workpiece carries out densification sintering in the state of having pressure, and the technique for realizing once sintered completion reduces more The cumbersome technique of secondary rolling sintering.
The technical solution adopted by the present invention is as follows:
A kind of vacuum sintering furnace making self-lubricating workpiece, including:
Vacuum furnace body;The vacuum furnace body is communicated with exhaust equipment;
Flue in the vacuum furnace body, the flue are equipped with the heating element for sintered self-lubricated workpiece;
The pressure exerting arrangement being connect with the flue;The pressure exerting arrangement can apply pressure to the surface of the self-lubricating workpiece.
It is used to support self-lubricating workpiece lower surface as a preferred embodiment, being additionally provided in the flue Support base;
The pressure exerting arrangement include be located in the flue and can to pressure head that the self-lubricating workpiece surface pushes, with it is described The pushing component of pressure head connection;The pushing component includes:It is threaded through the courage wall of the flue and the appearance of the vacuum furnace body Lifting cylinder sleeve on wall and the cylinder outside the vacuum furnace body;One end connection cylinder of the lifting cylinder sleeve, The other end connects the pressure head.
As a preferred embodiment, multiple pressure exerting arrangements are arranged along first direction;Multiple support bases It is arranged along the first direction.
As a preferred embodiment, the pressure head and support base are graphite material;The heating element packet Include at least one of graphite, molybdenum or MoSi2.
As a preferred embodiment, the cylinder is connected with pneumatic control valve;The pneumatic control valve can control The pressure of the cylinder, and then adjust surface pressing of the pressure head to the self-lubricating workpiece.
As a preferred embodiment, further including PID controller and temperature measurement component;The temperature measurement component can Detect the sintering temperature in the flue;The PID controller is connected with the temperature measurement component, the heating element, with root The sintering temperature detected according to the temperature measurement component controls the heating temperature of the heating element.
As a preferred embodiment, further including:Wind cooling unit;The wind cooling unit is passed through the vacuum furnace body It is internal;The flue is equipped with the gas outlet communicated with the air inlet communicated inside vacuum furnace body and with heat exchanger;The wind Cold unit can re-enter heat exchanger gas after cooling in flue through the air inlet.
As a preferred embodiment, the wind cooling unit includes wind turbine and cooling air source;The cooling air source It is connected to flue inside, to input inert gas into flue;The wind turbine can drive gas defeated by the air inlet Enter in flue.
As a preferred embodiment, further include water cooling unit, the length direction and horizontal plane of the vacuum furnace body It is parallel;The vacuum furnace body has container outer wall and container inner wall;First is equipped between the container outer wall and container inner wall Water cooling gap;
The exhaust equipment includes detecting the vacuum meter of vacuum degree in vacuum furnace body, the vacuum pump being connected with the vacuum furnace body And the water cooling component for being cooled down to the vacuum pump;The wind turbine is additionally provided with double-layer electric hood;The double-layer electric hood tool There is the second water cooling gap;
The water cooling unit is connected with first water cooling gap, the second water cooling gap and the water cooling component, with to institute State first water cooling gap, the second water cooling gap and water cooling component supply cold water.
As a preferred embodiment, the exhaust equipment can make the vacuum degree in the vacuum furnace body reach 6* 10-1Pa to 7*10-1Pa。
As a preferred embodiment, the vacuum furnace body includes the lid of cylinder and lid conjunction in cylinder one end; Hinge connection is used between the lid and the cylinder, and is locked by zigzag retainer;The courage wall of the flue is equipped with Insulating layer;The link position of the pressure exerting arrangement and the flue is equipped with sealing structure.
Advantageous effect:
The vacuum sintering furnace for the making self-lubricating workpiece that present embodiment is provided utilizes pressure exerting arrangement by being equipped with pressure exerting arrangement Apply pressure on the surface of sintering workpiece, so that workpiece surface is carried out densification sintering in the state of having pressure, realize primary It is sintered the technique completed, reduces the cumbersome technique of repeatedly rolling sintering.
With reference to following description and accompanying drawings, only certain exemplary embodiments of this invention is disclosed in detail, specifies the original of the present invention Reason can be in a manner of adopted.It should be understood that embodiments of the present invention are not so limited in range.In appended power In the range of the spirit and terms that profit requires, embodiments of the present invention include many changes, modifications and are equal.
The feature for describing and/or showing for a kind of embodiment can be in a manner of same or similar one or more It is used in a other embodiment, it is combined with the feature in other embodiment, or substitute the feature in other embodiment.
