CN108251198A - A kind of environment-friendly biomass lubricating oil and its preparation process - Google Patents
A kind of environment-friendly biomass lubricating oil and its preparation process Download PDFInfo
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- CN108251198A CN108251198A CN201810113210.XA CN201810113210A CN108251198A CN 108251198 A CN108251198 A CN 108251198A CN 201810113210 A CN201810113210 A CN 201810113210A CN 108251198 A CN108251198 A CN 108251198A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/087—Boron oxides, acids or salts
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/02—Hydroxy compounds
- C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
- C10M2207/0225—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/287—Partial esters
- C10M2207/289—Partial esters containing free hydroxy groups
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
- C10M2207/401—Fatty vegetable or animal oils used as base material
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
- C10M2207/402—Castor oils
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/022—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of hydrocarbons, e.g. olefines
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
- C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
- C10M2219/066—Thiocarbamic type compounds
- C10M2219/068—Thiocarbamate metal salts
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
- C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
- C10M2219/083—Dibenzyl sulfide
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/041—Triaryl phosphates
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
- C10M2223/045—Metal containing thio derivatives
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/049—Phosphite
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/56—Boundary lubrication or thin film lubrication
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/72—Extended drain
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- Chemical & Material Sciences (AREA)
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- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
A kind of environment-friendly biomass lubricating oil of the present invention, composition are as follows according to the mass fraction：10~20 parts of glycerine, 20~35 parts of palm oil, 14~23 parts of castor oil, 10~20 parts of turkey red oil, 10~30 parts of peanut oil, 2~8 parts of lube oil additive；Especially employ by the mixed base oil that is formed of the natural biomass such as glycerine, palm oil, castor oil oil, natural biomass can natural degradation, will not pollute, it is environmentally protective.
Description
Technical field
The present invention is more particularly directed to a kind of environment-friendly biomass lubricating oil and its preparation processes.
Background technology
The phenomenon that fretting wear is generally existing in friction process, according to statistics, a performance in more than 1/3rd world
The loss in source carrys out self-friction, and therefore, economic loss caused by reducing friction and wear is of great significance.And it is to reduce to lubricate
Rub, reduce or avoid the effective technology of abrasion.
It for the working fluid generally used from present society, whether synthesizes, semi-synthetic portion's majority big absolutely all has breast
Change, is rotten, smelly, having corrosion to human skin and muscle, more polluting environment, it pollutes environment, is easily caused greatly to the mankind
Harm.And most of lubricants are to improve its performance to add in a variety of lubricating additives, and traditional additive is to pass through object
Reason is adsorbed and chemically reacts to realize good tribological property, it is impossible to accomplish the zero abrasion of material and the damage to material
Play repair.Lubricating additive largely determines oneself of the performance of lubricant, exploitation and development of new
Lubricating additive is repaired, blended lubricating oil product are come with this, so as to reduce friction, reduce abrasion, there is important meaning to national economy
Justice.
Invention content
The present invention proposes a kind of environment-friendly biomass lubricating oil and its preparation process regarding to the issue above.
Specific technical solution is as follows：
A kind of environment-friendly biomass lubricating oil, which is characterized in that composition is as follows according to the mass fraction：
10~20 parts of glycerine, 20~35 parts of palm oil, 14~23 parts of castor oil, 10~20 parts of turkey red oil, 10~30 parts of peanut oil,
2~8 parts of lube oil additive.
Further, the constituent of the lube oil additive is according to the mass fraction：Diisooctyl phosphordithiic acid
10~22 parts of molybdenum, 18~28 parts of triphenyl phosphate, 15~20 parts of antiwear additive, 10~30 parts of antioxidant.
Further, the antiwear additive is the mixture in sulfide isobutene, kodalk, potassium metaborate.
Further, the antiwear additive mass mixing ratio is sulfide isobutene：Kodalk：In potassium metaborate=2~5:
4~6：1~4:3~7.
Further, the antioxidant is β-positive octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid, dioxane
Base zinc dithiocarbamate, molybdenum dialkyldithiocarbamacompositions, antimony dialkyl-dithiocarbamate mixture.
