CN108244108B - 一种能主动引诱苍蝇并使其致死的长效灭蝇挂条 - Google Patents

一种能主动引诱苍蝇并使其致死的长效灭蝇挂条 Download PDF

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CN108244108B
CN108244108B CN201611233772.5A CN201611233772A CN108244108B CN 108244108 B CN108244108 B CN 108244108B CN 201611233772 A CN201611233772 A CN 201611233772A CN 108244108 B CN108244108 B CN 108244108B
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周其奎
姜友法
沈阳
贾炜
郁杨
武斌
邹富清
刘如广
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Jiangsu Yangnong Chemical Co Ltd
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Abstract

本发明公开了一种能主动引诱苍蝇并使其致死的长效灭蝇挂条，由均一溶液浸泡或涂刷载体挂条后制备而成的：均一溶液由以下重量百分比的组分复配而成：活性成份A 0.1％‑5％、活性成份B 0.1％‑10％、引诱成分0.1％‑10％、助剂75％‑99.7％；活性成份A为氯氟醚菊酯，活性成份B为高效氯氟氰菊酯、联苯菊酯、氯菊酯、吡虫啉、甲基吡噁磷中的任意一种，引诱成分为自葡萄糖、果糖、蔗糖、冰糖、麦芽糖、蜂蜜、乳糖、半乳糖、山梨糖醇、麦芽糖醇、木糖醇、甜菊糖、香醋、酱油、吲哚、诱虫烯中的任意一种、两种及以上以任意比例混合而成的混合物。本发明的挂条悬挂于室内，可持续引诱苍蝇并将其击倒致死，提供一种方便、便捷、卫生的持效灭蝇方法，持效期可长达一个月。

