CN108252126A - A kind of low temperature dyeing accelerant and preparation method thereof - Google Patents
A kind of low temperature dyeing accelerant and preparation method thereof Download PDFInfo
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- CN108252126A CN108252126A CN201711326646.9A CN201711326646A CN108252126A CN 108252126 A CN108252126 A CN 108252126A CN 201711326646 A CN201711326646 A CN 201711326646A CN 108252126 A CN108252126 A CN 108252126A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/60—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing polyethers
- D06P1/607—Nitrogen-containing polyethers or their quaternary derivatives
- D06P1/6076—Nitrogen-containing polyethers or their quaternary derivatives addition products of amines and alkylene oxides or oxiranes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
- D06P1/621—Compounds without nitrogen
- D06P1/622—Sulfonic acids or their salts
- D06P1/623—Aliphatic, aralophatic or cycloaliphatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/647—Nitrogen-containing carboxylic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65125—Compounds containing ester groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65131—Compounds containing ether or acetal groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
Abstract
The invention discloses a kind of low temperature dyeing accelerant and preparation method thereof, the low temperature dyeing accelerant is made of the raw material of following parts by weight：10 15 parts of tallow amine polyoxyethylene ether, 59 parts of triethylene glycol butyl ether, 13 parts of soda ash, 13 parts of sodium sulphate, 35 parts of amion acetic acid, 37 parts of alkyl glycosides, 37 parts of sodium secondary alkyl sulfonate, 59 parts of biowax, 13 parts of emulsifier, 20 30 parts of deionized water.The low temperature dyeing accelerant of the present invention has good low temperature colourability, level-dyeing property, dispersion permeability, is needed simultaneously with bleeding agent, dispersant, low temperature dyeing assistant etc. in being dyed instead of Conventional cryogenic, the technique for simplifying low temperature dyeing.The low temperature dyeing accelerant of the present invention can shorten dyeing time, reduce energy loss, improve the dyeing quality of fiber, fabric.
Description
Technical field
The invention belongs to field of fabric producing technology, specifically relate to a kind of low temperature dyeing accelerant and preparation method thereof.
Background technology
Low temperature dyeing is always the hot spot studied.In recent years, the fiber of some non-refractories, such as wool, silk, vinegar it is fine and
Spandex etc. is restricted in terms of high-temperature dyeing.On the one hand low temperature dyeing can reduce energy consumption, on the other hand, can avoid high temperature to ammonia
The influence of the non-refractories fiber such as synthetic fibre, wool and silk, enables the advantage of various fibers to give full play to, and obtains high-quality dyeing
Fabric.
Dyeing accelerant plays plasticization in dyeing to fiber, is more prone to the molecule segment activity of amorphous region, glass
Changing temperature reduces, and accelerates the diffusion velocity of dyestuff in the fibre, so as to which dyeing is made to carry out at normal temperatures and pressures.Currently on the market
The dyeing accelerant used is mainly gaultherolin, methyl naphthalene, phthalic acid ester and o-phenyl phenol etc., these substance smells compared with
Greatly, there is certain toxicity, pollute the environment, just gradually limited the use of.Therefore, developing nontoxic, efficient low temperature dyeing accelerant has
Very big realistic meaning.
Invention content
The purpose of the present invention is to provide a kind of low temperature dyeing accelerant and preparation method thereof, to solve to carry in above-mentioned background technology
The problem of going out.
To achieve the above object, the present invention provides following technical solution：
A kind of low temperature dyeing accelerant, according to parts by weight, including following components：10-15 parts of tallow amine polyoxyethylene ether, three second
5-9 parts of glycol monobutyl ether, 1-3 parts of soda ash, 1-3 parts of sodium sulphate, 3-5 parts of amion acetic acid, 3-7 parts of alkyl glycosides, secondary alkyl sulfonic acid
3-7 parts of sodium, 5-9 parts of biowax, 1-3 parts of emulsifier, 20-30 parts of deionized water.
Preferably, the biowax is beeswax and/or palm wax.
Preferably, the emulsifier is polysorbas20, polysorbate40, polysorbate60, Tween 80, Span 20, Span 40, Span
60th, it is one or more than one kinds of in Span 80.
Preferably, the low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether 10
Part, 5 parts of triethylene glycol butyl ether, 1 part of soda ash, 1 part of sodium sulphate, 3 parts of amion acetic acid, 3 parts of alkyl glycosides, sodium secondary alkyl sulfonate 3
Part, 5 parts of biowax, 1 part of emulsifier, 20 parts of deionized water.
