CN108252094A - A kind of artificial leather surface conditioning agent and preparation method thereof - Google Patents
A kind of artificial leather surface conditioning agent and preparation method thereof Download PDFInfo
- Publication number
- CN108252094A CN108252094A CN201711428609.9A CN201711428609A CN108252094A CN 108252094 A CN108252094 A CN 108252094A CN 201711428609 A CN201711428609 A CN 201711428609A CN 108252094 A CN108252094 A CN 108252094A
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- artificial leather
- surface conditioning
- leather surface
- conditioning agent
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/227—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of hydrocarbons, or reaction products thereof, e.g. afterhalogenated or sulfochlorinated
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Synthetic Leather, Interior Materials Or Flexible Sheet Materials (AREA)
Abstract
The present invention relates to a kind of artificial leather surface conditioning agents and preparation method thereof, belong to technical field of artificial leather.The inorganic agent includes 15 20 parts of acrylate resin, 10 15 parts of polymethacrylate resin, 5 10 parts of plastic of poly vinyl acetate, 15 20 parts of diethylbenzene, 5 10 parts of methyl ethyl ketone, 10 15 parts of acetic acid fourth vinegar, 10 15 parts of dimethylformamide, 10 15 parts of dimethylacetylamide, 5 10 parts of hexamethylene.The present invention is on the basis of the action principle of the Interaction Force of molecule, fully consider solvent nature, such as influence of dissolving power, evaporation rate, wetting ability for the performance of inorganic agent, according to the principle of similar compatibility, prepare artificial leather surface conditioning agent, increase effective bond area, improve just viscous, whole viscous intensity.
Description
Technical field
The present invention relates to a kind of surface conditioning agent and preparation method thereof, it is more particularly related to a kind of artificial leather
Surface conditioning agent and preparation method thereof belongs to technical field of artificial leather.
Background technology
Artificial leather surface conditioning agent is by " the bridging agent " between viscous material and adhesive, and effect is：One end anchors
In by viscous material, the other end is anchored in glue-line, plays a part of to increase adhesive strength.
State Intellectual Property Office discloses a Publication No. CN102926208A, entitled " skin sense in 2013.02.13
Polyurethane resin artificial leather surface conditioning agent " invention, a kind of disclosure of the invention polyurethane resin artificial leather table of skin sense
Surface treatment agent, the polyurethane resin artificial leather surface conditioning agent of the skin sense include the non yellowing polyurethane resin of 90 ~ 96% mass parts
The non yellowing siloxanes paste composition of solution and 4 ~ 10% mass parts.Coating or painting caused by the surface conditioning agent of the present invention
Film not only assigns polyurethane artificial leather surface with the elasticity and fat wiping sense style as skin, but also the coating or film have
Anti-yellowing function makes surface conditioning agent that can be applicable in dark high-grade polyurethane artificial leather demand but also be applicable in light top grade and gathers
Urethane artificial leather demand.
Existing artificial leather surface conditioning agent is increasing effective bond area, improve it is just viscous, eventually viscous intensity invention effect compared with
Difference.
Invention content
Present invention seek to address that the problems of the prior art, provide a kind of artificial leather surface conditioning agent, which can have
The effective bond area of effect increase improves and just glues, glues intensity eventually.
In order to achieve the above-mentioned object of the invention, specific technical solution is as follows：
A kind of artificial leather surface conditioning agent, it is characterised in that：Including following raw materials by weight：
15-20 parts of acrylate resin
10-15 parts of polymethacrylate resin
5-10 parts of polyethylene-vinyl acetate
15-20 parts of diethylbenzene
5-10 parts of methyl ethyl ketone
10-15 parts of acetic acid fourth vinegar
10-15 parts of dimethylformamide
10-15 parts of dimethylacetylamide
5-10 parts of hexamethylene.
The solid content of acrylate resin of the present invention is 30-35%.
The ethylene contents of polyethylene-vinyl acetate of the present invention are 15%.
A kind of preparation method of artificial leather surface conditioning agent, it is characterised in that：It comprises the following steps that：
A, it is first added in by diethylbenzene, first in the four round flask with charge door, electric mixer, condenser pipe and thermometer
The mixed solvent that ethyl ketone, acetic acid fourth vinegar, dimethylformamide, dimethylacetylamide and hexamethylene form；
B, temperature is risen to 50-60 DEG C, sequentially adds polymethacrylate resin and polyethylene-vinyl acetate, in above-mentioned temperature
Dissolving 1.5-2h is slowly stirred under degree；
C, after polymethacrylate resin and polyethylene-vinyl acetate are completely dissolved, acrylate resin is added in, is filled
Divide and be stirred 2-3h；
D, room temperature, discharging, packaging are cooled the temperature to.
The advantageous effects that the present invention is brought：
The present invention fully considers solvent nature on the basis of the action principle of the Interaction Force of molecule, and such as dissolving power is waved
The influence for the performance of inorganic agent such as speed, wetting ability is sent out, according to the principle of similar compatibility, is prepared at artificial leather surface
Agent is managed, increases effective bond area, improves just viscous, whole viscous intensity.
Specific embodiment
Embodiment 1
A kind of artificial leather surface conditioning agent, including following raw materials by weight：
15 parts of acrylate resin
10 parts of polymethacrylate resin
5 parts of polyethylene-vinyl acetate
15 parts of diethylbenzene
5 parts of methyl ethyl ketone
10 parts of acetic acid fourth vinegar
10 parts of dimethylformamide
10 parts of dimethylacetylamide
5 parts of hexamethylene.