Description

一种能主动引诱苍蝇并使其致死的长效灭蝇挂条
技术领域
本发明涉及一种新型灭蝇产品及其制备方法，具体涉及一种能主动引诱苍蝇并使其致死的长效灭蝇挂条。
背景技术
目前市场上常用的灭蝇产品主要是粉剂、悬浮剂和颗粒饵剂，苍蝇接触滞留喷洒表面或饵剂后杀灭，属于被动杀灭。粉剂、悬浮剂作用方式主要是滞留喷洒，需要喷洒在物体表面，使表面全部覆盖药剂，用量大，且不能用于与人亲密接触的室内、宾馆等高档场所。颗粒饵剂布施后遇潮湿天气或环境易发霉变质，影响药效；容易发生儿童或宠物误食现象，存在一定的安全隐患；且颗粒饵剂持效期不长，如饵剂中添加的蝇引诱剂诱虫烯，蒸气压4.7mPa(27℃)，较低易挥发，添加后引诱性只能持续数天，需要频繁更换药剂或补充药剂，增加药剂成本和人工成本。
本发明将有效成分、引诱剂、抑制挥发剂和其他辅料混合后，布药在挂条上，悬挂于室内，可主动持续引诱苍蝇并将其击倒致死。本发明采用有效成份结合载体、添加引诱剂、抑制挥发剂及辅料共同作用，使药效能长达一个月，且外观类似于布条彩带，外形美观，施药方便，只需悬挂即可，为灭蝇提供了一种方便、便捷、卫生的消杀方法，且大大节约了成本。
发明内容
本发明所要解决的技术问题是针对现有技术中存在的不足，而提供一种新型灭蝇产品，该产品可持续引诱苍蝇并将其击倒致死，提供一种方便、便捷、卫生的持效灭蝇方法，持效期可长达一个月。
为了实现上述目的，本发明采用如下技术方案：
一种能主动引诱苍蝇并使其致死的长效灭蝇挂条，由均一溶液浸泡或涂刷载体挂条后制备而成的；所述的均一溶液由以下重量百分比的组分复配而成：活性成份A0.1％-5％、活性成份B0.1％-10％、引诱成分0.1％-10％、助剂75％-99.7％。
上述技术方案中，所述的活性成份A为氯氟醚菊酯。
上述技术方案中，所述的活性成份B为高效氯氟氰菊酯、联苯菊酯、氯菊酯、吡虫啉、甲基吡噁磷中的任意一种。
上述技术方案中，所述的引诱成分为自葡萄糖、果糖、蔗糖、冰糖、麦芽糖、蜂蜜、乳糖、半乳糖、山梨糖醇、麦芽糖醇、木糖醇、甜菊糖、香醋、酱油、吲哚、诱虫烯中的任意一种、两种及以上以任意比例混合而成的混合物。
上述技术方案中，所述的助剂由抑制挥发剂、溶剂、乳化剂按照1：20-500：10-150的重量比复配而成；其中：
所述的抑制挥发剂为糊精、聚乙烯、甲基纤维素，羟甲基纤维素，羟丙基甲基纤维素中的任意一种、两种及以上以任意比例混合而成的混合物；
所述的溶剂为有机溶剂和水，二者的重量比为2-20：1；所述的有机溶剂为无味煤油、无水乙醇中的任意一种，或两种以任意比例混合而成的混合物；
所述的乳化剂为非离子型羟基聚环氧乙烷嵌段共聚物、烷基酚聚氧乙烯醚、脂肪醇聚氧乙烯醚、脂肪胺聚氧乙烯醚、苯乙基酚聚氧乙烯基醚磷酸酯、脂肪酸聚氧乙烯酯、甘油脂肪酸酯聚氧乙烯醚中的任意一种、两种及以上以任意比例混合而成的混合物。
上述技术方案中，所述的载体挂条，材质为涤纶、尼龙、腈纶、丝绸、棉布、纸片中的任意一种，颜色为红色或蓝色。
本发明还提供一种上述的能主动引诱苍蝇并使其致死的长效灭蝇挂条的制备方法，包括以下步骤：
将所述比例的活性成份A、活性成份B、乳化剂溶解于有机溶剂中，搅拌至所加成份完全溶解得到溶液I；将所述比例的引诱成分、抑制挥发剂溶解于溶剂水中搅拌至所加成份完全溶解得到溶液II；将溶液I和II合并后搅拌均匀得到一溶液，用均一溶液浸泡或涂刷载体挂条，待完全浸润后晾干或烘干，即为本发明所述的灭蝇挂条。
上述技术方案中，所述的均一溶液浸泡载体挂条时，每克载体需5-20g的均一溶液浸泡，浸泡5-60分钟；所述的均一溶液涂刷载体挂条，每平方厘米载体涂刷0.01-1g的均一溶液。
本发明的能主动引诱苍蝇并使其致死的长效灭蝇挂条的靶标为家蝇、市蝇、丝光绿蝇、大头金蝇、厩腐蝇、厕蝇、亮绿蝇、红头丽蝇、伏蝇中的一种或多种。
本发明的能主动引诱苍蝇并使其致死的长效灭蝇挂条，使用时将其挂在室内或者室外，其灭蝇持效期可长达一个月。
本发明主要能持续引诱蝇并将其击倒致死，提供一种方便、便捷、卫生的持效灭蝇方法，持效期可长达一个月。
具体实施方式
以下对本发明技术方案的具体实施方式详细描述，但本发明并不限于以下描述内容：
实施例1～16
按以下制备方法制备应用实施例：将所述的活性成份A、活性成份B、乳化剂溶解在有机溶剂中，搅拌至所加成份完全溶解得到均一溶液，引诱成份、抑制挥发剂溶解或溶胀在溶剂水中，将两者混合搅拌的到均一溶液，用均一溶液浸泡或涂刷挂条，待完全浸润后晾干或烘干，即为本发明所述的灭蝇挂条。各实施例配方如表1所示：
表1制备实施例1～16
Figure GDA0003120762950000031
Figure GDA0003120762950000041
Figure GDA0003120762950000051
对比实施例1～5
按制备实施例相同制备方法制备对比实施例，配方如表2所示：
表2对比实施例1～5
Figure GDA0003120762950000052
Figure GDA0003120762950000061
测试实施例1
微量点滴法进行毒力测定实验，试虫为淡色库蚊，羽化后3-5天未吸血雌蚊；具体过程为用乙醚麻醉后置于培养皿中备用，将培养皿内试虫逐头进行点滴处理，点滴于试虫前胸背板上，每头点滴药剂1.0μL，点滴后将试虫移至正常条件下饲养。每个处理重复4次，每次 10头试虫。实验结果如表3所示：
表3点滴法测试结果
Figure GDA0003120762950000062
如表3所示，氯氟醚菊酯：吡虫啉按10：1复配(制备实施例9)共毒系数大于120，有明显的增效作用。
测试实施例2
将挂条按照GB/T13917.10-2009进行灭蝇室内药效测定实验，试虫为家蝇，3-4天雌雄各半成虫；具体过程为用吸蚊管吸取100头试虫(家蝇)放入模拟房中，待试虫恢复正常活动后将挂条悬挂于模拟房中间；观察2小时内引诱试虫次数，每隔一定时间记录被击倒的试虫数，120分钟后将被击倒试虫移至清洁饲养笼内，恢复标准饲养，用5％糖水棉球饲喂，未被击倒的试虫不回收，计入 24 小时活虫数。
结果如表4所示：
表4实施例3与对比实施例1、2、3、4、5对比结果
测试样 生测方式 2h引诱次数 2h击倒率 24h死亡率
实施例3(初期) 模拟房 197 93％ 90％
对比实施例1(初期) 模拟房 201 95％ 91％
实施例3(施药后30天) 模拟房 156 80％ 75％
对比实施例1(施药后30天) 模拟房 33 26％ 13％
对比实施例2 模拟房 27 15％ 11％
对比实施例3 模拟房 186 54％ 43％
对比实施例4 模拟房 191 42％ 39％
对比实施例5 模拟房 181 45％ 38％
从实施例3与对比实施例1初期和30天药效对比可以看出，对比实施例1缺少挥发抑制剂，初期药效与实施例3相当，后期药效明显差于实施例3，缺乏药效持久性。
从实施例3与对比实施例2对比可以看出，对比实施例2缺少引诱剂，引诱性差、药效远差于实施例3。
从实施例3与对比实施例3对比可以看出，对比实施例3缺少乳化剂，击倒率和死亡率差于实施例3。
从实施例3与对比实施例4对比可以看出，对比实施例4缺少活性成份A，药效差于实施例3。
从实施例3与对比实施例5对比可以看出，对比实施例5缺少活性成份B，药效差于实施例3。
测试实施例3
将挂条按照GB/T13917.10-2009进行灭蝇室内药效测定实验，试虫为家蝇，3-4天雌雄各半成虫；具体过程为用吸蚊管吸取100头试虫(家蝇)放入模拟房中，待试虫恢复正常活动后将挂条悬挂于模拟房中间；观察2小时内引诱试虫次数，每隔一定时间记录被击倒的试虫数，120分钟后将被击倒试虫移至清洁饲养笼内，恢复标准饲养，用5％糖水棉球饲喂，未被击倒的试虫不回收，计入24小时活虫数。结果如表5所示：
表5测试实施例3测试结果
Figure GDA0003120762950000071
Figure GDA0003120762950000081
经测试，以上实施例24h药效死亡率均达到90％。
上述实例只是为说明本发明的技术构思以及技术特点，并不能以此限制本发明的保护范围。凡根据本发明的实质所做的等效变换或修饰，都应该涵盖在本发明的保护范围之内。

