CN108250934A - A kind of anti-near-infrared of anti-blue light is combined coating and preparation method thereof, application - Google Patents
A kind of anti-near-infrared of anti-blue light is combined coating and preparation method thereof, application Download PDFInfo
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- CN108250934A CN108250934A CN201711267874.3A CN201711267874A CN108250934A CN 108250934 A CN108250934 A CN 108250934A CN 201711267874 A CN201711267874 A CN 201711267874A CN 108250934 A CN108250934 A CN 108250934A
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- blue light
- infrared
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/08—Polyurethanes from polyethers
-
- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/20—Filters
-
- G—PHYSICS
- G02—OPTICS
- G02C—SPECTACLES; SUNGLASSES OR GOGGLES INSOFAR AS THEY HAVE THE SAME FEATURES AS SPECTACLES; CONTACT LENSES
- G02C7/00—Optical parts
- G02C7/10—Filters, e.g. for facilitating adaptation of the eyes to the dark; Sunglasses
-
- G—PHYSICS
- G02—OPTICS
- G02C—SPECTACLES; SUNGLASSES OR GOGGLES INSOFAR AS THEY HAVE THE SAME FEATURES AS SPECTACLES; CONTACT LENSES
- G02C7/00—Optical parts
- G02C7/10—Filters, e.g. for facilitating adaptation of the eyes to the dark; Sunglasses
- G02C7/102—Photochromic filters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Physics & Mathematics (AREA)
- Ophthalmology & Optometry (AREA)
- Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
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Abstract
Coating and preparation method thereof is combined the present invention relates to a kind of anti-near-infrared of anti-blue light and a kind of using protection glass of the coating preparation and preparation method thereof, the anti-near-infrared of the anti-blue light is combined coating and includes following components in percentage by weight：Photochromic powder 1.0 3.0%, multicomponent alcoholics compound 15.0 20.5%, Curanate BL 393 20.0 25.0%, IPDI 7.5 8.5%, nanometer Cs2WO4Powder 15.0 28.0%, anti-blue light powder 0.01 0.03%, solvent 23.0 25.0%, auxiliary agent 1.5 2.0%.Anti- blue light function is combined by the present invention with anti-infrared performance, not only can effectively slow down the swollen feeling of the red acid of people's long-time eye generation, absorption of the augen to infrared ray can also be reduced, by obstructing infrared ray with the health of comprehensive protect eyes.
Description
Technical field
The invention belongs to protection glass fields, and in particular to the eyeglass and its preparation that a kind of anti-near-infrared of anti-blue light is combined
The anti-near-infrared of anti-blue light of method and use on the protection glass is combined coating and preparation method thereof.
Background technology
Infrared ray is the electromagnetic wave that wavelength is situated between microwave and visible ray, and wavelength is between 760-4000000 nanometers
The wavelength non-visible light longer than feux rouges.In infrared spectral range, to human body, most beneficial wave band is 4000-14000 nanometers, is being cured
Art circle is known as " fertility light ".Because the infrared ray of this wave band plays the role of promotion to the growth of life, to activating cell
Tissue, blood circulation have good effect, can improve the immunity of people, strengthen the metabolism of human body.Infrared therapy is made
Basis is thermogenetic effect.Under infrared radiation, tissue temperature raising, telangiectasis, blood flow quickening, metabolism
Enhancing, tissue cell activity and power of regeneration improve.
Infrared ray can promote object quickly to heat up, can also cause high temperature injury to human body, especially as a kind of heat radiation
It is that injury to eyes is even more serious.This is because eyes contain the liquid more than comparison, absorption infrared ray is strong, and eyeground film radiates
Property it is poor, also have led to the rapid fever in mulch part, be damaged so as to also have led to eyes.
Infrared ray can also cause retina choroid to be burnt, and lesion only occurs in macular area, obvious solar lentigines to regard
Nethike embrane choroid burns victims, the central fovea of macula of eye has yellowish-white dot, serious to lead to tradition, detached retina etc..It is logical
In the case of often, infrared ray can damage eyes, visual impairment.
Moreover, near infrared ray is often ignored the injury of human eye by people, what long wavelength part damage eyes without, but
Be shortwave it is can have injury to eyes, short infrared (800-2000 nanometer of wavelength) can be by the iris in eyes and crystal suction
It receives, so as to cause the generation of cataract.
In addition, commonly used with 3C Product, race of bowing is more and more, and the blue light of 3C Product can make the eyes of people
Into serious harm, cause the people with eye diseases such as macula lutea, denaturation more and more, therefore, pre- anti-blue light injury is had become as people
Common recognition.
However, currently on the market and there is no the protection glass that can be combined with anti-blue light, counter infrared ray simultaneously.