It should be emphasized that term "comprises/comprising" refers to the presence of feature, one integral piece, step or component when being used herein, but simultaneously It is not excluded for the presence or additional of one or more other features, one integral piece, step or component.
Description of the drawings
In order to more clearly explain the embodiment of the invention or the technical proposal in the existing technology, to embodiment or will show below There is attached drawing needed in technology description to be briefly described, it should be apparent that, the accompanying drawings in the following description is only this Some embodiments of invention for those skilled in the art without having to pay creative labor, can be with root Other attached drawings are obtained according to these attached drawings.
Fig. 1 is a kind of vacuum sintering furnace structural schematic diagram making self-lubricating workpiece that embodiment of the present invention provides;
Fig. 2 is the sectional view of Fig. 1;
Fig. 3 is the profilograph of Fig. 1;
Fig. 4 is the pressure exerting arrangement structural schematic diagram of Fig. 1;
Fig. 5 is a kind of vacuum sintering method flow chart making self-lubricating workpiece that embodiment of the present invention provides.
Specific implementation mode
In order to make those skilled in the art more fully understand the technical solution in the present invention, below in conjunction with of the invention real The attached drawing in example is applied, technical scheme in the embodiment of the invention is clearly and completely described, it is clear that described implementation Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common The every other embodiment that technical staff is obtained without making creative work, should all belong to guarantor of the present invention The range of shield.
It should be noted that when element is referred to as " being set to " another element, it can be directly on another element Or there may also be elements placed in the middle.When an element is considered as " connection " another element, it can be directly connected to To another element or it may be simultaneously present centering elements.Term as used herein " vertical ", " horizontal ", " left side ", " right side " and similar statement for illustrative purposes only, are not offered as being unique embodiment.
Unless otherwise defined, all of technologies and scientific terms used here by the article and belong to the technical field of the present invention The normally understood meaning of technical staff is identical.Used term is intended merely to description tool in the description of the invention herein The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term as used herein "and/or" includes one or more Any and all combinations of relevant Listed Items.
It please refers to Fig.1 to Fig.4, a kind of vacuum-sintering furnace structure making self-lubricating workpiece is provided in embodiment of the present invention Schematic diagram.Wherein, self-lubricating workpiece 22 includes but not limited to self-lubricating bearing, self-lubricating slide board.The making self-lubricating workpiece Vacuum sintering furnace includes:Vacuum furnace body;The vacuum furnace body is communicated with exhaust equipment;Flue 5 in the vacuum furnace body, The flue 5 is equipped with the heating element 26 for sintered self-lubricated workpiece 22;The pressure exerting arrangement being connect with the flue 5;Institute Pressure can be applied to the surface of the self-lubricating workpiece 22 by stating pressure exerting arrangement.
The vacuum sintering furnace for the making self-lubricating workpiece that present embodiment is provided utilizes pressure by being equipped with pressure exerting arrangement Mechanism applies pressure on the surface of sintering workpiece 22, and 22 surface of workpiece is made to carry out densification sintering in the state of having pressure, real The technique for having showed once sintered completion reduces the cumbersome technique of repeatedly rolling sintering.
Meanwhile the vacuum sintering furnace of making self-lubricating workpiece that present embodiment is provided is by being equipped with vacuum furnace body, and Flue 5 is set in vacuum furnace body, realizes and is sintered under vacuum totally-enclosed state, is not necessarily to atmosphere protection, this aspect subtracts The loss of few protective gas, does not discharge externally when being on the other hand sintered, realizes pollution-free and clean environment, and avoid making With the generation of hydrogen insecurity.
In addition, the vacuum sintering furnace for the making self-lubricating workpiece that present embodiment is provided is certainly by being equipped with vacuum furnace body The sintering for lubricating workpiece 22 provides vacuum environment, is made in the way of vacuum oil immersion in self-lubricating workpiece 22 by the vacuum environment Portion oil content increases, and when surface forms tiny structure to workpiece 22 in the case of both surface friction, makes internal oil is automatic to overflow.
In the present embodiment, pressure exerting arrangement can apply mechanical pressure to the surface of self-lubricating workpiece 22.The flue 5 Inside it is additionally provided with the support base 25 for being used to support 22 lower surface of self-lubricating workpiece.Wherein, the pressure exerting arrangement includes being located at institute It states in flue 5 and the pressure head 8 that 22 upper surface of self-lubricating workpiece can be pushed, the pushing component being connect with the pressure head 8;Institute Stating pushing component includes:Be threaded through the courage wall of the flue 5 and lifting cylinder sleeve 13 on the chamber wall of the vacuum furnace body, with And the cylinder 14 outside the vacuum furnace body.One end of the lifting cylinder sleeve 13 connects the cylinder 14, the other end connects institute State pressure head 8.