Claims (9)

1.一种能主动引诱苍蝇并使其致死的长效灭蝇挂条，由均一溶液浸泡或涂刷载体挂条后制备而成的，其特征在于：
所述的均一溶液由以下重量百分比的组分复配而成：活性成份A 0.1％-5％、活性成份B 0.1％-10％、引诱成分0.1％-10％、助剂75％-99.7％；
所述的活性成份A为氯氟醚菊酯；所述的活性成份B为高效氯氟氰菊酯、联苯菊酯、氯菊酯、吡虫啉、甲基吡噁磷中的任意一种；
所述的载体挂条，材质为涤纶、尼龙、腈纶、丝绸、棉布、纸片中的任意一种。
2.根据权利要求1所述的长效灭蝇挂条，其特征在于：所述的引诱成分为葡萄糖、果糖、蔗糖、冰糖、麦芽糖、蜂蜜、乳糖、半乳糖、山梨糖醇、麦芽糖醇、木糖醇、甜菊糖、香醋、酱油、吲哚、诱虫烯中的任意一种、两种及以上以任意比例混合而成的混合物。
3.根据权利要求1所述的长效灭蝇挂条，其特征在于：所述的助剂由抑制挥发剂、溶剂、乳化剂按照1：20-500：10-150的重量比复配而成。
4.根据权利要求3所述的长效灭蝇挂条，其特征在于：所述的抑制挥发剂为糊精、聚乙烯、甲基纤维素，羟甲基纤维素，羟丙基甲基纤维素中的任意一种、两种及以上以任意比例混合而成的混合物。
5.根据权利要求3所述的长效灭蝇挂条，其特征在于：所述的溶剂为有机溶剂和水，二者的重量比为2-20：1；所述的有机溶剂为无味煤油、无水乙醇中的任意一种，或两种以任意比例混合而成的混合物。
6.根据权利要求3所述的长效灭蝇挂条，其特征在于：所述的乳化剂为非离子型羟基聚环氧乙烷嵌段共聚物、烷基酚聚氧乙烯醚、脂肪醇聚氧乙烯醚、脂肪胺聚氧乙烯醚、苯乙基酚聚氧乙烯基醚磷酸酯、脂肪酸聚氧乙烯酯、甘油脂肪酸酯聚氧乙烯醚中的任意一种、两种及以上以任意比例混合而成的混合物。
7.一种权利要求1-6任一项所述的长效灭蝇挂条的制备方法，其特征在于，包括以下步骤：将所述比例的活性成份A、活性成份B、乳化剂溶解于有机溶剂中，搅拌至所加成份完全溶解得到溶液I；将所述比例的引诱成分、抑制挥发剂溶 解于溶剂水中搅拌至所加成份完全溶解得到溶液II；将溶液I和II合并后搅拌均匀得到一溶液，用均一溶液浸泡或涂刷载体挂条，待完全浸润后晾干或烘干，即为本发明所述的灭蝇挂条。
8.根据权利要求7所述的制备方法，其特征在于，所述的均一溶液浸泡载体挂条时，每克载体需5-20g的均一溶液浸泡，浸泡5-60分钟；所述的均一溶液涂刷载体挂条，每平方厘米载体涂刷0.01-1g的均一溶液。
9.根据权利要求1所述的长效灭蝇挂条，其特征在于：长效灭蝇挂条的靶标为家蝇、市蝇、丝光绿蝇、大头金蝇、厩腐蝇、厕蝇、亮绿蝇、红头丽蝇、伏蝇中的一种或多种。
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