Preferably, the low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether 13
Part, 7 parts of triethylene glycol butyl ether, 2 parts of soda ash, 2 parts of sodium sulphate, 4 parts of amion acetic acid, 5 parts of alkyl glycosides, sodium secondary alkyl sulfonate 5
Part, 7 parts of biowax, 2 parts of emulsifier, 25 parts of deionized water.
Preferably, the low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether 15
Part, 9 parts of triethylene glycol butyl ether, 3 parts of soda ash, 3 parts of sodium sulphate, 5 parts of amion acetic acid, 7 parts of alkyl glycosides, sodium secondary alkyl sulfonate 7
Part, 9 parts of biowax, 3 parts of emulsifier, 30 parts of deionized water.
Preferably, the preparation method of the low temperature dyeing accelerant, specific steps include：
Step 1,5-9 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 80-100 DEG C；
Step 2,20-30 parts of deionized water, 1-3 parts of emulsifier are added in, 500-1000 revs/min, is stirred 20-30 minutes；
Step 3,10-15 parts of tallow amine polyoxyethylene ether, rate of addition 5-10mL/ are slowly added to by constant pressure funnel
Min, 500-1000 rev/min are stirred 10-20 minutes；
Step 4,5-9 parts of triethylene glycol butyl ether, 3-5 parts of amion acetic acid, 3-7 parts of alkyl glycosides, secondary alkyl sulfonic acid are added in
3-7 parts of sodium, stirs 20-30 minutes by 500-1000 revs/min；
Step 5,1-3 parts of soda ash, 1-3 parts of sodium sulphate are added in, 500-1000 revs/min, is stirred 10-20 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, low temperature dyeing accelerant coloring of the invention is good, small to fiber, fabric damage.
2nd, low temperature dyeing accelerant of the invention has good low temperature colourability, level-dyeing property, dispersion permeability, instead of tradition
It is needed simultaneously with bleeding agent, dispersant, low temperature dyeing assistant etc. in low temperature dyeing, the technique for simplifying low temperature dyeing.
3rd, low temperature dyeing accelerant of the invention can shorten dyeing time, reduce energy loss, improve the dyeing of fiber, fabric
Quality.
4th, low temperature dyeing accelerant manufacturing process of the invention is simple to operation, and low in raw material price easily obtains, and nontoxic,
Human body is not stimulated, volatility is low.
5th, mutual compatibility, synergistic effect between various raw materials used in low temperature dyeing accelerant of the invention, it is excellent to collectively constitute performance
Different product.
6th, simplify technique, safe operation is simple, is easy to industrialized production.
7th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether
10-15 parts, 5-9 parts of triethylene glycol butyl ether, 1-3 parts of soda ash, 1-3 parts of sodium sulphate, 3-5 parts of amion acetic acid, alkyl glycosides 3-7
Part, 3-7 parts of sodium secondary alkyl sulfonate, 5-9 parts of biowax, 1-3 parts of emulsifier, 20-30 parts of deionized water.
The present invention also provides a kind of preparation method of low temperature dyeing accelerant, specific steps include：
Step 1,5-9 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 80-100 DEG C；
Step 2,20-30 parts of deionized water, 1-3 parts of emulsifier are added in, 500-1000 revs/min, is stirred 20-30 minutes；
Step 3,10-15 parts of tallow amine polyoxyethylene ether, rate of addition 5-10mL/ are slowly added to by constant pressure funnel
Min, 500-1000 rev/min are stirred 10-20 minutes；
Step 4,5-9 parts of triethylene glycol butyl ether, 3-5 parts of amion acetic acid, 3-7 parts of alkyl glycosides, secondary alkyl sulfonic acid are added in
3-7 parts of sodium, stirs 20-30 minutes by 500-1000 revs/min；
Step 5,1-3 parts of soda ash, 1-3 parts of sodium sulphate are added in, 500-1000 revs/min, is stirred 10-20 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 1
The invention discloses a kind of low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether
10 parts, 5 parts of triethylene glycol butyl ether, 1 part of soda ash, 1 part of sodium sulphate, 3 parts of amion acetic acid, 3 parts of alkyl glycosides, sodium secondary alkyl sulfonate
3 parts, 5 parts of biowax, 1 part of emulsifier, 20 parts of deionized water.