Further, multiple pressure exerting arrangements are arranged along first direction;Multiple support bases 25 are along the first party To arrangement.Wherein, first direction can be the length direction of vacuum furnace body.In the present embodiment, vacuum furnace body is horizontal circle Barrel structure, and target site location is supported in by stove leg 21.The pressure head 8 and support base 25 are graphite material.It is described Heating element 26 includes graphite, molybdenum or MoSi2At least one of.For example, heating element 26 can be Si-Mo rod, graphite heating Band, silicon molybdenum heating tape.
As shown in Figures 1 to 4, the pressure exerting arrangement is in flue 5(Cavity)Top can be designed as it is multiple, pressure The pressure head 8 of mechanism can be made by graphite material.Pressure uses cylinder 14 to be used as pressure output, cylinder 14 and graphite material It is the lifting cylinder sleeve 13 equipped with water cooling plant 44 between the pressure head 8 of matter.13 top of lifting cylinder sleeve passes through bolt cylinder and cylinder 14 It is connected, 8 center of graphite pressure head is connected again by screw rod 45 with lifting cylinder sleeve 13.The applying mechanism relies on the liter of cylinder 14 It drops to realize the lifting of graphite pressure head 8.Lifting cylinder sleeve 13 is sealed using vacuum-packed method and vacuum furnace body courage.
Wherein, the cylinder 14 is connected with pneumatic control valve;The pneumatic control valve can control the pressure of the cylinder 14, And then adjust surface pressing of the pressure head 8 to the self-lubricating workpiece 22.The pressure size of cylinder 14 is controlled by gas pressure Valve is realized to the control of the pressure of lifting cylinder 14, to achieve the purpose that adjust compacting sintering surface pressure.
Pressure exerting arrangement as shown in Figure 4, top is cylinder 14, intermediate for lifting cylinder sleeve 13, and the medium design of cylinder sleeve 13 has Cooling line 44.The cooling line 44 may include water inlet pipe and return pipe.The lower part of lifting cylinder sleeve 13 is connected with graphite material Pressure head 8, the centre of graphite pressure head 8 is connecting hole, and by heat resisting steel bolt with lifting cylinder sleeve 13 be connected.
Specifically, lifting cylinder sleeve 13 connects cylinder 14.Specifically, screw rod can be passed through between lifting cylinder sleeve 13 and cylinder 14 To realize support.The link position of the pressure exerting arrangement and the flue 5 is equipped with sealing structure.Specifically, lifting 13 He of cylinder sleeve Vacuum sealing between flue 5 passes through flue 5(It is referred to as furnace body)On interface 12 realize that lifting cylinder sleeve 13 passes through should Interface 12 realizes sealing between interface 12 and lifting cylinder sleeve 13 by sealing rubber ring.The pressure head 8 of heating room inside vacuum furnace body It is made for graphite material, and cylinder 14 is used to be used as pressure output, the pressure size of cylinder 14 is by gas-pressure controlling valve It realizes to the control of the pressure of lifting cylinder 14, to achieve the purpose that adjust compacting sintering surface pressure.
The vacuum furnace body includes the lid 23 of cylinder 6 and lid conjunction in 6 one end of cylinder;The lid 23 and the cylinder Hinge connection is used between body 6, and is locked by zigzag retainer.The length direction of the vacuum furnace body is parallel with horizontal plane; The vacuum furnace body has container outer wall and container inner wall;The first water cooling is equipped between the container outer wall and container inner wall Gap.
In the present embodiment, the opening and closing of retainer can be controlled by cylinder, and can be grasped with button switch Make.The main trepanning of furnace body has 9 thermometer holes, heating electrode hole, thermocouple hole, safe valve opening, qi of chong channel ascending adversely deflation valve opening, high pressure Wind turbine wiring hole, heat exchanger hole cooling water hole, pressure transmitter hole etc..
Specifically, the vacuum furnace body is horizontal circular, double-layer steel plate structure may be used in the wall of vacuum furnace body.The vacuum drying oven Body can be made of the lid 23 of the cylinder 6 of intermediate double-layer heating, double-layer structure.Lid 23 is equipped with ring flange 11.First water Cold clearance is present in lid 23 on cylinder 6, and the first water cooling gap is used for the flowing of cooling water.For ease of the flowing of cooling water, To preferably radiate, double-layer interlayer(First water cooling gap)Inside it is additionally provided with cooling water water conservancy diversion guide plate.