Invention content
In order to solve the above technical problems, the present invention provides a kind of anti-near-infrareds of anti-blue light to be combined coating and its preparation side
Method and a kind of utilize protection glass of the coating preparation and preparation method thereof.
To achieve the above object, the anti-near-infrared of a kind of anti-blue light provided by the present invention is combined the concrete scheme of coating such as
Under：
A kind of anti-near-infrared of anti-blue light is combined coating, including following components in percentage by weight：
Further, the anti-near-infrared of the anti-blue light be combined coating include following components in percentage by weight：
Further, the photochromic powder is the mixing of blue photochromic powder and green photochromic powder；
Preferably, the blue photochromic powder and the ratio of green photochromic powder weight percent are 1:1.
Further, the multicomponent alcoholics compound is the mixing of PTMEG 500 and TEMPIC；
Preferably, the ratio of the PTMEG 500 and TEMPIC weight percent is 1:4-3:7.
Further, the solvent is toluene.
Further, the auxiliary agent is the mixing of levelling agent BYK 358, stabilizer 1726, light stabilizer 292；
Preferably, the levelling agent BYK 358, stabilizer 1726,292 weight percent of light stabilizer ratio be 1:2:
2。
The present invention also provides the preparation methods that a kind of above-mentioned anti-near-infrared of anti-blue light is combined coating, include the following steps：
(1) each component raw material is weighed by weight percentage；
(2) blue photochromic powder and photochromic powder are added in toluene, stirred 30 minutes until being uniformly dissolved；
(3) anti-blue light powder, stabilizer 1726, light stabilizer 292, levelling agent BYK 358 are added in, continues stirring 30 minutes directly
The solution uniform to formation；
(4) PTMEG 500, TEMPIC are disposably added in, continues stirring 30 minutes until forming uniform solution；
(5) Curanate BL 393, IPDI are sequentially added, continues stirring 60 minutes until forming uniform solution；
(6) nanometer Cs is disposably added in2WO4Powder continues stirring 60 minutes until forming uniform solution, obtains into
Product.
The present invention also provides a kind of above-mentioned anti-near-infrareds of anti-blue light to be combined application of the coating on protection glass：
A kind of anti-near-infrared of anti-blue light is combined protection glass, is combined including ground, priming coat, the anti-near-infrared of anti-blue light
Coating, stiffening layer, the coating that the anti-near-infrared of anti-blue light is combined coating are combined painting for the above-mentioned anti-near-infrared of anti-blue light
Material.
Further, the material of the priming coat is Easepi 900.
The present invention also provides the preparation method that a kind of above-mentioned anti-near-infrared of anti-blue light is combined protection glass, including following step
Suddenly：
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) it is coated with the above-mentioned anti-near-infrared of anti-blue light and is combined coating, 120 degree are toasted 120 minutes until being completely dried, shape
Coating is combined into the anti-near-infrared of anti-blue light；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Wherein：
PTMEG 500 of the present invention is polytetramethylene ether diol, is the polymer of tetrahydrofuran, is had excellent
Hydrolytic stability, gas permeability, wearability and cryogenic mechanics performance.
IPDI of the present invention is isophorone diisocyanate, has excellent photostability and chemical-resistant resistance
Property.
Nanometer Cs of the present invention2WO4Powder is a nanometer wolframic acid caesium, is made as near-infrared shielding material thermal insulation film
With.
Easepi 900 of the present invention is a kind of suitable for coating, the adhesion promoter of ink system, can be had
Effect promotes the adhesive force of ground so that protection glass prepared by the present invention has high adhesion force.
The beneficial effects of the present invention are：
Anti- blue light function is combined by the present invention with anti-infrared performance, not only can effectively be slowed down people and be produced for a long time with eye
The feeling that raw red acid is swollen can also reduce absorption of the augen to infrared ray, with comprehensive protect eyes by obstructing infrared ray
Health.
Specific embodiment
The embodiment of the present invention is described below in detail, the example of the embodiment is intended to be used to explain the present invention, and cannot
It is interpreted as limitation of the present invention.In the examples where no specific technique or condition is specified, according to described by document in the art
Technology or condition or carried out according to product description.Reagents or instruments used without specified manufacturer is that can lead to
Cross the conventional products of acquisition purchased in market.
Embodiment 1：A kind of anti-near-infrared of anti-blue light is combined the preparation of coating
The 1 anti-near-infrared of embodiment 1-4 anti-blue lights of table is combined formulation for coating material table (w/w%)
Composition of raw materials：It is shown in Table 1.
