CN108276959A - A kind of automobile Novel anti-mist agent and its process - Google Patents
A kind of automobile Novel anti-mist agent and its process Download PDFInfo
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- CN108276959A CN108276959A CN201711141485.6A CN201711141485A CN108276959A CN 108276959 A CN108276959 A CN 108276959A CN 201711141485 A CN201711141485 A CN 201711141485A CN 108276959 A CN108276959 A CN 108276959A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/18—Materials not provided for elsewhere for application to surfaces to minimize adherence of ice, mist or water thereto; Thawing or antifreeze materials for application to surfaces
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Abstract
The invention discloses a kind of automobile Novel anti-mist agent of the production technical field of antifoggant, the composition of the automobile Novel anti-mist agent includes in parts by weight：Acetylcholine bromide：1~2 part；Phenacetin：1~2 part；Lauryl sodium sulfate：1~3 part；Sodium secondary alkyl sulfonate：1~3 part；Fatty alcohol sodium isethionate：1~3 part；Cocoanut fatty acid diethanolamide：0.5~2 part；Hydroxyl synthol polyoxyethylene：0.5~2 part；Alkyl glycosides：0.5~2 part；Sodium citrate：0.2~1 part；Glacial acetic acid：2~7 parts；Absolute ethyl alcohol：60~75 parts；Water softening agent：8~15 parts；Preservative：0.2~1 part；Water：16~32 parts, the process of the automobile Novel anti-mist agent includes the following steps：Sorting, stirring, batch mixing, filtering and finished product, the antifoggant can quick demisting, while persistence and lower temperature resistance greatly improve.
Description
Technical field
The present invention relates to the production technical field of antifoggant more particularly to a kind of automobile Novel anti-mist agent and its technique sides
Method.
Background technology
Glass surface fogging leverages the transmission of light, the reason is that small droplets form is formed in glass surface
Many spherical small water droplets, and each small water droplet all plays a part of lens, and light is scattered towards all directions or is not advised
It then reflects, to prevent external light from being directed through.Therefore external image just produce one cannot see clearly it is fuzzy
Image, and the curvature of water droplet is bigger, the scattering and irregular reflection of light are more apparent, especially in cold winter or rainy season,
Vapor in driver's cabin or in interior hot-air can be condensed into dewdrop in cold glass surface, substantially reduce the light transmission of glass
Rate influences sight, brings big inconvenience to driving, or even can cause danger, existing solution has：1, heat transfer is developed
Undesirable glass blows hot wind in glass inner face, it is therefore an objective to not make to drop to dew point or less at a temperature of glass inner face；2, with removing
Wet device reduces indoor humidity；3, one layer of anti-fog thin film is coated on glass；4, one layer of antifoggant is smeared on glass, even if water steams
Vapour condenses in glass surface, does not also allow it to exist with drops, but it is made to be changed into the high moisture film of transparency, but the
One, two kinds of methods install air-conditioning in medium-to-high grade automobile and use anti-fog properties preferable windshield, but to most of masses
Change automobile, such as truck, bus, this method is too expensive, the third method, must be applied in the manufacturing process of glass, work
Skill is complicated, and processes inconvenience to finished glass；Fourth method, using antifoggant, antifoggant traditional at present mainly has following
It is several：1, the glass antidimmer of hydrophobic coating is formed in glass surface after use, mainly by metallic soap, silicon, zirconium compounds etc.
Lyophobic dust is formulated.Such antifoggant using effect is general, and lower temperature resistance is poor, inconvenient to use；2, after use
Glass surface formed hydrophilic coating glass antidimmer, mainly using water soluble surfactant active as main component prepare and
At such antifoggant effect is fair, but effect persistence and lower temperature resistance are low, for this purpose, we have proposed a kind of automobile is new
Type antifoggant and its process.
Invention content
The purpose of the present invention is to solve antifoggant effect persistence in the prior art and lower temperature resistance are low, and propose
A kind of automobile Novel anti-mist agent and its process.