As shown in Figure 1 to Figure 3, it is interconnected by rocking arm fixed seat 34, rocking arm 35 between cylinder 6 and lid 23. Cylinder 6 is equipped with charge valve interface 31, thermocouple interface 32, electrode interface 33 and electrode 37, vent valve 38, pressure sensor 39, relief valve connection(15、36), at least one of heat exchanger interface 16 and stove leg 21.Wherein, pressure sensor 39 can To detect the pressure size in vacuum furnace body.Electrode 37 connects above-mentioned heating element 26 by electrode interface 33, to be heating Element 26 is powered.
Specifically, the trepanning on cylinder 6 includes mainly:9 thermometer holes, heating electricity for measuring vacuum furnace body temperature Pole hole(Electrode interface 33), thermocouple hole(The connector of following temperature measurement components), safe valve opening(For connection safety valve door), punching Gas deflation valve opening, high pressure positive blower wiring hole(Following wind turbines connect string holes), heat exchanger hole cooling water hole, pressure transmitter hole(Institute The service cable for stating heating element 26 connects the pressure transmitter hole, to be connect with pressure transmitter)Deng.
The exhaust equipment include detect the vacuum meter of vacuum degree in vacuum furnace body, be connected with the vacuum furnace body it is true Sky pump and the water cooling component for being cooled down to the vacuum pump.Wherein, vacuum furnace body is equipped with and vacuumizes interface 10.Vacuum pump May include slide valve pump, sliding vane rotary pump 41 or lobe pump 40.Wherein, slide valve pump or sliding vane rotary pump 41 can be used as fore pump, lobe pump 40 can be used as main pump.Specifically, the exhaust equipment can also have cap of high-vacuum baffle valve 43, electromagnetic belt vent valve 38, manually The elements such as vent valve 38, valve for pressure difference, bellows 42.The exhaust equipment can make the vacuum degree in the vacuum furnace body reach 6* 10-1Pa to 7*10-1Pa.Preferably, the final vacuum that the exhaust equipment can be formed is up to 6.7*10-1Pa。
As shown in Figure 2 and Figure 3, the courage wall of the flue 5 is equipped with insulating layer.The heat preservation layer material carbon felt or graphite Felt structure.Flue 5 is equipped with heating element 26, insulating part 3, heating siege support base 251, heating element support base 252, heating Electrode 4(It can be connected with above-mentioned electrode 37), pressure head interface 12, graphite pressure head 8, lifting cylinder sleeve 13, cylinder 14, pressure head 8 pad Plate 9 and self-lubricating workpiece 22, cooling air channel 24, siege pillar(The support base 25), heat preservation deflector 27 and heating power supply Transformer etc..26 material of heating element can be that high purity graphite or molybdenum heat band structure.The insulating part 3 is 99 potteries Porcelain piece, the heating siege(One kind of heating element 26)It is graphite with 8 material of pressure head.
In the present embodiment, the vacuum sintering furnace for making self-lubricating workpiece further includes PID controller and thermometric Component.The temperature measurement component can detect the sintering temperature in the flue 5;The PID controller and the temperature measurement component, institute It states heating element 26 to be connected, the heating temperature of the heating element 26 is controlled with the sintering temperature detected according to the temperature measurement component Degree.
Specifically, the heating element 26 can connect silicon-controlled heating pressure regulator.In this way, the confession of the heating element 26 Electricity is powered using low-voltage, high current mode, and carry out closed loop control using silicon-controlled heating pressure regulator as core, can be real Now the braking of heating pid parameter is adjusted.Temperature thermocouple may be used in the temperature measurement component, specifically, temperature thermocouple uses Twin-core S types(Platinum rhodium 10- platinum)Thermocouple, a core are used for temperature control, and another core is for record and overtemperature alarm.
In the present embodiment, the vacuum sintering furnace of the making self-lubricating workpiece further includes:Wind cooling unit;The air-cooled list Member is passed through the inside of the vacuum furnace body;The flue 5 be equipped with the air inlet communicated inside vacuum furnace body and with heat exchange The gas outlet that device communicates.Heat exchanger gas after cooling can be re-entered flue by the wind cooling unit through the air inlet In 5.Specifically, the wind cooling unit includes wind turbine and cooling air source;The cooling air source is connected to 5 inside of the flue, To input inert gas into flue 5;The wind turbine can drive gas to be inputted in flue 5 by the air inlet.The heat exchanger (Cooling heat exchanger)It is installed in vacuum furnace body, and in the downstream of wind turbine outlet air.