The present invention also provides a kind of preparation method of low temperature dyeing accelerant, specific steps include：
Step 1,5 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 80 DEG C；
Step 2,20 parts of deionized water, 1 part of emulsifier are added in, 500 revs/min, is stirred 20 minutes；
Step 3,10 parts of tallow amine polyoxyethylene ether is slowly added to by constant pressure funnel, rate of addition 5mL/min, 500
Rev/min, it stirs 10 minutes；
Step 4,5 parts of triethylene glycol butyl ether, 3 parts of amion acetic acid, 3 parts of alkyl glycosides, 3 parts of sodium secondary alkyl sulfonate are added in,
It 500 revs/min, stirs 20 minutes；
Step 5,1 part of soda ash, 1 part of sodium sulphate are added in, 500 revs/min, is stirred 10 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 2
The invention discloses a kind of low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether
13 parts, 7 parts of triethylene glycol butyl ether, 2 parts of soda ash, 2 parts of sodium sulphate, 4 parts of amion acetic acid, 5 parts of alkyl glycosides, sodium secondary alkyl sulfonate
5 parts, 7 parts of biowax, 2 parts of emulsifier, 25 parts of deionized water.
The present invention also provides a kind of preparation method of low temperature dyeing accelerant, specific steps include：
Step 1,5 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 90 DEG C；
Step 2,25 parts of deionized water, 2 parts of emulsifier are added in, 800 revs/min, is stirred 25 minutes；
Step 3,13 parts of tallow amine polyoxyethylene ether is slowly added to by constant pressure funnel, rate of addition 8mL/min, 800
Rev/min, it stirs 15 minutes；
Step 4,7 parts of triethylene glycol butyl ether, 4 parts of amion acetic acid, 5 parts of alkyl glycosides, 5 parts of sodium secondary alkyl sulfonate are added in,
It 800 revs/min, stirs 25 minutes；
Step 5,2 parts of soda ash, 2 parts of sodium sulphate are added in, 800 revs/min, is stirred 15 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 3
The invention discloses a kind of low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether
15 parts, 9 parts of triethylene glycol butyl ether, 3 parts of soda ash, 3 parts of sodium sulphate, 5 parts of amion acetic acid, 7 parts of alkyl glycosides, sodium secondary alkyl sulfonate
7 parts, 9 parts of biowax, 3 parts of emulsifier, 30 parts of deionized water.
The present invention also provides a kind of preparation method of low temperature dyeing accelerant, specific steps include：
Step 1,9 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 100 DEG C；
Step 2,30 parts of deionized water, 3 parts of emulsifier are added in, 1000 revs/min, is stirred 30 minutes；
Step 3,15 parts, rate of addition 10mL/min of tallow amine polyoxyethylene ether is slowly added to by constant pressure funnel,
It 1000 revs/min, stirs 20 minutes；
Step 4,9 parts of triethylene glycol butyl ether, 5 parts of amion acetic acid, 7 parts of alkyl glycosides, 7 parts of sodium secondary alkyl sulfonate are added in,
It 1000 revs/min, stirs 30 minutes；
Step 5,3 parts of soda ash, 3 parts of sodium sulphate are added in, 1000 revs/min, is stirred 20 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
Embodiment 4
The invention discloses a kind of low temperature dyeing accelerant, according to parts by weight, including following components：Tallow amine polyoxyethylene ether
10 parts, 7 parts of triethylene glycol butyl ether, 3 parts of soda ash, 2 parts of sodium sulphate, 5 parts of amion acetic acid, 7 parts of alkyl glycosides, sodium secondary alkyl sulfonate
7 parts, 9 parts of biowax, 3 parts of emulsifier, 25 parts of deionized water.
