CN1082349C - Edible tree fungi extracting liquid containing amino acids and its application - Google Patents
Edible tree fungi extracting liquid containing amino acids and its application Download PDFInfo
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- CN1082349C CN1082349C CN99117323A CN99117323A CN1082349C CN 1082349 C CN1082349 C CN 1082349C CN 99117323 A CN99117323 A CN 99117323A CN 99117323 A CN99117323 A CN 99117323A CN 1082349 C CN1082349 C CN 1082349C
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Abstract
The present invention relates to an edible tree fungus extracting solution containing various amino acids. Edible tree fungus, concentrated sulphuric acid, light calcium carbonate or lime, water, etc. are proportioned by weight, and finished products can be obtained after the edible tree fungus is pulped and hydrolyzed, and the pulp is neutralized, filtered and concentrated. Various components contained in edible tree fungus, which are beneficial to human health, are hydrolyzed in a strong acid medium and converted into water-soluble substances capable of being absorbed by the intestine and stomach, which are reserved in the solution for use. The edible tree fungus extracting solution contains 16 amino acids, calcium, dextrose, etc.; the edible tree fungus extracting solution can be directly eaten by people or made into health care beverages; the edible tree fungus extracting solution can be used as an additive for food and feedstuff and can also be used in medicine. The edible tree fungus extracting solution has the advantages of stable performance, no side effect, simple formula, low price, easy acquirement of raw materials and simple technology; the edible tree fungus extracting solution can be used as both medicine and food and form large-scale production.
Description
The invention relates to a nutrient for food health care, in particular to an edible fungus extract rich in various amino acid components.
Edible and medicinal values of edible fungi have been reported on publications. Since Auricularia itself contains amino acids, proteins, fats, carbohydrates, crude fiber and carotene, VB2K, Na, Mg, etc., and trace amounts of lecithin, cephalin, sphingomyelin, and protopanoxatin D2And anti-tumor active polysaccharide, which plays an important role in the health care of human bodies (or animals), and is particularly beneficial to the healthy growth of infants in the lactation period. Therefore, artificial edible fungus has been widely cultivated in western Sichuan countries in China, people are also researching how to effectively utilize natural edible fungus resources and develop the sales market of the artificial edible fungus to develop edible fungus health-care food, and the edible fungus health-care food supplements various amino acids, calcium, trace magnesium, copper and other metal elements for human bodies to increase gastric acid, regulate the digestion and absorption of gastrointestinal functions, treat cardiac failure and the like, thereby improving the physical quality of people. Although the Chinese patent gazette discloses a document containing the raw material of the fungus as a nutriment (mainly a health drink), the raw materials have different components and different preparation methods, and have different characteristics, and the formula and the preparation method which are the same as those of the invention are not reported.
The invention aims to fully utilize agaric resources and develop the market of artificial agaric, and extracts various amino acids and calcium, trace magnesium, copper and other metal elements required by human bodies from agaric so as to provide health care nutrition for the human bodies. The Auricularia extract contains 16 amino acids, and can be directly eaten, or processed into health beverage, or used as additive of food and feed, and used in medicine.
Amino acids are a prerequisite for many biomolecules, which form proteins and polypeptides in the organism, while proteins are involved in all vital activities. The protein is composed of 18 amino acids, asparagine and glutamine, which are derivatives of two amino acids (dehydrated to each other and connected into polypeptide chains by peptide bonds, and the different polypeptide chains are twisted into the protein by hydrogen bonds). The 18 amino acids are serine, threonine, aspartic acid, glutamic acid, methionine, histidine, lysine, arginine, alanine, valine, leucine, isoleucine, phenylalanine, histidine, tryptophan, glycine, proline, cystine, and asparagine and glutamine, which are derivatives of two additional amino acids, constitute the structural units of the protein. Different proteins function differently in organisms.
The technical scheme of the invention is based on that various components contained in the agaric are hydrolyzed in a strong acid medium, and all the components are changed into water-soluble substances which can be absorbed by intestines and stomach and are kept in the solution for eating.