Further, the mass mixing ratio of the antioxidant is β-(3,5- di-tert-butyl-hydroxy phenyl) propionic acid is just
Octadecanol ester：Zinc dialkyl dithiocarbamate：Molybdenum dialkyldithiocarbamacompositions：Dialkyldithiocarbamacompositions
Antimony=1~2：2~5:1~3：4~8.
The preparation method of a kind of environment-friendly biomass lubricating oil and its preparation process, which is characterized in that preparation process is as follows：
（1）, antiwear additive preparation：Load weighted antiwear additive raw material is stirred evenly or put into ball mill mixing, three rollers of merging are ground
It is ground in grinding machine, 45~55 minutes time, obtains antiwear additive；
（2nd, the preparation of antioxidant：Load weighted antioxidant raw material is stirred evenly or put into ball mill mixing, three rollers of merging are ground
It is ground in grinding machine, 1~2 hour time, obtains antioxidant；
（3）, additive prepare：By molybdenum diisooctyl dithiophosphate, triphenyl phosphate, that antiwear additive is heated to 180~200 is Celsius
It after degree, reconstitutes and is mixed via condiment drum turning and compressed air, 1~2 hour time, add in antioxygen after mixing
Agent continues mixing 40~60 minutes, obtains additive；
（4）Prepared by lubricating oil, glycerine, palm oil, castor oil, turkey red oil, peanut oil are put into reaction kettle and are mixed, and mixes
Mixing time is 2~3 hours, and mixing temperature is 130~150 degrees Celsius, and 60~80 degrees Celsius are cooled to after the completion of mixing, is added in
Additive continues to mix, incorporation time be 30~70 minutes, then naturally cool to room temperature is sufficient.
Beneficial effects of the present invention are：
Especially employ the mixed base oil being made of the natural biomass such as glycerine, palm oil, castor oil oil, natural life
Substance can natural degradation, will not pollute, it is environmentally protective.
Using special lube oil additive, by sulfide isobutene, benzyl disulfide, di-n-butyl phosphite, metaboric acid
The antiwear additive that sodium, potassium metaborate material are formed can cause lubricating oil generating chemical reaction film with metal surface chemically reactive,
Lubricating action is played, scratches on metal surface or even melting welding is prevented, increases substantially the self-lubricating property of lubricating oil, wear-resistant selfreparing
Effect is good.Particular arrangement multicomponent antioxidant has fabulous anti-aging antioxygenic property, can be high delay lubricating oil
Service life improves the practicality energy.
Specific embodiment
For technical scheme of the present invention is made to be more clear clearly, below the present invention is described further, it is any to this
The technical characteristic of inventive technique scheme carries out the scheme that equivalencing is obtained with conventional reasoning and each falls within the scope of the present invention.This
Mixing plant in invention is reaction kettle.
Embodiment 1
A kind of environment-friendly biomass lubricating oil and its preparation process, preparation process are as follows：
（1）, antiwear additive preparation：By sulfide isobutene, kodalk, potassium metaborate with 2:4：1:3 mass ratio input ball
Grinding machine mixing, then be placed in three-roll grinder and grind, 45 minutes time, obtain antiwear additive；
（2nd, the preparation of antioxidant：By β-positive octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyls) propionic acid, dialkyl disulfides
For carbaminate, molybdenum dialkyldithiocarbamacompositions, antimony dialkyl-dithiocarbamate with 1：2:1：4 mass ratio
After mixing, it is ground in merging three-roll grinder, 1 hour time, obtains antioxidant；
（3）, additive prepare：10 parts of molybdenum diisooctyl dithiophosphate, 18 parts of triphenyl phosphate, 15 parts of antiwear additive are heated to
It after 180 degrees Celsius, reconstitutes and is mixed via condiment drum turning and compressed air, 1 hour time, add in after mixing,
10 parts of antioxidant continues mixing 40 minutes, obtains additive；
（4）Prepared by lubricating oil, 10 parts of glycerine, 20 parts of palm oil, 14 parts of castor oil, 10 parts of turkey red oil, 10 parts of peanut oil are put into instead
It answers in kettle and is mixed, it is 2 hours that the time, which is mixed, and mixing temperature is 130 degrees Celsius, and it is Celsius to be cooled to 60 after the completion of mixing
Degree, add in 2 parts of additive, continue to mix, incorporation time be 30 minutes, then naturally cool to room temperature is sufficient.