The present invention also provides a kind of preparation method of low temperature dyeing accelerant, specific steps include：
Step 1,9 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 100 DEG C；
Step 2,25 parts of deionized water, 3 parts of emulsifier are added in, 800 revs/min, is stirred 20 minutes；
Step 3,10 parts of tallow amine polyoxyethylene ether is slowly added to by constant pressure funnel, rate of addition 8mL/min, 1000
Rev/min, it stirs 10 minutes；
Step 4,7 parts of triethylene glycol butyl ether, 5 parts of amion acetic acid, 7 parts of alkyl glycosides, 7 parts of sodium secondary alkyl sulfonate are added in,
It 1000 revs/min, stirs 20 minutes；
Step 5,3 parts of soda ash, 2 parts of sodium sulphate are added in, 1000 revs/min, is stirred 10 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
Test case
Using embodiment 1,2,3,4 low temperature dyeing accelerant handle polyester cotton, by obtained polyester cotton into
Row performance test, test result is as follows：
The above-mentioned various embodiments enumerated, under the premise of reconcilable, can be combined with each other implementation, those skilled in the art
It can combine above to the explanation of embodiment, as the foundation being combined to the technical characteristic in different embodiments.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (7)
1. a kind of low temperature dyeing accelerant, it is characterised in that：The low temperature dyeing accelerant includes the raw material of following parts by weight：Tallow amine gathers
10-15 parts of ethylene oxide ether, 5-9 parts of triethylene glycol butyl ether, 1-3 parts of soda ash, 1-3 parts of sodium sulphate, 3-5 parts of amion acetic acid, alkyl
3-7 parts of glucosides, 3-7 parts of sodium secondary alkyl sulfonate, 5-9 parts of biowax, 1-3 parts of emulsifier, 20-30 parts of deionized water.
2. low temperature dyeing accelerant according to claim 1, it is characterised in that：The biowax is beeswax and/or palm wax.
3. low temperature dyeing accelerant according to claim 1, it is characterised in that：The emulsifier is polysorbas20, polysorbate40, spits
It is one or more than one kinds of in temperature 60, Tween 80, Span 20, Span 40, Span 60, Span 80.
4. low temperature dyeing accelerant according to claim 1, it is characterised in that：According to parts by weight, including following components：Tallow
10 parts of amine polyoxyethylene ether, 5 parts of triethylene glycol butyl ether, 1 part of soda ash, 1 part of sodium sulphate, 3 parts of amion acetic acid, 3 parts of alkyl glycosides,
3 parts of sodium secondary alkyl sulfonate, 5 parts of biowax, 1 part of emulsifier, 20 parts of deionized water.
5. low temperature dyeing accelerant according to claim 1, it is characterised in that：According to parts by weight, including following components：Tallow
13 parts of amine polyoxyethylene ether, 7 parts of triethylene glycol butyl ether, 2 parts of soda ash, 2 parts of sodium sulphate, 4 parts of amion acetic acid, 5 parts of alkyl glycosides,
5 parts of sodium secondary alkyl sulfonate, 7 parts of biowax, 2 parts of emulsifier, 25 parts of deionized water.
6. low temperature dyeing accelerant according to claim 1, it is characterised in that：According to parts by weight, including following components：Tallow
15 parts of amine polyoxyethylene ether, 9 parts of triethylene glycol butyl ether, 3 parts of soda ash, 3 parts of sodium sulphate, 5 parts of amion acetic acid, 7 parts of alkyl glycosides,
7 parts of sodium secondary alkyl sulfonate, 9 parts of biowax, 3 parts of emulsifier, 30 parts of deionized water.
7. a kind of preparation method using any one of the claims 1-6 low temperature dyeing accelerants, it is characterised in that：Specifically
Step includes：
Step 1,5-9 parts of biowax is added in a kettle, and oil bath heating, condensing reflux, raising temperature is to 80-100 DEG C；
Step 2,20-30 parts of deionized water, 1-3 parts of emulsifier are added in, 500-1000 revs/min, is stirred 20-30 minutes；
Step 3,10-15 parts, rate of addition 5-10mL/min of tallow amine polyoxyethylene ether is slowly added to by constant pressure funnel,
It 500-1000 revs/min, stirs 10-20 minutes；
Step 4,5-9 parts of triethylene glycol butyl ether, 3-5 parts of amion acetic acid, 3-7 parts of alkyl glycosides, sodium secondary alkyl sulfonate 3-7 are added in
Part, it 500-1000 revs/min, stirs 20-30 minutes；
Step 5,1-3 parts of soda ash, 1-3 parts of sodium sulphate are added in, 500-1000 revs/min, is stirred 10-20 minutes；
Step 6, stirring is shut down, obtains prepared liquid cryogen dyeing accelerant；
Step 7, it stands and is cooled in reaction kettle liquid cryogen dyeing accelerant and is less than 20 DEG C, blowing encapsulation, finished product.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112482056A (en) * | 2020-11-30 | 2021-03-12 | 淄博鲁瑞精细化工有限公司 | Preparation method of imide dye-guiding agent |
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