To achieve the goals above, present invention employs following technical solutions：A kind of automobile Novel anti-mist agent, the automobile
Include in parts by weight with the composition of Novel anti-mist agent：
Acetylcholine bromide：1~2 part；
Phenacetin：1~2 part；
Lauryl sodium sulfate：1~3 part；
Sodium secondary alkyl sulfonate：1~3 part；
Fatty alcohol sodium isethionate：1~3 part；
Cocoanut fatty acid diethanolamide：0.5~2 part；
Hydroxyl synthol polyoxyethylene：0.5~2 part；
Alkyl glycosides：0.5~2 part；
Sodium citrate：0.2~1 part；
Glacial acetic acid：2~7 parts；
Absolute ethyl alcohol：60~75 parts；
Water softening agent：8~15 parts；
Preservative：0.2~1 part；
Water：16~32 parts.
Preferably, the water softening agent+preservative：Water=1：2.
Preferably, the preservative is sodium benzoate.
The process of a kind of process of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes following step
Suddenly：
S1：Stock：Acetylcholine bromide is weighed in parts by weight：1~2 part；Phenacetin：1~2 part；Dodecyl sulphur
Sour sodium：1~3 part；Sodium secondary alkyl sulfonate：1~3 part；Fatty alcohol sodium isethionate：1~3 part；Coco-nut oil fatty acid diethanol
Amide：0.5~2 part；Hydroxyl synthol polyoxyethylene：0.5~2 part；Alkyl glycosides：0.5~2 part；Sodium citrate：0.2~1
Part；Glacial acetic acid：2~7 parts；Absolute ethyl alcohol：60~75 parts；Water softening agent：8~15 parts；Preservative：0.2~1 part；Water：16~
32 parts；
S2：Stirring：The water that will be weighed in step S1：16~32 parts are taken out part as basic liquid, by the basal liquid of taking-up,
Glacial acetic acid：2~7 parts and absolute ethyl alcohol：60~75 parts are added in reaction kettle and stir, until stopping stirring when reaction starts heat release
It mixes, obtains solution A, for future use, by lauryl sodium sulfate：1~3 part；Sodium secondary alkyl sulfonate：1~3 part；Fatty alcohol hydroxyl second
Base sodium sulfonate：1~3 part；Cocoanut fatty acid diethanolamide：0.5~2 part；Hydroxyl synthol polyoxyethylene：0.5~2 part；
Alkyl glycosides：0.5~2 part is put into successively in another reaction kettle, is stood 15 minutes after being sufficiently mixed uniformly, is obtained molten
Liquid B, for future use；
S3：Batch mixing：Into step S2 to solution B in sodium citrate is added：It 0.2~1 part, is sufficiently mixed, stands 15
The solution A obtained in step S2 is added after minute, the rear water that remainder in step S2 is added is added in solution, is sufficiently stirred
30 minutes, object to be mixed was in clear state, obtains mixed liquor；
S4：Filtering：The mixed liquor obtained in step S3 is crossed into 300 mesh sieve, obtains antifoggant semi-finished product；
S5：Finished product：Antifoggant semi-finished product obtained in step S4 are subjected to mechanization tinning packaging, obtain antifoggant
Finished product.
In the present invention, acetylcholine bromide has strong adhesive force, surface tension small as a kind of brominated quaternary ammonium salt
Advantage can promote spreadability of the droplet on glass；Phenacetin then can further enhance bromine using its polar functional group
Change the adhesive force of acetylcholine, can quick demisting, while persistence and lower temperature resistance greatly improve.
Description of the drawings
Fig. 1 is operating procedure flow chart of the present invention.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, below in conjunction with specific embodiment, to this
Invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, not
For limiting the present invention.
Embodiment one
The composition of a kind of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes in parts by weight：
Acetylcholine bromide：1 part；
Phenacetin：1 part；
Lauryl sodium sulfate：1 part；
Sodium secondary alkyl sulfonate：1 part；
Fatty alcohol sodium isethionate：1 part；
Cocoanut fatty acid diethanolamide：0.5 part；
Hydroxyl synthol polyoxyethylene：0.5 part；
Alkyl glycosides：0.5 part；
Sodium citrate：0.2 part；
Glacial acetic acid：2 parts；
Absolute ethyl alcohol：70 parts；
Water softening agent：8 parts；
Preservative：0.2 part；
Water：14 parts.
Wherein, the water softening agent+preservative：Water=1：2；The preservative is sodium benzoate.