The agaric extracting solution comprises the following raw materials in parts by weight: 0.8-1.2 parts of agaric, 4-7.5 parts of concentrated sulfuric acid, 5.5-8.5 parts of light calcium carbonate and 50-80 parts of drinking water. The Auricularia can be natural black or white Auricularia, or artificially cultured yellow Auricularia or white Auricularia.
The weight parts of the raw materials are as follows: 1 part of yellow and white fungus or white fungus, 6-6.5 parts of concentrated sulfuric acid, 65-7 parts of light calcium carbonate and 60-65 parts of drinking water.
The agaric extracting solution is prepared by the following steps in sequence:
a. preparing the raw materials in parts by weight, wherein the drinking water comprises the water content of the pulp in the step b and the water added into the reactor in the step c;
b. soaking Auricularia in water for 3-8 hr, cleaning, and grinding into slurry (the water content of the slurry is no more than 23% of the total water content of the ingredients);
c. putting the slurry into a reactor, adding drinking water, gradually adding concentrated sulfuric acid into the reactor, and stirring the slurry while adding;
d. heating the reactor to make the agaric in the slurry and sulfuric acid produce hydrolysis reaction, its reaction temperature is 90-110 deg.C, and its reaction time is 4-10 hr (in the course of said reaction the polysaccharide and protein are hydrolyzed, and the reaction can produce soluble sugar, polypeptide and amino acid, and other components in the agaric also can be added into the solution);
e. stopping heating, gradually adding light calcium carbonate while stirring when the slurry is cooled to 25-45 deg.C, and regulating pH value of the slurry to 5-7 (at this time ， Due to CaCO4Slightly soluble in water, so a small amount of CaCO4Dissolved in solution as a source of calcitonin);
f. e, filtering and washing slag of the slurry obtained in the step e, collecting filtrate and discarding waste slag of the filtrate;
g. and finally, heating and concentrating the filtrate in a concentrator to obtain a liquid finished product.
In the step b: soaking Auricularia in water at 40-60 deg.C for 3-5 hr until the water content of the paste is no more than 23% of the total water content of the materials;
in the step d: heating the slurry in the reactor with steam or fire directly to boil the slurry for 4-6 hr;
in the step e: when the slurry is cooled to normal temperature by circulating water, slowly adding light calcium carbonate;
in the step f: the slurry was placed in a centrifuge to separate the resulting separated liquid, and the separated liquid was filtered again.
The light calcium carbonate can be replaced by quicklime or marble powder.
The reactor can be a red copper vessel or an acid-resistant lined reactor.
The agaric extracting solution is prepared by adopting the raw material components and the mixture ratio and the process steps as follows: the edible fungus contains saccharide, fat, protein, etc. which are heated in acid medium to hydrolyze to respectively generate soluble saccharide, and the protein is hydrolyzed to generate polypeptide and amino acid; during the neutralization of sulfuric acid, light calcium carbonate or lime is added to produce gypsum to eliminate great amount of sulfate radical ion and hydrogen ion, and trace amount of gypsum is dissolved in the solution and ionized, so that the extracted agaric liquid contains amino acids, rich calcium ion, magnesium ion and copper ion. Amino acids are a class of compounds of special significance because many of them are basic constituent units of proteins closely related to life origin and life activities, are substances essential to the human body, and some are directly used as drugs; calcium is an important component of animal bones, and trace magnesium and copper ions are cofactors of some proteases in animals and human bodies and are genes for enhancing enzyme activity, namely, the enzymes lack the metal ions and lose the catalytic activity in organisms, so that the metabolism of cells is hindered. The amino acids contained in the edible fungus extract are tested by Sichuan antibiotic industrial research institute (see attachment 1, wherein the sample name is 'edible fungus beverage' which is the edible fungus extract), the main health-care components are 16 of 18 amino acids (namely serine, threonine, aspartic acid, glutamic acid, methionine, histidine, lysine, arginine, alanine, valine, leucine, isoleucine, phenylalanine, histidine, tryptophan and glycine), and the content of ten amino acids (namely threonine, egg, lysine, valine, leucine, isoleucine, phenylalanine, tryptophan, essence and histidine, which are necessary for human body, can not be synthesized by human body and can only be provided by food) is rich (wherein two kinds of the essential amino acids and the group amino acids are necessary amino acids for infants); the nutrient components of the product also contain rich monosaccharide such as active calcium, glucose and the like (see an attachment 2, wherein the sample name 'agaric beverage' is agaric extracting solution). The Auricularia auricula of the products inspected by the accessories 1 and 2 is artificially cultured yellow and white Auricularia, and if the Auricularia auricula is natural Auricularia auricula, the content is higher than the test data. Animal (dog) experiment shows that the said agaric extracting liquid has excellent effect, especially on young mammal. Other animals are now being tested for further comparisons (reports on supplementation). Therefore, the agaric extracting solution has the direct effects of supplementing calcium and nourishing brain and building body for human bodies, and is particularly beneficial to the healthy growth of infants in the lactation period.