Preparation method：
(1) each component raw material is weighed by weight percentage；
(2) blue photochromic powder and photochromic powder are added in toluene, stirred 30 minutes until being uniformly dissolved；
(3) anti-blue light powder, stabilizer 1726, light stabilizer 292, levelling agent BYK 358 are added in, continues stirring 30 minutes directly
The solution uniform to formation；
(4) PTMEG 500, TEMPIC are disposably added in, continues stirring 30 minutes until forming uniform solution；
(5) Curanate BL 393, IPDI are sequentially added, continues stirring 60 minutes until forming uniform solution；
(6) nanometer Cs is disposably added in2WO4Powder continues stirring 60 minutes until forming uniform solution, obtains into
Product.
Embodiment 2：A kind of anti-near-infrared of anti-blue light is combined the preparation of coating
Composition of raw materials：It is shown in Table 1.The preparation method is the same as that of Example 1.
Embodiment 3：A kind of anti-near-infrared of anti-blue light is combined the preparation of coating
Composition of raw materials：It is shown in Table 1.The preparation method is the same as that of Example 1.
Embodiment 4：A kind of anti-near-infrared of anti-blue light is combined the preparation of coating
Composition of raw materials：It is shown in Table 1.The preparation method is the same as that of Example 1.
Embodiment 5：A kind of anti-near-infrared of anti-blue light is combined the preparation of protection glass
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) the anti-near-infrared of the anti-blue light of coating Examples 1 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Embodiment 6：A kind of anti-near-infrared of anti-blue light is combined the preparation of protection glass
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) the anti-near-infrared of the anti-blue light of coating Examples 2 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Embodiment 7：A kind of anti-near-infrared of anti-blue light is combined the preparation of protection glass
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) the anti-near-infrared of the anti-blue light of coating Examples 3 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Embodiment 8：A kind of anti-near-infrared of anti-blue light is combined the preparation of protection glass
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) the anti-near-infrared of the anti-blue light of coating Examples 4 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Comparative example 1：A kind of preparation of eyeglass
(1) ground is cleaned up；
(2) the anti-near-infrared of the anti-blue light of coating Examples 1 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(3) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Comparative example 2：A kind of preparation of eyeglass
(1) ground is cleaned up；
(2) the anti-near-infrared of the anti-blue light of coating Examples 2 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(3) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Comparative example 3：A kind of preparation of eyeglass
(1) ground is cleaned up；
(2) the anti-near-infrared of the anti-blue light of coating Examples 3 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(3) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Comparative example 4：A kind of preparation of eyeglass
(1) ground is cleaned up；
(2) the anti-near-infrared of the anti-blue light of coating Examples 4 is combined coating, and 120 degree are toasted 120 minutes until completely dry
It is dry, it forms the anti-near-infrared of anti-blue light and is combined coating；
(3) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Comparative example 5：A kind of preparation of eyeglass
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) common coating is coated with, 120 degree are toasted 120 minutes until being completely dried, formation inter coat；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Comparative example 6：A kind of preparation of eyeglass
(1) ground is cleaned up；
(2) common coating is coated with, 120 degree are toasted 120 minutes until being completely dried, formation inter coat；
(3) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
Performance test：
By above-mentioned the performance test results it is found that the present invention is with nanometer Cs2WO4The increase of powder additive amount, anti-infrared
Performance is also promoted；With the increase of anti-blue light powder additive amount, anti-blue light performance is also promoted；It is coated with primary coat Easepi
900, be conducive to the attachment that the anti-near-infrared of anti-blue light is combined coating.
Although specifically showing and describing the present invention with reference to preferred embodiment, those skilled in the art should be bright
In vain, it is not departing from the spirit and scope of the present invention that the appended claims are limited, it in the form and details can be right
The present invention makes a variety of changes, and is protection scope of the present invention.
Claims (10)
1. a kind of anti-near-infrared of anti-blue light is combined coating, which is characterized in that including following components in percentage by weight：
2. the anti-near-infrared of anti-blue light according to claim 1 is combined coating, which is characterized in that including following weight percent
The component of ratio：
3. the anti-near-infrared of anti-blue light according to claim 1 is combined coating, which is characterized in that the photochromic powder is
The mixing of blue photochromic powder and green photochromic powder；
Preferably, the blue photochromic powder and the ratio of green photochromic powder weight percent are 1:1.
4. the anti-near-infrared of anti-blue light according to claim 1 is combined coating, which is characterized in that the polyalcohols chemical combination
Object is the mixing of PTMEG 500 and TEMPIC；
Preferably, the ratio of the PTMEG 500 and TEMPIC weight percent is 1:4-3:7.
5. the anti-near-infrared of anti-blue light according to claim 1 is combined coating, which is characterized in that the solvent is toluene.
6. the anti-near-infrared of anti-blue light according to claim 1 is combined coating, which is characterized in that the auxiliary agent is levelling agent
The mixing of BYK 358, stabilizer 1726, light stabilizer 292；
Preferably, the levelling agent BYK 358, stabilizer 1726,292 weight percent of light stabilizer ratio be 1:2:2.