Embodiment 2
A kind of artificial leather surface conditioning agent, including following raw materials by weight：
20 parts of acrylate resin
15 parts of polymethacrylate resin
10 parts of polyethylene-vinyl acetate
20 parts of diethylbenzene
10 parts of methyl ethyl ketone
15 parts of acetic acid fourth vinegar
15 parts of dimethylformamide
15 parts of dimethylacetylamide
10 parts of hexamethylene.
Embodiment 3
A kind of artificial leather surface conditioning agent, including following raw materials by weight：
17 parts of acrylate resin
12 parts of polymethacrylate resin
12 parts of polyethylene-vinyl acetate
17 parts of diethylbenzene
12 parts of methyl ethyl ketone
13 parts of acetic acid fourth vinegar
12 parts of dimethylformamide
12 parts of dimethylacetylamide
12 parts of hexamethylene.
Embodiment 4
A kind of preparation method of artificial leather surface conditioning agent, comprises the following steps that：
A, it is first added in by diethylbenzene, first in the four round flask with charge door, electric mixer, condenser pipe and thermometer
The mixed solvent that ethyl ketone, acetic acid fourth vinegar, dimethylformamide, dimethylacetylamide and hexamethylene form；
B, temperature is risen to 50 DEG C, sequentially adds polymethacrylate resin and polyethylene-vinyl acetate, at above-mentioned temperature
It is slowly stirred dissolving 1.5h；
C, after polymethacrylate resin and polyethylene-vinyl acetate are completely dissolved, acrylate resin is added in, is filled
Divide and be stirred 2h；
D, room temperature, discharging, packaging are cooled the temperature to.
Embodiment 5
A kind of preparation method of artificial leather surface conditioning agent, comprises the following steps that：
A, it is first added in by diethylbenzene, first in the four round flask with charge door, electric mixer, condenser pipe and thermometer
The mixed solvent that ethyl ketone, acetic acid fourth vinegar, dimethylformamide, dimethylacetylamide and hexamethylene form；
B, temperature is risen to 60 DEG C, sequentially adds polymethacrylate resin and polyethylene-vinyl acetate, at above-mentioned temperature
It is slowly stirred dissolving 2h；
C, after polymethacrylate resin and polyethylene-vinyl acetate are completely dissolved, acrylate resin is added in, is filled
Divide and be stirred 3h；
D, room temperature, discharging, packaging are cooled the temperature to.
Embodiment 6
A kind of preparation method of artificial leather surface conditioning agent, comprises the following steps that：
A, it is first added in by diethylbenzene, first in the four round flask with charge door, electric mixer, condenser pipe and thermometer
The mixed solvent that ethyl ketone, acetic acid fourth vinegar, dimethylformamide, dimethylacetylamide and hexamethylene form；
B, temperature is risen to 55 DEG C, sequentially adds polymethacrylate resin and polyethylene-vinyl acetate, at above-mentioned temperature
It is slowly stirred dissolving 1.75h；
C, after polymethacrylate resin and polyethylene-vinyl acetate are completely dissolved, acrylate resin is added in, is filled
Divide and be stirred 2.5h；
D, room temperature, discharging, packaging are cooled the temperature to.
Claims (4)
1. a kind of artificial leather surface conditioning agent, it is characterised in that：Including following raw materials by weight：
15-20 parts of acrylate resin
10-15 parts of polymethacrylate resin
5-10 parts of polyethylene-vinyl acetate
15-20 parts of diethylbenzene
5-10 parts of methyl ethyl ketone
10-15 parts of acetic acid fourth vinegar
10-15 parts of dimethylformamide
10-15 parts of dimethylacetylamide
5-10 parts of hexamethylene.
2. a kind of artificial leather surface conditioning agent according to claim 1, it is characterised in that：The polyacrylate gluing
The solid content of agent is 30-35%.
3. a kind of artificial leather surface conditioning agent according to claim 1, it is characterised in that：The polyethylene-acetic acid second
The ethylene contents of enester are 15%.
4. a kind of preparation method of artificial leather surface conditioning agent according to claim 1, it is characterised in that：Including following work
Skill step：
A, it is first added in by diethylbenzene, first in the four round flask with charge door, electric mixer, condenser pipe and thermometer
The mixed solvent that ethyl ketone, acetic acid fourth vinegar, dimethylformamide, dimethylacetylamide and hexamethylene form；
B, temperature is risen to 50-60 DEG C, sequentially adds polymethacrylate resin and polyethylene-vinyl acetate, in above-mentioned temperature
Dissolving 1.5-2h is slowly stirred under degree；
C, after polymethacrylate resin and polyethylene-vinyl acetate are completely dissolved, acrylate resin is added in, is filled
Divide and be stirred 2-3h；
D, room temperature, discharging, packaging are cooled the temperature to.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711428609.9A CN108252094A (en) | 2017-12-26 | 2017-12-26 | A kind of artificial leather surface conditioning agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711428609.9A CN108252094A (en) | 2017-12-26 | 2017-12-26 | A kind of artificial leather surface conditioning agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108252094A true CN108252094A (en) | 2018-07-06 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711428609.9A Withdrawn CN108252094A (en) | 2017-12-26 | 2017-12-26 | A kind of artificial leather surface conditioning agent and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN108252094A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110878182A (en) * | 2019-11-18 | 2020-03-13 | 清远市美佳乐环保新材股份有限公司 | Water-based PVC artificial leather treating agent and preparation method and application thereof |
-
2017
- 2017-12-26 CN CN201711428609.9A patent/CN108252094A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110878182A (en) * | 2019-11-18 | 2020-03-13 | 清远市美佳乐环保新材股份有限公司 | Water-based PVC artificial leather treating agent and preparation method and application thereof |
| CN110878182B (en) * | 2019-11-18 | 2021-10-29 | 清远市美佳乐环保新材股份有限公司 | Water-based PVC artificial leather treating agent and preparation method and application thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20180706 |