The invention has the characteristics that: the product has stable performance and no side effect, and is suitable for infants, middle-aged and elderly people, teenagers and middle-aged and elderly people to drink; the formula is simple, the product is cheap and good, and the product can be used as both medicine and food; the raw materials are easy to obtain and cheap (12-14 yuan per kilogram of artificial agaric, 400 yuan per ton of sulfuric acid and 400 yuan per ton, and about 3 yuan per kilogram of light calcium carbonate), the process is simple, large-scale production can be realized, and good social and economic benefits are achieved.
The invention is further illustrated by the following examples:
the first embodiment is as follows: the raw materials comprise 1kg of yellow and white fungus, 6.2kg of concentrated sulfuric acid (98% density is 1.84g/mL), 7kg of light calcium carbonate and 63-65kg of drinking water (total water amount of hydrolyzed fungus slurry and fungus).
The preparation method of the agaric extracting solution comprises the following procedures of material preparation, agaric grinding, agaric hydrolysis, serous fluid neutralization, filtration and filtrate concentration, and the finished product is prepared according to the following sequential steps:
(1) and mixing the raw materials according to the weight. (2)Firstly, placing the agaric in a container, soaking the agaric in hot water of about 45 ℃ for 3-5 hours (or soaking the agaric in cold water for 5-8 hours, and controlling the time according to different seasons), fully soaking and expanding the agaric, cleaning the agaric, and grinding the agaric on an iron mill or a meat grinder into pulp (the water content of the pulp is required to be not more than 15kg, namely the water content of the pulp is not more than 23% of the total water content of ingredients). (3) The slurry was completely placed in a reactor, and then the whole amount of the drinking water (about 50 kg) after the slurry was ground was added to the reactor, and concentrated sulfuric acid was slowly added thereto, and the slurry was stirred with a pestle while adding the concentrated sulfuric acid (to avoid bumping). (4) Heating the reactor with water vapor (or directly heating with fire) to make Auricularia in the slurry and sulfuric acid produce hydrolysis reaction at 95-105 deg.C for 5-6 hr. (5) Stopping heating, slowly adding light calcium carbonate while stirring the slurry (without adding quickly to avoid overflowing the slurry) when the slurry is cooled to normal temperature by circulating water3Then, the pH value of the slurry is checked by using pH paper to determine whether the pH value is about 6.5, and if the pH value is less than 6.5, a small amount of lime slurry can be added to increase the pH value to about 6.5. (6) And (3) filtering the agaric slurry obtained in the step (5) in a filter press (or a centrifugal machine), washing residues, collecting filtrate, and discarding residues. (7) And finally, heating the filtrate obtained in the step (6) by a concentrator (at 90-110 ℃) and concentrating until the volume is about 63L (weight is 63Kg), thus obtaining the finished product.The sample is sent by Shimmy 370252, and the amino acid analysis report and the detection report of glucose, calcium and the like are shown in annexes 1 and 2 respectively.
In the step (6), the slurry obtained in the step (5) can also be put into a centrifugal separator for separation, the obtained separation liquid is filtered again, and finally the filtrate is concentrated by introducing steam into the concentrator to obtain a liquid finished product.
The light calcium carbonate in the raw material can be replaced by quicklime or marble powder; the reactor can be an acid-resistant lined common steel or silicate reactor (such as a porcelain reaction kettle and the like) or a red copper heating container.
