CN108265311A - A kind of production technology of novel sterilizing water - Google Patents

A kind of production technology of novel sterilizing water Download PDF

Info

Publication number
CN108265311A
CN108265311A CN201810059694.4A CN201810059694A CN108265311A CN 108265311 A CN108265311 A CN 108265311A CN 201810059694 A CN201810059694 A CN 201810059694A CN 108265311 A CN108265311 A CN 108265311A
Authority
CN
China
Prior art keywords
solution
sterilizing water
production technology
novel sterilizing
added
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810059694.4A
Other languages
Chinese (zh)
Inventor
蓝栋林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201810059694.4A priority Critical patent/CN108265311A/en
Publication of CN108265311A publication Critical patent/CN108265311A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • C25B1/01Products
    • C25B1/24Halogens or compounds thereof
    • C25B1/26Chlorine; Compounds thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)

Abstract

The invention discloses a kind of production technologies of novel sterilizing water, it is characterised in that includes the following steps:A. chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;B. contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 35 into step A;C. the solution in step B is added in electrolysis reactor, the electrolysis reactor is made of at least one cathode chamber with cathode and at least one anode chamber with anode, wherein described anode chamber spatially especially separates, and apply DC voltage on electrode by electric current by permeable membrane or diaphragm with the cathode chamber;D. buffer solution is added in the solution into step C and adjusts pH value to 6.5 7.5.The purpose of invention is to overcome shortcoming of the prior art, provides a kind of simple for process, easy to make, production technology of the relatively high novel sterilizing water of concentration.

Description

A kind of production technology of novel sterilizing water
Technical field
The present invention relates to a kind of production technologies of novel sterilizing water.
Background technology
Chlorine-containing disinfectant is one of most common effective sterilised products in agriculture, food industry and environmental protection, effectively Ingredient is hypochlorous acid or hypochlorous acid salt.It is studied according to U.S. environment protection mechanism (EPA), hypochlorous acid is under the same conditions Sterilizing ability is the tens of to hundreds of times of hypochlorous acid salt.Existing hypochlorite solution's production method is relatively complicated, secondary chlorine The concentration loudness of acid is relatively low, can not meet the needs of user.
Invention content
The purpose of the invention is to overcome shortcoming of the prior art, provide it is a kind of simple for process, it is easy to make, The production technology of the relatively high novel sterilizing water of concentration.
A kind of production technology of novel sterilizing water, it is characterised in that include the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 3-5 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one the moon with cathode Pole room and at least one anode chamber with anode are formed, wherein the anode chamber spatially especially by permeable membrane or diaphragm with The cathode chamber separates, and applies DC voltage on electrode by electric current;
D, buffer solution is added in the solution into step C and adjusts pH value to 6.5-7.5.
The production technology of novel sterilizing water as described above, it is characterised in that oxidation-reduction potential is adjusted in step C 1040mV~1860mV.
The production technology of novel sterilizing water as described above, it is characterised in that buffer solution described in step D is carbonate.
The production technology of novel sterilizing water as described above, it is characterised in that further include step E:Using reverse osmosis membrane to step Solution in rapid D is filtered.
In conclusion beneficial effects of the present invention:
Present invention process is simple, easy to make, and process conditions are suitable, and the hypochlorous acid concentration prepared is high, and impurity is small, smell It is small.
Specific embodiment
The present invention is described further With reference to embodiment:
Embodiment 1
A kind of production technology of novel sterilizing water, includes the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 3 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one the moon with cathode Pole room and at least one anode chamber with anode are formed, wherein the anode chamber spatially especially by permeable membrane or diaphragm with The cathode chamber separates, and applies DC voltage on electrode by electric current;
D, buffer solution is added in the solution into step C and adjusts pH value to 6.5.
Embodiment 2
A kind of production technology of novel sterilizing water, includes the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 5 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one the moon with cathode Pole room and at least one anode chamber with anode are formed, wherein the anode chamber spatially especially by permeable membrane or diaphragm with The cathode chamber separates, and applies DC voltage on electrode by electric current;
D, buffer solution is added in the solution into step C and adjusts pH value to 7.5.
Embodiment 3
A kind of production technology of novel sterilizing water, includes the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 4 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one the moon with cathode Pole room and at least one anode chamber with anode are formed, wherein the anode chamber spatially especially by permeable membrane or diaphragm with The cathode chamber separates, and applies DC voltage on electrode by electric current;Oxidation-reduction potential is adjusted to 1040mV;
D, carbonate is added in the solution into step C and adjusts pH value to 7;
E, the solution in step D is filtered using reverse osmosis membrane.
Embodiment 4
A kind of production technology of novel sterilizing water, includes the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 3 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one the moon with cathode Pole room and at least one anode chamber with anode are formed, wherein the anode chamber spatially especially by permeable membrane or diaphragm with The cathode chamber separates, and applies DC voltage on electrode by electric current;Oxidation-reduction potential is adjusted to 1860mV;
D, carbonate is added in the solution into step C and adjusts pH value to 6.8;
E, the solution in step D is filtered using reverse osmosis membrane.
Embodiment 5
A kind of production technology of novel sterilizing water, includes the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 4 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one the moon with cathode Pole room and at least one anode chamber with anode are formed, wherein the anode chamber spatially especially by permeable membrane or diaphragm with The cathode chamber separates, and applies DC voltage on electrode by electric current;Oxidation-reduction potential is adjusted to 1440mV;
D, carbonate is added in the solution into step C and adjusts pH value to 7.2;
E, including step E:The solution in step D is filtered using reverse osmosis membrane.