In the present embodiment, the vacuum sintering furnace of the making self-lubricating workpiece further includes:Water cooling unit.The wind turbine is also Equipped with the cover of double-casing motor 19 20.The cover of double-casing motor 19 20 is connected with cylinder 6 by flange 18.20 tool of the cover of the double-casing motor 19 There is the second water cooling gap.The water cooling unit and first water cooling gap, the second water cooling gap and the water cooling component phase Connection, to supply cold water to the first water cooling gap, the second water cooling gap and the water cooling component.Wherein, water cooling Unit can be water circulating pump.
Specifically, the two poles of the earth high-voltage motor 19 forms wind turbine with the installation of impeller 30.The air outlet position or vacuum drying oven of wind turbine The air inlet position of body is equipped with wind guiding device 17.Wind guiding device 17 can be equipped with deflector 29.Draught fan impeller 30 is directly pacified It is installed together on the output shaft of motor 19 and with the other end of cylinder 6 back to lid 23.When self-lubricating workpiece 22 heats After when being cooled down, be filled with the inert gas of great Yue≤1bar into stove using the charge valve interface 31 by air source, Starting fan, air-flow is from wind turbine by heating room(The inside of vacuum chamber is known as heating room)Crack between flue 5 is rapid Workpiece 22 is blowed to, the thermal current come out from self-lubricating workpiece 22 is cooled down by gas outlet to heat exchanger 28, is handed over by heat 28 gas after cooling of parallel operation presses to self-lubricating workpiece 22 by wind turbine again, forms a circulation loop.
Meanwhile the inert gas of circulative convection can be made further fully cold using the first water cooling gap of vacuum furnace body But, to accelerate the cooling velocity of self-lubricating workpiece 22.The startup of the motor 19 of high pressure positive blower uses the side of frequency converter or soft start Formula, had not only reduced the impact of Current on Grid when motor 19 starts, but also can realize the adjusting of cooling velocity.It is cold in vacuum furnace body But heat exchanger is full red copper heat exchanger structure, and uses square array type structure.Welding is arranged at the copper pipe top of the cooling heat exchanger Formula fin, favorably with the absorption of heat, the efficiency with the evenly distributed raising heat absorption of copper tube with fins.
The air source can not only realize being quickly cooled down for part, additionally it is possible to realize heating when improve temperature uniformity it With.Air source can also connect that charge valve, electromagnetism are micro- to fill valve, manual flow control valve, fast when realizing cooling to both can control Speed inflation, and the vacuum degree in vacuum furnace body can be kept in a certain range, coming by the setting of vacuum meter by PLC controls Meet the pressurize heating uniform needs of furnace temperature.
The electric-control system of the vacuum sintering furnace of the making self-lubricating workpiece(Including above-mentioned gas pressure-control valve, PID control Device or even the controller of fan, Water-cooling circulating pump controller)Touch screen industrial computer may be used, be used for operating personnel Real-time, interactive.The slave computer of system uses programmable controller, is used for spot sensor part interactive information, realizes according to technique Flow automatically controls the operation of vacuum furnace body equipment components.The operation and monitoring of the vacuum sintering furnace of the making self-lubricating workpiece There is touch screen industrial computer to realize completely, it mainly have monitoring interface, alert interface, automatic running interface, formula interface, Manual interface, parameter setting, 7, curve interface interface composition.
Below by detailed description present embodiment making self-lubricating workpiece vacuum sintering furnace the course of work, so as to The preferably connection present invention.
The vacuum sintering furnace basic operation for making self-lubricating workpiece is as follows:Manual blow-on door fills workpiece 22, closes fire door →(Condition:Parameter setting alarm free(Parameters are set in parameter setting interface:Such as inflate superpressure pressure alarm 0.2MPa, cold But 100 degree of maximum temperature, 40 entry condition 800Pa of lobe pump, in-furnace temperature alarm maximum temperature in the stove that retainer is opened after 1200 degree, heating when minimum vacuum alarm vacuum degree 133Pa, minimum hydraulic pressure pressure alarm 0.1MPa, return water temperature alarm 35 degree, Deng)→ auto-start button opens → slide valve pump open (11KW) → main road flapper valve 43 open (solenoid valve) →(Condition:Vacuum degree 800Pa or more)Lobe pump 40 open (5.5KW) →(Condition:Vacuum degree is in 10Pa or more)(Heating process curve is finished)Heating is opened (150KW)→ (heating curves → end of run) heating pass → 43 passes of the main road vacuum flapper valve → pass of lobe pump 40 (5.5KW) → Slide valve pump, which closes (11KW) → charge valve, opens (solenoid valve) → (condition:Pressure selection pressure is charged to position) charge valve pass (solenoid valve) → Wind turbine opens (55KW) → (condition:Temperature is at 100 degree hereinafter, setting delay time arrives) wind turbine pass → (condition:Temperature is at 100 degree Vent valve opens (solenoid valve) → (delay 3 minutes, pressure is equal with air) vent valve pass → unit vent valve and opens (electromagnetism below) Valve) →(Delay 30 seconds)Unit vent valve pass → slide valve pump open (11KW) → main road flapper valve 43 open (solenoid valve) →(5 points of delay Clock)Retainer open (solenoid valve) →(Retainer reaches position)Slide valve pump closes (11KW) → main road flapper valve 43 and closes (solenoid valve) → technique It completes alarm → manual feeding and closes stove.