Example two: the raw materials comprise 0.8kg of natural black fungus, 4kg of concentrated sulfuric acid, 6kg of light calcium carbonate and about 60kg of drinking water. The preparation method of the agaric extracting solution comprises the following steps of material preparation, agaric grinding, agaric hydrolysis, serous fluid neutralization, filtration and filtrate concentration, and is different from the first embodiment:
the raw materials in the example are proportioned according to the weight in (1); in the step (2), the agaric is soaked in cold water for 5 to 7 hours, and the water content of the pulp after grinding is not more than 14 kg); directly heating the slurry in the reactor by fire in (4), boiling the slurry and keeping the boiling for 4-6 hours; when the slurry is naturally cooled to about 40 ℃ in the step (5), gradually adding light calcium carbonate while stirring, wherein the pH value of the slurry is required to be about 6.5, and if the pH value is 4-5, adding a little lime slurry to neutralize to about 6.5; in the step (6), the slurry obtained in the step (5) is put into a centrifugal separator for separation, and the obtained separation liquid is subjected to secondary filtration; (7) and finally, concentrating the filtrate in vacuum (at about 90 ℃) to about 60L (the weight is 60kg) to obtain a liquid finished product. The other steps are thesame as those of the first embodiment.
Example three: the raw materials comprise 1.2kg of tremella, 6kg of concentrated sulfuric acid, 7kg of light calcium carbonate and about 70kg of drinking water. The preparation method of the agaric extracting solution is implemented in the first step and the second step, and the finished product is about 70L.
Example four: the raw materials comprise 5kg of yellow and white fungus, 31kg of concentrated sulfuric acid (98% density is 1.84g/mL), 34kg of light calcium carbonate and about 315kg of drinking water (total water amount of hydrolyzed fungus slurry and fungus). The preparation method of the agaric extracting solution comprises the following steps of material preparation, agaric grinding, agaric hydrolysis, serous fluid neutralization, filtration and filtrate concentration, and is different from the first embodiment:
(1) proportioning according to the weight of the raw materials of the example; (2) soaking Auricularia in water at about 55 deg.C for 3-4 hr until the water content of the pulp is no more than 70 kg; (3) adding the whole drinking water (about 240 kg) after the pulp grinding into the reactor; (4) heating the reactor with water vapor (or directly heating with fire) to make Auricularia in the slurry and sulfuric acid perform hydrolysis reaction at about 100 deg.C for 4-5 hr (i.e. boiling the slurry and maintaining for 4-5 hr); (5) slowly adding light calcium carbonate when the slurry is cooled to normal temperature (or naturally cooled to about 40 ℃) by using circulating water; (7) heating and concentrating the filtrate obtained in the step (6) by a concentrator until the volume is about 315L (the weight is about 315Kg), thus obtaining the agaric extracting solution, and then checking, bottling (250mL multiplied by 1260 bottles), capping and labeling the extracting solution; the other steps are the same as those of the first embodiment.The finished product is inspected by sampling, and the amino acid analysis report and the glucose, calcium and other detection reports are respectively shown in accessories 1 and 2.
Example five: the raw materials comprise 1kg of agaric, 7kg of concentrated sulfuric acid, 8kg of light calcium carbonate and about 78kg of drinking water. The preparation method of the agaric extracting solution is implemented in the same way, and about 78L of finished products are obtained.
The above Auricularia extractive solution can be further heated and concentrated to make the volume of the liquid product smaller than that obtained in the examples, and the content of the components in per 100mL Auricularia extractive solution is larger than that in accessories 1 and 2.
The agaric extracting solution is applied to beverage processing. The preparation method for processing the agaric beverage comprises the following steps: taking about 63L of Auricularia extractive solution, adding 0.063kg sodium benzoate, 0.063kg citric acid, adding 3.15kg white sugar or 1.5kg Mel, stirring (adding appropriate amount of drinking water), and performing flow line production according to conventional process of sterile beverage production, or optionally bagging with CO as required2。
The Auricularia extract can be used as additive in the processing of flour food, and has an addition amount of 12-15%. Such as: adding 12-15Kg of the Auricularia extract into 85-88Kg of flour, stirring, tabletting, cutting into noodles, oven drying (at a temperature below 110 deg.C), and processing into cooked food and flour.