The process of a kind of process of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes following step
Suddenly：
S1：Stock：Lauryl sodium sulfate is weighed in parts by weight：1 part；Sodium secondary alkyl sulfonate：1 part；Fatty alcohol hydroxyl second
Base sodium sulfonate：1 part；Cocoanut fatty acid diethanolamide：0.5 part；Hydroxyl synthol polyoxyethylene：0.5 part；Alkyl glycosides：
0.5 part；Sodium citrate：0.2 part；Glacial acetic acid：2 parts；Absolute ethyl alcohol：70 parts；Water softening agent：8 parts；Preservative：0.2 part；Water：
14 parts；
S2：Stirring：The water that will be weighed in step S1：14 parts are taken out part as basic liquid, by the basal liquid of taking-up, ice vinegar
Acid：2 parts and absolute ethyl alcohol：70 parts are added in reaction kettle and stir, until reaction starts to stop stirring when heat release, obtain solution A,
For future use, by lauryl sodium sulfate：1 part；Sodium secondary alkyl sulfonate：1 part；Fatty alcohol sodium isethionate：1 part；Coconut oil
Fatty diglycollic amide：0.5 part；Hydroxyl synthol polyoxyethylene：0.5 part；Alkyl glycosides：In addition 0.5 part is put into successively
In one reaction kettle, 15 minutes are stood after being sufficiently mixed uniformly, obtains solution B, for future use；
S3：Batch mixing：Into step S2 to solution B in sodium citrate is added：It 0.2 part, is sufficiently mixed, stands 15 minutes
The solution A obtained in step S2 is added afterwards, the rear water that remainder in step S2 is added is added in solution, is sufficiently stirred 30 points
Clock, object to be mixed are in clear state, obtain mixed liquor；
S4：Filtering：The mixed liquor obtained in step S3 is crossed into 300 mesh sieve, obtains antifoggant semi-finished product；
S5：Finished product：Antifoggant semi-finished product obtained in step S4 are subjected to mechanization tinning packaging, obtain antifoggant
Finished product.
Embodiment two
The composition of a kind of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes in parts by weight：
Acetylcholine bromide：2 parts；
Phenacetin：2 parts；
Lauryl sodium sulfate：3 parts；
Sodium secondary alkyl sulfonate：3 parts；
Fatty alcohol sodium isethionate：3 parts；
Cocoanut fatty acid diethanolamide：2 parts；
Hydroxyl synthol polyoxyethylene：2 parts；
Alkyl glycosides：2 parts；
Sodium citrate：1 part；
Glacial acetic acid：7 parts；
Absolute ethyl alcohol：75 parts；
Water softening agent：15 parts；
Preservative：1 part；
Water：28 parts.
Wherein, the water softening agent+preservative：Water=1：2；The preservative is sodium benzoate.
The process of a kind of process of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes following step
Suddenly：
S1：Stock：Lauryl sodium sulfate is weighed in parts by weight：3 parts；Sodium secondary alkyl sulfonate：3 parts；Fatty alcohol hydroxyl second
Base sodium sulfonate：3 parts；Cocoanut fatty acid diethanolamide：2 parts；Hydroxyl synthol polyoxyethylene：2 parts；Alkyl glycosides：2 parts；
Sodium citrate：1 part；Glacial acetic acid：7 parts；Absolute ethyl alcohol：75 parts；Water softening agent：15 parts；Preservative：1 part；Water：28 parts；
S2：Stirring：The water that will be weighed in step S1：28 parts are taken out part as basic liquid, by the basal liquid of taking-up, ice vinegar
Acid：7 parts and absolute ethyl alcohol：75 parts are added in reaction kettle and stir, until reaction starts to stop stirring when heat release, obtain solution A,
For future use, by lauryl sodium sulfate：3 parts；Sodium secondary alkyl sulfonate：3 parts；Fatty alcohol sodium isethionate：3 parts；Coconut oil
Fatty diglycollic amide：2 parts；Hydroxyl synthol polyoxyethylene：2 parts；Alkyl glycosides：2 parts are put into another instead successively
It answers in kettle, stands 15 minutes after being sufficiently mixed uniformly, obtain solution B, for future use；
S3：Batch mixing：Into step S2 to solution B in sodium citrate is added：It 1 part, is sufficiently mixed, after standing 15 minutes
The solution A obtained in step S2 is added, the rear water that remainder in step S2 is added is added in solution, is sufficiently stirred 30 points
Clock, object to be mixed are in clear state, obtain mixed liquor；
S4：Filtering：The mixed liquor obtained in step S3 is crossed into 300 mesh sieve, obtains antifoggant semi-finished product；
S5：Finished product：Antifoggant semi-finished product obtained in step S4 are subjected to mechanization tinning packaging, obtain antifoggant
Finished product.