7. a kind of any anti-near-infrareds of anti-blue light of claim 1-6 are combined the preparation method of coating, which is characterized in that
Include the following steps：
(1) each component raw material is weighed by weight percentage；
(2) blue photochromic powder and photochromic powder are added in toluene, stirred 30 minutes until being uniformly dissolved；
(3) anti-blue light powder, stabilizer 1726, light stabilizer 292, levelling agent BYK 358 are added in, continues stirring 30 minutes until shape
Into uniform solution；
(4) PTMEG 500, TEMPIC are disposably added in, continues stirring 30 minutes until forming uniform solution；
(5) Curanate BL 393, IPDI are sequentially added, continues stirring 60 minutes until forming uniform solution；
(6) nanometer Cs is disposably added in2WO4Powder continues stirring 60 minutes until forming uniform solution, obtains finished product.
8. a kind of anti-near-infrared of anti-blue light is combined protection glass, which is characterized in that resists closely including ground, priming coat, anti-blue light
Infrared to be combined coating, stiffening layer, the coating that the anti-near-infrared of anti-blue light is combined coating is any described for claim 1-6
The anti-near-infrared of anti-blue light be combined coating.
9. the anti-near-infrared of anti-blue light according to claim 8 is combined protection glass, which is characterized in that the priming coat
Material is Easepi 900.
10. a kind of anti-near-infrared of anti-blue light according to any one of claims 8 is combined the preparation method of protection glass, which is characterized in that
Include the following steps：
(1) ground is cleaned up；
(2) 900,90 degree of coating primary coat Easepi bakings 20 minutes are until be completely dried, formation priming coat；
(3) any anti-near-infrareds of anti-blue light of coating claim 1-6 are combined coating, 120 degree bakings 120 minutes up to
It is completely dried, forms the anti-near-infrared of anti-blue light and be combined coating；
(4) stiffened coating is coated with, 120 degree are toasted 120 minutes until being completely dried, and formation stiffening layer obtains finished product.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711267874.3A CN108250934A (en) | 2017-12-05 | 2017-12-05 | A kind of anti-near-infrared of anti-blue light is combined coating and preparation method thereof, application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711267874.3A CN108250934A (en) | 2017-12-05 | 2017-12-05 | A kind of anti-near-infrared of anti-blue light is combined coating and preparation method thereof, application |
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| Publication Number | Publication Date |
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| CN108250934A true CN108250934A (en) | 2018-07-06 |
Family
ID=62722432
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| CN201711267874.3A Withdrawn CN108250934A (en) | 2017-12-05 | 2017-12-05 | A kind of anti-near-infrared of anti-blue light is combined coating and preparation method thereof, application |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2021109445A1 (en) * | 2019-12-06 | 2021-06-10 | 江苏康耐特光学有限公司 | Blue light and infrared light blocking resin lens having refractive index of 1.50 and preparation method therefor |
| CN113512302A (en) * | 2021-05-22 | 2021-10-19 | 福建华塑新材料有限公司 | High-hardness blue-light-filtering flame-retardant photodiffusion polycarbonate material |
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| CN1753922A (en) * | 2003-02-26 | 2006-03-29 | 拜尔材料科学股份公司 | Polyurethane Coating System |
| JP2011184502A (en) * | 2010-03-05 | 2011-09-22 | Bridgestone Corp | Polyurethane foam and method for producing polyurethane foam |
| CN103509454A (en) * | 2013-09-12 | 2014-01-15 | 苏州金海薄膜科技发展有限公司 | Coating liquid, film with coating liquid, and preparation method of film |
| CN107043594A (en) * | 2017-02-08 | 2017-08-15 | 江苏全真光学科技股份有限公司 | Photochromic lens and its manufacture method |
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2017
- 2017-12-05 CN CN201711267874.3A patent/CN108250934A/en not_active Withdrawn
Patent Citations (4)
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| CN1753922A (en) * | 2003-02-26 | 2006-03-29 | 拜尔材料科学股份公司 | Polyurethane Coating System |
| JP2011184502A (en) * | 2010-03-05 | 2011-09-22 | Bridgestone Corp | Polyurethane foam and method for producing polyurethane foam |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2021109445A1 (en) * | 2019-12-06 | 2021-06-10 | 江苏康耐特光学有限公司 | Blue light and infrared light blocking resin lens having refractive index of 1.50 and preparation method therefor |
| CN113512302A (en) * | 2021-05-22 | 2021-10-19 | 福建华塑新材料有限公司 | High-hardness blue-light-filtering flame-retardant photodiffusion polycarbonate material |
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Application publication date: 20180706 |