The agaric extracting solution is applied as an additive in feed, and the adding amount of the agaric extracting solution is 8-10%. Such as: taking 90-92kg of feed powder, adding 8-10kg of the agaric extracting solution, uniformly stirring, granulating and the like.
Attachment 1: "national institute of medical and pharmaceutical administration Sichuan institute of antibiotic Industrial research amino acid analysis report" a part
An accessory 2: one copy of detection report
Claims (8)
1. The agaric extracting solution is characterized by comprising the following raw materials in parts by weight:
0.8-1.2 parts of agaric
4-7.5 parts of concentrated sulfuric acid
5.5 to 8.5 portions of light calcium carbonate
50-80 parts of drinking water, namely,
the agaric extracting solution is prepared by the following steps in sequence:
a. preparing the raw materials in parts by weight, wherein the drinking water comprises the water content of the slurry in the step b and the water added into the reactor in the step c,
b. soaking Auricularia in water for 3-8 hr, cleaning, grinding into slurry,
c. putting the slurry into a reactor, adding drinking water, adding concentrated sulfuric acid into the reactor gradually while stirring,
d. heating the reactor to make the agaric in the serous fluid and the sulfuric acid generate hydrolysis reaction, the reaction temperature is 90-110 ℃, the reaction time is 4-10 hours,
e. stopping heating, gradually adding light calcium carbonate while stirring when the slurry is cooled to 25-45 deg.C, wherein the pH value of the slurry is 5-7,
f. e, filtering and washing slag of the slurry obtained in the step e in a filter press or a centrifuge, collecting filtrate, discarding waste slag,
g. heating and concentrating the filtrate in a concentrator to obtain a liquid finished product.
2. The agaric extracting solution according to claim 1, which is characterized by comprising the following raw materials in parts by weight:
1 part of yellow tremella or tremella
6-6.5 parts of concentrated sulfuric acid
6.5-7 parts of light calcium carbonate
60-65 parts of drinking water.
3. The agaric extract solution of claim 1, wherein:
soaking Auricularia in the solution b at 40-60 deg.C for 3-5 hr,
heating the reactor with steam or fire directly in d to boil the slurry for 4-6 hr,
e, gradually adding light calcium carbonate when the slurry is cooled to the normal temperature by using circulating water,
the slurry in f was again filtered through a centrifuge to obtain a separated liquid.
4. The agaric extract solution according to claim 1 or 2, wherein: the light calcium carbonate is replaced by quicklime or marble powder.
5. The agaric extract solution according to claim 1 or 2, wherein: the reactor is a red copper container or an acid-resistant lined reaction kettle.
6. The use of the extract of Auricularia as claimed in claim 1 in the processing of beverage.
7. The use of the extract of Auricularia as claimed in claim 1 as anadditive in the processing of flour food.
8. The use of the extract of Auricularia as claimed in claim 1 as an additive in feed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN99117323A CN1082349C (en) | 1999-10-21 | 1999-10-21 | Edible tree fungi extracting liquid containing amino acids and its application |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN99117323A CN1082349C (en) | 1999-10-21 | 1999-10-21 | Edible tree fungi extracting liquid containing amino acids and its application |
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| Publication Number | Publication Date |
|---|---|
| CN1256091A CN1256091A (en) | 2000-06-14 |
| CN1082349C true CN1082349C (en) | 2002-04-10 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN99117323A Expired - Fee Related CN1082349C (en) | 1999-10-21 | 1999-10-21 | Edible tree fungi extracting liquid containing amino acids and its application |
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| Country | Link |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106174596A (en) * | 2016-08-11 | 2016-12-07 | 塔城市星河生物工程有限责任公司 | A kind of production method of food plant amino acid dry powder |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1071060A (en) * | 1991-09-25 | 1993-04-21 | 梁芳亭 | Auricularia auriculajudae and tremella mycelium acidic technique for production of proteoglycan |
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1999
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Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1071060A (en) * | 1991-09-25 | 1993-04-21 | 梁芳亭 | Auricularia auriculajudae and tremella mycelium acidic technique for production of proteoglycan |
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| CN1256091A (en) | 2000-06-14 |
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