It is if you need to the operation for controlling into internal pressure during automatic running:Partial pressure switch opens → and lobe pump 40 closes → it micro- fills Valve opens →(Flow switching valve is adjusted manually)(Condition:Vacuum degree, which reaches, reaches the standard grade)It is micro- fill valve close →(Condition:Under vacuum degree reaches Line)It is micro- fill valve open →(Condition:Vacuum degree, which reaches, reaches the standard grade)Micro- valve that fills closes → reciprocation cycle successively, and if you need to close, partial pressure switch is opened →(Delay 1 minute)Lobe pump 40 is opened.
Referring to Fig. 5, the present invention also provides a kind of vacuum sintering method making self-lubricating workpiece, include the following steps:
S1, agglomerated material is obtained;
S2, it suppresses the agglomerated material to form embryo material;
S3, the embryo material is pasted on sintered base plate;
S4, the embryo material on the sintered base plate is sintered in vacuum environment, the embryo material surface is applied in sintering process Pressure;
S5, the workpiece formed after sintering is cooled down and takes out progress immersion oil processing.
Wherein, in step sl, the agglomerated material can be copper alloy powder(It wherein can be copper-iron alloy).It is obtaining It takes the copper alloy powder of sinter layer last, copper alloy powder input batch mixer is stirred uniformly mixed.It will mix again equal Even copper alloy powder carries out compacting and forms embryo material.
It to be formed in embryo material in described suppress the copper alloy powder, pressing pressure is 3-5T/cm every square centimeter2, pressure The embryo material size of system is controlled in 100cm2Within.Requirement of the thickness of compacting according to product, it is preferred that the embryo material thickness of compacting is small In or equal to 5 millimeters.In this step, the embryo material shape of compacting is rectangular blocks or axle sleeve shape.
The embryo material is pasted on sintered base plate in step described, the embryo material can be pasted on burning using glue Tie substrate(Usually steel plate)Surface on.Also, when pasting between embryo material and embryo material(As possible)It is adjacent to.In the upper of sintered base plate Surface and lower surface are pasted with embryo material, and then double-deck plate posted is put into sintering furnace and is sintered.
In step s 4, sintering furnace provides vacuum environment.It is both needed to place above and below substrate when putting sintered base plate Graphite planar.The graphite planar all covers the embryo material on sintered base plate.It is burnt by the pressure head compression of sintering furnace on top Knot.Wherein, the vacuum degree of the vacuum environment reaches 6*10-1Pa to 7*10-1Pa.Preferably, the vacuum degree of vacuum environment is general It will be 6.7 × 10-1Pa or so.It forms vacuum environment and two-stage vacuum pump may be used, there is sliding vane rotary pump or slide valve pump and Roots's pump group Unit is vacuumized at two-stage.In the step S4, sintering temperature is within 920 degree to 1000 degree.Sintering is completed, in sintering furnace Interior to be cooled down by heat exchange, the product of sintering, which is cooled to 100 degree or less, to be taken out.
In step s 5, the workpiece taken out in sintering furnace is put into progress immersion oil processing in vacuum oil immersion equipment.Immersion oil Finishing can metalworking formation self-lubricating finished workpart.The vacuum sintering method of the making self-lubricating workpiece can utilize above-mentioned system Make the vacuum sintering furnace of self-lubricating workpiece, it is of course possible to which, using the sintering furnace of other constructions, present embodiment is not limited thereto.
Present embodiment provided making self-lubricating workpiece vacuum sintering method by using vacuum-sintering mode, It is pre-configured with a kind of copper alloy powder, the main component of the alloyed powder is to carry low melting point, in sintering process, due to the work of vacuum With, therefore the powder for being readily able to melt is taken away, and microcosmic porous state is formed.The vacuum sintering method of the making self-lubricating workpiece is main It is to be easily formed porous, the porous organization of the copper-clad iron of self-assembling formation after being sintered such as copper-iron alloy using the natural thawing of powder Deng.In view of the wearability of the frictional layer of sintering, the formula of sinter layer has certain more characteristics, it not only have can be formed it is microcosmic Porous organization, it is often more important that sinter layer itself has very strong wearability and seizure resistance.