Embodiment 2
A kind of environment-friendly biomass lubricating oil and its preparation process, preparation process are as follows：
（1）, antiwear additive preparation：By sulfide isobutene, kodalk, potassium metaborate with 5:6：4:7 mass ratio input ball
Grinding machine mixing, then be placed in three-roll grinder and grind, 55 minutes time, obtain antiwear additive；
（2nd, the preparation of antioxidant：By β-positive octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyls) propionic acid, dialkyl disulfides
For carbaminate, molybdenum dialkyldithiocarbamacompositions, antimony dialkyl-dithiocarbamate with 2：5:3：8 mass ratio
After mixing, it is ground in merging three-roll grinder, time 2 h obtains antioxidant；
（3）, additive prepare：22 parts of molybdenum diisooctyl dithiophosphate, 28 parts of triphenyl phosphate, 20 parts of antiwear additive are heated to
After 200 degrees Celsius, reconstituting and mixed via condiment drum turning and compressed air, time 2 h adds in after mixing,
30 parts of antioxidant continues mixing 60 minutes, obtains additive；
（4）Prepared by lubricating oil, 20 parts of glycerine, 35 parts of palm oil, 23 parts of castor oil, 20 parts of turkey red oil, 30 parts of peanut oil are put into
It is mixed in reaction kettle, it is 3 hours that the time, which is mixed, and mixing temperature is 150 degrees Celsius, and being cooled to 80 after the completion of mixing takes the photograph
Family name's degree, add in 8 parts of additive, continue to mix, incorporation time be 30~70 minutes, then naturally cool to room temperature is sufficient.
Embodiment 3
A kind of environment-friendly biomass lubricating oil and its preparation process, preparation process are as follows：
（1）, antiwear additive preparation：By sulfide isobutene, kodalk, potassium metaborate with 4:5:2:6 mass ratio input ball
Grinding machine mixing, then be placed in three-roll grinder and grind, 50 minutes time, obtain antiwear additive；
（2nd, the preparation of antioxidant：By β-positive octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyls) propionic acid, dialkyl disulfides
For carbaminate, molybdenum dialkyldithiocarbamacompositions, antimony dialkyl-dithiocarbamate with 2：3:2：7 mass ratio
After mixing, it is ground in merging three-roll grinder, 1.5 hours time, obtains antioxidant；
（3）, additive prepare：15 parts of molybdenum diisooctyl dithiophosphate, 19 parts of triphenyl phosphate, 17 parts of antiwear additive are heated to
It after 190 degrees Celsius, reconstitutes and is mixed via condiment drum turning and compressed air, 1.5 hours time added after mixing
Enter, 13 parts of antioxidant, continue mixing 55 minutes, obtain additive；
（4）Prepared by lubricating oil, 15 parts of glycerine, 25 parts of palm oil, 17 parts of castor oil, 15 parts of turkey red oil, 24 parts of peanut oil are put into
It is mixed in reaction kettle, it is 2.5 hours that the time, which is mixed, and mixing temperature is 140 degrees Celsius, and 65 are cooled to after the completion of mixing
Degree Celsius, add in 6 parts of additive, continue to mix, incorporation time be 50 minutes, then naturally cool to room temperature is sufficient.
Beneficial effects of the present invention are：
Especially employ the mixed base oil being made of the natural biomass such as glycerine, palm oil, castor oil oil, natural life
Substance can natural degradation, will not pollute, it is environmentally protective.
Using special lube oil additive, by sulfide isobutene, benzyl disulfide, di-n-butyl phosphite, metaboric acid
The antiwear additive that sodium, potassium metaborate material are formed can cause lubricating oil generating chemical reaction film with metal surface chemically reactive,
Lubricating action is played, scratches on metal surface or even melting welding is prevented, increases substantially the self-lubricating property of lubricating oil, wear-resistant selfreparing
Effect is good.Particular arrangement multicomponent antioxidant has fabulous anti-aging antioxygenic property, can be high delay lubricating oil
Service life improves the practicality energy.