Claims (4)

1. a kind of production technology of novel sterilizing water, it is characterised in that include the following steps:
A, chlorine is passed through into sodium hydroxide solution, liquor natrii hypochloritis must be contained;
B, contain addition salt acid for adjusting pH value in liquor natrii hypochloritis to 3-5 into step A;
C, the solution in step B is added in electrolysis reactor, the electrolysis reactor is by least one cathode chamber with cathode Formed at least one anode chamber with anode, wherein the anode chamber spatially especially by permeable membrane or diaphragm with it is described Cathode chamber separates, and applies DC voltage on electrode by electric current;
D, buffer solution is added in the solution into step C and adjusts pH value to 6.5-7.5.
2. the production technology of novel sterilizing water according to claim 1, it is characterised in that oxidation-reduction potential tune in step C It saves as 1040mV~1860mV.
3. the production technology of novel sterilizing water according to claim 1, it is characterised in that buffer solution described in step D is carbon Hydrochlorate.
4. the production technology of novel sterilizing water according to claim 1, it is characterised in that further include step E:Using reverse osmosis Permeable membrane is filtered the solution in step D.
CN201810059694.4A 2018-01-22 2018-01-22 A kind of production technology of novel sterilizing water Pending CN108265311A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810059694.4A CN108265311A (en) 2018-01-22 2018-01-22 A kind of production technology of novel sterilizing water

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810059694.4A CN108265311A (en) 2018-01-22 2018-01-22 A kind of production technology of novel sterilizing water

Publications (1)

Publication Number Publication Date
CN108265311A true CN108265311A (en) 2018-07-10

Family

ID=62776365

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810059694.4A Pending CN108265311A (en) 2018-01-22 2018-01-22 A kind of production technology of novel sterilizing water

Country Status (1)

Country Link
CN (1) CN108265311A (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2344412Y (en) * 1998-11-17 1999-10-20 尹智黎 High-intensity oxidative active sterilized medical water formation equipment
CN1899975A (en) * 2005-06-16 2007-01-24 培尔梅烈克电极股份有限公司 Method of sterilization and electrolytic water ejecting apparatus
CN101638262A (en) * 2008-07-28 2010-02-03 解凤桐 Process for producing electrolyzed oxidizing water and bottled package
CN104271513A (en) * 2012-07-13 2015-01-07 菅野稔 Sterile water generation device and sterilizing cleaning method
CN104903251A (en) * 2013-01-28 2015-09-09 德诺拉工业有限公司 Electrolyzed water generating method and generator
CN205874555U (en) * 2016-03-29 2017-01-11 山东康辉水处理设备有限公司 Subacidity brineelectrolysis generater

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN2344412Y (en) * 1998-11-17 1999-10-20 尹智黎 High-intensity oxidative active sterilized medical water formation equipment
CN1899975A (en) * 2005-06-16 2007-01-24 培尔梅烈克电极股份有限公司 Method of sterilization and electrolytic water ejecting apparatus
CN101638262A (en) * 2008-07-28 2010-02-03 解凤桐 Process for producing electrolyzed oxidizing water and bottled package
CN104271513A (en) * 2012-07-13 2015-01-07 菅野稔 Sterile water generation device and sterilizing cleaning method
CN104903251A (en) * 2013-01-28 2015-09-09 德诺拉工业有限公司 Electrolyzed water generating method and generator
CN205874555U (en) * 2016-03-29 2017-01-11 山东康辉水处理设备有限公司 Subacidity brineelectrolysis generater

Similar Documents

Publication Publication Date Title
WO2014071127A3 (en) Three electrode electrolytic cell and method for making hypochlorous acid
CN1181977A (en) Electrolytic functional water, its making method and device
JP3481761B2 (en) Method of generating electrolyzed water
WO2007093395A3 (en) Process for producing a disinfectant by electrochemical activation (eca) of water, disinfectant produced in such a manner and use thereof
CN112042667A (en) Stable hypochlorous acid disinfectant and preparation method thereof
JPH10309582A (en) Production method of acidic electrolytic water and acidic electrolytic water
US20140170059A1 (en) Electrodiaphragmalysis
CN105483748A (en) Disinfectant preparing device
KR20150028222A (en) Sterile water generation device and sterilizing cleaning method
DE602004006244D1 (en) Process for the production of hydrogen
JPH11123381A (en) Preparation of electrolytic ionic water and prepared water
CN108265311A (en) A kind of production technology of novel sterilizing water
CN108609693A (en) A kind of preparation method of acid water and alkaline water
WO2013068599A2 (en) Process for producing an anolyte composition
JP4181170B2 (en) Drinking electrolyzed water and method for producing the same
KR20000021417A (en) Device for pasteurizing and desalting food waste
CN101391832B (en) Method for preparing acidic high oxidation water
CN111560623B (en) Method for continuously and stably preparing hypochlorous acid
CN115874198B (en) Method for producing slightly acidic hypochlorous acid water without adding hydrochloric acid in diaphragm-free electrolytic cell
CN219195148U (en) Plasma enhanced diaphragm electrolysis device for preparing spectacle lens disinfectant
Yoon et al. Alternative electrode materials and ceramic filter minimize disinfection byproducts in point-of-use electrochemical water treatment
JP3970426B2 (en) Method for producing electrolyzed sterilized water
CN114097818A (en) High-efficiency disinfectant and preparation method thereof
JPH105764A (en) Production of acidic electrolyzed water and acidic electrolyzed water
JPH11319831A (en) Production of electrolytic function water and its apparatus

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20180710

RJ01 Rejection of invention patent application after publication