Herein cited any digital value all include between lower limiting value to upper limit value with the lower value of an incremented and The all values of upper value, there are the intervals of at least two units between any lower value and any much higher value.For example, such as Fruit elaborates the quantity or process variable of a component(Such as temperature, pressure, time etc.)Value be from 1 to 90, preferably from 20 To 80, more preferably from 30 to 70, then purpose is arrived in order to illustrate also clearly listing such as 15 to 85,22 in the specification 68,43 to 51,30 to 32 is equivalent.For the value less than 1, suitably think that a unit is 0.0001,0.001,0.01,0.1. These are only intended to the example clearly expressed, it is believed that the numerical value enumerated between minimum and peak is possible to Combination is all expressly set forth in the specification in a similar manner.
Unless otherwise indicated, all ranges all include all numbers between endpoint and endpoint.It is used together with range " about " or " approximation " be suitable for two endpoints of the range.Thus, " about 20 to 30 " are intended to covering " about 20 to about 30 ", including at least the endpoint indicated.
All articles and reference disclosed, including patent application and publication, for various purposes by quoting knot Together in this.The term " substantially by ... constitute " for describing combination should include identified element, ingredient, component or step and reality Other elements, ingredient, component or the step of the basic novel feature of the combination are not influenced in matter.Using term "comprising" or " comprising " describes the combination of element here, ingredient, component or step it is also contemplated that substantially by these elements, ingredient, component Or the embodiment that step is constituted.Here by using term " can with ", it is intended to illustrate that " can with " includes described any Attribute is all optional.
Multiple element, ingredient, component or step can be provided by single integrated component, ingredient, component or step.Optionally Ground, single integrated component, ingredient, component or step can be divided into multiple element, ingredient, component or the step of separation.It is used for The open "a" or "an" for describing element, ingredient, component or step is not said to exclude other elements, ingredient, component Or step.
It should be understood that above description is to illustrate rather than to be limited.By reading above-mentioned retouch It states, many embodiments and many applications except the example provided all will be aobvious and easy for a person skilled in the art See.Therefore, the range of this introduction should not be determined with reference to foregoing description, but should with reference to appended claims and this The full scope of the equivalent that a little claims are possessed determines.For comprehensive purpose, all articles and with reference to including special The disclosure of profit application and bulletin is all by reference to being incorporated herein.Theme disclosed herein is omitted in preceding claims Any aspect is not intended to abandon the body matter, also should not be considered as inventor the theme is not thought of as it is disclosed A part for subject matter.

Claims (11)

1. a kind of vacuum sintering furnace making self-lubricating workpiece, which is characterized in that including:
Vacuum furnace body;The vacuum furnace body is communicated with exhaust equipment;
Flue in the vacuum furnace body, the flue are equipped with the heating element for sintered self-lubricated workpiece;
The pressure exerting arrangement being connect with the flue;The pressure exerting arrangement can apply pressure to the surface of the self-lubricating workpiece.
2. making the vacuum sintering furnace of self-lubricating workpiece as described in claim 1, it is characterised in that:It is additionally provided in the flue It is used to support the support base of self-lubricating workpiece lower surface;
The pressure exerting arrangement include be located in the flue and can to pressure head that the self-lubricating workpiece surface pushes, with it is described The pushing component of pressure head connection;The pushing component includes:It is threaded through the courage wall of the flue and the appearance of the vacuum furnace body Lifting cylinder sleeve on wall and the cylinder outside the vacuum furnace body;One end connection cylinder of the lifting cylinder sleeve, The other end connects the pressure head.
3. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 2, it is characterised in that:Multiple pressure exerting arrangements It is arranged along first direction;Multiple support bases are arranged along the first direction.
4. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 2 or claim 3, it is characterised in that:The pressure head and Support base is graphite material;The heating element includes at least one of graphite, molybdenum or MoSi2.
5. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 2, it is characterised in that:The cylinder is connected with gas Pressure control valve;The pneumatic control valve can control the pressure of the cylinder, and then adjust the pressure head to the self-lubricating workpiece Surface pressing.
6. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 2, it is characterised in that:Further include PID controller, And temperature measurement component;The temperature measurement component can detect the sintering temperature in the flue;The PID controller and the thermometric Component, the heating element are connected, and adding for the heating element is controlled with the sintering temperature detected according to the temperature measurement component Hot temperature.
7. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 6, it is characterised in that:Further include:Wind cooling unit; The wind cooling unit is passed through the inside of the vacuum furnace body;The flue be equipped with the air inlet communicated inside vacuum furnace body, And the gas outlet communicated with heat exchanger;The wind cooling unit can be salty through the air inlet by heat exchanger gas after cooling In new input flue.
8. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 7, it is characterised in that:The wind cooling unit includes Wind turbine and cooling air source;It is connected to inside the cooling air source and the flue, to input inert gas into flue;It is described Wind turbine can drive gas to be inputted in flue by the air inlet.
9. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 8, it is characterised in that:Further include water cooling unit, The length direction of the vacuum furnace body is parallel with horizontal plane;The vacuum furnace body has container outer wall and container inner wall;It is described The first water cooling gap is equipped between container outer wall and container inner wall;
The exhaust equipment includes detecting the vacuum meter of vacuum degree in vacuum furnace body, the vacuum pump being connected with the vacuum furnace body And the water cooling component for being cooled down to the vacuum pump;The wind turbine is additionally provided with double-layer electric hood;The double-layer electric hood tool There is the second water cooling gap;
The water cooling unit is connected with first water cooling gap, the second water cooling gap and the water cooling component, with to institute State first water cooling gap, the second water cooling gap and water cooling component supply cold water.
10. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 9, it is characterised in that:The exhaust equipment energy The vacuum degree in the vacuum furnace body is set to reach 6*10-1Pa to 7*10-1Pa。
11. making the vacuum sintering furnace of self-lubricating workpiece as claimed in claim 9, it is characterised in that:The vacuum furnace body packet It includes cylinder and covers the lid closed in cylinder one end;Hinge connection is used between the lid and the cylinder, and passes through sawtooth Shape retainer is locked;The courage wall of the flue is equipped with insulating layer;The link position of the pressure exerting arrangement and the flue is equipped with close Seal structure.
CN201810122033.1A 2018-02-07 2018-02-07 A kind of vacuum sintering furnace making self-lubricating workpiece Pending CN108278894A (en)

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CN108405854A (en) * 2018-02-07 2018-08-17 苏州金言来新材料科技有限公司 A kind of vacuum sintering method making self-lubricating workpiece
CN109931780A (en) * 2019-01-10 2019-06-25 嘉兴市鹏程磁钢有限公司 A kind of magnet steel vacuum sintering furnace
CN112331471A (en) * 2020-11-17 2021-02-05 江西理工大学 Sintering device for sintering neodymium-iron-boron magnet and using method thereof
CN115466122A (en) * 2022-06-21 2022-12-13 陕西固勤材料技术有限公司 Preparation system of reaction sintering carborundum roller stick
CN116379767A (en) * 2022-12-26 2023-07-04 无锡海古德新技术有限公司 Three-dimensional hot-pressing vibration sintering furnace
CN117428189A (en) * 2023-12-19 2024-01-23 厦门大鸿翰金属材料科技有限公司 Cemented carbide sintering process

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Publication number Priority date Publication date Assignee Title
CN108405854A (en) * 2018-02-07 2018-08-17 苏州金言来新材料科技有限公司 A kind of vacuum sintering method making self-lubricating workpiece
CN109931780A (en) * 2019-01-10 2019-06-25 嘉兴市鹏程磁钢有限公司 A kind of magnet steel vacuum sintering furnace
CN112331471A (en) * 2020-11-17 2021-02-05 江西理工大学 Sintering device for sintering neodymium-iron-boron magnet and using method thereof
CN112331471B (en) * 2020-11-17 2022-04-26 江西理工大学 Sintering device for sintering neodymium-iron-boron magnet and using method thereof
CN115466122A (en) * 2022-06-21 2022-12-13 陕西固勤材料技术有限公司 Preparation system of reaction sintering carborundum roller stick
CN116379767A (en) * 2022-12-26 2023-07-04 无锡海古德新技术有限公司 Three-dimensional hot-pressing vibration sintering furnace
CN116379767B (en) * 2022-12-26 2023-10-10 无锡海古德新技术有限公司 Three-dimensional hot-pressing oscillation sintering furnace
CN117428189A (en) * 2023-12-19 2024-01-23 厦门大鸿翰金属材料科技有限公司 Cemented carbide sintering process
CN117428189B (en) * 2023-12-19 2024-03-08 厦门大鸿翰金属材料科技有限公司 Cemented carbide sintering process

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