Embodiment three
The composition of a kind of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes in parts by weight：
Acetylcholine bromide：1 part；
Phenacetin：2 parts；
Lauryl sodium sulfate：2 parts；
Sodium secondary alkyl sulfonate：2 parts；
Fatty alcohol sodium isethionate：2 parts；
Cocoanut fatty acid diethanolamide：1 part；
Hydroxyl synthol polyoxyethylene：1 part；
Alkyl glycosides：1 part；
Sodium citrate：0.5 part；
Glacial acetic acid：5 parts；
Absolute ethyl alcohol：60 parts；
Water softening agent：12 parts；
Preservative：0.5 part；
Water：22 parts.
Wherein, the water softening agent+preservative：Water=1：2；The preservative is sodium benzoate.
The process of a kind of process of automobile Novel anti-mist agent, the automobile Novel anti-mist agent includes following step
Suddenly：
S1：Stock：Lauryl sodium sulfate is weighed in parts by weight：2 parts；Sodium secondary alkyl sulfonate：2 parts；Fatty alcohol hydroxyl second
Base sodium sulfonate：2 parts；Cocoanut fatty acid diethanolamide：1 part；Hydroxyl synthol polyoxyethylene：1 part；Alkyl glycosides：1 part；
Sodium citrate：0.5 part；Glacial acetic acid：5 parts；Absolute ethyl alcohol：60 parts；Water softening agent：12 parts；Preservative：0.5 part；Water：22 parts；
S2：Stirring：The water that will be weighed in step S1：22 parts are taken out part as basic liquid, by the basal liquid of taking-up, ice vinegar
Acid：5 parts and absolute ethyl alcohol：60 parts are added in reaction kettle and stir, until reaction starts to stop stirring when heat release, obtain solution A,
For future use, by lauryl sodium sulfate：2 parts；Sodium secondary alkyl sulfonate：2 parts；Fatty alcohol sodium isethionate：2 parts；Coconut oil
Fatty diglycollic amide：1 part；Hydroxyl synthol polyoxyethylene：1 part；Alkyl glycosides：1 part is put into another instead successively
It answers in kettle, stands 15 minutes after being sufficiently mixed uniformly, obtain solution B, for future use；
S3：Batch mixing：Into step S2 to solution B in sodium citrate is added：It 0.5 part, is sufficiently mixed, stands 15 minutes
The solution A obtained in step S2 is added afterwards, the rear water that remainder in step S2 is added is added in solution, is sufficiently stirred 30 points
Clock, object to be mixed are in clear state, obtain mixed liquor；
S4：Filtering：The mixed liquor obtained in step S3 is crossed into 300 mesh sieve, obtains antifoggant semi-finished product；
S5：Finished product：Antifoggant semi-finished product obtained in step S4 are subjected to mechanization tinning packaging, obtain antifoggant
Finished product.
According to experimental data it is known that density, thermal coefficient and the drying shrinkage of slurry A obtained products after molding
Maximum, and the density of slurry C obtained product after molding, thermal coefficient and drying shrinkage are minimum, so slurry C is physical
Can preferably, the density of product has reached ultralight requirement, and heat-proof quality is good.
| Preservative sample | A | B | C |
| Defrosting time (s) | 63 | 59 | 55 |
| Persistence (h) | 350 | 365 | 380 |
Wherein, A is the preservative sample of embodiment one, and B is the preservative sample of embodiment two, and C is the anti-of embodiment three
Rotten agent sample, the defrosting time of C is most fast as can be seen from the table, and the time longest kept.
Claims (4)
1. a kind of automobile Novel anti-mist agent, it is characterised in that：The composition of the automobile Novel anti-mist agent wraps in parts by weight
It includes：
Acetylcholine bromide：1~2 part；
Phenacetin：1~2 part；
Lauryl sodium sulfate：1~3 part；
Sodium secondary alkyl sulfonate：1~3 part；
Fatty alcohol sodium isethionate：1~3 part；
Cocoanut fatty acid diethanolamide：0.5~2 part；
Hydroxyl synthol polyoxyethylene：0.5~2 part；
Alkyl glycosides：0.5~2 part；
Sodium citrate：0.2~1 part；
Glacial acetic acid：2~7 parts；
Absolute ethyl alcohol：60~75 parts；
Water softening agent：8~15 parts；
Preservative：0.2~1 part；
Water：16~32 parts.