Claims (7)
1. a kind of environment-friendly biomass lubricating oil, which is characterized in that composition is as follows according to the mass fraction：
10~20 parts of glycerine, 20~35 parts of palm oil, 14~23 parts of castor oil, 10~20 parts of turkey red oil, 10~30 parts of peanut oil,
2~8 parts of lube oil additive.
2. a kind of environment-friendly biomass lubricating oil and its preparation process as described in claim/1, it is characterized in that, the lubrication
The constituent of oil additive is according to the mass fraction：10~22 parts of molybdenum diisooctyl dithiophosphate, triphenyl phosphate 18~
28 parts, 15~20 parts of antiwear additive, 10~30 parts of antioxidant.
3. a kind of environment-friendly biomass lubricating oil as claimed in claim 2 and its preparation process, it is characterized in that, the antiwear additive
For the mixture in sulfide isobutene, kodalk, potassium metaborate.
4. a kind of environment-friendly biomass lubricating oil as claimed in claim 3 and its preparation process, it is characterized in that, the antiwear additive
Mass mixing ratio is sulfide isobutene：Kodalk：In potassium metaborate=2~5:4~6：1~4:3~7.
5. a kind of environment-friendly biomass lubricating oil as claimed in claim 2 and its preparation process, it is characterized in that, the antioxidant
For β-positive octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyls) propionic acid, zinc dialkyl dithiocarbamate, dialkyl group two
The mixture of thiocarbamic acid molybdenum, antimony dialkyl-dithiocarbamate.
6. a kind of environment-friendly biomass lubricating oil as claimed in claim 5 and its preparation process, it is characterized in that, the antioxidant
Mass mixing ratio be β-positive octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyls) propionic acid：Dialkyl dithio amino
Zinc formate：Molybdenum dialkyldithiocarbamacompositions：Antimony dialkyl-dithiocarbamate=1~2：2~5:1~3：4~8.
7. the preparation method of a kind of environment-friendly biomass lubricating oil and its preparation process, which is characterized in that preparation process is as follows：
（1）, antiwear additive preparation：Load weighted antiwear additive raw material is stirred evenly or put into ball mill mixing, three rollers of merging are ground
It is ground in grinding machine, 45~55 minutes time, obtains antiwear additive；
（2nd, the preparation of antioxidant：Load weighted antioxidant raw material is stirred evenly or put into ball mill mixing, three rollers of merging are ground
It is ground in grinding machine, 1~2 hour time, obtains antioxidant；
（3）, additive prepare：By molybdenum diisooctyl dithiophosphate, triphenyl phosphate, that antiwear additive is heated to 180~200 is Celsius
It after degree, reconstitutes and is mixed via condiment drum turning and compressed air, 1~2 hour time, add in antioxygen after mixing
Agent continues mixing 40~60 minutes, obtains additive；
（4）Prepared by lubricating oil, glycerine, palm oil, castor oil, turkey red oil, peanut oil are put into reaction kettle and are mixed, and mixes
Mixing time is 2~3 hours, and mixing temperature is 130~150 degrees Celsius, and 60~80 degrees Celsius are cooled to after the completion of mixing, is added in
Additive continues to mix, incorporation time be 30~70 minutes, then naturally cool to room temperature is sufficient.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI664284B (en) * | 2018-12-03 | 2019-07-01 | National Formosa University | Nano Granulated Coffee Lubricants |
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| CN104403757A (en) * | 2014-12-25 | 2015-03-11 | 常熟市江南锻造有限公司 | Antibacterial metal working fluid |
| CN107164023A (en) * | 2017-06-15 | 2017-09-15 | 合肥市闵葵电力工程有限公司 | It is a kind of for lube oil additive of electromechanical equipment and preparation method thereof |
| CN107164057A (en) * | 2017-06-15 | 2017-09-15 | 合肥市闵葵电力工程有限公司 | It is a kind of for environment-protective lubricant oil of electromechanical equipment and preparation method thereof |
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2018
- 2018-02-05 CN CN201810113210.XA patent/CN108251198A/en active Pending
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