2. a kind of automobile Novel anti-mist agent according to claim 1, it is characterised in that：Water softening agent+the anti-corrosion
Agent：Water=1：2.
3. a kind of automobile Novel anti-mist agent according to claim 1, it is characterised in that：The preservative is benzoic acid
Sodium.
4. a kind of process of automobile Novel anti-mist agent, it is characterised in that：The process of the automobile Novel anti-mist agent
Include the following steps：
S1：Stock：Acetylcholine bromide is weighed in parts by weight：1~2 part；Phenacetin：1~2 part；Lauryl sodium sulfate：
1~3 part；Sodium secondary alkyl sulfonate：1~3 part；Fatty alcohol sodium isethionate：1~3 part；Cocoanut fatty acid diethanolamide：
0.5~2 part；Hydroxyl synthol polyoxyethylene：0.5~2 part；Alkyl glycosides：0.5~2 part；Sodium citrate：0.2~1 part；Ice vinegar
Acid：2~7 parts；Absolute ethyl alcohol：60~75 parts；Water softening agent：8~15 parts；Preservative：0.2~1 part；Water：16~32 parts；
S2：Stirring：The water that will be weighed in step S1：16~32 parts are taken out part as basic liquid, by the basal liquid of taking-up, ice vinegar
Acid：2~7 parts and absolute ethyl alcohol：60~75 parts are added in reaction kettle and stir, until reaction starts to stop stirring when heat release, obtain
To solution A, for future use, by lauryl sodium sulfate：1~3 part；Sodium secondary alkyl sulfonate：1~3 part；Fatty alcohol isethionic acid
Sodium：1~3 part；Cocoanut fatty acid diethanolamide：0.5~2 part；Hydroxyl synthol polyoxyethylene：0.5~2 part；Alkyl sugar
Glycosides：0.5~2 part is put into successively in another reaction kettle, is stood 15 minutes after being sufficiently mixed uniformly, is obtained solution B, in case
After use；
S3：Batch mixing：Into step S2 to solution B in sodium citrate is added：It 0.2~1 part, is sufficiently mixed, stands 15 minutes
The solution A obtained in step S2 is added afterwards, the rear water that remainder in step S2 is added is added in solution, is sufficiently stirred 30 points
Clock, object to be mixed are in clear state, obtain mixed liquor；
S4：Filtering：The mixed liquor obtained in step S3 is crossed into 300 mesh sieve, obtains antifoggant semi-finished product；
S5：Finished product：Antifoggant semi-finished product obtained in step S4 are subjected to mechanization tinning packaging, obtain antifoggant at
Product.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711141485.6A CN108276959A (en) | 2017-11-17 | 2017-11-17 | A kind of automobile Novel anti-mist agent and its process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711141485.6A CN108276959A (en) | 2017-11-17 | 2017-11-17 | A kind of automobile Novel anti-mist agent and its process |
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| Publication Number | Publication Date |
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| CN108276959A true CN108276959A (en) | 2018-07-13 |
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ID=62801331
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711141485.6A Pending CN108276959A (en) | 2017-11-17 | 2017-11-17 | A kind of automobile Novel anti-mist agent and its process |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113105951A (en) * | 2021-04-12 | 2021-07-13 | 重庆多次元新材料科技有限公司 | Formula and preparation method of high-corrosion-resistance automobile glass water |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106497518A (en) * | 2016-11-01 | 2017-03-15 | 重庆返璞科技有限公司 | A kind of nano-glass antifoggant and preparation method thereof |
-
2017
- 2017-11-17 CN CN201711141485.6A patent/CN108276959A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106497518A (en) * | 2016-11-01 | 2017-03-15 | 重庆返璞科技有限公司 | A kind of nano-glass antifoggant and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113105951A (en) * | 2021-04-12 | 2021-07-13 | 重庆多次元新材料科技有限公司 | Formula and preparation method of high-corrosion-resistance automobile glass water |
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Application publication date: 20180713 |